#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/27/2232729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232729_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Al-Youbi, Abdulrahman O.' 'Khan, Salman A.' 'Tahir, M. Nawaz' _publ_section_title ; 2-[(3,5-Dimethyl-1-phenyl-1H-pyrazol-4-yl)methylidene]indan-1,3-dione ; _journal_coeditor_code HB6509 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3419 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.251 _cell_angle_gamma 90.000 _cell_length_a 14.6655 _cell_length_b 7.8902 _cell_length_c 28.6651 _exptl_crystal_F_000 1376.00 _reflns_d_resolution_high 0.8331 _[local]_cod_data_source_file hb6509Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NAS8_0m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 325.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28208.66 25048.50 340.58 o 4 0 0 1775.52 1780.94 31.74 o 6 0 0 28602.81 28642.81 444.54 o 8 0 0 0.56 -2.49 8.12 o 10 0 0 8113.57 8447.92 189.02 o 12 0 0 397.77 506.71 36.65 o 14 0 0 153.90 106.77 28.17 o 16 0 0 91.44 45.61 19.88 o 1 1 0 1378.52 1103.08 15.37 o 3 1 0 4035.01 3866.22 31.94 o 5 1 0 122.97 112.79 5.56 o 7 1 0 4.21 24.04 5.73 o 9 1 0 110.68 134.67 9.39 o 11 1 0 519.21 503.28 25.12 o 13 1 0 498.06 464.49 32.50 o 15 1 0 14.78 7.48 10.93 o 17 1 0 43.49 41.66 14.28 o 0 2 0 98068.04 90228.88 1414.04 o 2 2 0 42167.77 40318.61 386.17 o 4 2 0 9998.10 10134.85 83.33 o 6 2 0 0.08 -5.75 3.83 o 8 2 0 3467.76 3439.92 46.71 o 10 2 0 2030.32 2183.49 37.04 o 12 2 0 2.74 6.66 6.61 o 14 2 0 36.72 58.72 13.19 o 16 2 0 220.92 247.35 23.35 o 1 3 0 2115.31 1913.67 34.73 o 3 3 0 397.02 411.37 12.98 o 5 3 0 3738.52 3775.30 51.12 o 7 3 0 28.10 15.72 6.02 o 9 3 0 112.25 122.42 11.27 o 11 3 0 1509.78 1425.03 47.15 o 13 3 0 533.01 528.88 30.34 o 15 3 0 3.80 -8.37 10.28 o 0 4 0 1838.59 1990.10 60.73 o 2 4 0 17976.88 17798.24 226.81 o 4 4 0 5445.20 5328.93 86.30 o 6 4 0 129.58 130.36 11.51 o 8 4 0 8.22 9.30 11.22 o 10 4 0 8.01 32.49 13.71 o 12 4 0 587.95 576.02 52.71 o 14 4 0 6.42 14.07 14.43 o 1 5 0 938.29 898.32 30.02 o 3 5 0 104.30 134.78 14.82 o 5 5 0 7.25 5.36 6.53 o 7 5 0 4.45 -6.71 8.11 o 9 5 0 939.50 1025.47 41.65 o 11 5 0 47.57 81.11 21.53 o 13 5 0 0.46 12.37 15.35 o 0 6 0 524.25 516.65 40.49 o 2 6 0 11.24 4.41 10.49 o 4 6 0 164.52 177.73 22.92 o 6 6 0 0.31 -1.22 10.15 o 8 6 0 103.56 91.18 25.61 o 10 6 0 128.50 124.22 32.42 o 12 6 0 145.56 149.17 30.00 o 1 7 0 172.99 159.80 22.29 o 3 7 0 100.64 88.27 19.69 o 5 7 0 109.36 115.52 24.63 o 7 7 0 186.10 134.79 28.68 o 9 7 0 89.88 91.25 20.65 o 11 7 0 30.90 50.26 43.03 o 0 8 0 14.20 -5.12 23.56 o 2 8 0 171.23 86.85 55.32 o 4 8 0 163.88 144.57 31.24 o 6 8 0 8.90 12.50 19.83 o 8 8 0 33.06 63.10 24.79 o 1 9 0 6.38 -3.04 20.13 o 3 9 0 41.21 39.98 30.22 o 5 9 0 13.59 14.23 22.40 o -17 1 1 12.91 15.13 13.30 o -15 1 1 73.12 63.59 13.88 o -13 1 1 831.25 706.69 42.58 o -11 1 1 2620.65 2531.01 54.38 o -9 1 1 1195.58 1220.46 26.20 o -7 1 1 440.72 526.09 22.29 o -5 1 1 7739.49 7770.62 70.80 o -3 1 1 7288.32 6816.23 51.61 o -1 1 1 4703.44 4231.13 43.01 o 1 1 1 17489.15 16530.12 158.23 o 3 1 1 1353.73 1194.04 17.18 o 5 1 1 520.28 590.81 14.17 o 7 1 1 207.45 252.80 9.69 o 9 1 1 16.26 11.18 5.88 o 11 1 1 126.16 96.98 14.59 o 13 1 1 6.62 8.01 9.56 o 15 1 1 0.58 -7.73 10.08 o 17 1 1 0.48 -9.53 11.39 o -16 2 1 2.94 3.21 11.25 o -14 2 1 6.73 20.07 11.47 o -12 2 1 105.43 75.69 9.95 o -10 2 1 76.61 79.73 8.27 o -8 2 1 3776.88 3821.76 48.65 o -6 2 1 2592.41 2945.78 33.76 o -4 2 1 3344.33 3265.26 30.56 o -2 2 1 106179.52 100173.27 907.81 o 0 2 1 99185.95 91724.25 932.80 o 2 2 1 22862.99 21611.71 197.36 o 4 2 1 9098.15 9307.22 84.51 o 6 2 1 160.94 153.43 7.71 o 8 2 1 1506.20 1610.38 24.58 o 10 2 1 2836.77 2975.88 63.10 o 12 2 1 650.34 581.63 29.33 o 14 2 1 0.31 3.33 12.35 o 16 2 1 121.56 120.83 18.72 o -15 3 1 289.59 332.09 26.25 o -13 3 1 419.02 432.82 27.64 o -11 3 1 159.48 182.38 18.63 o -9 3 1 928.48 914.59 27.39 o -7 3 1 10.56 -1.59 5.91 o -5 3 1 803.84 849.47 18.39 o -3 3 1 3757.34 3570.46 45.47 o -1 3 1 4934.95 4761.62 68.73 o 1 3 1 1842.03 1880.72 30.96 o 3 3 1 416.17 400.47 16.57 o 5 3 1 43.24 33.18 5.77 o 7 3 1 0.43 -0.27 5.32 o 9 3 1 24.75 51.91 7.37 o 11 3 1 24.18 50.69 18.93 o 13 3 1 13.86 13.37 10.69 o 15 3 1 14.59 9.25 11.83 o -14 4 1 64.73 45.23 18.07 o -12 4 1 12.95 29.91 14.01 o -10 4 1 57.88 58.63 15.10 o -8 4 1 194.54 162.53 18.36 o -6 4 1 1779.89 1667.34 32.24 o -4 4 1 6154.15 6202.40 87.93 o -2 4 1 733.11 720.01 29.13 o 0 4 1 696.84 648.93 24.38 o 2 4 1 350.58 416.65 57.08 o 4 4 1 392.67 381.61 26.20 o 6 4 1 1586.63 1656.09 46.58 o 8 4 1 85.19 116.58 17.30 o 10 4 1 2021.70 1935.16 62.55 o 12 4 1 562.30 607.48 39.36 o 14 4 1 17.26 15.46 15.09 o -13 5 1 12.81 26.45 16.20 o -11 5 1 315.21 308.35 28.18 o -9 5 1 35.58 60.17 15.76 o -7 5 1 1334.21 1295.91 31.25 o -5 5 1 1715.63 1729.00 32.82 o -3 5 1 188.74 204.15 17.49 o -1 5 1 1247.14 1242.33 40.86 o 1 5 1 2.38 -8.69 8.73 o 3 5 1 78.04 50.74 14.12 o 5 5 1 712.13 713.56 27.21 o 7 5 1 502.44 466.10 51.67 o 9 5 1 120.06 145.81 21.44 o 11 5 1 42.61 62.84 17.77 o 13 5 1 9.07 -1.52 13.78 o -12 6 1 5.88 9.88 18.38 o -10 6 1 237.18 211.34 30.92 o -8 6 1 587.33 535.22 35.36 o -6 6 1 451.40 483.67 27.80 o -4 6 1 2448.99 2369.95 56.71 o -2 6 1 878.58 845.01 34.93 o 0 6 1 214.41 185.29 18.42 o 2 6 1 442.55 472.96 31.32 o 4 6 1 811.25 726.15 32.19 o 6 6 1 436.70 430.45 32.45 o 8 6 1 401.77 410.90 37.93 o 10 6 1 119.58 121.73 21.70 o 12 6 1 118.75 83.92 25.10 o -11 7 1 44.29 28.36 19.52 o -9 7 1 0.01 3.52 19.10 o -7 7 1 3.41 -2.90 16.61 o -5 7 1 3.28 29.71 18.11 o -3 7 1 128.14 140.42 23.92 o -1 7 1 58.79 60.33 16.64 o 1 7 1 180.70 124.84 20.64 o 3 7 1 385.54 424.70 70.40 o 5 7 1 1.47 -18.91 12.61 o 7 7 1 499.14 495.71 84.51 o 9 7 1 41.94 81.89 24.61 o 11 7 1 7.20 7.22 20.56 o -8 8 1 8.37 49.79 23.77 o -6 8 1 26.22 43.01 23.53 o -4 8 1 48.60 60.95 23.18 o -2 8 1 165.77 125.53 27.10 o 0 8 1 69.08 57.30 22.01 o 2 8 1 14.28 6.54 17.74 o 4 8 1 127.51 177.29 31.85 o 6 8 1 9.34 -16.63 21.51 o 8 8 1 87.11 78.40 26.43 o -5 9 1 84.01 44.34 25.32 o -3 9 1 72.38 77.51 47.12 o -1 9 1 4.49 9.73 19.56 o 1 9 1 372.43 388.26 65.56 o 3 9 1 192.02 201.62 35.72 o 5 9 1 78.15 95.82 28.95 o -16 0 2 71.41 93.86 35.85 o -14 0 2 1433.89 1290.22 55.27 o -12 0 2 3379.57 3187.38 91.31 o -10 0 2 130.79 136.48 27.15 o -8 0 2 24676.41 26072.98 510.14 o -6 0 2 271.22 266.11 12.79 o -4 0 2 9249.96 9418.08 118.28 o -2 0 2 66804.84 59038.02 723.98 o 0 0 2 0.43 -1.33 0.89 o 2 0 2 46328.69 41221.66 558.30 o 4 0 2 24.01 17.47 4.42 o 6 0 2 5790.81 5657.75 98.46 o 8 0 2 2202.99 2787.16 119.34 o 10 0 2 2033.07 2017.19 65.61 o 12 0 2 462.03 430.95 35.68 o 14 0 2 1380.82 1255.77 57.34 o 16 0 2 49.95 58.76 20.28 o -17 1 2 54.89 59.66 14.68 o -15 1 2 564.38 564.98 44.51 o -13 1 2 658.98 645.34 27.92 o -11 1 2 5.25 6.04 7.72 o -9 1 2 0.30 -2.17 4.90 o -7 1 2 267.80 213.84 12.42 o -5 1 2 1327.13 1314.09 14.75 o -3 1 2 1677.63 1684.89 15.41 o -1 1 2 4630.31 4252.93 55.58 o 1 1 2 399.79 302.84 8.36 o 3 1 2 2437.96 2363.18 27.64 o 5 1 2 4513.36 4487.77 47.04 o 7 1 2 4.49 9.92 4.67 o 9 1 2 581.16 579.02 20.22 o 11 1 2 204.93 191.22 16.94 o 13 1 2 190.55 198.79 25.58 o 15 1 2 8.49 0.49 10.51 o 17 1 2 20.98 -3.31 13.31 o -16 2 2 1.36 -9.05 10.48 o -14 2 2 50.54 61.69 13.64 o -12 2 2 4.90 3.63 7.22 o -10 2 2 11.36 9.77 5.89 o -8 2 2 4196.20 4464.58 55.52 o -6 2 2 68.92 74.64 5.04 o -4 2 2 5619.27 5530.48 48.39 o -2 2 2 9395.94 9364.90 100.53 o 0 2 2 550.82 463.01 14.01 o 2 2 2 43109.62 41638.99 396.33 o 4 2 2 4583.71 4327.05 48.15 o 6 2 2 4601.03 5079.13 57.18 o 8 2 2 1318.44 1401.77 27.59 o 10 2 2 3564.72 3498.61 53.50 o 12 2 2 1072.12 946.14 51.46 o 14 2 2 734.59 722.35 42.88 o 16 2 2 120.98 98.80 18.20 o -15 3 2 35.21 44.08 13.09 o -13 3 2 13.31 -7.58 9.36 o -11 3 2 4.71 0.80 10.79 o -9 3 2 15.83 12.09 8.58 o -7 3 2 2153.48 2114.08 31.91 o -5 3 2 146.10 157.84 8.36 o -3 3 2 10305.30 10489.11 115.13 o -1 3 2 8209.02 8130.71 120.49 o 1 3 2 316.93 327.95 45.88 o 3 3 2 791.10 728.90 21.73 o 5 3 2 784.65 804.42 18.63 o 7 3 2 1042.42 1049.54 22.38 o 9 3 2 1932.40 1886.00 45.83 o 11 3 2 84.17 92.90 14.58 o 13 3 2 13.41 27.09 11.97 o 15 3 2 0.05 17.77 12.22 o -14 4 2 246.44 318.05 30.57 o -12 4 2 273.09 255.84 26.32 o -10 4 2 80.70 56.98 14.58 o -8 4 2 62.12 58.57 13.37 o -6 4 2 857.86 901.51 20.81 o -4 4 2 13617.91 13594.09 160.87 o -2 4 2 278.70 261.90 17.22 o 0 4 2 839.03 847.89 26.54 o 2 4 2 1674.03 1608.51 64.51 o 4 4 2 2614.06 2499.89 73.84 o 6 4 2 3669.69 3989.83 69.98 o 8 4 2 744.85 764.56 32.70 o 10 4 2 455.08 456.22 32.68 o 12 4 2 4.88 -10.85 12.21 o 14 4 2 117.56 127.38 22.26 o -13 5 2 3.05 -0.71 13.85 o -11 5 2 5.86 2.90 12.57 o -9 5 2 132.27 115.67 23.92 o -7 5 2 23.25 13.00 6.91 o -5 5 2 43.75 39.29 8.30 o -3 5 2 7.19 14.60 11.25 o -1 5 2 36.15 46.27 13.24 o 1 5 2 552.78 546.71 30.13 o 3 5 2 48.95 57.58 15.64 o 5 5 2 41.07 30.89 17.93 o 7 5 2 21.93 22.59 12.08 o 9 5 2 170.02 188.15 19.85 o 11 5 2 187.05 175.08 23.00 o 13 5 2 88.56 103.36 21.78 o -12 6 2 18.60 33.25 18.30 o -10 6 2 12.39 34.41 18.46 o -8 6 2 345.96 304.88 27.53 o -6 6 2 838.81 753.89 24.92 o -4 6 2 172.79 193.05 16.59 o -2 6 2 15.41 28.30 12.89 o 0 6 2 10.13 3.10 12.07 o 2 6 2 749.36 729.66 39.42 o 4 6 2 247.10 244.74 14.23 o 6 6 2 98.34 89.16 18.03 o 8 6 2 203.87 182.08 28.73 o 10 6 2 564.36 472.40 43.78 o 12 6 2 32.86 31.76 20.56 o -11 7 2 1.17 21.34 34.83 o -9 7 2 0.12 -23.13 26.63 o -7 7 2 37.63 20.28 17.74 o -5 7 2 0.09 16.19 16.19 o -3 7 2 509.96 450.72 33.26 o -1 7 2 563.64 515.06 35.45 o 1 7 2 347.91 349.52 29.92 o 3 7 2 256.79 286.99 34.98 o 5 7 2 128.16 122.35 22.32 o 7 7 2 168.80 146.67 23.68 o 9 7 2 59.04 81.53 25.23 o 11 7 2 98.50 18.78 21.59 o -8 8 2 136.19 156.47 31.50 o -6 8 2 417.52 408.88 42.99 o -4 8 2 19.79 -24.43 16.29 o -2 8 2 35.81 32.06 17.52 o 0 8 2 9.66 1.30 15.46 o 2 8 2 12.89 -14.10 13.79 o 4 8 2 22.79 57.39 25.35 o 6 8 2 226.75 250.45 36.58 o 8 8 2 173.30 234.39 38.06 o -5 9 2 157.89 133.93 40.46 o -3 9 2 0.78 4.00 19.67 o -1 9 2 45.01 110.70 28.95 o 1 9 2 128.92 65.05 25.35 o 3 9 2 106.20 101.38 73.76 o 5 9 2 76.84 85.31 28.55 o -17 1 3 7.44 -9.37 10.12 o -15 1 3 2.15 19.01 11.09 o -13 1 3 111.85 102.00 13.75 o -11 1 3 19.72 17.36 10.35 o -9 1 3 1416.89 1438.97 28.77 o -7 1 3 178.42 234.34 11.10 o -5 1 3 3556.62 3678.19 32.95 o -3 1 3 400.68 435.16 6.50 o -1 1 3 3017.51 3008.64 30.23 o 1 1 3 5903.21 5680.16 53.68 o 3 1 3 12430.85 11781.50 109.24 o 5 1 3 5742.26 5667.61 66.12 o 7 1 3 4.59 11.13 3.84 o 9 1 3 851.01 804.40 18.84 o 11 1 3 1466.02 1565.08 54.27 o 13 1 3 758.48 740.65 54.12 o 15 1 3 57.78 67.89 14.85 o 17 1 3 0.05 0.67 12.51 o -16 2 3 528.21 545.85 31.51 o -14 2 3 1870.08 1822.91 61.95 o -12 2 3 2270.41 2060.93 42.32 o -10 2 3 1830.27 1845.87 37.85 o -8 2 3 531.63 661.27 29.31 o -6 2 3 214.77 314.00 9.84 o -4 2 3 2190.13 2096.68 20.20 o -2 2 3 38666.59 37704.22 359.86 o 0 2 3 4042.11 3905.17 61.13 o 2 2 3 10073.47 9773.84 98.55 o 4 2 3 186.17 167.60 6.89 o 6 2 3 4018.20 4300.28 52.73 o 8 2 3 21.41 13.09 4.84 o 10 2 3 35.34 37.50 7.84 o 12 2 3 73.03 79.34 13.89 o 14 2 3 6.39 15.02 11.14 o 16 2 3 9.78 48.56 14.84 o -15 3 3 9.87 6.69 13.83 o -13 3 3 58.69 47.66 15.31 o -11 3 3 714.12 731.46 35.75 o -9 3 3 1.00 -5.72 6.45 o -7 3 3 69.22 80.07 8.35 o -5 3 3 600.03 558.17 15.44 o -3 3 3 576.11 590.44 15.68 o -1 3 3 2437.02 2316.27 43.36 o 1 3 3 66.21 54.38 7.44 o 3 3 3 1990.01 1908.19 65.50 o 5 3 3 4306.89 4253.57 72.45 o 7 3 3 973.79 988.67 21.71 o 9 3 3 352.32 396.55 16.78 o 11 3 3 652.45 630.01 26.54 o 13 3 3 5.28 -2.39 10.74 o 15 3 3 1.72 14.48 12.73 o -14 4 3 68.20 55.16 17.96 o -12 4 3 332.56 348.38 29.35 o -10 4 3 1869.46 1826.02 55.68 o -8 4 3 0.08 2.22 6.56 o -6 4 3 7.04 3.30 5.83 o -4 4 3 3712.67 3692.96 57.74 o -2 4 3 11368.35 11332.80 191.85 o 0 4 3 5398.30 5112.81 110.60 o 2 4 3 11789.26 12066.26 248.78 o 4 4 3 75.68 135.14 25.61 o 6 4 3 856.17 845.43 47.39 o 8 4 3 134.68 169.30 19.04 o 10 4 3 1164.49 1049.34 46.97 o 12 4 3 389.23 464.57 34.46 o 14 4 3 33.26 35.73 19.59 o -13 5 3 38.52 30.05 15.82 o -11 5 3 0.86 -2.86 12.63 o -9 5 3 142.50 128.41 17.93 o -7 5 3 20.06 22.88 7.19 o -5 5 3 1030.25 1053.45 30.46 o -3 5 3 4326.42 4320.76 90.65 o -1 5 3 3606.61 3488.96 96.30 o 1 5 3 1635.51 1574.17 44.25 o 3 5 3 5.87 11.87 8.83 o 5 5 3 199.62 217.64 27.27 o 7 5 3 1885.80 1825.36 67.91 o 9 5 3 2206.27 2237.43 56.39 o 11 5 3 88.83 80.20 16.36 o 13 5 3 29.16 1.78 18.65 o -12 6 3 36.45 26.42 18.70 o -10 6 3 402.99 350.78 36.22 o -8 6 3 31.98 37.68 22.40 o -6 6 3 541.22 527.22 22.26 o -4 6 3 109.05 100.12 13.41 o -2 6 3 375.67 325.39 26.52 o 0 6 3 431.60 408.77 46.12 o 2 6 3 81.97 99.22 17.84 o 4 6 3 841.61 913.05 83.48 o 6 6 3 151.87 148.56 21.48 o 8 6 3 104.76 92.53 23.61 o 10 6 3 12.31 -0.53 13.91 o 12 6 3 126.14 110.87 22.58 o -11 7 3 51.94 52.91 22.32 o -9 7 3 7.70 27.66 19.56 o -7 7 3 326.81 307.54 29.21 o -5 7 3 142.52 136.72 22.41 o -3 7 3 212.65 244.63 33.76 o -1 7 3 34.93 47.73 16.57 o 1 7 3 0.66 6.65 14.04 o 3 7 3 1545.72 1619.40 56.83 o 5 7 3 539.04 580.02 39.41 o 7 7 3 0.03 6.20 18.82 o 9 7 3 284.12 245.24 29.17 o 11 7 3 51.38 78.65 27.32 o -8 8 3 3.36 33.02 21.70 o -6 8 3 20.01 44.08 22.08 o -4 8 3 1.74 38.21 17.29 o -2 8 3 0.30 -16.55 13.50 o 0 8 3 51.84 49.88 18.16 o 2 8 3 74.11 88.97 20.63 o 4 8 3 130.70 184.23 66.59 o 6 8 3 682.42 745.67 48.86 o 8 8 3 318.65 368.40 43.39 o -5 9 3 6.47 -1.31 22.08 o -3 9 3 123.06 102.63 28.95 o -1 9 3 0.31 -9.53 18.17 o 1 9 3 0.89 16.60 19.16 o 3 9 3 252.72 176.64 34.75 o -16 0 4 731.34 684.80 88.61 o -14 0 4 695.26 708.52 75.81 o -12 0 4 287.09 360.81 44.05 o -10 0 4 1456.29 1504.22 50.35 o -8 0 4 5910.19 6502.84 84.04 o -6 0 4 32.16 39.79 5.91 o -4 0 4 26.35 16.54 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