#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/27/2232715.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232715_Fobs loop_ _publ_author_name 'Wei, Ang Chee' 'Ali, Mohamed Ashraf' 'Choon, Tan Soo' 'Quah, Ching Kheng' 'Fun, Hoong-Kun' _publ_section_title ; 7'-Phenyl-5',6',7',7a'-tetrahydrodipiro[indan-2,5'-pyrrolo[1,2-c][1,3]thiazole-6',2''-indan]-1,3,1''-trione ; _journal_coeditor_code HB6489 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3218 _journal_page_last o3219 _journal_volume 67 _journal_year 2011 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 127.817 _cell_angle_gamma 90.000 _cell_length_a 19.3315 _cell_length_b 9.6523 _cell_length_c 29.9731 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.7079 _[local]_cod_data_source_file hb6489Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' astp1_0m in P2/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 444.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 46.72 -1.48 4.44 o 2 0 0 2991.29 3198.19 76.58 o 3 0 0 23.28 44.93 11.90 o 4 0 0 197337.69 203139.28 3331.51 o 5 0 0 409.56 363.11 23.53 o 6 0 0 6175.63 6234.43 126.26 o 7 0 0 6.74 -9.21 9.21 o 8 0 0 3465.93 3212.17 97.69 o 9 0 0 1187.52 1187.65 99.17 o 10 0 0 156.97 77.26 26.34 o 11 0 0 154.41 140.01 40.87 o 12 0 0 1237.62 1250.69 109.28 o 13 0 0 938.25 874.16 73.73 o 14 0 0 1752.40 1557.98 88.73 o 15 0 0 208.34 196.62 47.32 o 16 0 0 1463.18 1828.32 216.00 o 17 0 0 208.06 53.69 129.26 o 18 0 0 892.93 1283.36 240.59 o 19 0 0 0.02 72.58 169.37 o 20 0 0 0.89 1.76 147.10 o 21 0 0 46.32 196.59 168.52 o 0 1 0 0.71 -3.14 3.14 o 1 1 0 34034.63 30679.96 365.71 o 2 1 0 0.00 4.74 4.84 o 3 1 0 14718.73 13552.11 160.34 o 4 1 0 66160.98 64722.95 686.68 o 5 1 0 19983.12 19250.78 215.53 o 6 1 0 3602.42 3661.40 60.64 o 7 1 0 6787.75 7273.41 99.97 o 8 1 0 1669.11 1797.00 39.30 o 9 1 0 9.00 4.15 11.35 o 10 1 0 1139.62 1126.22 39.35 o 11 1 0 422.36 464.60 29.29 o 12 1 0 312.38 266.69 25.74 o 13 1 0 4.40 11.76 18.93 o 14 1 0 2136.82 2047.02 71.27 o 15 1 0 20.59 24.33 25.32 o 16 1 0 55.53 79.70 37.48 o 17 1 0 31.34 -63.52 136.64 o 18 1 0 449.76 1059.64 197.41 o 19 1 0 450.85 431.76 197.09 o 20 1 0 77.27 113.33 87.52 o 21 1 0 467.62 470.93 148.91 o 0 2 0 2103.38 1797.15 43.52 o 1 2 0 14366.98 13420.30 240.63 o 2 2 0 415.35 420.76 14.24 o 3 2 0 296.65 345.77 17.25 o 4 2 0 2359.69 2213.61 37.38 o 5 2 0 70913.09 75193.36 800.01 o 6 2 0 10.41 12.44 7.83 o 7 2 0 10186.44 10748.49 132.67 o 8 2 0 951.36 897.10 30.25 o 9 2 0 33632.56 35365.27 446.57 o 10 2 0 866.77 845.48 36.74 o 11 2 0 2626.75 2507.01 62.20 o 12 2 0 186.08 187.50 36.28 o 13 2 0 2287.39 2022.17 74.61 o 14 2 0 26.79 58.40 27.80 o 15 2 0 277.22 275.71 45.20 o 16 2 0 247.24 206.07 43.16 o 17 2 0 58.27 135.50 103.45 o 18 2 0 552.64 628.89 135.79 o 19 2 0 215.42 542.04 130.03 o 20 2 0 570.21 788.14 155.41 o 21 2 0 14.48 -60.13 104.39 o 0 3 0 266.42 209.20 17.48 o 1 3 0 1103.93 1056.34 24.16 o 2 3 0 246.09 253.47 13.69 o 3 3 0 175.09 214.53 13.04 o 4 3 0 295.14 334.56 17.29 o 5 3 0 1944.30 2042.79 40.46 o 6 3 0 228.00 205.72 15.25 o 7 3 0 3581.75 3669.66 69.13 o 8 3 0 441.71 473.36 27.22 o 9 3 0 2800.91 3038.65 79.74 o 10 3 0 2284.43 2191.57 61.42 o 11 3 0 3626.77 3539.25 84.12 o 12 3 0 0.10 5.85 19.28 o 13 3 0 9.39 9.51 18.90 o 14 3 0 271.34 290.79 36.19 o 15 3 0 342.27 393.69 48.43 o 16 3 0 206.98 249.16 90.38 o 17 3 0 959.83 1092.52 145.52 o 18 3 0 82.67 293.83 100.25 o 19 3 0 11.73 96.83 102.42 o 20 3 0 342.34 591.39 144.50 o 0 4 0 72588.38 72983.16 1237.59 o 1 4 0 474.35 540.54 20.07 o 2 4 0 1261.47 1198.67 28.80 o 3 4 0 61.24 79.48 10.50 o 4 4 0 15000.14 14734.61 182.59 o 5 4 0 162.34 155.23 13.03 o 6 4 0 1265.15 1432.55 38.11 o 7 4 0 9.55 1.47 9.85 o 8 4 0 2965.99 2770.95 61.01 o 9 4 0 272.85 312.48 28.51 o 10 4 0 2012.75 2014.36 94.23 o 11 4 0 21.58 22.81 16.98 o 12 4 0 474.34 453.55 34.85 o 13 4 0 137.87 111.59 25.83 o 14 4 0 3707.42 4082.90 213.24 o 15 4 0 371.03 437.54 156.32 o 16 4 0 300.92 459.84 148.29 o 17 4 0 90.05 316.26 86.31 o 18 4 0 70.21 154.79 115.41 o 19 4 0 0.88 110.38 91.19 o 20 4 0 1253.40 1674.63 200.44 o 0 5 0 23139.00 24036.50 430.98 o 1 5 0 0.74 -8.18 8.18 o 2 5 0 292.22 357.42 19.86 o 3 5 0 106.73 93.45 11.78 o 4 5 0 1.49 27.55 9.26 o 5 5 0 154.14 134.09 15.35 o 6 5 0 1097.66 1154.87 34.10 o 7 5 0 431.40 417.52 28.33 o 8 5 0 95.95 48.58 17.96 o 9 5 0 0.15 -13.88 19.36 o 10 5 0 708.33 747.34 57.00 o 11 5 0 34.42 30.55 18.79 o 12 5 0 340.75 321.37 66.76 o 13 5 0 250.89 170.49 81.87 o 14 5 0 32.66 4.45 73.43 o 15 5 0 666.59 865.33 132.25 o 16 5 0 632.27 747.03 125.71 o 17 5 0 189.05 425.55 235.64 o 18 5 0 1147.69 1343.69 166.24 o 19 5 0 0.00 -144.63 144.63 o 0 6 0 3366.53 3470.30 90.06 o 1 6 0 2691.33 2619.84 52.59 o 2 6 0 150.54 119.94 14.91 o 3 6 0 2039.60 1935.73 48.14 o 4 6 0 80.24 73.38 15.67 o 5 6 0 1226.99 1153.80 41.34 o 6 6 0 3553.45 3394.18 81.94 o 7 6 0 3146.54 2925.08 93.44 o 8 6 0 277.38 322.61 31.84 o 9 6 0 4003.85 3730.65 107.61 o 10 6 0 425.41 364.04 46.34 o 11 6 0 198.92 266.23 86.39 o 12 6 0 0.83 77.06 147.57 o 13 6 0 1503.29 1597.23 161.88 o 14 6 0 9.09 13.68 80.21 o 15 6 0 366.96 400.29 111.85 o 16 6 0 1.44 -36.85 128.10 o 17 6 0 85.39 186.74 105.26 o 18 6 0 0.17 159.28 175.91 o 19 6 0 143.19 17.91 170.19 o 0 7 0 219.77 205.72 26.21 o 1 7 0 17.32 0.86 10.22 o 2 7 0 0.18 5.26 13.90 o 3 7 0 1135.88 973.76 38.27 o 4 7 0 442.09 475.64 33.45 o 5 7 0 14.68 13.05 21.44 o 6 7 0 6.40 10.61 26.39 o 7 7 0 6372.16 6093.52 203.10 o 8 7 0 5.39 77.94 33.17 o 9 7 0 1852.44 1627.89 79.44 o 10 7 0 17.78 46.41 27.17 o 11 7 0 71.66 93.57 39.52 o 12 7 0 133.29 103.66 51.14 o 13 7 0 68.27 97.84 65.62 o 14 7 0 46.44 143.03 101.22 o 15 7 0 2119.74 2385.50 151.92 o 16 7 0 209.53 227.33 71.17 o 17 7 0 535.81 642.66 103.43 o 18 7 0 35.04 70.58 71.59 o 0 8 0 3595.29 3653.64 123.47 o 1 8 0 822.31 897.95 46.14 o 2 8 0 1993.23 1841.02 60.43 o 3 8 0 2326.74 2038.89 74.01 o 4 8 0 1370.73 1372.26 64.21 o 5 8 0 337.42 332.81 44.64 o 6 8 0 3278.24 2966.09 105.70 o 7 8 0 857.85 854.05 68.24 o 8 8 0 307.63 293.50 44.27 o 9 8 0 0.70 110.98 47.60 o 10 8 0 94.96 96.52 48.59 o 11 8 0 12.87 64.86 45.16 o 12 8 0 696.14 763.05 123.46 o 13 8 0 372.08 433.96 103.50 o 14 8 0 561.91 576.83 113.80 o 15 8 0 286.81 343.51 79.56 o 16 8 0 230.63 343.41 117.68 o 17 8 0 27.85 89.61 176.39 o 0 9 0 61.72 89.13 49.61 o 1 9 0 782.70 877.20 54.44 o 2 9 0 765.06 983.69 58.36 o 3 9 0 2.53 84.01 43.15 o 4 9 0 2.97 34.15 26.14 o 5 9 0 250.10 292.24 49.09 o 6 9 0 563.72 759.66 66.82 o 7 9 0 0.02 46.90 33.11 o 8 9 0 390.44 458.53 71.56 o 9 9 0 168.62 174.12 53.47 o 10 9 0 937.68 1191.16 125.79 o 11 9 0 189.95 294.11 69.63 o 12 9 0 270.58 265.06 108.53 o 13 9 0 106.19 176.15 90.55 o 14 9 0 22.41 23.21 83.59 o 15 9 0 21.27 86.92 84.50 o 16 9 0 600.74 1146.91 185.28 o 0 10 0 307.06 345.62 75.16 o 1 10 0 169.94 182.04 45.74 o 2 10 0 891.80 827.78 72.51 o 3 10 0 988.99 1005.24 80.24 o 4 10 0 163.51 183.25 57.76 o 5 10 0 278.03 282.66 63.90 o 6 10 0 1735.50 1681.32 87.74 o 7 10 0 180.89 173.88 61.82 o 8 10 0 17.96 64.02 54.22 o 9 10 0 802.60 1098.98 147.06 o 10 10 0 88.12 84.69 60.63 o 11 10 0 3.34 10.74 69.82 o 12 10 0 72.43 127.15 73.77 o 13 10 0 313.75 285.72 98.33 o 14 10 0 352.20 651.40 145.45 o 0 11 0 17.65 11.97 59.98 o 1 11 0 451.35 542.21 66.70 o 2 11 0 17.56 102.91 44.85 o 3 11 0 1874.92 1816.01 119.79 o 4 11 0 42.93 127.43 52.87 o 5 11 0 183.00 215.10 64.78 o 6 11 0 18.19 111.32 57.85 o 7 11 0 183.67 321.40 74.93 o 8 11 0 106.70 90.30 62.60 o 9 11 0 9.15 22.60 55.67 o 10 11 0 200.67 141.89 71.53 o 11 11 0 218.97 304.84 112.08 o 12 11 0 5.84 102.88 132.94 o 0 12 0 265.27 256.15 92.47 o 1 12 0 4.18 85.64 72.81 o 2 12 0 1.45 56.61 58.41 o 3 12 0 1.23 65.46 56.99 o 4 12 0 50.20 132.14 60.11 o 5 12 0 55.06 64.23 69.27 o 6 12 0 2.27 44.83 56.82 o 7 12 0 0.81 53.09 61.80 o 8 12 0 142.34 140.24 109.00 o 9 12 0 192.60 188.38 121.50 o 10 12 0 0.01 206.88 127.54 o 0 13 0 2536.36 2850.63 183.97 o 1 13 0 284.18 459.67 125.47 o 2 13 0 35.15 194.03 106.36 o 3 13 0 61.76 374.16 100.05 o 4 13 0 452.41 717.45 143.81 o 5 13 0 55.00 321.25 163.35 o 6 13 0 0.13 15.73 167.54 o -21 1 1 670.52 674.60 271.47 o -20 1 1 303.45 380.60 126.45 o -19 1 1 202.82 381.87 118.54 o -18 1 1 72.22 87.39 89.48 o -17 1 1 287.02 341.46 105.51 o -16 1 1 28.00 55.91 51.69 o -15 1 1 1070.09 1037.12 58.44 o -14 1 1 64.39 58.84 22.01 o -13 1 1 522.31 520.99 42.90 o -12 1 1 48.38 37.40 16.12 o -11 1 1 990.01 892.42 36.26 o -10 1 1 341.66 313.71 24.03 o -9 1 1 88.11 93.45 15.33 o -8 1 1 227.83 244.44 20.56 o -7 1 1 1981.01 2402.88 49.55 o -6 1 1 1315.06 1513.50 35.62 o -5 1 1 18790.89 18338.40 227.36 o -4 1 1 43209.64 41714.13 533.94 o -3 1 1 17899.00 16652.93 203.95 o -2 1 1 1483.23 1287.21 21.56 o -1 1 1 28437.02 26185.10 291.16 o 0 1 1 304.69 282.62 7.13 o 1 1 1 18341.51 16720.62 235.48 o 2 1 1 2367.35 2225.86 34.57 o 3 1 1 11962.26 11058.46 133.49 o 4 1 1 7096.03 6715.16 78.19 o 5 1 1 16296.44 15650.74 180.63 o 6 1 1 282.64 289.89 15.63 o 7 1 1 11259.25 11430.73 146.32 o 8 1 1 663.91 698.57 29.78 o 9 1 1 1025.17 942.76 37.88 o 10 1 1 4843.53 4741.93 109.94 o 11 1 1 373.98 319.98 27.27 o 12 1 1 290.66 224.26 21.07 o 13 1 1 337.42 234.93 39.66 o 14 1 1 1433.44 1419.35 74.38 o 15 1 1 176.54 206.33 40.95 o 16 1 1 0.17 112.40 73.16 o 17 1 1 222.48 347.83 106.82 o 18 1 1 80.96 255.57 149.61 o 19 1 1 156.19 325.17 130.04 o 20 1 1 200.47 269.42 128.65 o 21 1 1 54.67 49.17 138.31 o -21 2 1 71.08 382.41 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21.77 o 14 2 1 7.82 -2.34 21.82 o 15 2 1 1.50 20.44 26.56 o 16 2 1 352.01 373.81 54.39 o 17 2 1 52.12 3.13 82.71 o 18 2 1 52.51 241.36 95.48 o 19 2 1 137.92 365.41 116.33 o 20 2 1 131.28 65.98 87.36 o -21 3 1 876.90 1238.64 180.87 o -20 3 1 156.98 331.90 117.47 o -19 3 1 140.63 147.02 147.14 o -18 3 1 325.50 300.63 112.03 o -17 3 1 531.01 719.75 125.80 o -16 3 1 674.47 727.13 108.62 o -15 3 1 147.71 142.47 43.70 o -14 3 1 1293.74 1208.27 70.34 o -13 3 1 790.70 766.05 59.96 o -12 3 1 1098.51 1084.93 55.84 o -11 3 1 593.75 712.75 42.57 o -10 3 1 2525.83 2744.86 69.77 o -9 3 1 833.14 796.51 42.81 o -8 3 1 6995.59 7535.93 132.25 o -7 3 1 2018.65 1941.00 50.40 o -6 3 1 811.58 1025.77 29.23 o -5 3 1 479.44 494.70 19.25 o -4 3 1 4001.20 3897.24 58.24 o -3 3 1 1729.44 1633.87 29.75 o -2 3 1 6601.92 6253.98 81.98 o -1 3 1 474.47 499.63 18.68 o 0 3 1 2063.10 2015.09 35.59 o 1 3 1 1644.42 1567.83 31.72 o 2 3 1 3408.51 3267.50 90.44 o 3 3 1 224.02 240.18 13.65 o 4 3 1 62.33 101.13 12.19 o 5 3 1 540.77 554.34 20.59 o 6 3 1 235.38 398.90 22.68 o 7 3 1 326.40 415.87 27.00 o 8 3 1 372.14 429.37 32.40 o 9 3 1 620.95 634.11 29.72 o 10 3 1 4266.51 4108.04 83.51 o 11 3 1 222.42 221.99 30.26 o 12 3 1 31.14 4.93 15.97 o 13 3 1 123.41 112.01 26.86 o 14 3 1 3907.54 3826.88 126.31 o 15 3 1 2.93 44.61 61.30 o 16 3 1 194.46 283.30 97.54 o 17 3 1 91.18 200.42 96.41 o 18 3 1 2436.50 2574.17 201.86 o 19 3 1 80.33 186.80 112.14 o 20 3 1 320.53 690.46 142.44 o -20 4 1 171.88 475.36 173.99 o -19 4 1 243.65 810.42 220.35 o -18 4 1 146.06 191.34 91.80 o -17 4 1 564.92 535.78 192.57 o -16 4 1 104.85 162.73 83.35 o -15 4 1 48.35 118.36 176.84 o -14 4 1 242.99 215.51 40.24 o -13 4 1 316.33 233.46 33.24 o -12 4 1 399.85 371.03 37.08 o -11 4 1 337.92 330.32 35.07 o -10 4 1 1028.53 1116.79 46.91 o -9 4 1 1331.30 1451.90 49.84 o -8 4 1 784.95 734.83 36.71 o -7 4 1 271.04 283.84 24.83 o -6 4 1 2459.37 2578.51 59.84 o -5 4 1 1387.44 1644.02 36.21 o -4 4 1 838.52 907.17 28.51 o -3 4 1 1405.30 1545.01 42.46 o 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5 1 677.19 678.46 43.66 o -8 5 1 488.52 482.17 32.69 o -7 5 1 471.85 603.51 34.12 o -6 5 1 374.98 383.52 53.37 o -5 5 1 103.27 172.19 18.14 o -4 5 1 77.14 71.56 11.42 o -3 5 1 10120.29 10272.15 148.26 o -2 5 1 15.73 8.73 9.58 o -1 5 1 1143.67 1336.58 78.37 o 0 5 1 109.59 109.02 12.04 o 1 5 1 7147.61 6951.45 102.10 o 2 5 1 79.92 85.88 11.96 o 3 5 1 0.58 3.28 7.75 o 4 5 1 121.65 119.63 14.40 o 5 5 1 7764.69 7640.94 119.10 o 6 5 1 51.40 40.38 12.89 o 7 5 1 3250.42 3448.19 132.75 o 8 5 1 126.03 113.33 18.74 o 9 5 1 5301.76 5281.11 122.66 o 10 5 1 508.37 535.58 42.97 o 11 5 1 749.35 691.57 57.28 o 12 5 1 589.24 592.68 103.16 o 13 5 1 894.46 970.45 133.38 o 14 5 1 36.26 66.97 68.12 o 15 5 1 3796.95 4060.77 224.76 o 16 5 1 55.42 119.18 81.60 o 17 5 1 21.52 127.33 138.26 o 18 5 1 55.05 -144.56 144.56 o 19 5 1 55.22 182.94 127.39 o -19 6 1 104.02 176.23 110.07 o -18 6 1 192.62 -19.38 107.23 o -17 6 1 54.16 56.29 99.71 o -16 6 1 5.93 29.16 97.01 o -15 6 1 10.69 -84.78 130.07 o -14 6 1 329.30 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5 28 149.90 217.47 43.06 o -4 5 28 211.60 215.82 81.11 o -3 5 28 1.35 -24.95 40.06 o -2 5 28 31.78 101.28 45.49 o -1 5 28 0.10 11.16 42.37 o 0 5 28 147.17 188.08 48.47 o 1 5 28 1.70 42.70 44.42 o 2 5 28 270.17 283.36 103.17 o 3 5 28 244.02 293.58 115.81 o -24 6 28 9.39 -0.09 73.94 o -23 6 28 24.39 -68.79 68.79 o -22 6 28 0.35 -1.96 106.95 o -21 6 28 252.45 178.65 142.68 o -20 6 28 43.58 -14.92 72.70 o -19 6 28 180.51 157.95 78.82 o -18 6 28 21.84 -45.72 70.39 o -17 6 28 665.34 852.25 109.09 o -16 6 28 58.21 49.58 61.67 o -15 6 28 200.15 186.50 53.39 o -14 6 28 85.58 -18.92 40.98 o -13 6 28 8.02 1.82 41.00 o -12 6 28 95.93 98.39 46.37 o -11 6 28 323.92 378.15 94.19 o -10 6 28 15.28 51.15 43.28 o -9 6 28 446.50 532.47 69.02 o -8 6 28 284.33 329.93 60.36 o -7 6 28 208.59 266.12 83.84 o -6 6 28 50.67 119.30 49.50 o -5 6 28 509.09 596.72 73.60 o -4 6 28 1.08 36.93 80.70 o -3 6 28 393.50 398.42 83.89 o -2 6 28 42.01 94.95 51.18 o -1 6 28 761.62 610.79 133.22 o 0 6 28 6.15 93.45 106.11 o 1 6 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109.73 77.32 o -12 8 28 7.33 30.02 48.21 o -11 8 28 33.44 58.64 49.79 o -10 8 28 90.91 186.63 63.43 o -9 8 28 434.66 408.95 70.26 o -8 8 28 141.68 124.67 99.04 o -7 8 28 335.63 442.89 117.57 o -6 8 28 155.87 142.37 85.36 o -5 8 28 271.65 245.80 127.44 o -4 8 28 67.84 129.42 90.07 o -3 8 28 441.17 402.44 86.79 o -2 8 28 573.74 570.31 77.35 o -18 9 28 162.26 146.73 79.07 o -17 9 28 52.18 -12.08 73.83 o -16 9 28 0.38 -45.70 68.91 o -15 9 28 18.95 104.93 58.52 o -14 9 28 484.12 485.97 79.53 o -13 9 28 121.84 150.99 67.06 o -12 9 28 64.75 92.11 54.31 o -11 9 28 0.10 1.69 66.93 o -10 9 28 728.09 827.15 123.31 o -9 9 28 0.20 102.55 105.09 o -8 9 28 7.43 133.19 135.57 o -7 9 28 4.11 113.73 111.51 o -6 9 28 1884.42 2439.64 170.47 o -5 9 28 18.58 218.65 63.85 o -4 9 28 0.29 144.70 239.97 o -13 10 28 65.86 99.46 79.56 o -12 10 28 24.77 33.80 60.53 o -11 10 28 29.48 30.91 77.40 o -10 10 28 583.27 632.59 140.70 o -9 10 28 205.31 246.36 75.78 o -27 1 29 19.56 -3.85 56.05 o -26 1 29 0.35 27.32 47.24 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1004.04 1155.47 134.72 o -6 5 29 861.21 886.23 88.69 o -5 5 29 804.56 690.71 71.84 o -4 5 29 31.90 38.27 54.31 o -3 5 29 940.38 948.61 86.30 o -2 5 29 42.89 84.28 47.58 o -1 5 29 92.57 232.36 59.31 o 0 5 29 68.48 47.17 58.02 o 1 5 29 147.32 174.66 52.25 o 2 5 29 92.51 71.66 62.41 o -23 6 29 151.60 -19.96 80.80 o -22 6 29 1.24 50.88 74.27 o -21 6 29 32.10 -13.96 68.03 o -20 6 29 351.10 320.63 92.12 o -19 6 29 203.55 147.49 76.34 o -18 6 29 16.58 12.42 60.03 o -17 6 29 0.00 -57.80 57.80 o -16 6 29 45.61 62.27 62.25 o -15 6 29 73.49 81.53 47.46 o -14 6 29 194.79 142.52 52.41 o -13 6 29 66.01 43.10 43.94 o -12 6 29 4.10 -5.56 39.68 o -11 6 29 3.23 32.34 46.17 o -10 6 29 90.07 90.97 55.94 o -9 6 29 421.22 510.64 69.63 o -8 6 29 0.07 29.09 49.48 o -7 6 29 400.72 485.06 68.02 o -6 6 29 67.75 74.10 46.50 o -5 6 29 85.34 144.12 53.60 o -4 6 29 231.10 277.93 59.51 o -3 6 29 238.80 117.22 61.55 o -2 6 29 193.73 93.50 58.46 o -1 6 29 14.94 115.76 62.52 o 0 6 29 445.95 464.58 124.34 o 1 6 29 47.51 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