#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/28/2232835.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232835_Fobs loop_ _publ_author_name 'Xiao, Zuo-an' 'Jiang, Ting-ting' _publ_section_title ; (Nitrato-\kO){N,N,N',N'-tetrakis[(1H-benzimidazol-2-yl-\kN^3^)methyl]cyclohexane-1,2-diamine}lead(II) hemiaqua{N,N,N',N'-tetrakis[(1H-benzimidazol-2-yl-\kN^3^)methyl]cyclohexane-1,2-diamine}lead(II) trinitrate dihydrate ; _journal_coeditor_code LH5344 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1854 _journal_page_last m1855 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 64.516 _cell_angle_beta 81.957 _cell_angle_gamma 79.675 _cell_length_a 12.5485 _cell_length_b 18.5378 _cell_length_c 19.2839 _exptl_crystal_F_000 1972.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file lh5344Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 514.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2434.68 2206.77 218.54 o 2 0 0 53604.62 62148.25 1510.38 o 3 0 0 623.66 612.78 60.70 o 4 0 0 27274.04 30568.37 799.87 o 5 0 0 2106.07 2394.99 162.20 o 6 0 0 16938.01 16582.54 501.79 o 7 0 0 7312.35 7189.69 287.19 o 8 0 0 44871.08 45891.80 1246.28 o 9 0 0 2455.20 2221.91 232.56 o 10 0 0 2833.93 2962.63 303.48 o 11 0 0 465.39 480.70 134.67 o 12 0 0 449.82 626.48 161.39 o 13 0 0 2449.43 2855.22 283.63 o 14 0 0 2803.28 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o -12 3 0 5197.41 4382.06 540.76 o -11 3 0 3532.90 3388.05 344.00 o -10 3 0 10487.62 10280.29 428.65 o -9 3 0 1714.08 1689.47 182.24 o -8 3 0 7854.10 7730.15 323.99 o -7 3 0 16.48 61.10 57.65 o -6 3 0 6518.75 6870.31 226.41 o -5 3 0 794.90 813.26 79.23 o -4 3 0 37643.43 39919.43 890.26 o -3 3 0 755.43 725.49 63.66 o -2 3 0 12028.07 12653.26 352.17 o -1 3 0 290.86 295.38 35.09 o 0 3 0 502.83 496.18 42.13 o 1 3 0 1753.27 1512.36 107.52 o 2 3 0 58726.21 65286.41 1377.68 o 3 3 0 2938.02 2949.80 134.01 o 4 3 0 50619.54 56041.73 1403.48 o 5 3 0 11300.28 11251.93 290.84 o 6 3 0 12985.23 13284.32 423.52 o 7 3 0 62.52 -51.17 56.19 o 8 3 0 268.64 470.10 104.07 o 9 3 0 2852.87 2952.94 260.43 o 10 3 0 13610.74 12531.00 472.39 o 11 3 0 5696.08 5334.42 350.34 o 12 3 0 11101.65 10857.34 469.35 o 13 3 0 2447.59 2421.71 261.87 o 14 3 0 93.40 150.67 150.42 o 15 3 0 105.57 284.74 399.68 o -14 4 0 2127.56 2689.26 375.96 o -13 4 0 1293.95 1625.84 264.78 o -12 4 0 1948.93 1617.46 266.87 o -11 4 0 4.10 64.09 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762.55 1034.66 169.46 o -8 5 0 664.06 682.35 173.01 o -7 5 0 95.46 71.81 69.61 o -6 5 0 20020.01 20029.91 519.64 o -5 5 0 945.54 1038.47 96.80 o -4 5 0 72200.73 74506.19 1617.54 o -3 5 0 61.41 125.77 50.04 o -2 5 0 35564.91 38871.42 866.85 o -1 5 0 24.27 13.98 33.74 o 0 5 0 9751.27 10839.68 277.94 o 1 5 0 264.59 197.30 49.34 o 2 5 0 39158.71 44693.43 973.03 o 3 5 0 3165.55 3258.25 124.45 o 4 5 0 102927.13 112182.09 2370.49 o 5 5 0 2620.31 2587.96 147.94 o 6 5 0 2744.68 2536.77 140.54 o 7 5 0 99.10 142.82 52.98 o 8 5 0 236.33 319.52 98.27 o 9 5 0 899.41 811.95 134.84 o 10 5 0 7544.91 7747.01 351.00 o 11 5 0 4836.26 4543.33 511.67 o 12 5 0 6455.79 6523.49 607.16 o 13 5 0 1776.72 1723.58 225.32 o 14 5 0 38.00 140.50 132.37 o 15 5 0 18.54 51.10 192.15 o -13 6 0 2009.15 2242.63 316.54 o -12 6 0 1314.43 1467.34 265.87 o -11 6 0 4.76 -31.72 139.00 o -10 6 0 1187.02 1044.97 207.32 o -9 6 0 1085.45 852.30 151.86 o -8 6 0 7596.76 7308.00 325.39 o -7 6 0 2703.16 2752.77 224.55 o -6 6 0 27318.27 27001.21 672.69 o -5 6 0 1383.34 1362.86 121.97 o -4 6 0 5303.27 5426.87 310.59 o -3 6 0 221.68 189.14 107.05 o -2 6 0 9845.11 10134.79 280.47 o -1 6 0 1916.79 1798.45 113.04 o 0 6 0 112213.09 119546.77 2526.59 o 1 6 0 3171.97 3125.78 124.35 o 2 6 0 102293.62 112375.13 2679.90 o 3 6 0 134.48 169.04 78.57 o 4 6 0 4452.51 4602.43 165.36 o 5 6 0 2739.53 2456.17 128.33 o 6 6 0 12487.27 12178.04 340.34 o 7 6 0 8332.05 8037.43 455.13 o 8 6 0 16312.51 15186.14 847.85 o 9 6 0 2701.67 2610.32 213.04 o 10 6 0 1751.43 2003.76 293.09 o 11 6 0 2.68 -72.65 105.25 o 12 6 0 861.41 784.53 170.09 o 13 6 0 900.32 1103.78 190.98 o 14 6 0 913.77 647.33 246.60 o 15 6 0 1626.37 1690.07 254.58 o -13 7 0 230.66 357.13 187.41 o -12 7 0 2852.07 2649.66 349.06 o -11 7 0 941.82 901.63 208.93 o -10 7 0 6892.78 6415.26 675.44 o -9 7 0 135.33 259.86 281.17 o -8 7 0 2958.81 3004.69 288.58 o -7 7 0 337.24 213.62 82.44 o -6 7 0 9539.40 8888.45 299.98 o -5 7 0 160.88 161.48 62.27 o -4 7 0 57569.24 58004.27 1297.77 o -3 7 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