#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/27/2232739.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232739_Fobs loop_ _publ_author_name 'Arshad, Muhammad Nadeem' 'Khan, Islam Ullah' 'Zia-ur-Rehman, Muhammad' 'Danish, Muhammad' 'Holman, K. Travis' _publ_section_title ; Methyl 4-hydroxy-1,1-dioxo-2-(2-phenylethyl)-2H-1\l^6^,2-benzothiazine-3-carboxylate ; _journal_coeditor_code HB6520 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3445 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.441 _cell_angle_gamma 90.000 _cell_length_a 9.0178 _cell_length_b 19.0259 _cell_length_c 10.1931 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.7474 _[local]_cod_data_source_file hb6520Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 10104 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 232.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2647.44 2691.20 93.30 o 2 0 0 197.14 206.43 11.74 o 3 0 0 3934.68 3849.71 135.32 o 4 0 0 652.44 675.31 29.97 o 5 0 0 7506.15 7248.43 253.72 o 6 0 0 198.11 225.32 17.14 o 7 0 0 466.60 394.56 61.99 o 8 0 0 552.69 500.18 45.08 o 9 0 0 7.63 4.36 16.13 o 10 0 0 134.68 113.73 26.96 o 11 0 0 282.56 271.26 46.21 o 1 1 0 7435.70 7513.22 208.02 o 2 1 0 3053.75 3084.58 76.65 o 3 1 0 5.25 -0.61 4.98 o 4 1 0 202.37 190.41 9.71 o 5 1 0 1702.98 1630.42 44.59 o 6 1 0 2003.35 1918.17 52.21 o 7 1 0 173.78 195.53 21.72 o 8 1 0 111.00 103.15 15.33 o 9 1 0 5.02 13.19 11.09 o 10 1 0 68.12 72.29 16.13 o 11 1 0 2.06 -5.62 14.09 o 0 2 0 676.85 594.80 22.88 o 1 2 0 300.18 344.11 12.54 o 2 2 0 3993.31 3964.77 112.23 o 3 2 0 4598.14 4527.69 112.32 o 4 2 0 45.79 41.86 5.99 o 5 2 0 58.87 64.56 7.20 o 6 2 0 89.10 81.59 12.79 o 7 2 0 903.76 831.71 32.25 o 8 2 0 429.87 422.68 29.20 o 9 2 0 2.51 4.28 11.66 o 10 2 0 461.92 459.99 32.50 o 11 2 0 4.60 1.19 14.41 o 1 3 0 1.56 -3.62 3.62 o 2 3 0 1466.75 1447.90 44.10 o 3 3 0 61.83 51.51 7.35 o 4 3 0 4656.15 4486.40 121.36 o 5 3 0 504.70 497.29 21.41 o 6 3 0 50.49 45.18 9.32 o 7 3 0 110.95 126.69 13.40 o 8 3 0 155.11 152.93 18.71 o 9 3 0 385.04 379.56 27.47 o 10 3 0 262.06 281.73 35.79 o 11 3 0 306.90 276.42 27.97 o 0 4 0 130.99 129.53 11.11 o 1 4 0 4.62 5.38 5.19 o 2 4 0 23.02 45.14 7.23 o 3 4 0 6.36 10.42 6.46 o 4 4 0 363.80 331.83 16.38 o 5 4 0 47.23 38.30 8.99 o 6 4 0 223.66 228.11 15.56 o 7 4 0 550.01 542.83 25.53 o 8 4 0 290.91 273.89 22.66 o 9 4 0 110.99 111.44 17.03 o 10 4 0 172.62 201.80 22.88 o 11 4 0 146.45 139.62 29.12 o 1 5 0 7806.62 7311.24 209.55 o 2 5 0 134.97 148.59 9.30 o 3 5 0 2674.95 2780.10 82.21 o 4 5 0 7.29 8.59 7.45 o 5 5 0 116.17 116.02 15.49 o 6 5 0 1458.83 1458.24 49.38 o 7 5 0 198.28 230.29 32.34 o 8 5 0 299.82 284.64 19.84 o 9 5 0 32.57 40.76 14.41 o 10 5 0 40.87 19.15 14.03 o 11 5 0 141.75 152.86 32.33 o 0 6 0 9094.62 9056.11 314.05 o 1 6 0 158.24 197.49 11.34 o 2 6 0 141.94 115.31 9.79 o 3 6 0 1296.38 1285.51 42.39 o 4 6 0 1.94 -3.69 8.36 o 5 6 0 374.89 371.32 19.30 o 6 6 0 2.32 0.45 8.81 o 7 6 0 554.74 525.29 25.84 o 8 6 0 51.00 58.02 12.81 o 9 6 0 22.51 21.20 13.89 o 10 6 0 106.99 124.51 19.47 o 11 6 0 285.00 333.60 61.99 o 1 7 0 17.61 22.97 8.31 o 2 7 0 2913.60 3101.46 84.68 o 3 7 0 619.38 685.89 27.90 o 4 7 0 488.69 514.19 22.90 o 5 7 0 426.08 525.25 23.72 o 6 7 0 29.39 32.19 10.84 o 7 7 0 613.93 627.04 29.44 o 8 7 0 8.50 14.89 10.87 o 9 7 0 331.80 317.76 27.28 o 10 7 0 16.89 16.74 18.38 o 0 8 0 228.81 255.08 19.23 o 1 8 0 930.15 1013.50 33.78 o 2 8 0 18.07 17.96 6.92 o 3 8 0 617.23 637.53 21.51 o 4 8 0 1279.44 1423.36 48.20 o 5 8 0 0.94 -7.92 8.28 o 6 8 0 94.76 65.45 12.33 o 7 8 0 1396.27 1351.53 48.86 o 8 8 0 62.57 71.99 14.35 o 9 8 0 281.36 278.96 23.72 o 10 8 0 195.09 165.70 23.22 o 1 9 0 1628.05 1560.13 51.62 o 2 9 0 1959.04 2049.58 60.01 o 3 9 0 12.11 14.72 6.91 o 4 9 0 1565.34 1546.70 52.60 o 5 9 0 0.01 6.25 9.53 o 6 9 0 442.98 486.55 26.96 o 7 9 0 482.05 461.92 25.98 o 8 9 0 237.86 249.75 20.96 o 9 9 0 1180.80 1204.89 60.97 o 10 9 0 14.27 9.83 19.93 o 0 10 0 1031.05 1101.39 49.09 o 1 10 0 197.55 178.75 15.08 o 2 10 0 826.33 847.50 28.65 o 3 10 0 110.90 89.24 11.56 o 4 10 0 138.09 141.48 14.98 o 5 10 0 138.54 144.67 15.67 o 6 10 0 41.69 19.25 11.43 o 7 10 0 337.64 341.95 23.28 o 8 10 0 127.80 120.93 16.99 o 9 10 0 145.56 145.29 19.06 o 10 10 0 81.28 99.29 25.00 o 1 11 0 162.15 238.65 16.64 o 2 11 0 1175.24 1141.87 36.36 o 3 11 0 405.59 399.41 23.22 o 4 11 0 231.83 217.53 18.64 o 5 11 0 410.17 449.61 25.56 o 6 11 0 0.20 -0.59 10.88 o 7 11 0 30.61 21.39 13.52 o 8 11 0 5.20 -9.37 13.09 o 9 11 0 266.43 337.77 30.06 o 10 11 0 9.25 39.04 19.31 o 0 12 0 3356.73 3502.17 132.15 o 1 12 0 532.06 534.97 30.57 o 2 12 0 0.20 8.39 8.94 o 3 12 0 3583.50 3663.48 121.30 o 4 12 0 5.04 10.21 11.61 o 5 12 0 127.42 140.55 17.15 o 6 12 0 13.61 28.48 13.20 o 7 12 0 10.90 -1.27 13.02 o 8 12 0 285.17 316.11 25.53 o 9 12 0 39.51 72.41 17.73 o 10 12 0 118.84 132.76 25.70 o 1 13 0 122.61 157.06 13.94 o 2 13 0 2.69 -6.86 9.35 o 3 13 0 162.73 168.98 18.52 o 4 13 0 59.48 68.46 14.60 o 5 13 0 325.85 373.22 30.22 o 6 13 0 39.98 23.31 15.67 o 7 13 0 47.15 37.19 15.24 o 8 13 0 183.71 186.56 22.28 o 9 13 0 142.03 117.85 27.27 o 0 14 0 1292.23 1438.50 63.10 o 1 14 0 16.15 13.15 10.86 o 2 14 0 1581.72 1495.59 46.58 o 3 14 0 388.17 373.03 25.49 o 4 14 0 131.92 128.90 17.87 o 5 14 0 39.01 41.54 15.29 o 6 14 0 580.73 628.77 34.04 o 7 14 0 888.71 909.66 42.93 o 8 14 0 15.95 -4.79 16.08 o 9 14 0 58.94 41.24 20.00 o 1 15 0 2905.70 2844.14 86.04 o 2 15 0 618.42 626.60 33.28 o 3 15 0 75.35 42.99 18.19 o 4 15 0 1427.33 1490.87 79.27 o 5 15 0 103.57 121.61 18.39 o 6 15 0 919.53 1053.68 67.67 o 7 15 0 47.69 38.53 16.75 o 8 15 0 464.57 458.89 32.61 o 9 15 0 15.14 0.20 19.60 o 0 16 0 199.07 210.08 23.13 o 1 16 0 22.32 61.02 13.50 o 2 16 0 889.68 986.22 43.99 o 3 16 0 56.23 43.17 15.08 o 4 16 0 97.55 74.43 16.52 o 5 16 0 36.13 31.28 15.15 o 6 16 0 29.26 40.16 17.03 o 7 16 0 27.39 31.54 16.95 o 8 16 0 84.46 123.48 22.49 o 9 16 0 13.91 -5.07 45.65 o 1 17 0 55.79 55.04 13.24 o 2 17 0 1299.37 1359.64 54.29 o 3 17 0 1269.55 1267.68 52.00 o 4 17 0 34.44 16.91 15.70 o 5 17 0 27.41 35.56 16.65 o 6 17 0 766.40 926.78 67.34 o 7 17 0 395.34 416.37 45.18 o 8 17 0 78.74 61.21 33.41 o 0 18 0 470.83 600.84 42.38 o 1 18 0 243.88 205.65 22.35 o 2 18 0 108.85 127.38 19.96 o 3 18 0 511.66 458.44 31.20 o 4 18 0 117.28 86.13 18.86 o 5 18 0 79.97 100.00 20.23 o 6 18 0 0.15 17.08 18.62 o 7 18 0 4.55 8.58 23.40 o 8 18 0 71.07 50.40 48.27 o 1 19 0 1.30 -1.00 14.53 o 2 19 0 379.10 389.97 29.49 o 3 19 0 109.34 89.93 28.72 o 4 19 0 0.28 -2.84 17.41 o 5 19 0 38.61 44.46 20.18 o 6 19 0 18.17 26.02 19.61 o 7 19 0 101.85 137.03 27.53 o 0 20 0 42.70 73.60 25.97 o 1 20 0 2.76 -18.64 18.64 o 2 20 0 0.08 -3.49 17.84 o 3 20 0 0.53 8.27 18.56 o 4 20 0 96.58 106.43 25.11 o 5 20 0 166.13 198.43 33.43 o 6 20 0 59.25 86.17 26.98 o 7 20 0 92.60 131.86 59.17 o 1 21 0 90.66 88.66 25.82 o 2 21 0 18.93 -0.01 21.29 o 3 21 0 141.84 162.27 27.58 o 4 21 0 23.21 40.89 25.25 o 5 21 0 25.48 31.73 29.52 o 6 21 0 7.35 34.37 45.08 o 1 22 0 1.79 8.25 29.86 o 2 22 0 4.15 -1.61 29.56 o 3 22 0 1.56 -29.87 29.87 o 4 22 0 9.07 19.72 37.76 o 5 22 0 58.21 135.81 51.28 o 1 23 0 235.14 194.41 92.42 o 2 23 0 3.21 -14.81 52.97 o 3 23 0 289.82 391.02 90.44 o 4 23 0 24.18 0.73 35.48 o 2 24 0 19.71 23.83 35.43 o 3 24 0 46.77 137.56 45.24 o 2 25 0 0.20 5.64 81.71 o -11 1 1 10.23 3.21 14.06 o -10 1 1 998.47 924.89 46.23 o -9 1 1 53.89 44.04 12.97 o -8 1 1 543.70 552.78 30.98 o -7 1 1 112.39 81.65 12.02 o -6 1 1 49.91 37.09 9.13 o -5 1 1 5445.15 4953.68 129.73 o -4 1 1 249.16 221.31 11.07 o -3 1 1 3559.96 3285.15 93.28 o -2 1 1 121.41 122.68 6.43 o -1 1 1 0.43 6.81 2.14 o 0 1 1 6779.97 7016.53 222.11 o 1 1 1 408.77 380.94 11.57 o 2 1 1 0.52 8.01 4.84 o 3 1 1 3371.69 3248.50 82.03 o 4 1 1 423.30 345.68 14.06 o 5 1 1 1500.75 1411.03 39.95 o 6 1 1 404.32 428.00 20.79 o 7 1 1 182.08 161.87 17.29 o 8 1 1 1172.45 1160.90 50.99 o 9 1 1 6.99 -0.36 11.66 o 10 1 1 688.95 602.59 37.82 o -11 2 1 145.90 127.19 22.98 o -10 2 1 285.31 264.82 26.52 o -9 2 1 0.36 -8.37 10.64 o -8 2 1 184.93 158.84 16.99 o -7 2 1 269.61 258.51 20.05 o -6 2 1 2.33 10.28 8.02 o -5 2 1 157.32 182.40 10.51 o -4 2 1 5413.41 5375.29 133.19 o -3 2 1 362.27 302.19 11.27 o -2 2 1 101.56 115.86 7.50 o -1 2 1 8610.34 8564.16 237.08 o 0 2 1 86.11 61.88 4.81 o 1 2 1 10627.06 10385.08 252.66 o 2 2 1 13588.27 13238.89 322.14 o 3 2 1 1.56 5.92 5.15 o 4 2 1 98.88 103.45 8.27 o 5 2 1 77.36 64.68 8.11 o 6 2 1 1332.85 1207.31 42.02 o 7 2 1 312.73 283.11 19.59 o 8 2 1 45.38 44.30 12.95 o 9 2 1 62.63 62.28 15.15 o 10 2 1 288.42 251.90 36.76 o -11 3 1 61.39 75.33 17.46 o -10 3 1 228.67 262.01 24.73 o -9 3 1 115.00 103.97 16.45 o -8 3 1 142.50 134.78 16.26 o -7 3 1 364.65 356.70 21.92 o -6 3 1 118.62 114.97 11.35 o -5 3 1 10.88 4.28 5.83 o -4 3 1 915.94 949.42 27.21 o -3 3 1 445.60 417.28 13.69 o -2 3 1 592.23 553.61 16.42 o -1 3 1 137.62 123.31 6.37 o 0 3 1 12198.33 11874.67 287.14 o 1 3 1 2360.35 2262.20 80.49 o 2 3 1 6048.84 5953.05 146.72 o 3 3 1 147.66 142.87 8.03 o 4 3 1 483.88 513.37 17.91 o 5 3 1 0.10 -2.11 5.69 o 6 3 1 239.53 236.97 16.20 o 7 3 1 319.41 276.73 18.52 o 8 3 1 112.04 115.32 16.39 o 9 3 1 96.25 86.80 18.95 o 10 3 1 18.09 27.79 14.80 o -11 4 1 426.68 410.18 32.58 o -10 4 1 128.66 97.35 16.87 o -9 4 1 240.56 213.29 21.55 o -8 4 1 187.96 165.09 17.26 o -7 4 1 167.59 200.32 16.18 o -6 4 1 337.87 324.88 17.62 o -5 4 1 0.40 -5.23 5.23 o -4 4 1 2492.57 2429.20 71.67 o -3 4 1 558.52 544.54 18.20 o -2 4 1 35.88 43.45 5.02 o -1 4 1 24951.17 23616.69 599.68 o 0 4 1 233.14 182.90 9.16 o 1 4 1 247.23 269.21 16.87 o 2 4 1 1202.89 1164.07 32.01 o 3 4 1 66.81 76.37 6.34 o 4 4 1 222.93 193.26 10.04 o 5 4 1 513.33 559.45 23.85 o 6 4 1 517.10 479.33 23.16 o 7 4 1 147.60 130.09 14.35 o 8 4 1 25.42 23.45 12.05 o 9 4 1 231.93 231.74 22.97 o 10 4 1 8.47 20.08 15.12 o -11 5 1 18.19 15.97 16.10 o -10 5 1 126.93 146.11 20.33 o -9 5 1 13.75 8.70 11.90 o -8 5 1 873.43 843.04 49.93 o -7 5 1 126.67 99.48 13.24 o -6 5 1 160.31 179.75 14.40 o -5 5 1 1015.66 984.01 34.51 o -4 5 1 929.78 1022.05 34.90 o -3 5 1 956.04 1089.78 35.87 o -2 5 1 896.00 857.69 25.12 o -1 5 1 328.67 380.58 15.04 o 0 5 1 2348.00 2154.54 58.97 o 1 5 1 174.46 170.62 10.53 o 2 5 1 972.36 1036.58 29.59 o 3 5 1 64.35 84.17 5.87 o 4 5 1 3422.82 3651.10 111.21 o 5 5 1 412.93 426.72 20.82 o 6 5 1 148.18 144.79 15.37 o 7 5 1 263.33 237.04 18.02 o 8 5 1 1.71 2.48 10.85 o 9 5 1 45.55 39.18 14.67 o 10 5 1 289.42 312.66 36.60 o -11 6 1 83.02 61.36 18.82 o -10 6 1 36.91 28.15 14.56 o -9 6 1 270.64 287.81 32.94 o -8 6 1 219.37 221.47 19.74 o -7 6 1 89.50 89.47 19.43 o -6 6 1 156.13 170.49 14.44 o -5 6 1 91.64 100.94 11.33 o -4 6 1 5.14 12.07 7.04 o -3 6 1 749.52 777.60 23.51 o -2 6 1 220.99 203.21 10.64 o -1 6 1 136.31 148.94 10.01 o 0 6 1 957.60 943.43 30.59 o 1 6 1 1056.33 928.45 46.91 o 2 6 1 14.36 20.99 5.49 o 3 6 1 80.29 93.40 6.20 o 4 6 1 32.26 24.32 8.40 o 5 6 1 27.11 19.57 9.64 o 6 6 1 13.75 18.59 9.70 o 7 6 1 5.56 -9.19 9.19 o 8 6 1 30.69 31.48 12.72 o 9 6 1 653.27 653.42 38.50 o 10 6 1 144.39 133.82 20.72 o -11 7 1 130.03 139.13 21.69 o -10 7 1 276.51 271.42 26.77 o -9 7 1 462.65 448.41 30.64 o -8 7 1 644.68 650.05 32.03 o -7 7 1 942.94 939.41 37.13 o -6 7 1 16.82 11.05 9.56 o -5 7 1 183.43 189.53 14.78 o -4 7 1 964.40 1017.60 36.28 o -3 7 1 716.63 736.65 23.14 o -2 7 1 1106.52 1102.18 32.41 o -1 7 1 1183.98 1204.80 35.92 o 0 7 1 4.73 -6.77 6.77 o 1 7 1 1500.80 1313.07 58.60 o 2 7 1 33.12 25.77 6.47 o 3 7 1 56.34 25.06 8.39 o 4 7 1 676.60 674.50 27.66 o 5 7 1 16.31 20.93 9.14 o 6 7 1 1.30 4.05 9.68 o 7 7 1 1163.58 1112.21 42.49 o 8 7 1 7.54 -11.05 11.05 o 9 7 1 623.19 613.80 37.11 o 10 7 1 193.60 211.73 25.28 o -10 8 1 24.28 37.30 15.29 o -9 8 1 13.11 7.51 12.88 o -8 8 1 377.75 389.83 25.04 o -7 8 1 63.31 79.11 17.30 o -6 8 1 599.74 618.10 28.23 o -5 8 1 317.29 327.31 25.24 o -4 8 1 760.03 763.41 30.24 o -3 8 1 3062.26 3263.82 84.07 o -2 8 1 299.10 286.19 13.95 o -1 8 1 8270.95 8613.66 249.70 o 0 8 1 115.79 142.27 13.45 o 1 8 1 391.94 362.00 18.33 o 2 8 1 209.96 160.03 11.55 o 3 8 1 344.20 396.11 15.56 o 4 8 1 224.26 248.51 16.75 o 5 8 1 2.29 7.24 9.23 o 6 8 1 235.96 244.05 18.74 o 7 8 1 300.52 253.86 20.67 o 8 8 1 448.55 397.63 25.56 o 9 8 1 1.04 16.18 14.83 o 10 8 1 178.01 183.90 24.68 o -10 9 1 70.74 66.89 18.55 o -9 9 1 4.25 1.95 12.68 o -8 9 1 0.41 -6.26 11.21 o -7 9 1 0.15 -2.76 10.43 o -6 9 1 419.04 434.67 24.10 o -5 9 1 756.95 786.17 32.05 o -4 9 1 84.57 106.11 12.94 o -3 9 1 647.79 696.27 23.79 o -2 9 1 736.65 787.98 26.60 o -1 9 1 350.19 397.62 19.69 o 0 9 1 3.13 3.83 7.85 o 1 9 1 1.29 4.23 8.04 o 2 9 1 5.68 18.79 7.89 o 3 9 1 23.53 23.76 6.83 o 4 9 1 211.16 220.85 16.96 o 5 9 1 8.65 16.39 10.22 o 6 9 1 227.87 231.87 18.95 o 7 9 1 4.22 1.30 11.43 o 8 9 1 33.71 44.49 14.42 o 9 9 1 2.22 11.04 14.78 o 10 9 1 22.81 30.10 18.00 o -10 10 1 5.45 -0.22 15.62 o -9 10 1 16.53 17.57 15.18 o -8 10 1 125.83 139.42 18.75 o -7 10 1 411.48 420.70 25.39 o -6 10 1 642.27 675.80 31.50 o -5 10 1 13.85 5.89 9.78 o -4 10 1 1021.32 1078.32 58.18 o -3 10 1 19.94 24.97 8.00 o -2 10 1 1154.66 1258.89 38.70 o -1 10 1 6385.95 6162.40 167.49 o 0 10 1 376.72 369.28 18.60 o 1 10 1 486.77 446.56 30.29 o 2 10 1 0.06 7.69 8.11 o 3 10 1 222.74 246.03 18.48 o 4 10 1 1359.02 1355.49 48.57 o 5 10 1 22.59 35.20 11.93 o 6 10 1 693.80 705.61 32.66 o 7 10 1 346.94 329.74 23.76 o 8 10 1 9.06 -0.77 12.71 o 9 10 1 757.74 789.54 57.91 o 10 10 1 150.91 153.27 35.70 o -10 11 1 3.30 26.45 17.10 o -9 11 1 0.03 14.33 15.64 o -8 11 1 811.83 857.95 46.20 o -7 11 1 360.41 361.82 24.66 o -6 11 1 45.67 34.65 12.31 o -5 11 1 1021.50 1026.14 40.69 o -4 11 1 0.26 -9.50 9.77 o -3 11 1 921.46 954.54 31.39 o -2 11 1 478.31 419.44 19.54 o -1 11 1 638.65 784.34 45.94 o 0 11 1 720.66 765.18 29.15 o 1 11 1 202.55 185.04 14.16 o 2 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