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Information card for entry 2232871
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| Coordinates | 2232871.cif |
|---|---|
| Structure factors | 2232871.hkl |
| Original IUCr paper | HTML |
| Chemical name | Tris(tetrahydrofuran-κ<i>O</i>)tris[tris(thiophen-2-yl)methanolato- κ<i>O</i>]terbium(III) tetrahydrofuran monosolvate |
|---|---|
| Formula | C55 H59 O7 S9 Tb |
| Calculated formula | C54.99 H58.92 O7 S9 Tb |
| Title of publication | Tris(tetrahydrofuran-κ<i>O</i>)tris[tris(thiophen-2-yl)methanolato-κ<i>O</i>]terbium(III) tetrahydrofuran monosolvate |
| Authors of publication | Veith, Michael; Belot, Celine; Huch, Volker |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 12 |
| Pages of publication | m1712 |
| a | 13.9131 ± 0.0004 Å |
| b | 13.9131 ± 0.0004 Å |
| c | 24.6789 ± 0.0007 Å |
| α | 90° |
| β | 90° |
| γ | 120° |
| Cell volume | 4137.2 ± 0.2 Å3 |
| Cell temperature | 132 ± 2 K |
| Ambient diffraction temperature | 132 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 146 |
| Hermann-Mauguin space group symbol | R 3 :H |
| Hall space group symbol | R 3 |
| Residual factor for all reflections | 0.0351 |
| Residual factor for significantly intense reflections | 0.035 |
| Weighted residual factors for significantly intense reflections | 0.085 |
| Weighted residual factors for all reflections included in the refinement | 0.0852 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181250 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/28. |
2232871.cif 2232871.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2232871.cif 2232871.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2232871.cif 2232871.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2232871.cif 2232871.hkl |
| 31968 | 2012-01-03 | hkl/ Adding automatically assigned IUCr Fobs data for the rest of the year 2001 structures. |
2232871.cif 2232871.hkl |
| 31753 | 2012-01-02 | ../uploads/cif-deposit/cod/cif Adding structures of 2232871 via cif-deposit CGI script. |
2232871.cif |
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