#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:32:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181249 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/27/2232753.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232753_Fobs loop_ _publ_author_name 'Malathy, Sevaiyan' 'Muthiah, Packianathan Thomas' _publ_section_title ; 2-Amino-4,6-dimethylpyrimidin-1-ium 2,3,5-triiodobenzoate 2,3,5-triiodobenzoic acid monosolvate ; _journal_coeditor_code HG5115 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3241 _journal_page_last o3242 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.366 _cell_angle_gamma 90.000 _cell_length_a 9.4654 _cell_length_b 9.6683 _cell_length_c 31.1553 _exptl_crystal_F_000 2024.00 _reflns_d_resolution_high 0.6795 _cod_data_source_file hg5115Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PTMKT400 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 605.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13579.61 14085.52 260.18 o 2 0 0 41237.18 40725.38 733.70 o 3 0 0 337431.09 335296.63 9774.56 o 4 0 0 94915.50 90627.76 1618.22 o 5 0 0 59656.48 60475.70 1102.98 o 6 0 0 18020.12 17256.77 440.11 o 7 0 0 7586.32 7723.66 250.11 o 8 0 0 3627.63 3794.76 173.23 o 9 0 0 2707.36 2904.05 161.75 o 10 0 0 1642.26 2203.26 157.80 o 11 0 0 1522.63 2669.06 250.87 o 12 0 0 4.22 90.84 131.29 o 13 0 0 560.14 410.90 174.58 o 1 1 0 570.44 867.98 16.65 o 2 1 0 15291.87 16439.93 216.68 o 3 1 0 44807.74 47673.69 605.53 o 4 1 0 24832.00 23731.55 405.63 o 5 1 0 151.36 432.60 46.26 o 6 1 0 798.69 1556.93 64.28 o 7 1 0 1481.01 1611.68 112.11 o 8 1 0 55.97 217.39 54.11 o 9 1 0 807.08 870.38 84.81 o 10 1 0 135.88 160.74 91.58 o 11 1 0 45.34 127.01 91.86 o 12 1 0 0.05 -20.66 91.33 o 13 1 0 157.99 309.88 115.78 o 0 2 0 3025.70 2974.50 43.52 o 1 2 0 19619.29 21692.91 225.50 o 2 2 0 23951.63 24402.29 288.12 o 3 2 0 14817.61 13964.24 164.44 o 4 2 0 3976.32 3591.31 78.28 o 5 2 0 3.44 74.78 25.51 o 6 2 0 19831.96 19378.58 344.23 o 7 2 0 3000.79 2728.69 115.95 o 8 2 0 12793.58 12341.45 299.05 o 9 2 0 3427.99 3819.92 153.48 o 10 2 0 70.00 93.19 82.89 o 11 2 0 4369.65 4213.35 317.58 o 12 2 0 1480.63 2192.03 173.24 o 13 2 0 9.52 268.45 108.36 o 1 3 0 34677.66 38909.76 343.94 o 2 3 0 4163.21 4238.53 58.75 o 3 3 0 1.98 61.32 21.03 o 4 3 0 21140.48 21836.23 254.00 o 5 3 0 39455.22 37152.44 526.46 o 6 3 0 2095.63 2388.00 66.96 o 7 3 0 3564.05 4300.76 208.64 o 8 3 0 10411.94 10514.53 268.27 o 9 3 0 2725.45 4248.24 201.66 o 10 3 0 1770.16 1887.14 146.94 o 11 3 0 848.62 1420.24 137.63 o 12 3 0 377.51 900.92 193.03 o 13 3 0 280.89 259.74 158.61 o 0 4 0 1740.69 1876.71 42.31 o 1 4 0 5481.35 6109.56 71.05 o 2 4 0 28377.76 29575.73 423.51 o 3 4 0 23031.70 23560.55 253.66 o 4 4 0 4666.42 4725.48 120.18 o 5 4 0 5427.18 4989.25 93.46 o 6 4 0 26440.42 27269.37 404.49 o 7 4 0 2256.65 2676.49 88.78 o 8 4 0 838.81 1084.54 89.31 o 9 4 0 3040.15 3484.32 179.98 o 10 4 0 36.06 -46.48 113.19 o 11 4 0 273.73 484.35 162.51 o 12 4 0 177.79 279.61 158.97 o 13 4 0 4.90 -122.77 122.77 o 1 5 0 3916.06 3812.36 90.80 o 2 5 0 6338.60 6418.59 84.82 o 3 5 0 3225.37 3715.29 68.97 o 4 5 0 18589.60 18683.86 240.96 o 5 5 0 1214.35 1231.04 47.90 o 6 5 0 11331.06 10674.78 194.46 o 7 5 0 652.07 398.58 64.59 o 8 5 0 1761.38 2106.10 119.37 o 9 5 0 3009.31 3008.99 260.45 o 10 5 0 140.43 229.58 132.00 o 11 5 0 2.79 -117.45 117.45 o 12 5 0 18.74 -129.87 129.87 o 0 6 0 6254.30 5948.63 160.79 o 1 6 0 18444.60 17812.41 170.22 o 2 6 0 3361.96 3496.53 72.83 o 3 6 0 3.79 63.12 57.28 o 4 6 0 8203.55 8073.62 192.28 o 5 6 0 236.59 202.43 39.99 o 6 6 0 166.24 81.31 52.34 o 7 6 0 1240.83 1297.78 141.05 o 8 6 0 825.01 1075.06 277.30 o 9 6 0 489.60 611.23 118.51 o 10 6 0 745.76 1181.60 195.16 o 11 6 0 99.07 83.03 137.32 o 12 6 0 58.39 167.13 151.51 o 1 7 0 16421.54 17020.72 174.46 o 2 7 0 22485.93 23191.83 247.95 o 3 7 0 3934.59 4019.28 79.42 o 4 7 0 8585.79 8146.82 171.47 o 5 7 0 48.13 139.27 46.87 o 6 7 0 6003.72 6072.56 180.76 o 7 7 0 5730.30 4777.67 258.85 o 8 7 0 2936.83 2842.33 152.64 o 9 7 0 377.47 375.08 84.02 o 10 7 0 1602.56 1698.35 134.15 o 11 7 0 789.04 1075.54 162.69 o 12 7 0 2.50 195.87 153.29 o 0 8 0 3221.92 2557.56 113.64 o 1 8 0 1912.55 1880.74 61.54 o 2 8 0 8371.05 8050.52 145.96 o 3 8 0 2625.97 2292.23 72.19 o 4 8 0 142.92 372.43 43.77 o 5 8 0 1675.59 1693.12 120.97 o 6 8 0 45.95 -48.72 57.31 o 7 8 0 1104.00 836.03 99.31 o 8 8 0 223.53 240.40 79.84 o 9 8 0 764.63 855.78 147.89 o 10 8 0 963.90 1107.24 108.27 o 11 8 0 29.88 55.49 104.91 o 1 9 0 1648.55 1335.88 73.14 o 2 9 0 516.87 600.85 59.11 o 3 9 0 5.04 128.05 48.38 o 4 9 0 238.83 280.42 65.99 o 5 9 0 1886.01 1861.10 165.35 o 6 9 0 226.56 189.25 85.03 o 7 9 0 8.50 7.57 59.05 o 8 9 0 386.28 500.74 97.33 o 9 9 0 53.95 14.44 65.94 o 10 9 0 318.49 92.48 113.38 o 0 10 0 1373.59 1378.89 193.38 o 1 10 0 12756.74 12785.44 384.71 o 2 10 0 12172.07 12043.06 228.25 o 3 10 0 2717.43 2567.29 129.98 o 4 10 0 2050.03 1996.72 254.59 o 5 10 0 2498.02 2588.87 199.06 o 6 10 0 4116.07 3632.44 236.32 o 7 10 0 119.65 161.80 111.42 o 8 10 0 247.76 140.16 113.19 o 9 10 0 180.92 13.13 111.77 o 1 11 0 711.50 646.87 126.86 o 2 11 0 82.96 111.39 109.12 o 3 11 0 1027.98 994.25 97.53 o 4 11 0 140.99 215.30 91.68 o 5 11 0 1932.59 2208.15 161.63 o 6 11 0 49.18 32.29 113.55 o 7 11 0 166.59 205.80 122.42 o 8 11 0 164.96 151.51 119.93 o 0 12 0 1155.84 1096.79 211.84 o 1 12 0 532.58 459.29 134.73 o 2 12 0 86.86 298.01 133.95 o 3 12 0 805.85 988.21 200.13 o 4 12 0 887.15 801.92 189.13 o 5 12 0 121.60 55.10 90.93 o 6 12 0 314.99 254.77 120.64 o 7 12 0 378.32 295.22 133.77 o 1 13 0 134.88 352.67 132.59 o 2 13 0 131.05 167.56 127.71 o 3 13 0 473.90 736.99 207.58 o 4 13 0 13.38 -46.84 149.74 o 5 13 0 11.17 248.74 160.38 o 1 14 0 53.27 79.13 182.38 o -13 1 1 147.24 217.68 113.24 o -12 1 1 883.84 971.96 134.81 o -11 1 1 54.34 -82.32 82.32 o -10 1 1 1280.56 1693.68 145.11 o -9 1 1 5902.48 5945.61 193.11 o -8 1 1 3263.37 3555.00 233.91 o -7 1 1 176.62 250.21 57.62 o -6 1 1 42482.82 42163.96 689.05 o -5 1 1 27530.67 26704.62 334.27 o -4 1 1 16383.03 17623.49 233.62 o -3 1 1 13447.38 14493.92 197.95 o -2 1 1 5773.59 5842.00 79.49 o -1 1 1 13328.89 13554.70 160.63 o 0 1 1 3946.96 4109.28 38.60 o 1 1 1 15986.34 17700.71 215.22 o 2 1 1 107127.20 112569.55 1705.29 o 3 1 1 2427.03 2417.05 46.39 o 4 1 1 3565.15 3548.78 68.89 o 5 1 1 69802.80 67479.30 860.77 o 6 1 1 2162.47 2085.40 69.25 o 7 1 1 333.41 472.77 52.34 o 8 1 1 7744.09 7657.91 185.01 o 9 1 1 447.28 554.78 63.99 o 10 1 1 1995.05 1797.54 146.23 o 11 1 1 110.25 159.55 92.09 o 12 1 1 393.21 130.20 101.49 o 13 1 1 58.58 -20.33 98.61 o -13 2 1 246.06 482.82 125.97 o -12 2 1 599.03 861.03 128.09 o -11 2 1 605.06 1092.97 133.94 o -10 2 1 262.87 81.15 137.32 o -9 2 1 5286.17 5986.09 194.27 o -8 2 1 50.93 68.66 54.95 o -7 2 1 1482.31 1320.14 84.52 o -6 2 1 414.61 498.42 53.54 o -5 2 1 3490.78 3328.32 105.42 o -4 2 1 523.13 432.05 70.17 o -3 2 1 61214.14 59254.74 639.31 o -2 2 1 19305.59 19043.42 228.11 o -1 2 1 1043.46 1131.60 24.43 o 0 2 1 2811.32 3340.62 33.95 o 1 2 1 78989.83 87603.80 877.43 o 2 2 1 5953.79 5261.20 94.66 o 3 2 1 1648.06 2016.58 37.93 o 4 2 1 26789.93 28229.17 411.29 o 5 2 1 3.44 9.83 23.12 o 6 2 1 61.35 319.11 43.30 o 7 2 1 13292.75 12563.18 292.28 o 8 2 1 1230.19 1910.69 106.50 o 9 2 1 2153.91 3023.78 138.67 o 10 2 1 3832.68 3376.32 302.85 o 11 2 1 325.01 718.94 118.38 o 12 2 1 343.24 295.07 101.99 o 13 2 1 617.20 656.94 133.60 o -13 3 1 68.17 20.94 132.71 o -12 3 1 2454.00 3196.34 296.64 o -11 3 1 42.91 86.00 90.07 o -10 3 1 1892.85 1569.41 135.24 o -9 3 1 11994.11 13550.95 450.11 o -8 3 1 2003.18 1624.19 102.93 o -7 3 1 20957.33 21008.34 552.15 o -6 3 1 4950.21 4504.78 105.72 o -5 3 1 15267.71 14797.67 229.85 o -4 3 1 42916.93 43453.72 480.68 o -3 3 1 27477.53 27757.42 332.92 o -2 3 1 20437.12 22235.28 234.30 o -1 3 1 41584.44 44920.04 410.60 o 0 3 1 41671.84 43656.28 353.57 o 1 3 1 80120.63 83983.59 727.91 o 2 3 1 65467.49 70646.17 712.25 o 3 3 1 43414.53 45411.71 530.51 o 4 3 1 3970.83 4675.77 73.31 o 5 3 1 2825.26 2727.44 115.66 o 6 3 1 9747.02 9614.17 194.16 o 7 3 1 912.10 966.50 99.93 o 8 3 1 790.37 991.47 111.55 o 9 3 1 4835.87 5889.90 245.55 o 10 3 1 637.99 795.94 122.42 o 11 3 1 198.09 612.63 173.34 o 12 3 1 828.44 1869.98 245.90 o 13 3 1 7.09 37.61 140.87 o -13 4 1 12.59 149.11 197.47 o -12 4 1 5.13 8.52 139.09 o -11 4 1 502.93 656.80 174.93 o -10 4 1 614.49 785.96 168.55 o -9 4 1 46.29 210.16 85.07 o -8 4 1 36.40 2.91 53.35 o -7 4 1 330.64 515.23 48.32 o -6 4 1 1399.21 1357.47 74.41 o -5 4 1 6538.45 6037.83 106.34 o -4 4 1 4487.31 4975.38 145.25 o -3 4 1 17408.39 17230.89 191.15 o -2 4 1 1727.46 2194.35 55.87 o -1 4 1 122977.16 134590.19 1113.22 o 0 4 1 2.30 16.38 9.92 o 1 4 1 89357.02 93817.15 812.25 o 2 4 1 26925.77 29313.13 291.59 o 3 4 1 11798.83 11379.45 128.51 o 4 4 1 57853.95 59498.16 749.97 o 5 4 1 1571.47 1784.83 53.87 o 6 4 1 17911.02 17823.84 321.86 o 7 4 1 4839.34 4364.80 116.16 o 8 4 1 3413.53 3999.80 151.30 o 9 4 1 526.13 676.71 101.64 o 10 4 1 1488.30 1792.62 219.64 o 11 4 1 521.29 659.64 176.00 o 12 4 1 203.19 373.29 162.51 o 13 4 1 222.95 216.09 166.42 o -12 5 1 254.76 364.06 172.45 o -11 5 1 3.86 -125.97 125.97 o -10 5 1 43.96 95.81 113.90 o -9 5 1 521.39 490.74 137.68 o -8 5 1 248.45 135.90 124.19 o -7 5 1 38.99 147.79 75.13 o -6 5 1 969.40 1012.39 53.87 o -5 5 1 2331.06 2216.81 62.46 o -4 5 1 34872.41 34268.17 415.17 o -3 5 1 2896.12 3496.29 66.31 o -2 5 1 6487.50 6339.57 104.63 o -1 5 1 39383.30 40507.04 350.72 o 0 5 1 11967.15 12818.30 113.65 o 1 5 1 1119.13 1020.81 31.95 o 2 5 1 267.95 429.31 36.13 o 3 5 1 31442.49 31721.93 317.37 o 4 5 1 316.94 509.79 81.31 o 5 5 1 3794.25 3620.04 79.12 o 6 5 1 2086.16 2014.23 72.09 o 7 5 1 595.03 668.65 68.04 o 8 5 1 4607.00 3966.92 158.60 o 9 5 1 4815.58 5300.51 336.03 o 10 5 1 41.61 36.90 115.32 o 11 5 1 210.76 -71.68 123.84 o 12 5 1 226.82 333.54 169.61 o -12 6 1 49.80 16.01 154.53 o -11 6 1 24.94 -25.19 126.68 o -10 6 1 235.69 457.38 150.80 o -9 6 1 277.59 77.19 64.78 o -8 6 1 21.45 129.18 96.16 o -7 6 1 15265.70 13358.55 736.30 o -6 6 1 1129.00 1229.87 71.73 o -5 6 1 91.60 55.28 58.84 o -4 6 1 25281.55 24010.62 447.91 o -3 6 1 25624.04 25647.34 298.48 o -2 6 1 11848.58 11960.36 139.77 o -1 6 1 477.89 468.13 28.24 o 0 6 1 36148.12 36605.83 308.64 o 1 6 1 41628.88 41695.95 364.51 o 2 6 1 5179.70 5002.10 79.47 o 3 6 1 2010.73 2090.73 65.96 o 4 6 1 23764.46 23494.43 328.88 o 5 6 1 12447.38 12297.14 241.61 o 6 6 1 384.37 394.75 51.79 o 7 6 1 8280.74 7452.08 419.38 o 8 6 1 1397.97 1555.40 232.77 o 9 6 1 359.25 386.17 80.07 o 10 6 1 635.87 491.80 152.58 o 11 6 1 259.92 265.77 152.93 o 12 6 1 508.98 268.25 168.19 o -12 7 1 7.30 318.64 167.13 o -11 7 1 474.22 577.54 127.28 o -10 7 1 53.75 104.24 130.32 o -9 7 1 36.19 -25.44 64.47 o -8 7 1 2820.05 2989.43 199.95 o -7 7 1 1111.53 1347.53 237.74 o -6 7 1 227.11 190.08 76.00 o -5 7 1 5435.21 5842.65 149.95 o -4 7 1 3694.32 3634.27 89.38 o -3 7 1 3162.72 3092.09 69.41 o -2 7 1 7582.48 7883.73 106.38 o -1 7 1 194.38 180.23 40.21 o 0 7 1 6166.44 5588.04 78.88 o 1 7 1 5676.35 6281.36 83.00 o 2 7 1 781.26 752.35 59.84 o 3 7 1 2780.76 2567.98 69.25 o 4 7 1 1044.35 1147.24 60.77 o 5 7 1 3479.95 3734.02 136.80 o 6 7 1 47.27 184.55 95.85 o 7 7 1 6.59 0.57 76.82 o 8 7 1 516.06 619.82 92.61 o 9 7 1 124.96 93.80 170.14 o 10 7 1 4.54 68.24 107.51 o 11 7 1 47.68 101.48 140.16 o 12 7 1 1.99 182.03 144.77 o -11 8 1 60.96 21.19 68.45 o -10 8 1 16.75 104.00 68.78 o -9 8 1 45.50 133.65 69.20 o -8 8 1 1.09 28.63 73.37 o -7 8 1 1102.35 1274.73 169.15 o -6 8 1 39.38 18.78 54.58 o -5 8 1 848.30 507.31 123.79 o -4 8 1 884.25 1128.85 59.91 o -3 8 1 555.81 679.32 62.05 o -2 8 1 100.66 172.12 40.55 o -1 8 1 10.68 57.81 31.35 o 0 8 1 303.70 324.61 41.41 o 1 8 1 1003.84 1287.09 53.65 o 2 8 1 41.54 102.99 58.89 o 3 8 1 51.90 179.47 38.64 o 4 8 1 6903.55 6910.51 138.63 o 5 8 1 5352.91 5288.32 275.05 o 6 8 1 100.95 77.70 66.18 o 7 8 1 3101.27 3570.09 296.29 o 8 8 1 1592.83 1475.98 132.71 o 9 8 1 1933.30 2046.47 141.15 o 10 8 1 858.27 886.86 112.82 o 11 8 1 497.43 669.86 93.35 o -10 9 1 14.11 14.62 69.41 o -9 9 1 7.04 43.61 68.76 o -8 9 1 2822.09 3187.96 147.51 o -7 9 1 93.13 155.39 66.57 o -6 9 1 271.81 150.11 61.62 o -5 9 1 345.30 217.31 71.67 o -4 9 1 2868.56 2783.20 184.02 o -3 9 1 1731.37 1828.62 85.28 o -2 9 1 2334.19 2704.25 96.13 o -1 9 1 826.03 916.29 60.89 o 0 9 1 4633.40 4798.62 124.99 o 1 9 1 327.75 399.49 53.03 o 2 9 1 6986.06 6687.61 151.60 o 3 9 1 8937.46 9084.32 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795.56 1180.58 197.47 o 0 11 1 3570.62 3871.40 214.14 o 1 11 1 263.49 208.52 106.76 o 2 11 1 2861.15 3151.30 282.63 o 3 11 1 6.72 50.62 112.84 o 4 11 1 2787.24 2850.50 166.16 o 5 11 1 103.34 102.72 177.24 o 6 11 1 324.64 206.51 121.35 o 7 11 1 116.22 19.52 109.64 o 8 11 1 1.33 -0.71 109.29 o -7 12 1 104.15 -26.97 115.68 o -6 12 1 157.66 200.84 122.42 o -5 12 1 17.33 106.13 94.56 o -4 12 1 2.09 420.12 165.00 o -3 12 1 1452.85 1893.75 240.58 o -2 12 1 276.17 401.57 130.88 o -1 12 1 34.01 168.32 115.34 o 0 12 1 1.00 -103.03 103.33 o 1 12 1 677.29 928.13 146.91 o 2 12 1 1167.21 1402.43 167.00 o 3 12 1 568.50 944.92 199.42 o 4 12 1 360.48 382.16 172.09 o 5 12 1 34.91 142.61 135.01 o 6 12 1 156.16 -12.77 113.55 o 7 12 1 548.07 386.06 140.87 o -5 13 1 37.67 146.90 159.68 o -4 13 1 15.08 228.87 162.87 o -3 13 1 433.26 526.22 184.51 o -2 13 1 1454.74 1368.49 172.70 o -1 13 1 222.24 214.31 127.46 o 0 13 1 520.38 581.36 141.50 o 1 13 1 1025.83 1108.29 162.19 o 2 13 1 152.83 182.15 130.75 o 3 13 1 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