#------------------------------------------------------------------------------
#$Date: 2016-04-03 06:32:22 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181249 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/27/2232722.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2232722_Fobs
loop_
_publ_author_name
'Gon\,calves, Raoni S. B.'
'de Souza, Marcus V. N.'
'Wardell, James L.'
'Wardell, Solange M. S. V.'
'Tiekink, Edward R. T.'
_publ_section_title
;
 <i>tert</i>-Butyl
 2-{[2,8-bis(trifluoromethyl)quinolin-4-yl](hydroxy)methyl}piperidine-1-carboxylate
;
_journal_coeditor_code           HB6499
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o3315
_journal_page_last               o3316
_journal_volume                  67
_journal_year                    2011
_space_group_IT_number           19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   9.8876
_cell_length_b                   10.6965
_cell_length_c                   21.1582
_exptl_crystal_F_000             992.00
_reflns_d_resolution_high        0.8406
_cod_data_source_file            hb6499Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' 2011ncs0292a'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            112.90
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 516.05 407.76 5.59 o
4 0 0 3824.19 2599.20 48.97 o
6 0 0 322.69 362.93 21.38 o
8 0 0 276.96 271.88 5.18 o
10 0 0 36.20 33.97 4.98 o
3 1 0 470.42 562.19 12.77 o
4 1 0 6578.90 4476.95 19.78 o
5 1 0 62.49 55.54 1.98 o
6 1 0 1020.65 954.97 15.66 o
7 1 0 684.20 733.04 12.06 o
8 1 0 38.18 47.15 2.95 o
9 1 0 3.39 5.28 1.10 o
10 1 0 29.60 27.50 1.96 o
11 1 0 0.36 0.22 0.56 o
0 2 0 5151.61 2598.58 10.31 o
1 2 0 64.19 66.91 2.31 o
2 2 0 54.59 24.25 1.05 o
3 2 0 760.24 769.64 11.76 o
5 2 0 0.35 4.80 2.02 o
6 2 0 191.03 246.22 2.60 o
7 2 0 862.64 924.01 17.90 o
8 2 0 7.37 9.73 1.67 o
9 2 0 110.49 90.59 7.58 o
10 2 0 1.61 3.44 0.96 o
11 2 0 675.58 697.96 44.86 o
1 3 0 562.15 455.15 3.12 o
2 3 0 4229.72 2746.89 14.10 o
3 3 0 1165.29 1220.08 29.47 o
4 3 0 24.22 30.63 2.26 o
5 3 0 1612.43 1583.97 14.55 o
6 3 0 808.86 734.67 15.26 o
7 3 0 79.23 78.86 1.32 o
8 3 0 10.09 23.48 3.51 o
9 3 0 492.93 530.73 29.33 o
10 3 0 151.82 168.88 8.89 o
11 3 0 6.41 4.80 1.34 o
0 4 0 528.09 437.32 3.95 o
1 4 0 410.83 445.51 11.00 o
2 4 0 2319.94 2039.39 13.40 o
4 4 0 2895.72 2266.04 43.47 o
5 4 0 420.40 520.08 14.24 o
6 4 0 533.71 547.13 6.04 o
7 4 0 39.21 37.69 1.98 o
8 4 0 39.29 34.47 5.33 o
9 4 0 87.76 97.16 4.81 o
11 4 0 18.31 18.87 1.29 o
1 5 0 119.91 195.00 10.84 o
2 5 0 55.77 55.68 1.36 o
3 5 0 2906.01 2410.80 17.02 o
4 5 0 1.43 2.50 0.64 o
5 5 0 908.42 972.34 14.81 o
6 5 0 3.38 4.71 0.62 o
7 5 0 77.56 83.46 3.39 o
8 5 0 62.14 65.55 4.37 o
9 5 0 199.80 191.96 5.11 o
10 5 0 15.24 11.85 4.85 o
0 6 0 182.08 167.04 4.30 o
1 6 0 2461.98 2354.34 11.36 o
2 6 0 373.85 456.39 10.04 o
3 6 0 1555.45 1662.39 60.65 o
4 6 0 532.83 588.44 11.36 o
5 6 0 19.54 13.71 1.67 o
6 6 0 23.55 17.82 1.91 o
7 6 0 578.62 608.83 12.44 o
8 6 0 0.01 0.22 0.78 o
9 6 0 408.50 405.74 8.99 o
10 6 0 18.36 16.24 2.85 o
1 7 0 31.24 26.92 3.16 o
2 7 0 2085.88 2132.07 77.95 o
3 7 0 19.08 15.71 1.79 o
4 7 0 126.24 101.96 2.13 o
5 7 0 172.07 201.63 12.48 o
6 7 0 301.14 297.67 7.38 o
7 7 0 4.29 3.72 1.10 o
8 7 0 35.79 36.39 1.48 o
9 7 0 62.66 34.24 9.27 o
1 8 0 2.15 2.20 0.58 o
2 8 0 97.10 92.56 6.94 o
3 8 0 496.99 572.58 20.75 o
4 8 0 222.08 222.56 9.68 o
5 8 0 58.82 63.51 1.87 o
6 8 0 282.30 290.87 4.61 o
7 8 0 125.28 144.43 10.91 o
9 8 0 36.79 24.17 2.08 o
1 9 0 9.53 7.95 0.80 o
2 9 0 8.37 10.12 2.10 o
3 9 0 244.70 261.80 3.10 o
4 9 0 419.85 373.29 12.66 o
5 9 0 252.50 214.31 13.47 o
6 9 0 71.54 66.53 6.94 o
7 9 0 193.44 170.23 4.06 o
8 9 0 49.00 40.62 1.73 o
0 10 0 160.07 152.51 5.38 o
1 10 0 0.57 1.21 0.75 o
2 10 0 15.74 12.27 2.81 o
3 10 0 398.28 351.67 9.32 o
4 10 0 326.04 280.57 5.96 o
5 10 0 291.67 263.05 22.30 o
6 10 0 1.56 1.39 0.49 o
1 11 0 127.46 102.42 2.90 o
2 11 0 389.30 378.82 5.74 o
3 11 0 158.81 149.43 3.44 o
4 11 0 760.89 737.93 47.42 o
5 11 0 43.35 47.31 3.24 o
1 12 0 28.75 26.96 0.93 o
2 12 0 34.73 24.40 1.94 o
3 12 0 1.44 0.87 0.78 o
1 0 1 4855.83 2734.77 11.21 o
2 0 1 6181.94 3856.00 14.55 o
3 0 1 4163.23 2446.45 12.98 o
4 0 1 698.71 765.02 6.56 o
5 0 1 2695.71 2320.81 11.40 o
6 0 1 177.44 146.42 7.74 o
7 0 1 0.31 4.48 1.71 o
8 0 1 0.07 1.15 0.72 o
9 0 1 55.16 61.05 6.71 o
10 0 1 12.60 13.10 1.44 o
11 0 1 44.00 50.65 1.78 o
-11 1 1 47.90 44.45 1.65 o
-10 1 1 13.04 11.11 2.51 o
-9 1 1 300.71 321.22 4.07 o
-8 1 1 388.86 388.52 5.13 o
-7 1 1 694.94 733.18 20.00 o
-6 1 1 484.58 519.85 5.19 o
-5 1 1 1655.57 1622.13 7.92 o
-4 1 1 396.44 385.12 9.71 o
-3 1 1 2910.89 1977.70 16.37 o
-1 1 1 466.62 381.54 6.63 o
1 1 1 470.98 399.57 3.45 o
2 1 1 2717.44 1754.63 8.28 o
3 1 1 2894.12 1981.81 30.08 o
4 1 1 406.33 409.57 8.46 o
5 1 1 1652.20 1617.71 24.92 o
6 1 1 482.93 499.85 6.56 o
7 1 1 692.99 719.78 9.46 o
8 1 1 390.58 424.40 11.49 o
9 1 1 299.51 321.76 7.81 o
10 1 1 13.54 11.28 2.14 o
11 1 1 48.62 46.69 1.41 o
-11 2 1 15.69 8.55 4.11 o
-10 2 1 350.46 355.58 23.05 o
-9 2 1 243.26 261.80 9.28 o
-8 2 1 53.98 46.18 2.19 o
-7 2 1 1022.38 1028.26 13.34 o
-6 2 1 96.82 105.25 5.43 o
-5 2 1 2044.98 1974.13 17.17 o
-4 2 1 1432.59 1399.44 41.97 o
-3 2 1 3075.01 2186.59 17.90 o
0 2 1 195.77 191.92 1.99 o
3 2 1 3093.96 2189.76 36.14 o
4 2 1 1423.13 1460.33 12.89 o
5 2 1 2020.92 1940.19 10.78 o
6 2 1 95.13 101.99 2.68 o
7 2 1 1019.99 1087.07 14.84 o
8 2 1 53.26 43.72 2.56 o
9 2 1 245.42 263.58 5.07 o
10 2 1 345.67 365.31 8.72 o
11 2 1 16.63 14.28 1.34 o
-11 3 1 394.65 376.92 14.42 o
-10 3 1 6.40 4.45 1.87 o
-9 3 1 217.44 211.90 16.77 o
-8 3 1 154.08 155.47 2.55 o
-7 3 1 347.15 368.45 14.17 o
-6 3 1 87.74 88.83 5.17 o
-5 3 1 242.73 285.97 6.48 o
-4 3 1 1169.94 1232.97 21.28 o
-3 3 1 1808.77 1606.92 13.95 o
-2 3 1 8328.38 5717.73 38.62 o
1 3 1 668.96 562.33 3.08 o
2 3 1 8344.50 5318.29 67.99 o
3 3 1 1805.33 1608.79 11.85 o
4 3 1 1166.38 1268.84 10.56 o
5 3 1 242.58 296.05 6.29 o
6 3 1 89.90 94.07 3.19 o
7 3 1 342.31 363.70 8.78 o
8 3 1 154.65 144.33 1.81 o
9 3 1 211.71 200.95 9.45 o
10 3 1 5.80 3.27 1.36 o
11 3 1 398.59 397.57 15.11 o
-11 4 1 96.78 95.42 3.97 o
-10 4 1 19.90 18.94 2.34 o
-9 4 1 101.50 108.14 9.20 o
-8 4 1 398.59 445.34 9.04 o
-7 4 1 229.07 236.23 5.14 o
-6 4 1 344.72 350.00 5.48 o
-5 4 1 50.18 48.30 1.19 o
-4 4 1 2417.49 2207.31 15.64 o
-3 4 1 2694.44 2343.73 10.65 o
-2 4 1 2389.51 1921.18 45.53 o
-1 4 1 1001.98 931.10 9.27 o
1 4 1 993.16 910.91 34.59 o
2 4 1 2366.87 1914.23 11.96 o
3 4 1 2685.89 2305.82 16.71 o
4 4 1 2432.05 2210.81 15.28 o
5 4 1 50.35 50.40 1.46 o
6 4 1 347.38 339.93 5.37 o
7 4 1 228.91 240.42 14.15 o
8 4 1 401.02 446.27 5.68 o
9 4 1 100.93 103.04 2.30 o
10 4 1 20.19 19.05 2.63 o
11 4 1 96.88 88.53 3.75 o
-10 5 1 87.60 71.81 2.61 o
-9 5 1 15.09 13.07 3.15 o
-8 5 1 349.73 385.72 8.64 o
-7 5 1 188.12 190.06 3.66 o
-6 5 1 14.37 12.35 1.62 o
-5 5 1 13.10 14.33 1.87 o
-4 5 1 984.49 1029.60 26.93 o
-3 5 1 115.72 105.54 7.76 o
-2 5 1 23.26 24.72 3.72 o
-1 5 1 1273.86 1339.38 16.72 o
0 5 1 618.34 565.92 16.36 o
1 5 1 1276.36 1362.68 6.99 o
2 5 1 20.94 18.83 4.52 o
3 5 1 116.36 108.65 5.63 o
4 5 1 986.78 1056.95 24.55 o
5 5 1 13.58 14.00 1.86 o
6 5 1 14.68 13.50 1.06 o
7 5 1 185.83 188.09 9.38 o
8 5 1 356.12 391.37 6.94 o
9 5 1 15.65 12.42 2.68 o
10 5 1 87.25 78.27 4.97 o
-10 6 1 3.32 1.63 0.92 o
-9 6 1 165.31 154.18 3.95 o
-8 6 1 8.85 6.68 1.66 o
-7 6 1 867.04 869.52 24.74 o
-6 6 1 145.21 137.76 2.66 o
-5 6 1 456.52 490.08 10.70 o
-4 6 1 59.32 72.57 5.20 o
-3 6 1 953.01 1069.30 29.36 o
-2 6 1 287.92 321.49 6.90 o
-1 6 1 2025.01 2022.71 9.75 o
0 6 1 13.05 18.10 2.02 o
1 6 1 2014.24 2108.74 13.83 o
2 6 1 294.48 319.90 6.96 o
3 6 1 964.72 1059.78 16.35 o
4 6 1 58.04 62.36 3.38 o
5 6 1 458.41 499.94 11.45 o
6 6 1 141.73 138.00 2.69 o
7 6 1 861.54 869.03 10.25 o
8 6 1 9.46 7.89 1.86 o
9 6 1 168.87 159.24 7.67 o
10 6 1 3.61 2.46 1.21 o
-9 7 1 60.73 45.86 6.27 o
-8 7 1 128.14 101.41 6.06 o
-7 7 1 429.32 423.83 5.57 o
-6 7 1 178.98 176.81 5.36 o
-5 7 1 80.72 87.48 2.74 o
-4 7 1 350.11 342.18 6.10 o
-3 7 1 184.05 218.80 4.23 o
-2 7 1 532.76 508.23 4.58 o
-1 7 1 532.96 546.42 9.95 o
0 7 1 193.65 207.70 9.65 o
1 7 1 522.69 566.32 14.17 o
2 7 1 529.85 520.53 5.22 o
3 7 1 182.32 205.33 5.22 o
4 7 1 349.89 352.27 5.32 o
5 7 1 78.26 84.27 3.24 o
6 7 1 178.62 174.15 3.04 o
7 7 1 424.97 417.89 10.10 o
8 7 1 130.52 109.04 2.63 o
9 7 1 60.32 47.10 2.66 o
-9 8 1 91.09 73.26 3.39 o
-8 8 1 14.72 9.72 4.32 o
-7 8 1 279.35 261.16 6.32 o
-6 8 1 112.65 95.95 2.55 o
-5 8 1 67.97 55.77 1.72 o
-4 8 1 372.78 426.68 7.13 o
-3 8 1 113.34 111.52 2.14 o
-2 8 1 224.68 257.85 7.47 o
-1 8 1 165.35 182.01 4.81 o
0 8 1 106.96 106.32 1.51 o
1 8 1 166.57 171.27 8.19 o
2 8 1 222.22 257.59 10.24 o
3 8 1 115.71 114.34 3.58 o
4 8 1 367.01 417.55 13.11 o
5 8 1 66.33 57.59 2.90 o
6 8 1 112.18 101.27 3.02 o
7 8 1 281.88 273.77 3.72 o
8 8 1 15.09 13.01 3.57 o
9 8 1 92.46 69.04 3.18 o
-8 9 1 21.22 11.95 4.78 o
-7 9 1 8.64 7.41 3.25 o
-6 9 1 100.30 105.04 5.28 o
-5 9 1 49.36 53.01 2.02 o
-4 9 1 226.61 238.68 3.19 o
-3 9 1 16.96 12.64 3.08 o
-2 9 1 111.61 100.45 7.30 o
-1 9 1 132.26 121.84 3.52 o
0 9 1 61.04 61.33 3.68 o
1 9 1 132.54 121.36 1.99 o
2 9 1 111.87 102.00 8.35 o
3 9 1 16.53 11.13 1.78 o
4 9 1 231.95 237.90 4.19 o
5 9 1 49.16 55.50 2.13 o
6 9 1 100.50 103.36 5.61 o
7 9 1 8.72 6.71 1.93 o
8 9 1 20.91 12.49 3.55 o
-7 10 1 1.17 0.61 0.70 o
-6 10 1 131.02 116.10 17.95 o
-5 10 1 53.05 50.91 2.42 o
-4 10 1 41.08 41.95 7.12 o
-3 10 1 33.72 40.55 6.53 o
-2 10 1 28.74 30.61 5.85 o
0 10 1 71.61 76.39 2.18 o
1 10 1 440.57 476.12 10.11 o
2 10 1 29.96 19.62 4.95 o
3 10 1 32.70 30.35 1.46 o
4 10 1 41.91 37.19 2.34 o
5 10 1 51.30 52.17 2.09 o
6 10 1 131.46 113.82 18.64 o
-5 11 1 266.31 281.82 5.64 o
-4 11 1 224.39 233.53 6.12 o
-3 11 1 316.07 327.48 4.98 o
-2 11 1 487.58 510.42 6.93 o
-1 11 1 1.44 0.75 0.90 o
0 11 1 112.94 103.61 1.77 o
1 11 1 1.40 1.89 0.68 o
3 11 1 319.94 332.45 6.02 o
4 11 1 228.53 240.02 6.42 o
5 11 1 271.25 273.16 5.59 o
-3 12 1 24.26 25.65 1.96 o
-2 12 1 56.59 58.05 1.69 o
1 12 1 100.50 79.09 3.48 o
2 12 1 57.26 52.71 1.54 o
3 0 2 5210.08 3423.26 24.82 o
4 0 2 456.06 481.96 9.83 o
5 0 2 474.56 522.61 7.59 o
6 0 2 843.25 830.59 15.73 o
7 0 2 359.96 396.92 8.77 o
8 0 2 25.33 35.69 4.85 o
9 0 2 25.03 25.33 1.63 o
10 0 2 75.43 70.95 2.00 o
11 0 2 42.50 40.51 1.60 o
-11 1 2 109.97 95.63 11.65 o
-10 1 2 124.41 125.36 3.64 o
-9 1 2 236.13 253.24 12.48 o
-8 1 2 19.22 15.23 1.67 o
-7 1 2 47.80 32.35 5.34 o
-6 1 2 1754.96 1782.59 35.40 o
-4 1 2 861.19 960.40 10.59 o
-3 1 2 137.22 133.84 4.41 o
-1 1 2 5473.28 3271.77 18.03 o
0 1 2 71.79 82.94 0.76 o
1 1 2 5496.13 3292.37 18.05 o
3 1 2 134.13 131.17 5.32 o
4 1 2 876.23 950.22 17.18 o
5 1 2 868.85 817.70 12.18 o
6 1 2 1778.64 1842.99 23.83 o
7 1 2 45.46 39.50 5.33 o
8 1 2 19.56 18.06 1.62 o
9 1 2 237.70 258.63 3.69 o
10 1 2 126.41 136.41 2.74 o
11 1 2 110.47 104.21 6.83 o
-11 2 2 250.75 222.48 5.88 o
-10 2 2 51.92 48.39 2.93 o
-9 2 2 74.31 73.89 1.95 o
-8 2 2 293.28 316.24 9.34 o
-7 2 2 421.54 487.98 5.70 o
-6 2 2 827.15 913.06 12.38 o
-5 2 2 1229.93 1257.57 9.29 o
-4 2 2 207.81 228.42 5.96 o
-3 2 2 1263.72 1125.49 9.02 o
-2 2 2 2709.74 1911.83 8.67 o
-1 2 2 2216.20 1401.93 8.56 o
0 2 2 2671.33 1724.72 21.28 o
1 2 2 2224.98 1419.36 8.08 o
2 2 2 2712.18 1876.63 11.17 o
3 2 2 1272.64 1118.46 10.62 o
4 2 2 216.96 237.26 10.30 o
5 2 2 1238.64 1224.07 39.17 o
6 2 2 832.60 972.00 14.16 o
7 2 2 428.01 501.24 26.01 o
8 2 2 289.37 309.39 5.81 o
9 2 2 73.24 75.02 2.36 o
10 2 2 53.66 58.04 2.73 o
11 2 2 247.49 229.87 6.12 o
-11 3 2 54.03 46.11 4.24 o
-10 3 2 193.14 204.53 13.61 o
-9 3 2 166.40 180.49 18.02 o
-8 3 2 55.07 52.26 7.16 o
-7 3 2 63.08 54.69 5.75 o
-6 3 2 281.44 260.09 6.67 o
-5 3 2 123.94 120.66 1.81 o
-4 3 2 462.80 430.29 3.96 o
-3 3 2 1275.41 1363.55 8.41 o
-1 3 2 3999.55 2704.71 13.68 o
0 3 2 590.90 624.35 12.23 o
1 3 2 3993.70 2694.76 13.33 o
2 3 2 1509.79 1440.14 9.69 o
5 3 2 129.01 118.33 2.88 o
6 3 2 276.55 264.33 7.56 o
7 3 2 66.49 56.11 3.31 o
8 3 2 53.09 46.36 4.30 o
9 3 2 166.54 187.77 2.90 o
10 3 2 194.56 177.31 13.19 o
11 3 2 53.95 49.91 4.23 o
-11 4 2 17.63 16.66 1.38 o
-10 4 2 4.44 2.36 0.67 o
-9 4 2 35.58 33.26 3.59 o
-8 4 2 114.37 128.70 3.99 o
-7 4 2 214.78 225.86 5.75 o
-6 4 2 371.03 371.89 9.31 o
-5 4 2 82.01 104.23 5.79 o
-4 4 2 1584.55 1507.48 11.39 o
-3 4 2 4338.39 3468.81 80.11 o
-2 4 2 270.77 264.71 5.42 o
-1 4 2 929.40 933.35 14.30 o
0 4 2 324.30 323.71 5.29 o
2 4 2 269.41 253.26 4.22 o
3 4 2 4317.26 3555.51 41.59 o
5 4 2 84.19 104.19 4.47 o
6 4 2 372.58 351.42 11.89 o
7 4 2 222.12 248.05 7.47 o
8 4 2 117.76 133.83 3.54 o
9 4 2 36.95 38.66 2.00 o
10 4 2 4.67 1.92 0.85 o
11 4 2 18.40 17.18 1.24 o
-10 5 2 2.55 1.30 0.43 o
-9 5 2 32.20 29.51 4.45 o
-8 5 2 278.22 296.60 11.71 o
-7 5 2 152.02 158.77 4.18 o
-6 5 2 290.97 325.02 8.94 o
-5 5 2 403.59 437.90 8.40 o
-4 5 2 262.15 258.46 7.99 o
-1 5 2 3787.90 3264.16 91.68 o
0 5 2 121.95 155.47 3.21 o
2 5 2 2310.65 1917.99 13.43 o
4 5 2 262.61 269.68 8.04 o
5 5 2 397.44 455.82 9.03 o
6 5 2 287.81 304.85 4.72 o
7 5 2 147.73 151.40 5.77 o
8 5 2 277.52 294.08 3.89 o
9 5 2 31.49 26.07 1.85 o
10 5 2 2.56 1.86 0.64 o
-10 6 2 51.40 46.82 1.94 o
-9 6 2 59.63 58.94 4.06 o
-8 6 2 228.63 232.37 13.27 o
-7 6 2 182.66 154.05 7.44 o
-6 6 2 153.24 157.18 6.96 o
-5 6 2 86.17 76.47 2.76 o
-4 6 2 966.20 1066.22 21.45 o
-3 6 2 260.42 291.51 6.54 o
-2 6 2 124.48 128.89 3.85 o
-1 6 2 6.80 7.25 0.91 o
0 6 2 501.18 578.85 9.64 o
1 6 2 6.42 6.73 1.35 o
2 6 2 119.74 128.77 3.78 o
3 6 2 263.23 293.70 6.28 o
4 6 2 967.55 1084.68 17.80 o
5 6 2 86.81 72.18 2.69 o
6 6 2 154.65 162.06 4.37 o
7 6 2 181.47 157.49 3.50 o
8 6 2 234.01 236.49 6.32 o
9 6 2 58.93 53.67 2.67 o
10 6 2 51.62 43.46 3.98 o
-9 7 2 35.43 35.26 6.02 o
-8 7 2 202.60 171.49 6.49 o
-7 7 2 57.80 52.22 6.78 o
-6 7 2 194.23 203.79 5.08 o
-5 7 2 71.69 76.58 2.34 o
-4 7 2 601.28 712.44 14.20 o
-3 7 2 44.80 51.35 2.46 o
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1 1 18 287.60 281.16 11.87 o
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1 2 18 20.33 17.18 1.09 o
2 2 18 218.69 237.41 6.78 o
3 2 18 53.66 61.84 2.96 o
4 2 18 259.77 272.82 5.86 o
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1 3 18 8.81 9.88 1.66 o
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4 3 18 286.58 290.44 5.77 o
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1 4 18 40.34 39.30 1.45 o
2 4 18 25.74 23.87 3.21 o
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2 5 18 55.44 59.90 2.53 o
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1 8 18 131.15 127.46 10.91 o
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1 1 19 1.90 2.23 0.51 o
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1 2 19 158.42 168.39 3.98 o
2 2 19 92.32 83.41 5.80 o
3 2 19 620.09 667.41 18.93 o
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5 2 19 119.77 121.14 3.27 o
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-1 3 19 315.46 375.45 8.58 o
0 3 19 58.03 65.47 2.11 o
1 3 19 311.22 338.79 14.74 o
2 3 19 417.65 493.55 12.59 o
3 3 19 231.22 211.73 15.91 o
4 3 19 152.16 162.76 3.29 o
5 3 19 10.51 9.26 1.97 o
6 3 19 19.91 21.15 1.69 o
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0 4 19 7.75 13.50 1.98 o
1 4 19 366.73 354.54 13.08 o
2 4 19 69.99 84.71 4.56 o
3 4 19 198.76 221.35 3.39 o
4 4 19 9.92 8.84 1.70 o
5 4 19 143.72 145.28 3.31 o
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0 5 19 17.75 17.09 1.92 o
1 5 19 467.43 508.89 7.02 o
2 5 19 80.17 75.56 2.35 o
3 5 19 136.00 115.18 1.93 o
4 5 19 46.64 45.26 1.18 o
5 5 19 3.75 3.97 1.01 o
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1 6 19 57.32 49.05 8.65 o
2 6 19 9.60 8.69 0.88 o
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4 6 19 64.83 58.21 1.29 o
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0 7 19 112.47 105.63 3.11 o
1 7 19 250.48 262.34 9.39 o
2 7 19 34.41 26.85 1.56 o
3 7 19 13.15 11.57 1.16 o
0 8 19 18.33 19.71 1.79 o
1 8 19 177.82 188.40 2.20 o
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1 0 20 510.10 557.16 8.19 o
2 0 20 96.43 96.48 2.38 o
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4 0 20 269.72 258.53 13.37 o
5 0 20 120.68 99.53 3.66 o
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-1 1 20 357.82 371.89 9.34 o
0 1 20 687.18 734.24 19.81 o
1 1 20 361.59 373.23 14.98 o
2 1 20 494.51 523.69 16.73 o
3 1 20 256.05 260.28 5.35 o
4 1 20 77.47 80.50 3.20 o
5 1 20 22.20 16.85 3.50 o
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-2 2 20 555.38 591.01 27.08 o
-1 2 20 144.36 147.76 3.96 o
0 2 20 26.01 17.72 1.49 o
1 2 20 141.23 141.60 5.78 o
2 2 20 557.41 647.45 7.91 o
3 2 20 88.46 81.70 3.53 o
4 2 20 272.08 310.34 6.51 o
5 2 20 3.13 3.98 0.87 o
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-3 3 20 207.27 221.10 7.03 o
-2 3 20 314.13 354.08 7.85 o
-1 3 20 92.25 103.87 4.65 o
0 3 20 10.06 12.15 1.32 o
1 3 20 93.65 96.62 4.54 o
2 3 20 310.08 369.58 6.32 o
3 3 20 204.27 215.28 3.10 o
4 3 20 68.37 56.13 2.27 o
5 3 20 133.48 134.21 2.77 o
6 3 20 13.52 12.34 1.00 o
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-3 4 20 141.59 140.33 4.41 o
-2 4 20 59.38 48.76 2.10 o
-1 4 20 295.75 287.62 10.33 o
0 4 20 22.10 23.81 3.37 o
1 4 20 294.71 313.52 4.83 o
2 4 20 61.16 54.29 2.13 o
3 4 20 138.29 143.54 6.82 o
4 4 20 62.43 50.00 1.70 o
5 4 20 116.55 115.23 2.96 o
6 4 20 59.42 40.88 6.57 o
-5 5 20 41.46 39.66 2.50 o
-4 5 20 9.79 10.18 2.60 o
-3 5 20 26.26 24.49 1.69 o
-2 5 20 34.00 34.19 1.63 o
-1 5 20 118.95 117.05 3.47 o
0 5 20 186.64 232.59 11.93 o
1 5 20 118.43 128.43 2.53 o
2 5 20 33.65 33.20 1.59 o
3 5 20 25.76 21.82 1.10 o
4 5 20 9.65 7.90 1.12 o
5 5 20 40.42 35.77 2.96 o
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-3 6 20 31.18 26.74 1.80 o
-1 6 20 120.70 124.24 8.55 o
0 6 20 52.12 54.91 4.38 o
1 6 20 118.47 116.48 14.64 o
2 6 20 73.82 65.25 1.50 o
3 6 20 29.29 22.93 1.09 o
4 6 20 32.93 25.30 1.95 o
0 7 20 88.59 77.46 2.04 o
1 7 20 60.16 52.96 1.55 o
2 7 20 6.89 2.24 2.56 o
1 0 21 24.42 27.60 2.20 o
2 0 21 5.21 5.47 0.81 o
3 0 21 318.37 372.41 10.43 o
4 0 21 5.35 2.76 0.94 o
5 0 21 56.91 61.42 1.66 o
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-2 1 21 147.16 148.18 6.37 o
-1 1 21 181.19 181.58 2.48 o
0 1 21 52.04 48.95 2.50 o
1 1 21 180.23 174.94 4.12 o
2 1 21 145.93 168.46 13.58 o
3 1 21 389.80 413.11 16.26 o
4 1 21 24.04 23.26 1.72 o
5 1 21 226.17 222.50 4.92 o
-5 2 21 312.68 301.27 7.51 o
-4 2 21 54.62 47.05 8.47 o
-3 2 21 24.20 18.74 4.19 o
-2 2 21 441.13 481.87 20.26 o
-1 2 21 108.12 114.07 3.73 o
0 2 21 50.65 51.48 2.16 o
1 2 21 112.38 112.19 5.35 o
2 2 21 443.44 513.58 23.27 o
3 2 21 23.56 17.61 2.96 o
4 2 21 53.18 51.90 2.45 o
5 2 21 310.30 288.08 12.41 o
-5 3 21 21.24 19.48 2.48 o
-4 3 21 188.81 180.69 5.04 o
-3 3 21 280.22 267.72 11.34 o
-2 3 21 106.64 95.94 2.63 o
-1 3 21 57.31 54.68 3.52 o
0 3 21 3.52 2.01 0.57 o
1 3 21 56.22 55.88 1.90 o
2 3 21 102.81 95.83 3.69 o
3 3 21 279.99 295.39 10.50 o
4 3 21 190.44 196.42 5.57 o
5 3 21 21.66 18.70 1.69 o
-5 4 21 16.34 18.33 1.20 o
-4 4 21 59.84 63.85 2.26 o
-3 4 21 19.37 17.39 2.34 o
-2 4 21 13.45 13.40 1.96 o
-1 4 21 44.39 32.24 1.74 o
0 4 21 25.31 14.30 1.15 o
1 4 21 44.23 38.98 1.85 o
2 4 21 13.17 12.19 2.41 o
3 4 21 17.97 15.61 0.91 o
4 4 21 58.39 60.08 1.55 o
5 4 21 16.03 16.13 2.88 o
-4 5 21 245.76 218.95 23.37 o
-3 5 21 28.85 29.28 2.29 o
-2 5 21 13.14 11.55 0.62 o
-1 5 21 66.78 59.71 2.42 o
0 5 21 17.85 20.82 2.94 o
1 5 21 64.55 62.71 2.03 o
2 5 21 12.54 10.59 0.82 o
3 5 21 27.84 29.07 1.39 o
4 5 21 247.49 234.91 10.70 o
-2 6 21 1.07 0.13 0.55 o
-1 6 21 85.76 79.47 2.21 o
0 6 21 35.12 39.33 1.28 o
1 6 21 82.89 74.61 2.63 o
2 6 21 1.31 0.37 0.65 o
3 6 21 9.80 6.15 0.83 o
0 0 22 143.81 134.21 3.12 o
1 0 22 8.44 4.65 0.69 o
2 0 22 94.50 81.77 5.81 o
3 0 22 191.17 180.77 6.17 o
4 0 22 30.53 36.71 5.16 o
5 0 22 212.48 241.65 5.02 o
-5 1 22 45.13 38.94 2.53 o
-4 1 22 38.99 48.14 7.09 o
-3 1 22 193.85 189.82 21.18 o
-2 1 22 548.17 523.70 6.98 o
-1 1 22 509.05 508.41 7.49 o
0 1 22 534.32 575.39 8.70 o
1 1 22 513.11 486.69 9.57 o
2 1 22 553.53 603.62 12.72 o
3 1 22 192.70 192.76 5.75 o
4 1 22 38.47 39.65 4.16 o
5 1 22 46.42 38.78 4.13 o
-5 2 22 0.04 0.37 0.86 o
-4 2 22 95.58 94.74 3.54 o
-3 2 22 260.22 239.31 3.90 o
-2 2 22 136.66 140.93 4.55 o
-1 2 22 84.35 89.99 1.88 o
0 2 22 0.75 0.60 0.46 o
1 2 22 81.73 85.74 5.59 o
2 2 22 139.31 152.43 3.63 o
3 2 22 258.40 246.10 6.81 o
4 2 22 98.81 107.83 1.91 o
5 2 22 0.11 0.52 1.03 o
-4 3 22 90.06 82.96 2.35 o
-3 3 22 37.00 39.71 3.14 o
-2 3 22 108.33 103.99 2.83 o
-1 3 22 27.25 26.89 1.57 o
0 3 22 125.10 136.33 4.50 o
1 3 22 27.84 29.88 1.12 o
2 3 22 109.66 111.46 3.78 o
3 3 22 37.42 37.27 4.09 o
4 3 22 87.14 78.29 1.38 o
-4 4 22 106.92 97.04 7.25 o
-3 4 22 82.46 95.43 1.87 o
-2 4 22 15.79 14.24 1.20 o
-1 4 22 67.18 51.25 1.42 o
0 4 22 2.86 3.23 0.71 o
1 4 22 65.82 53.97 2.20 o
2 4 22 15.41 13.24 1.02 o
3 4 22 84.22 100.98 2.93 o
4 4 22 107.52 94.51 5.62 o
-2 5 22 56.31 58.87 1.77 o
-1 5 22 31.73 33.72 2.35 o
0 5 22 1.18 1.33 0.56 o
1 5 22 31.89 32.28 2.06 o
2 5 22 56.74 58.16 3.08 o
3 5 22 22.47 21.02 0.95 o
1 6 22 0.72 0.31 0.54 o
1 0 23 0.69 0.70 0.29 o
2 0 23 124.65 150.76 9.01 o
3 0 23 196.74 209.75 4.01 o
4 0 23 1.81 3.84 1.48 o
-4 1 23 4.45 2.93 1.13 o
-3 1 23 16.75 16.85 1.10 o
-2 1 23 144.44 145.67 6.52 o
-1 1 23 131.05 120.18 7.46 o
0 1 23 56.62 54.66 1.99 o
1 1 23 131.38 118.60 11.07 o
2 1 23 145.50 143.87 6.21 o
3 1 23 17.38 14.03 0.85 o
4 1 23 5.11 2.60 0.88 o
-4 2 23 23.62 18.73 1.15 o
-3 2 23 45.43 45.54 1.27 o
-2 2 23 16.20 11.83 1.20 o
-1 2 23 12.75 13.61 1.12 o
0 2 23 11.03 9.35 1.39 o
1 2 23 12.85 13.46 1.88 o
2 2 23 16.49 14.82 1.10 o
3 2 23 43.55 47.90 1.10 o
4 2 23 25.33 26.27 2.80 o
-3 3 23 232.55 212.10 16.19 o
-2 3 23 245.54 248.90 10.29 o
-1 3 23 20.25 18.49 0.69 o
0 3 23 0.45 0.07 0.34 o
1 3 23 19.33 17.13 1.38 o
2 3 23 247.51 278.26 5.35 o
3 3 23 231.35 226.54 4.47 o
-2 4 23 36.51 33.00 1.81 o
-1 4 23 215.38 200.46 4.32 o
0 4 23 3.43 2.07 0.64 o
1 4 23 214.85 189.58 12.62 o
2 4 23 36.11 32.78 2.26 o
0 5 23 33.40 29.52 1.12 o
1 5 23 27.11 21.53 1.41 o
0 0 24 8.40 5.17 1.71 o
1 0 24 9.38 3.59 1.14 o
2 0 24 68.78 77.41 3.40 o
3 0 24 48.03 46.85 1.91 o
-3 1 24 83.33 79.14 3.34 o
-2 1 24 22.73 18.97 1.18 o
-1 1 24 12.23 11.54 0.83 o
0 1 24 1.24 0.55 0.50 o
1 1 24 12.35 11.18 1.47 o
2 1 24 22.87 17.76 1.05 o
3 1 24 83.12 74.35 4.81 o
-2 2 24 104.11 100.02 6.29 o
-1 2 24 39.82 30.12 1.58 o
0 2 24 121.07 114.21 13.58 o
1 2 24 40.54 37.31 1.25 o
2 2 24 101.97 97.13 1.93 o
-2 3 24 16.61 16.64 1.06 o
-1 3 24 68.62 72.35 3.15 o
0 3 24 6.69 1.92 0.82 o
1 3 24 66.13 67.17 4.04 o
2 3 24 15.77 15.44 0.98 o
1 0 25 0.00 0.24 0.81 o
0 1 25 46.35 34.30 1.86 o