#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/27/2232706.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232706_Fobs loop_ _publ_author_name 'Szymczak, Nathaniel K.' 'Zakharov, Lev N.' 'Tyler, David R.' _publ_section_title ; Bis{1,2-bis[bis(3-methoxypropyl)phosphanyl]ethane-\k^2^P,P'}dichloridoosmium(II) ; _journal_coeditor_code HB6479 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1808 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.779 _cell_angle_gamma 90.000 _cell_length_a 12.6675 _cell_length_b 10.3215 _cell_length_c 18.7545 _exptl_crystal_F_000 1060.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file hb6479Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nate11 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 268.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 65280.23 68291.76 357.61 o 4 0 0 24929.31 26112.04 179.74 o 6 0 0 9628.95 8825.08 102.18 o 8 0 0 1495.29 1393.76 62.57 o 10 0 0 5458.73 5527.16 132.97 o 12 0 0 4358.08 4029.90 213.21 o 14 0 0 1749.71 1926.27 154.80 o 1 1 0 41247.20 45072.73 212.43 o 2 1 0 1713.24 1429.98 19.65 o 3 1 0 934.62 922.79 20.16 o 4 1 0 3249.06 3262.85 43.58 o 5 1 0 14822.35 15612.33 112.70 o 6 1 0 0.10 1.25 6.39 o 7 1 0 4057.74 3787.28 56.68 o 8 1 0 57.37 43.95 11.38 o 9 1 0 4273.02 4031.53 75.48 o 10 1 0 26.88 22.45 19.26 o 11 1 0 6604.20 6286.23 124.50 o 12 1 0 119.21 81.09 42.37 o 13 1 0 2116.15 2124.20 108.78 o 14 1 0 51.92 9.46 33.98 o 15 1 0 1477.50 1713.41 111.07 o 0 2 0 383.25 431.56 17.72 o 1 2 0 5508.51 5877.73 40.50 o 2 2 0 12764.15 13241.16 81.17 o 3 2 0 5381.07 5363.98 50.27 o 4 2 0 15785.79 15795.48 102.59 o 5 2 0 6036.58 6343.03 64.70 o 6 2 0 16486.83 17282.09 125.51 o 7 2 0 101.67 81.67 13.19 o 8 2 0 4927.98 4891.68 70.21 o 9 2 0 563.67 567.32 35.95 o 10 2 0 7127.29 6898.17 124.60 o 11 2 0 0.34 29.22 26.63 o 12 2 0 3453.20 3424.58 102.29 o 13 2 0 49.55 20.95 28.03 o 14 2 0 1125.23 1049.02 82.68 o 15 2 0 267.48 255.41 51.80 o 1 3 0 18154.72 19112.35 99.20 o 2 3 0 61.67 94.48 11.40 o 3 3 0 19658.91 20739.56 125.28 o 4 3 0 5149.81 5103.62 57.02 o 5 3 0 9395.83 9196.65 100.88 o 6 3 0 6.09 -14.31 9.54 o 7 3 0 11216.14 10858.55 121.83 o 8 3 0 28.94 30.17 14.91 o 9 3 0 9060.66 8714.71 120.10 o 10 3 0 642.16 709.60 56.87 o 11 3 0 4405.07 4637.34 109.63 o 12 3 0 213.03 201.20 34.67 o 13 3 0 2095.71 2033.17 106.83 o 14 3 0 380.83 355.57 54.26 o 15 3 0 1590.09 1675.56 214.80 o 0 4 0 3250.33 3405.63 56.94 o 1 4 0 891.12 862.53 21.59 o 2 4 0 8710.43 8851.99 71.99 o 3 4 0 319.59 314.51 18.92 o 4 4 0 6308.70 6043.33 75.03 o 5 4 0 80.11 99.20 12.72 o 6 4 0 1588.99 1581.73 45.44 o 7 4 0 466.93 477.92 32.81 o 8 4 0 12090.95 11956.86 195.17 o 9 4 0 305.63 311.72 30.71 o 10 4 0 3242.04 3376.62 80.69 o 11 4 0 64.01 96.73 25.60 o 12 4 0 3375.63 3431.33 101.72 o 13 4 0 24.59 20.21 31.58 o 14 4 0 3120.40 3135.52 125.87 o 1 5 0 14084.04 14089.63 97.96 o 2 5 0 2158.86 2139.99 35.80 o 3 5 0 20323.61 20284.36 141.03 o 4 5 0 2284.25 2098.04 43.28 o 5 5 0 6576.00 6683.49 80.45 o 6 5 0 1890.21 2015.39 52.67 o 7 5 0 6877.68 6555.89 99.68 o 8 5 0 87.13 96.72 19.02 o 9 5 0 5850.31 5776.87 103.86 o 10 5 0 28.02 63.46 26.77 o 11 5 0 2864.72 2759.87 90.54 o 12 5 0 4.94 35.23 28.07 o 13 5 0 5169.86 5377.24 160.89 o 14 5 0 0.69 28.89 41.04 o 0 6 0 6828.07 6726.16 116.62 o 1 6 0 2.12 -13.36 8.91 o 2 6 0 15956.61 15916.81 114.17 o 3 6 0 0.11 -1.98 10.33 o 4 6 0 8280.49 8103.03 92.17 o 5 6 0 37.84 26.56 13.48 o 6 6 0 2458.95 2543.11 61.40 o 7 6 0 278.94 322.82 28.75 o 8 6 0 5825.25 5452.13 98.92 o 9 6 0 338.19 307.01 31.93 o 10 6 0 2235.89 2196.29 75.33 o 11 6 0 267.31 193.51 31.12 o 12 6 0 2097.15 2048.90 92.64 o 13 6 0 64.48 35.74 32.48 o 14 6 0 2586.00 2761.50 178.63 o 1 7 0 12900.83 12982.54 109.09 o 2 7 0 2310.76 2273.99 49.32 o 3 7 0 15011.22 14432.13 130.35 o 4 7 0 388.23 396.79 27.10 o 5 7 0 4356.73 4158.11 78.04 o 6 7 0 589.09 582.05 37.34 o 7 7 0 5564.37 5424.42 97.73 o 8 7 0 618.18 634.95 46.29 o 9 7 0 3896.70 3839.20 90.65 o 10 7 0 645.21 658.48 47.61 o 11 7 0 525.92 452.99 44.05 o 12 7 0 2.66 5.49 29.61 o 13 7 0 1315.73 1337.90 94.76 o 0 8 0 7824.85 7748.23 138.64 o 1 8 0 1007.88 1027.65 39.85 o 2 8 0 8396.55 8111.36 99.78 o 3 8 0 3.18 25.04 14.16 o 4 8 0 12732.48 12431.04 143.63 o 5 8 0 104.86 57.23 20.60 o 6 8 0 11229.76 10781.56 139.72 o 7 8 0 315.78 356.38 35.76 o 8 8 0 7752.33 7655.00 126.82 o 9 8 0 108.39 169.65 32.40 o 10 8 0 2295.30 2217.82 91.02 o 11 8 0 33.13 49.20 30.59 o 12 8 0 1169.46 1378.81 97.44 o 1 9 0 2563.70 2747.26 69.94 o 2 9 0 73.70 76.95 17.51 o 3 9 0 4675.03 4720.03 81.34 o 4 9 0 404.50 462.12 35.23 o 5 9 0 7113.54 6858.39 111.35 o 6 9 0 671.93 761.63 53.03 o 7 9 0 5175.79 4794.14 119.13 o 8 9 0 732.65 791.61 56.88 o 9 9 0 2136.47 2226.39 92.66 o 10 9 0 149.76 102.73 33.06 o 11 9 0 1972.42 1831.31 94.03 o 0 10 0 3413.56 3618.66 150.47 o 1 10 0 18.54 23.17 27.06 o 2 10 0 2167.38 2261.81 79.26 o 3 10 0 517.80 608.95 53.10 o 4 10 0 2440.11 2579.41 81.68 o 5 10 0 28.94 30.89 23.11 o 6 10 0 4959.33 4673.26 111.65 o 7 10 0 637.16 555.22 49.38 o 8 10 0 1641.94 1751.50 84.73 o 9 10 0 150.41 156.36 36.37 o 10 10 0 2453.81 2303.83 113.70 o 1 11 0 3715.70 3974.17 118.35 o 2 11 0 144.66 214.85 40.16 o 3 11 0 741.90 768.85 63.72 o 4 11 0 7.87 37.01 25.31 o 5 11 0 2477.42 2475.92 88.81 o 6 11 0 60.54 66.28 27.80 o 7 11 0 1688.93 1729.45 91.77 o 8 11 0 19.20 27.47 29.16 o 0 12 0 5893.48 6219.87 335.12 o 1 12 0 56.36 128.14 83.52 o 3 12 0 16.26 -57.92 41.98 o 4 12 0 1371.91 1294.58 124.49 o 5 12 0 8.40 22.10 53.15 o 6 12 0 1472.58 1632.96 219.68 o 1 13 0 2899.88 2682.76 266.52 o 2 13 0 4.78 -1.43 72.25 o 3 13 0 1874.78 2033.09 247.39 o -15 0 1 1986.94 2135.78 171.14 o -13 0 1 3155.44 3078.50 242.03 o -11 0 1 14211.84 13629.85 305.47 o -9 0 1 8371.22 7968.18 150.65 o -7 0 1 15445.25 15514.21 202.18 o -5 0 1 31025.08 32061.14 220.39 o -3 0 1 51650.93 54884.61 306.61 o -1 0 1 47203.57 49856.57 271.21 o 1 0 1 61958.12 65312.00 414.81 o 3 0 1 831.73 953.22 25.71 o 5 0 1 23907.22 25809.39 192.75 o 7 0 1 2053.76 2307.62 55.25 o 9 0 1 3849.41 3810.44 105.09 o 11 0 1 6739.23 5915.98 311.14 o 13 0 1 1814.56 1854.26 182.56 o 15 0 1 2118.21 1847.29 247.71 o -15 1 1 339.11 267.33 55.98 o -14 1 1 1566.49 1452.23 95.75 o -13 1 1 2.60 30.64 37.93 o -12 1 1 4984.29 4922.73 144.81 o -11 1 1 321.15 331.24 35.25 o -10 1 1 5932.76 5615.85 109.40 o -9 1 1 698.47 743.49 60.01 o -8 1 1 3748.27 3639.07 87.18 o -7 1 1 356.01 368.47 22.08 o -6 1 1 18147.73 18063.36 125.92 o -5 1 1 9173.47 9331.19 97.00 o -4 1 1 20190.78 21515.44 133.63 o -3 1 1 23436.88 25214.52 139.64 o -2 1 1 39378.82 41945.45 179.88 o -1 1 1 228.97 200.28 6.32 o 0 1 1 49001.54 51992.46 248.23 o 1 1 1 2726.57 2681.83 22.88 o 2 1 1 7481.25 7834.41 48.91 o 3 1 1 52.81 33.64 6.93 o 4 1 1 22989.46 23107.48 118.98 o 5 1 1 339.30 335.75 15.17 o 6 1 1 13550.72 13307.48 93.26 o 7 1 1 210.63 200.13 16.37 o 8 1 1 2423.07 2367.89 48.74 o 9 1 1 86.31 75.58 16.89 o 10 1 1 6468.42 6343.17 118.44 o 11 1 1 217.30 189.05 31.19 o 12 1 1 1396.40 1422.25 88.74 o 13 1 1 202.16 217.49 43.79 o 14 1 1 1303.84 1307.51 92.76 o 15 1 1 0.02 -57.26 38.18 o -15 2 1 1417.81 1379.15 99.33 o -14 2 1 154.67 160.67 62.49 o -13 2 1 1217.96 1112.49 79.13 o -12 2 1 172.62 188.93 33.89 o -11 2 1 2407.82 2554.05 79.86 o -10 2 1 737.92 750.52 58.92 o -9 2 1 3511.87 3632.57 73.38 o -8 2 1 575.06 629.67 30.27 o -7 2 1 10876.18 10397.61 122.96 o -6 2 1 60.82 70.67 12.19 o -5 2 1 32726.96 33821.36 184.04 o -4 2 1 4107.47 4399.79 55.22 o -3 2 1 26573.57 27912.13 143.34 o -2 2 1 18880.49 20324.11 107.81 o -1 2 1 21614.22 22717.89 141.97 o 0 2 1 8075.99 8279.66 53.52 o 1 2 1 587.22 599.67 13.98 o 2 2 1 9419.04 9774.35 69.14 o 3 2 1 6490.64 7094.97 67.19 o 4 2 1 10313.98 10341.91 70.07 o 5 2 1 13257.21 13052.26 100.95 o 6 2 1 1840.25 1897.63 38.71 o 7 2 1 8912.94 8802.41 120.02 o 8 2 1 325.17 393.19 29.37 o 9 2 1 8282.73 8151.51 113.24 o 10 2 1 17.45 -22.63 18.19 o 11 2 1 4506.60 4528.31 107.43 o 12 2 1 353.96 384.80 42.72 o 13 2 1 1105.94 1068.92 81.60 o 14 2 1 46.37 20.77 36.66 o 15 2 1 1421.43 1030.04 176.17 o -15 3 1 494.97 570.77 67.40 o -14 3 1 1872.27 1773.58 91.04 o -13 3 1 0.52 9.41 26.26 o -12 3 1 2593.39 2597.03 88.02 o -11 3 1 1.97 -26.24 20.00 o -10 3 1 4261.16 4373.67 100.04 o -9 3 1 652.57 665.33 40.07 o -8 3 1 10757.69 10779.34 126.93 o -7 3 1 134.27 117.07 18.64 o -6 3 1 13127.75 13599.48 129.01 o -5 3 1 1094.87 1256.79 36.06 o -4 3 1 14770.95 15760.61 107.57 o -3 3 1 50.85 14.41 7.40 o -2 3 1 3946.71 4005.19 44.77 o -1 3 1 1344.35 1415.88 23.19 o 0 3 1 224.33 259.74 12.23 o 1 3 1 9284.73 9764.46 99.56 o 2 3 1 3065.57 3099.71 39.07 o 3 3 1 302.68 471.76 21.06 o 4 3 1 8673.16 8527.90 85.72 o 5 3 1 254.16 185.46 14.38 o 6 3 1 16333.33 15712.42 143.69 o 7 3 1 278.93 285.78 25.28 o 8 3 1 18421.63 18569.25 174.83 o 9 3 1 374.21 352.73 30.50 o 10 3 1 9466.21 9139.33 147.23 o 11 3 1 102.40 85.82 34.00 o 12 3 1 4306.90 4375.65 113.02 o 13 3 1 5.20 5.18 27.35 o 14 3 1 1315.20 1326.76 94.53 o 15 3 1 116.41 179.51 92.97 o -15 4 1 2291.88 2306.37 136.60 o -14 4 1 6.66 -3.58 39.39 o -13 4 1 3300.48 3289.50 107.02 o -12 4 1 14.58 11.67 23.57 o -11 4 1 3417.92 3481.99 97.04 o -10 4 1 724.49 782.32 47.02 o -9 4 1 5042.10 5051.74 92.74 o -8 4 1 231.87 229.80 25.58 o -7 4 1 10979.90 10852.32 125.55 o -6 4 1 101.28 105.05 15.95 o -5 4 1 3177.00 3089.86 61.41 o -4 4 1 4.37 4.62 8.46 o -3 4 1 12866.79 12764.95 98.52 o -2 4 1 5188.33 5305.00 50.58 o -1 4 1 2213.25 2146.76 32.07 o 0 4 1 1362.93 1334.05 25.89 o 1 4 1 8215.77 8175.60 65.40 o 2 4 1 68.40 105.60 10.54 o 3 4 1 13007.03 13380.87 120.21 o 4 4 1 0.53 5.97 8.92 o 5 4 1 8009.27 7887.23 81.98 o 6 4 1 5944.63 5766.92 86.51 o 7 4 1 13876.99 13766.60 153.20 o 8 4 1 15.39 7.97 13.90 o 9 4 1 9006.68 8876.16 127.39 o 10 4 1 599.27 531.43 40.03 o 11 4 1 3619.74 3520.32 98.77 o 12 4 1 16.57 -1.88 25.80 o 13 4 1 4346.35 4697.87 139.88 o 14 4 1 154.08 118.14 38.94 o -14 5 1 3437.56 3522.61 117.05 o -13 5 1 358.93 370.64 47.20 o -12 5 1 2544.09 2481.07 93.12 o -11 5 1 126.72 126.66 47.82 o -10 5 1 3954.11 3949.27 89.08 o -9 5 1 100.67 69.12 28.11 o -8 5 1 5576.75 5439.51 95.06 o -7 5 1 124.67 91.91 19.76 o -6 5 1 3223.88 3130.28 64.69 o -5 5 1 22.34 11.08 10.00 o -4 5 1 11974.76 11772.14 104.50 o -3 5 1 1122.28 1030.10 25.62 o -2 5 1 16210.03 15908.19 105.97 o -1 5 1 497.99 481.21 20.10 o 0 5 1 10375.83 10771.19 91.78 o 1 5 1 349.02 315.59 17.42 o 2 5 1 28483.26 28332.56 155.15 o 3 5 1 618.89 606.28 26.52 o 4 5 1 5798.72 5837.47 74.81 o 5 5 1 3857.22 3769.30 60.61 o 6 5 1 6652.99 6566.65 96.25 o 7 5 1 1222.60 1197.81 49.63 o 8 5 1 6262.91 6308.78 104.24 o 9 5 1 407.53 420.42 34.60 o 10 5 1 1135.85 1187.42 69.29 o 11 5 1 0.72 -2.63 23.39 o 12 5 1 4266.97 4498.77 134.02 o 13 5 1 60.38 47.04 32.77 o 14 5 1 3922.14 4213.88 171.66 o -14 6 1 6.34 -21.24 46.01 o -13 6 1 3411.61 3364.37 107.65 o -12 6 1 115.98 131.95 48.29 o -11 6 1 2252.71 2245.26 81.14 o -10 6 1 517.61 526.38 41.52 o -9 6 1 6671.75 6473.65 112.83 o -8 6 1 37.80 8.19 16.38 o -7 6 1 2802.91 2454.04 63.21 o -6 6 1 5.53 13.21 13.15 o -5 6 1 3524.25 3527.74 68.36 o -4 6 1 140.81 131.83 16.70 o -3 6 1 13481.06 12964.86 101.56 o -2 6 1 240.14 232.76 16.74 o -1 6 1 9250.24 9409.25 84.45 o 0 6 1 734.41 703.79 27.93 o 1 6 1 17837.60 17814.67 122.58 o 2 6 1 1769.74 1702.81 35.86 o 3 6 1 16149.00 16372.54 142.70 o 4 6 1 2050.61 1989.69 45.71 o 5 6 1 3764.02 3844.29 71.68 o 6 6 1 460.03 441.05 32.40 o 7 6 1 4311.31 4414.56 85.46 o 8 6 1 769.50 800.63 46.27 o 9 6 1 2026.23 1994.98 69.56 o 10 6 1 340.49 325.41 35.49 o 11 6 1 1142.06 1394.19 72.80 o 12 6 1 2.23 -18.00 27.19 o 13 6 1 3607.17 3490.77 127.16 o -13 7 1 89.65 112.74 36.25 o -12 7 1 1806.71 1900.88 92.43 o -11 7 1 162.22 212.76 32.38 o -10 7 1 3496.92 3512.57 91.68 o -9 7 1 1760.73 1772.73 70.59 o -8 7 1 9589.85 9415.16 146.80 o -7 7 1 103.28 166.58 25.38 o -6 7 1 6118.34 5984.85 98.02 o -5 7 1 95.28 104.36 25.68 o -4 7 1 12313.05 12089.43 120.14 o -3 7 1 209.31 151.13 18.56 o -2 7 1 13586.40 13390.21 111.02 o -1 7 1 216.96 242.00 19.17 o 0 7 1 10200.84 9856.12 98.06 o 1 7 1 932.60 976.26 32.73 o 2 7 1 12907.86 12727.69 119.66 o 3 7 1 756.55 775.64 34.69 o 4 7 1 8310.77 8297.82 99.17 o 5 7 1 221.13 213.81 22.95 o 6 7 1 2936.80 2733.38 67.01 o 7 7 1 458.87 379.28 40.30 o 8 7 1 3166.04 3144.46 78.89 o 9 7 1 939.12 876.14 52.97 o 10 7 1 1208.20 1245.67 71.13 o 11 7 1 5.40 22.18 24.71 o 12 7 1 1673.61 1703.78 99.93 o 13 7 1 16.18 46.16 52.99 o -12 8 1 321.71 284.49 47.62 o -11 8 1 1674.78 1670.30 96.53 o -10 8 1 99.72 45.07 24.99 o -9 8 1 5525.93 5457.31 111.77 o -8 8 1 2.45 0.72 19.70 o -7 8 1 10258.24 9786.54 149.50 o -6 8 1 109.67 175.10 24.91 o -5 8 1 9132.09 8963.16 121.63 o -4 8 1 0.54 21.44 14.54 o -3 8 1 10766.61 11102.85 119.94 o -2 8 1 1798.25 1833.65 48.44 o -1 8 1 6811.72 6669.48 81.91 o 0 8 1 57.96 83.70 14.52 o 1 8 1 8741.55 8612.73 107.64 o 2 8 1 1888.34 1737.26 46.59 o 3 8 1 9649.17 9444.75 110.18 o 4 8 1 3.51 29.71 14.69 o 5 8 1 7985.31 7804.30 113.67 o 6 8 1 1462.85 1374.08 56.43 o 7 8 1 5350.43 5129.08 112.11 o 8 8 1 10.27 41.44 22.96 o 9 8 1 2063.19 2049.23 86.11 o 10 8 1 75.21 83.04 29.73 o 11 8 1 1100.86 1084.33 71.67 o 12 8 1 2.86 -3.24 41.98 o -11 9 1 336.90 295.37 44.17 o -10 9 1 1848.79 1961.69 91.78 o -9 9 1 485.53 492.27 46.42 o -8 9 1 4172.86 4104.75 107.30 o -7 9 1 1410.41 1441.66 62.90 o -6 9 1 8221.39 8108.95 125.47 o -5 9 1 121.02 155.14 24.52 o -4 9 1 4931.43 4906.89 121.68 o -3 9 1 401.64 431.79 31.07 o -2 9 1 5529.29 5759.69 96.09 o -1 9 1 55.31 47.74 16.12 o 0 9 1 4156.00 3945.45 78.54 o 1 9 1 1494.09 1538.08 50.11 o 2 9 1 4067.59 4276.87 76.50 o 3 9 1 155.44 177.71 23.82 o 4 9 1 5428.98 5168.46 157.21 o 5 9 1 5.84 24.25 19.76 o 6 9 1 4310.84 4380.76 104.30 o 7 9 1 370.80 448.07 43.61 o 8 9 1 3006.48 2863.48 91.10 o 9 9 1 1.66 -34.30 22.86 o 10 9 1 2529.74 2645.59 101.36 o 11 9 1 58.77 57.59 37.93 o -10 10 1 93.94 84.08 34.39 o -9 10 1 1055.04 1029.61 102.65 o -8 10 1 390.62 454.46 49.11 o -7 10 1 2233.79 2200.02 87.50 o -6 10 1 17.42 9.90 23.66 o -5 10 1 3454.90 3413.04 93.50 o -4 10 1 1129.08 1193.84 63.28 o -3 10 1 1442.81 1562.54 72.54 o -2 10 1 257.65 286.27 30.30 o -1 10 1 3949.69 4036.40 95.85 o 0 10 1 16.98 -20.99 24.47 o 1 10 1 3305.79 3214.54 86.44 o 2 10 1 26.41 26.51 18.54 o 3 10 1 3678.65 3384.78 98.79 o 4 10 1 31.40 8.86 22.11 o 5 10 1 4631.67 4615.90 109.08 o 6 10 1 211.57 225.03 34.31 o 7 10 1 2723.84 2618.45 89.17 o 8 10 1 47.49 -2.14 25.38 o 9 10 1 2758.24 2756.62 141.17 o 10 10 1 113.45 123.31 54.09 o -9 11 1 38.82 163.84 65.98 o -8 11 1 416.18 381.04 76.27 o -7 11 1 23.98 74.93 74.07 o -6 11 1 1377.27 1396.39 102.86 o -5 11 1 46.52 40.90 36.97 o -4 11 1 750.55 699.66 73.23 o -3 11 1 0.13 -4.27 35.33 o -2 11 1 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