#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:31:57 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181248 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/26/2232697.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232697_Fobs loop_ _publ_author_name 'Al-Adiwish, Wedad M.' 'Yaacob, W. A.' 'Adan, D.' 'Mohamed Tahir, Mohamed Ibrahim' 'Kassim, Mohammad B.' _publ_section_title ; 3-Oxo-5-(piperidin-1-yl)-2,3-dihydro-1H-pyrazole-4-carbonitrile ; _journal_coeditor_code HB6450 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3318 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.280 _cell_angle_beta 75.934 _cell_angle_gamma 71.906 _cell_length_a 7.2667 _cell_length_b 7.9624 _cell_length_c 8.8306 _exptl_crystal_F_000 204.00 _reflns_d_resolution_high 0.8156 _cod_data_source_file hb6450Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wedad37_pbar1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 50.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.85 0.18 0.04 o 3 0 0 0.01 0.35 0.06 o 4 0 0 1.40 3.27 0.18 o 5 0 0 30.16 35.41 0.84 o 6 0 0 0.14 0.17 0.20 o 7 0 0 25.10 24.44 1.31 o 8 0 0 16.52 21.72 0.92 o -7 1 0 6.33 5.43 0.62 o -6 1 0 171.27 155.19 2.29 o -5 1 0 5.07 4.09 0.44 o -4 1 0 131.22 141.62 1.64 o -3 1 0 69.41 83.48 0.62 o -2 1 0 1096.71 1105.37 2.99 o -1 1 0 1187.37 1054.15 2.01 o 0 1 0 282.78 322.55 2.93 o 1 1 0 1543.11 1367.19 3.45 o 2 1 0 0.05 1.56 0.10 o 3 1 0 20.80 22.75 0.28 o 4 1 0 18.71 13.76 0.32 o 5 1 0 145.40 145.05 1.27 o 6 1 0 5.40 4.60 0.30 o 7 1 0 0.39 0.29 0.31 o 8 1 0 21.77 25.41 1.11 o -7 2 0 8.00 12.87 0.79 o -6 2 0 30.09 22.50 1.27 o -5 2 0 76.81 77.29 1.63 o -4 2 0 15.18 19.32 0.60 o -3 2 0 766.81 796.55 3.97 o -2 2 0 206.36 208.10 1.17 o -1 2 0 21.04 25.86 0.34 o 0 2 0 1324.67 1494.34 2.06 o 1 2 0 237.91 247.38 1.06 o 2 2 0 697.99 677.83 1.45 o 3 2 0 28.21 41.28 0.36 o 4 2 0 312.87 335.79 1.42 o 5 2 0 79.75 74.81 0.82 o 6 2 0 486.15 449.40 3.67 o 7 2 0 1.54 2.27 0.50 o 8 2 0 14.24 19.74 1.03 o -6 3 0 1.45 1.46 0.37 o -5 3 0 39.36 44.38 1.80 o -4 3 0 1.98 3.09 0.30 o -3 3 0 117.88 103.39 1.52 o -2 3 0 23.92 31.30 0.79 o -1 3 0 53.90 50.18 0.67 o 0 3 0 351.58 456.26 4.54 o 1 3 0 263.91 297.75 2.12 o 2 3 0 630.60 652.23 2.03 o 3 3 0 1.64 3.95 0.17 o 4 3 0 115.59 110.15 0.89 o 5 3 0 0.85 0.24 0.10 o 6 3 0 371.01 339.32 2.09 o 7 3 0 40.01 35.31 1.05 o 8 3 0 9.29 9.20 0.38 o -6 4 0 2.35 1.23 0.19 o -5 4 0 56.49 62.88 2.00 o -4 4 0 39.45 31.48 0.93 o -3 4 0 237.94 219.90 3.69 o -2 4 0 73.09 83.17 1.49 o -1 4 0 154.69 150.18 1.77 o 0 4 0 180.55 251.10 1.85 o 1 4 0 108.76 124.70 1.33 o 2 4 0 11.72 9.74 0.28 o 3 4 0 505.73 511.67 1.89 o 4 4 0 0.33 0.15 0.08 o 5 4 0 62.09 62.26 0.90 o 6 4 0 0.06 0.03 0.11 o 7 4 0 0.00 -0.07 0.19 o 8 4 0 14.67 14.34 0.48 o -5 5 0 3.64 4.32 0.34 o -4 5 0 50.39 44.04 0.84 o -3 5 0 146.09 135.85 1.50 o -2 5 0 16.83 14.59 0.99 o -1 5 0 9.76 14.65 1.43 o 0 5 0 182.33 227.21 1.95 o 1 5 0 11.20 12.77 0.40 o 2 5 0 51.46 55.36 0.95 o 3 5 0 4.87 4.40 0.26 o 4 5 0 5.78 6.23 0.32 o 5 5 0 39.60 32.25 0.74 o 6 5 0 212.71 200.46 2.14 o 7 5 0 10.68 8.60 0.43 o 8 5 0 0.88 1.37 0.14 o -4 6 0 0.00 0.02 0.28 o -3 6 0 3.01 2.47 0.26 o -2 6 0 3.77 2.79 0.27 o -1 6 0 40.89 37.48 0.91 o 0 6 0 47.59 60.16 1.13 o 1 6 0 0.92 1.12 0.22 o 2 6 0 15.80 20.38 0.82 o 3 6 0 225.42 224.28 2.13 o 4 6 0 54.26 52.15 1.07 o 5 6 0 120.31 114.77 1.21 o 6 6 0 3.33 3.75 0.26 o 7 6 0 3.13 3.45 0.23 o 8 6 0 0.69 0.92 0.16 o -3 7 0 1.35 2.06 0.24 o -2 7 0 1.58 1.07 0.23 o -1 7 0 0.74 1.68 0.28 o 0 7 0 30.58 32.18 1.05 o 1 7 0 1.03 1.30 0.31 o 2 7 0 0.79 0.20 0.15 o 3 7 0 177.90 163.64 2.42 o 4 7 0 87.19 73.22 1.56 o 5 7 0 15.16 11.66 0.52 o 6 7 0 2.65 2.50 0.30 o 7 7 0 5.77 7.03 0.27 o -2 8 0 2.10 3.30 0.26 o -1 8 0 1.42 1.81 0.34 o 0 8 0 22.59 28.33 0.92 o 1 8 0 60.14 58.40 2.53 o 2 8 0 40.99 38.47 1.14 o 3 8 0 2.41 2.14 0.44 o 4 8 0 18.19 14.17 0.54 o 5 8 0 1.06 0.32 0.19 o 6 8 0 13.00 13.16 0.54 o 0 9 0 3.86 3.23 1.57 o 1 9 0 24.95 26.78 0.90 o 2 9 0 0.30 0.24 0.14 o 3 9 0 0.06 0.15 0.12 o 4 9 0 4.69 3.95 0.32 o 5 9 0 0.17 0.27 0.13 o -5 -9 1 12.99 17.65 0.89 o -4 -9 1 18.20 16.18 0.71 o -3 -9 1 0.91 0.58 0.24 o -2 -9 1 0.56 0.54 0.24 o -1 -9 1 0.35 0.42 0.21 o 0 -9 1 48.59 60.17 1.47 o -6 -8 1 22.57 24.43 0.66 o -5 -8 1 22.23 24.56 0.66 o -4 -8 1 15.46 15.96 0.56 o -3 -8 1 0.20 0.06 0.34 o -2 -8 1 2.70 2.34 0.47 o -1 -8 1 5.08 3.73 0.40 o 0 -8 1 0.36 0.34 0.19 o 1 -8 1 0.28 -0.10 0.15 o 2 -8 1 3.94 4.39 0.43 o -7 -7 1 16.33 21.30 0.49 o -6 -7 1 0.10 0.39 0.12 o -5 -7 1 0.93 0.32 0.15 o -4 -7 1 119.72 108.78 1.88 o -3 -7 1 54.48 45.79 1.22 o -2 -7 1 2.44 1.22 0.18 o -1 -7 1 170.84 152.21 1.81 o 0 -7 1 162.99 169.26 3.82 o 1 -7 1 21.93 18.75 0.79 o 2 -7 1 57.90 51.41 2.21 o 3 -7 1 2.70 1.73 0.31 o -7 -6 1 24.67 26.32 0.64 o -6 -6 1 3.22 2.53 0.22 o -5 -6 1 0.52 0.12 0.12 o -4 -6 1 135.57 130.46 1.69 o -3 -6 1 0.05 0.23 0.18 o -2 -6 1 21.27 20.41 0.82 o -1 -6 1 0.66 0.96 0.20 o 0 -6 1 1.54 2.35 0.24 o 1 -6 1 275.48 256.93 1.64 o 2 -6 1 30.54 32.89 1.04 o 3 -6 1 6.68 6.39 0.38 o 4 -6 1 32.67 36.72 1.34 o -8 -5 1 30.14 39.48 0.80 o -7 -5 1 9.27 9.41 0.54 o -6 -5 1 0.74 0.42 0.17 o -5 -5 1 77.54 69.13 0.80 o -4 -5 1 19.88 19.05 0.44 o -3 -5 1 252.76 260.13 1.58 o -2 -5 1 51.18 59.91 0.91 o -1 -5 1 11.39 10.17 0.37 o 0 -5 1 393.63 436.12 4.31 o 1 -5 1 19.74 18.58 0.73 o 2 -5 1 82.29 81.55 1.57 o 3 -5 1 246.42 222.32 1.71 o 4 -5 1 34.63 29.29 0.71 o 5 -5 1 1.41 1.62 0.23 o -8 -4 1 6.40 6.86 0.36 o -7 -4 1 0.90 0.96 0.22 o -6 -4 1 124.04 104.39 1.87 o -5 -4 1 114.70 110.55 1.18 o -4 -4 1 51.61 52.19 0.75 o -3 -4 1 162.94 167.53 1.66 o -2 -4 1 224.91 227.37 1.11 o -1 -4 1 23.33 29.68 0.69 o 0 -4 1 5.81 8.29 0.32 o 1 -4 1 117.33 132.44 5.30 o 2 -4 1 233.54 256.42 2.84 o 3 -4 1 0.23 1.30 0.36 o 4 -4 1 0.08 0.73 0.25 o 5 -4 1 0.22 0.45 0.26 o 6 -4 1 0.36 1.76 0.30 o -8 -3 1 3.98 4.69 0.33 o -7 -3 1 17.07 15.99 0.60 o -6 -3 1 6.17 7.12 0.53 o -5 -3 1 11.41 11.66 0.35 o -4 -3 1 27.89 39.78 0.61 o -3 -3 1 575.32 635.54 3.23 o -2 -3 1 453.09 493.79 1.77 o -1 -3 1 75.52 78.57 0.50 o 0 -3 1 268.69 279.02 1.86 o 1 -3 1 48.20 53.08 1.37 o 2 -3 1 320.71 292.45 3.88 o 3 -3 1 40.74 42.08 1.92 o 4 -3 1 32.44 28.44 1.38 o 5 -3 1 54.71 46.05 1.81 o 6 -3 1 6.93 8.20 0.73 o 7 -3 1 3.49 5.24 0.46 o -8 -2 1 2.72 1.59 0.32 o -7 -2 1 11.34 10.98 0.96 o -6 -2 1 3.65 4.13 0.25 o -5 -2 1 102.85 102.39 1.10 o -4 -2 1 732.33 752.93 2.47 o -3 -2 1 205.96 243.94 1.36 o -2 -2 1 267.24 261.19 1.13 o -1 -2 1 628.15 630.72 2.54 o 0 -2 1 700.32 805.74 15.96 o 1 -2 1 66.89 65.09 0.84 o 2 -2 1 156.25 186.51 1.12 o 3 -2 1 13.84 18.91 0.35 o 4 -2 1 123.53 131.22 1.82 o 5 -2 1 50.37 42.64 1.38 o 6 -2 1 111.90 107.91 2.76 o 7 -2 1 7.27 5.88 0.56 o -8 -1 1 25.71 28.58 1.05 o -7 -1 1 26.51 22.13 1.27 o -6 -1 1 4.15 5.05 0.48 o -5 -1 1 122.72 123.13 1.56 o -4 -1 1 0.98 1.14 0.10 o -3 -1 1 335.27 348.77 1.48 o -2 -1 1 63.85 75.59 0.54 o -1 -1 1 2.09 4.27 0.14 o 0 -1 1 92.62 95.53 0.46 o 1 -1 1 2.23 0.85 0.06 o 2 -1 1 326.23 301.29 0.83 o 3 -1 1 365.04 403.95 1.32 o 4 -1 1 0.79 0.47 0.12 o 5 -1 1 43.49 43.06 0.80 o 6 -1 1 0.18 0.18 0.17 o 7 -1 1 0.90 2.09 0.42 o -7 0 1 21.41 24.07 1.26 o -6 0 1 8.82 6.75 0.53 o -5 0 1 101.72 93.00 1.37 o -4 0 1 19.11 12.85 0.36 o -3 0 1 41.79 54.42 0.56 o -2 0 1 104.96 116.57 1.04 o -1 0 1 739.05 695.40 8.85 o 0 0 1 682.38 765.66 3.00 o 1 0 1 0.05 1.25 0.06 o 2 0 1 260.29 263.11 0.86 o 3 0 1 786.04 804.89 2.24 o 4 0 1 246.72 284.55 1.67 o 5 0 1 7.68 9.52 0.44 o 6 0 1 150.78 142.86 1.68 o 7 0 1 6.79 5.00 0.65 o 8 0 1 2.59 1.89 0.24 o -7 1 1 0.47 -0.05 0.26 o -6 1 1 200.77 183.48 2.98 o -5 1 1 207.82 201.13 2.07 o -4 1 1 3.47 2.83 0.24 o -3 1 1 255.89 248.38 1.36 o -2 1 1 299.37 331.06 1.15 o -1 1 1 260.11 287.94 1.54 o 0 1 1 58.75 38.23 2.91 o 1 1 1 471.62 411.69 6.97 o 2 1 1 203.32 210.07 1.44 o 3 1 1 695.04 706.53 2.18 o 4 1 1 0.24 0.72 0.08 o 5 1 1 22.09 18.11 0.45 o 6 1 1 19.27 16.75 0.56 o 7 1 1 30.07 28.96 1.51 o 8 1 1 2.92 1.91 0.38 o -7 2 1 13.23 12.46 0.71 o -6 2 1 14.62 16.51 1.07 o -5 2 1 59.92 66.28 1.22 o -4 2 1 1.36 1.32 0.18 o -3 2 1 59.35 53.97 0.78 o -2 2 1 174.50 197.14 1.22 o -1 2 1 58.72 52.23 0.81 o 0 2 1 0.03 6.47 0.16 o 1 2 1 1618.46 1586.67 3.63 o 2 2 1 166.37 162.31 1.41 o 3 2 1 55.44 57.30 0.49 o 4 2 1 6.15 9.89 0.22 o 5 2 1 29.64 27.78 0.49 o 6 2 1 36.45 31.02 0.72 o 7 2 1 1.52 2.33 0.62 o 8 2 1 11.44 11.99 0.65 o -6 3 1 28.40 31.41 1.30 o -5 3 1 23.34 20.72 0.84 o -4 3 1 65.21 65.94 0.88 o -3 3 1 61.23 64.30 0.92 o -2 3 1 85.89 102.48 1.21 o -1 3 1 321.87 328.85 2.04 o 0 3 1 1326.95 1494.19 5.36 o 1 3 1 3.12 7.37 0.29 o 2 3 1 187.92 169.90 1.83 o 3 3 1 31.23 43.01 0.48 o 4 3 1 446.37 470.51 2.33 o 5 3 1 359.48 386.47 2.26 o 6 3 1 54.26 49.76 0.73 o 7 3 1 0.36 0.32 0.18 o 8 3 1 1.68 2.53 0.30 o -6 4 1 3.63 2.87 0.58 o -5 4 1 0.60 0.30 0.29 o -4 4 1 170.09 155.63 1.87 o -3 4 1 8.86 8.42 0.43 o -2 4 1 413.15 384.40 2.59 o -1 4 1 20.60 25.82 0.63 o 0 4 1 73.04 92.73 0.92 o 1 4 1 565.94 581.62 1.94 o 2 4 1 46.72 58.76 0.65 o 3 4 1 353.33 362.13 1.98 o 4 4 1 13.07 13.38 0.43 o 5 4 1 0.00 0.26 0.14 o 6 4 1 0.90 1.85 0.16 o 7 4 1 10.95 11.05 0.49 o 8 4 1 27.48 28.04 0.69 o -5 5 1 1.11 0.24 0.24 o -4 5 1 0.49 0.39 0.15 o -3 5 1 92.29 90.37 1.24 o -2 5 1 0.26 1.28 0.17 o -1 5 1 139.76 160.04 1.72 o 0 5 1 6.92 8.28 0.33 o 1 5 1 12.69 10.63 0.43 o 2 5 1 238.32 239.39 1.99 o 3 5 1 0.09 0.49 0.14 o 4 5 1 97.33 100.88 1.23 o 5 5 1 0.01 0.51 0.18 o 6 5 1 235.83 218.93 2.18 o 7 5 1 0.04 0.10 0.15 o 8 5 1 0.26 0.29 0.15 o -4 6 1 1.18 2.53 0.44 o -3 6 1 33.92 28.98 0.77 o -2 6 1 3.62 4.16 0.39 o -1 6 1 6.31 5.29 0.35 o 0 6 1 315.68 359.76 4.80 o 1 6 1 27.29 21.78 0.83 o 2 6 1 5.90 8.72 0.44 o 3 6 1 71.05 70.50 1.23 o 4 6 1 88.15 83.96 1.18 o 5 6 1 45.89 43.10 0.61 o 6 6 1 2.20 2.02 0.21 o 7 6 1 0.51 0.83 0.16 o 8 6 1 0.30 0.51 0.11 o -3 7 1 0.57 0.74 0.23 o -2 7 1 0.38 0.12 0.15 o -1 7 1 119.85 125.09 3.44 o 0 7 1 78.28 82.83 1.66 o 1 7 1 0.35 0.52 0.22 o 2 7 1 65.61 62.98 1.21 o 3 7 1 86.66 73.30 3.12 o 4 7 1 38.03 39.49 1.06 o 5 7 1 11.13 10.84 0.61 o 6 7 1 2.64 2.45 0.26 o 7 7 1 4.78 3.46 0.21 o -2 8 1 0.14 0.06 0.14 o -1 8 1 2.62 2.78 0.36 o 0 8 1 76.31 79.88 1.48 o 1 8 1 126.14 120.01 1.91 o 2 8 1 59.65 51.93 1.31 o 3 8 1 11.84 10.90 0.90 o 4 8 1 9.80 8.11 0.77 o 5 8 1 24.78 23.17 0.80 o 6 8 1 21.83 23.61 0.74 o 7 8 1 5.99 7.44 0.29 o 0 9 1 2.12 2.21 0.33 o 1 9 1 1.22 0.96 0.18 o 2 9 1 0.08 0.14 0.19 o 3 9 1 3.63 3.37 0.31 o 4 9 1 3.11 2.64 0.28 o 5 9 1 17.81 19.30 0.84 o -4 -9 2 1.05 0.47 0.12 o -3 -9 2 6.35 7.24 0.32 o -2 -9 2 32.55 39.41 1.33 o -1 -9 2 0.01 0.20 0.19 o 0 -9 2 0.46 1.46 0.27 o -6 -8 2 1.74 1.20 0.23 o -5 -8 2 0.50 0.64 0.20 o -4 -8 2 21.80 19.59 1.10 o -3 -8 2 8.85 7.73 0.72 o -2 -8 2 7.43 6.29 0.46 o -1 -8 2 1.83 1.06 0.36 o 0 -8 2 0.05 0.49 0.29 o 1 -8 2 9.86 9.04 0.70 o 2 -8 2 1.05 0.67 0.23 o -6 -7 2 25.95 26.65 0.78 o -5 -7 2 0.01 0.15 0.16 o -4 -7 2 36.90 33.06 1.02 o -3 -7 2 0.02 0.28 0.20 o -2 -7 2 72.26 66.28 2.11 o -1 -7 2 214.60 201.17 3.72 o 0 -7 2 35.15 34.81 1.58 o 1 -7 2 56.32 52.55 1.88 o 2 -7 2 0.85 0.23 0.26 o 3 -7 2 9.34 11.81 0.77 o -7 -6 2 13.51 15.96 0.58 o -6 -6 2 0.71 0.12 0.14 o -5 -6 2 6.05 7.07 0.49 o -4 -6 2 0.13 0.44 0.15 o -3 -6 2 43.41 40.30 0.79 o -2 -6 2 45.92 47.00 0.99 o -1 -6 2 11.65 11.16 0.63 o 0 -6 2 95.97 99.02 1.47 o 1 -6 2 1.74 1.14 0.16 o 2 -6 2 24.28 23.40 0.98 o 3 -6 2 5.69 7.24 0.50 o 4 -6 2 0.72 1.56 0.33 o -7 -5 2 6.24 7.41 0.46 o -6 -5 2 10.68 6.79 0.49 o -5 -5 2 14.99 16.63 0.62 o -4 -5 2 75.46 72.32 1.54 o -3 -5 2 12.64 12.27 0.50 o -2 -5 2 3.04 4.11 0.22 o -1 -5 2 1.07 1.32 0.14 o 0 -5 2 1.71 3.61 0.27 o 1 -5 2 112.64 106.13 4.19 o 2 -5 2 10.93 10.95 0.49 o 3 -5 2 13.43 14.28 0.58 o 4 -5 2 1.13 0.94 0.18 o 5 -5 2 0.04 0.02 0.21 o -7 -4 2 0.50 1.12 0.23 o -6 -4 2 42.95 41.39 1.18 o -5 -4 2 251.94 242.81 1.76 o -4 -4 2 2.42 2.56 0.21 o -3 -4 2 2.50 2.21 0.18 o -2 -4 2 179.39 159.91 1.18 o -1 -4 2 0.35 0.18 0.08 o 0 -4 2 232.23 293.15 1.77 o 1 -4 2 57.41 70.37 0.98 o 2 -4 2 241.02 242.88 2.52 o 3 -4 2 37.26 33.91 1.01 o 4 -4 2 274.80 245.88 2.29 o 5 -4 2 74.91 72.40 2.19 o 6 -4 2 21.63 19.11 0.97 o -7 -3 2 27.81 25.76 0.70 o -6 -3 2 25.46 22.25 0.87 o -5 -3 2 3.67 4.34 0.37 o -4 -3 2 103.43 105.93 1.03 o -3 -3 2 95.45 91.68 0.78 o -2 -3 2 258.23 282.52 1.79 o -1 -3 2 3.42 3.70 0.18 o 0 -3 2 925.37 1064.42 6.94 o 1 -3 2 18.83 16.32 0.37 o 2 -3 2 97.90 100.82 1.45 o 3 -3 2 2.23 2.14 0.25 o 4 -3 2 0.68 0.68 0.29 o 5 -3 2 61.83 57.80 1.91 o 7 -3 2 4.52 4.30 0.43 o -7 -2 2 0.27 0.29 0.13 o -6 -2 2 210.47 193.53 2.08 o -5 -2 2 32.12 29.96 0.79 o -4 -2 2 34.21 37.58 0.70 o -3 -2 2 286.79 271.03 1.35 o -2 -2 2 72.41 81.91 0.86 o -1 -2 2 1560.86 1366.36 8.98 o 0 -2 2 0.04 0.99 0.06 o 1 -2 2 271.92 286.91 1.83 o 2 -2 2 72.63 88.19 0.79 o 3 -2 2 78.49 77.18 1.01 o 4 -2 2 5.56 5.97 0.34 o 5 -2 2 57.99 56.34 1.33 o 6 -2 2 10.61 11.48 0.89 o -7 -1 2 7.39 5.58 0.85 o -6 -1 2 55.38 48.08 1.30 o -5 -1 2 356.41 348.19 3.29 o -4 -1 2 46.53 42.41 0.75 o 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