#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/28/2232880.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232880_Fobs loop_ _publ_author_name 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; Tris(ethylenediamine-\k^2^N,N')nickel(II) naphthalene-2,7-disulfonate ; _journal_coeditor_code NK2123 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1817 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.152 _cell_angle_gamma 90.000 _cell_length_a 23.6237 _cell_length_b 14.2032 _cell_length_c 14.7149 _exptl_crystal_F_000 2208.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file nk2123Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 687.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 4150.31 3783.11 52.21 o 6 0 0 22484.48 24918.73 295.54 o 8 0 0 51351.92 55231.81 497.89 o 10 0 0 598.71 633.85 11.60 o 12 0 0 15590.03 15952.88 165.97 o 14 0 0 59197.93 61411.74 1551.15 o 16 0 0 317.06 235.28 21.36 o 18 0 0 4680.46 4927.34 66.11 o 20 0 0 4971.57 5252.21 45.55 o 22 0 0 1429.63 1335.08 27.93 o 24 0 0 4054.08 4042.31 60.97 o 26 0 0 3938.39 4130.71 99.50 o 3 1 0 54753.44 56510.95 308.43 o 5 1 0 79.66 71.78 5.10 o 7 1 0 5114.52 5301.53 22.68 o 9 1 0 12688.65 13007.91 54.30 o 11 1 0 197.12 216.38 7.36 o 13 1 0 3692.76 3635.42 21.33 o 15 1 0 2202.53 2459.56 21.58 o 17 1 0 17491.55 16709.17 92.53 o 19 1 0 281.51 300.25 15.35 o 21 1 0 131.39 102.34 15.15 o 23 1 0 209.43 215.91 16.59 o 25 1 0 165.18 170.37 16.35 o 27 1 0 989.56 1153.82 54.07 o 2 2 0 37503.78 41988.00 219.64 o 4 2 0 10075.73 10642.34 52.73 o 6 2 0 40042.48 41054.97 199.06 o 8 2 0 15909.79 17321.90 81.21 o 10 2 0 19120.26 19517.03 93.88 o 12 2 0 24168.69 24063.46 120.71 o 14 2 0 9389.85 9402.71 49.85 o 16 2 0 1929.52 2185.46 23.14 o 18 2 0 327.57 290.79 16.64 o 20 2 0 4951.60 4953.09 40.55 o 22 2 0 433.35 474.23 18.33 o 24 2 0 222.72 224.22 18.79 o 26 2 0 2781.94 3077.71 33.42 o 1 3 0 48115.94 50554.43 276.68 o 3 3 0 36430.26 36924.54 195.86 o 5 3 0 24635.54 26919.71 144.28 o 7 3 0 15363.08 16269.10 92.10 o 9 3 0 23977.09 26762.19 131.30 o 11 3 0 16784.86 15186.29 73.77 o 13 3 0 724.34 820.71 13.84 o 15 3 0 999.81 973.85 25.99 o 17 3 0 2432.61 2612.19 38.28 o 19 3 0 3003.94 3030.18 33.37 o 21 3 0 1352.07 1256.52 26.59 o 23 3 0 780.37 783.45 28.27 o 25 3 0 476.18 509.52 31.19 o 27 3 0 0.22 7.21 18.08 o 0 4 0 191116.20 202011.80 2038.89 o 2 4 0 7768.41 7356.79 41.96 o 4 4 0 448.92 606.65 14.78 o 6 4 0 10127.91 10598.59 59.30 o 8 4 0 668.77 670.72 14.27 o 10 4 0 1134.90 1134.03 14.87 o 12 4 0 743.53 638.94 17.68 o 14 4 0 171.03 202.00 12.94 o 16 4 0 341.55 384.91 14.14 o 18 4 0 1263.92 1144.86 30.19 o 20 4 0 512.69 471.52 18.86 o 22 4 0 3.28 -3.04 14.41 o 24 4 0 513.52 453.67 22.89 o 26 4 0 256.73 240.96 28.39 o 1 5 0 867.45 956.66 12.42 o 3 5 0 3969.44 3859.88 26.58 o 5 5 0 3779.07 3281.82 24.04 o 7 5 0 410.95 500.86 13.47 o 9 5 0 22223.52 23273.17 133.44 o 11 5 0 6.45 49.60 8.48 o 13 5 0 17.94 24.60 10.92 o 15 5 0 954.43 1037.45 18.36 o 17 5 0 2711.38 2751.57 27.47 o 19 5 0 12.47 1.32 12.98 o 21 5 0 3.06 13.27 10.50 o 23 5 0 2249.08 2248.09 36.39 o 25 5 0 22.57 24.25 21.30 o 0 6 0 5482.71 5384.07 79.49 o 2 6 0 87.47 27.16 9.70 o 4 6 0 3866.41 3664.29 26.31 o 6 6 0 19147.37 18730.97 104.49 o 8 6 0 706.41 928.08 16.46 o 10 6 0 4550.41 3923.40 35.13 o 12 6 0 8757.55 8189.68 55.58 o 14 6 0 2323.31 2131.41 20.18 o 16 6 0 2601.99 2752.16 24.13 o 18 6 0 5.93 2.02 9.59 o 20 6 0 3411.76 3410.59 42.54 o 22 6 0 160.62 88.38 11.39 o 24 6 0 86.15 97.21 19.69 o 26 6 0 273.65 263.53 26.41 o 1 7 0 25377.17 26522.11 147.76 o 3 7 0 21872.51 22752.11 129.67 o 5 7 0 3880.62 3628.73 37.45 o 7 7 0 413.22 436.16 19.46 o 9 7 0 19.29 44.59 14.72 o 11 7 0 2640.93 2424.59 27.92 o 13 7 0 6.70 7.60 13.33 o 15 7 0 2351.42 2131.21 28.94 o 17 7 0 90.71 55.20 11.63 o 19 7 0 120.38 112.42 12.43 o 21 7 0 2.92 16.20 10.85 o 23 7 0 368.01 408.88 24.69 o 25 7 0 62.51 97.63 31.42 o 0 8 0 26061.92 26931.90 226.51 o 2 8 0 4472.80 4207.01 38.99 o 4 8 0 1572.85 1607.29 20.20 o 6 8 0 12343.25 12431.56 77.24 o 8 8 0 6466.41 6477.86 46.74 o 10 8 0 2075.63 2047.93 27.56 o 12 8 0 15259.97 14977.19 99.63 o 14 8 0 9047.42 8720.90 66.31 o 16 8 0 1344.40 1513.94 27.72 o 18 8 0 413.39 435.74 19.05 o 20 8 0 2871.87 2630.92 37.30 o 22 8 0 1174.90 1259.70 30.35 o 24 8 0 209.77 273.81 46.61 o 1 9 0 8279.15 7716.48 54.30 o 3 9 0 15458.98 15428.40 94.17 o 5 9 0 22449.99 21950.26 133.53 o 7 9 0 1681.56 1608.27 23.87 o 9 9 0 20113.11 19563.93 124.04 o 11 9 0 870.50 643.59 30.27 o 13 9 0 11090.14 10969.85 88.42 o 15 9 0 1965.91 2095.57 33.18 o 17 9 0 4097.16 3911.97 39.06 o 19 9 0 22.00 29.89 12.87 o 21 9 0 4.98 4.44 24.27 o 23 9 0 712.63 871.86 75.18 o 0 10 0 53389.62 54255.50 481.85 o 2 10 0 7127.65 7220.15 56.51 o 4 10 0 2348.35 2195.53 34.76 o 6 10 0 55.51 44.83 17.78 o 8 10 0 3349.56 3466.58 42.64 o 10 10 0 574.49 529.99 26.66 o 12 10 0 7359.27 7235.85 58.03 o 14 10 0 7247.70 7298.35 67.92 o 16 10 0 9.80 26.85 13.35 o 18 10 0 431.02 417.93 21.74 o 20 10 0 520.52 434.27 24.71 o 22 10 0 1387.47 1536.30 43.31 o 1 11 0 9016.14 9255.29 69.77 o 3 11 0 23613.47 23465.33 146.47 o 5 11 0 16232.98 15977.94 113.02 o 7 11 0 532.88 488.77 24.32 o 9 11 0 6665.77 6530.27 54.42 o 11 11 0 5989.51 6177.61 54.10 o 13 11 0 364.59 327.28 33.02 o 15 11 0 4397.09 4308.14 46.62 o 17 11 0 4877.06 4715.36 55.03 o 19 11 0 567.64 489.33 30.51 o 21 11 0 2174.73 2413.11 42.51 o 0 12 0 164.15 115.78 26.14 o 2 12 0 427.22 427.91 26.49 o 4 12 0 1742.13 1548.92 31.05 o 6 12 0 308.53 377.97 21.93 o 8 12 0 102.25 96.00 21.69 o 10 12 0 2560.06 2573.40 39.70 o 12 12 0 2115.50 1973.69 48.08 o 14 12 0 660.21 641.45 27.10 o 16 12 0 151.74 157.50 25.88 o 18 12 0 134.91 186.58 20.50 o 20 12 0 316.05 328.51 31.51 o 1 13 0 17.08 30.41 22.97 o 3 13 0 7100.07 7039.39 68.14 o 5 13 0 4993.06 4643.50 56.64 o 7 13 0 1242.21 1204.52 77.24 o 9 13 0 3525.84 3356.45 42.62 o 11 13 0 9489.31 9389.38 81.76 o 13 13 0 619.16 668.63 28.76 o 15 13 0 513.42 493.68 31.68 o 17 13 0 2278.87 2044.70 36.71 o 19 13 0 689.14 688.43 41.78 o 0 14 0 529.85 581.58 39.24 o 2 14 0 323.69 262.77 25.36 o 4 14 0 5.68 -5.88 23.69 o 6 14 0 1094.84 1106.71 36.37 o 8 14 0 592.83 611.70 31.07 o 10 14 0 112.42 159.55 26.00 o 12 14 0 414.34 414.32 36.28 o 14 14 0 72.79 48.63 27.73 o 16 14 0 61.53 25.26 25.12 o 18 14 0 84.16 30.82 20.41 o 1 15 0 17.70 25.11 22.48 o 3 15 0 149.36 202.19 26.64 o 5 15 0 646.03 600.54 42.35 o 7 15 0 9.52 32.32 26.79 o 9 15 0 1023.53 1052.46 34.14 o 11 15 0 8.62 -13.63 23.63 o 13 15 0 3.03 6.77 26.25 o 15 15 0 32.20 50.30 32.10 o 0 16 0 1888.58 1773.78 57.28 o 2 16 0 36.06 59.19 29.35 o 4 16 0 153.07 143.01 36.24 o 6 16 0 87.22 97.07 31.24 o 8 16 0 211.69 220.34 30.18 o 10 16 0 1435.58 1598.74 57.27 o 12 16 0 102.93 112.93 30.01 o 1 17 0 105.50 95.03 35.33 o 3 17 0 401.53 336.93 32.73 o 5 17 0 525.45 608.27 39.75 o 7 17 0 334.58 356.14 37.13 o 9 17 0 1147.99 1247.75 41.79 o 0 18 0 843.51 895.76 68.83 o 2 18 0 10.84 -1.36 29.34 o 4 18 0 102.97 85.27 31.17 o -27 1 1 1099.17 1329.30 33.66 o -25 1 1 288.97 293.75 21.05 o -23 1 1 170.54 184.71 18.51 o -21 1 1 158.96 209.59 20.13 o -19 1 1 5102.76 5035.61 48.93 o -17 1 1 11081.46 11208.95 60.98 o -15 1 1 15.08 6.22 9.08 o -13 1 1 4832.59 5000.92 31.77 o -11 1 1 1802.26 1714.28 11.74 o -9 1 1 10754.87 10868.45 52.41 o -7 1 1 5764.88 5223.56 23.72 o -5 1 1 24308.66 24640.17 295.17 o 3 1 1 329.11 558.85 6.55 o 5 1 1 49720.95 54349.85 230.28 o 7 1 1 3052.52 3208.39 18.35 o 9 1 1 7406.70 7356.04 29.75 o 11 1 1 10073.54 10780.24 48.19 o 13 1 1 7151.87 7384.33 39.94 o 15 1 1 1897.79 1961.30 17.85 o 17 1 1 228.63 242.82 14.10 o 19 1 1 3440.69 3466.07 32.14 o 21 1 1 106.37 78.00 16.46 o 23 1 1 392.50 421.22 17.90 o 25 1 1 56.37 53.76 15.80 o -28 2 1 111.57 135.33 25.92 o -26 2 1 46.01 24.75 14.67 o -24 2 1 2150.33 2009.62 35.45 o -22 2 1 104.19 109.37 20.40 o -20 2 1 1951.89 1882.66 30.41 o -18 2 1 197.54 244.56 15.46 o -16 2 1 1930.87 1998.39 33.90 o -14 2 1 47.41 47.19 8.75 o -12 2 1 741.11 874.07 10.28 o -10 2 1 6786.46 6429.06 32.27 o -8 2 1 6810.58 7150.59 37.64 o -6 2 1 81724.91 94107.34 582.00 o -4 2 1 1801.43 1330.05 10.90 o -2 2 1 141.45 291.64 7.56 o 0 2 1 333.22 229.44 4.79 o 2 2 1 557.39 978.88 14.61 o 4 2 1 5106.28 5643.36 26.14 o 6 2 1 87.82 122.45 14.33 o 8 2 1 2035.24 1856.69 33.32 o 10 2 1 10522.41 11216.95 67.64 o 12 2 1 14.70 33.15 8.21 o 14 2 1 2555.27 2503.48 22.61 o 16 2 1 729.37 828.94 16.12 o 18 2 1 8117.81 7811.11 46.73 o 20 2 1 504.04 458.94 19.19 o 22 2 1 409.05 403.43 20.14 o 24 2 1 860.62 858.68 23.30 o 26 2 1 74.72 73.75 22.05 o -27 3 1 1260.06 1338.39 42.20 o -25 3 1 727.53 720.43 23.66 o -23 3 1 3682.25 3891.07 38.51 o -21 3 1 1809.34 1638.38 26.23 o -19 3 1 2202.34 2167.44 37.29 o -17 3 1 6445.93 6699.67 42.99 o -15 3 1 9289.22 9209.07 47.94 o -13 3 1 1264.94 1357.85 14.06 o -11 3 1 13678.99 13727.19 106.93 o -9 3 1 39162.54 39337.19 350.18 o -7 3 1 20526.22 21182.47 113.42 o -5 3 1 9320.98 9680.31 50.09 o -3 3 1 71727.13 77716.32 461.33 o -1 3 1 42325.55 47745.25 259.30 o 1 3 1 1928.84 1503.95 11.22 o 3 3 1 57396.62 65134.78 432.46 o 5 3 1 128375.17 138909.73 922.76 o 7 3 1 46411.27 50085.26 234.30 o 9 3 1 27735.70 28602.58 143.02 o 11 3 1 22972.66 23144.11 121.00 o 13 3 1 11192.51 11500.45 60.62 o 15 3 1 530.59 565.08 14.18 o 17 3 1 11472.07 11485.19 66.00 o 19 3 1 4401.73 4513.27 33.74 o 21 3 1 298.13 323.28 39.50 o 23 3 1 2295.49 2306.77 37.82 o 25 3 1 2820.64 2694.50 47.20 o -26 4 1 36.65 6.87 20.07 o -24 4 1 427.90 417.30 22.39 o -22 4 1 114.26 78.35 17.47 o -20 4 1 557.33 625.86 34.36 o -18 4 1 196.09 212.33 9.66 o -16 4 1 3372.14 3473.17 28.14 o -14 4 1 1026.38 879.85 16.32 o -12 4 1 2231.64 2302.78 22.36 o -10 4 1 4619.29 4665.80 31.68 o -8 4 1 2786.85 3405.01 25.09 o -6 4 1 94511.12 99127.50 626.49 o -4 4 1 21064.89 22562.47 124.87 o -2 4 1 8385.24 9098.38 48.62 o 0 4 1 2165.42 1968.00 58.10 o 2 4 1 42152.50 44928.22 251.06 o 4 4 1 2137.25 2146.38 16.19 o 6 4 1 2837.61 3617.37 25.24 o 8 4 1 66003.22 73135.03 399.45 o 10 4 1 2381.13 2219.77 17.46 o 12 4 1 2611.97 2398.44 21.58 o 14 4 1 1023.76 1039.88 16.89 o 16 4 1 3368.89 3445.12 26.29 o 18 4 1 144.76 106.59 13.74 o 20 4 1 1861.81 1614.94 19.82 o 22 4 1 1897.43 1996.01 26.83 o 24 4 1 763.73 737.17 48.17 o 26 4 1 10.51 5.30 20.10 o -27 5 1 3.68 13.65 17.72 o -25 5 1 207.82 219.19 20.45 o -23 5 1 8718.66 8717.70 75.95 o -21 5 1 4234.89 4066.05 60.99 o -19 5 1 95.23 128.29 10.80 o -17 5 1 28.10 31.37 8.36 o -15 5 1 11655.02 11248.97 63.34 o -13 5 1 7.75 31.23 7.93 o -11 5 1 15293.37 14355.93 82.59 o -9 5 1 34870.78 38299.18 223.41 o -7 5 1 69316.80 74014.75 453.43 o -5 5 1 31785.65 31622.63 211.75 o -3 5 1 11262.03 11935.85 64.91 o -1 5 1 10566.16 10709.17 56.41 o 1 5 1 5182.14 4830.02 30.12 o 3 5 1 72495.59 76097.38 462.73 o 5 5 1 72861.09 80543.80 495.09 o 7 5 1 25222.11 25378.35 144.75 o 9 5 1 3526.86 2822.67 36.74 o 11 5 1 15125.89 15392.30 72.46 o 13 5 1 1801.40 1809.83 17.75 o 15 5 1 6.07 30.08 11.29 o 17 5 1 21167.62 21079.24 123.60 o 19 5 1 1268.70 1440.95 24.08 o 21 5 1 1039.20 929.26 23.43 o 23 5 1 1145.97 1011.92 53.39 o 25 5 1 5529.30 5671.26 57.68 o -26 6 1 1337.55 1363.53 53.53 o -24 6 1 1094.07 985.73 35.61 o -22 6 1 69.49 38.06 11.94 o -20 6 1 4186.02 3997.42 59.43 o -18 6 1 310.03 365.00 21.41 o -16 6 1 1814.51 1873.75 19.39 o -14 6 1 709.48 819.57 13.84 o -12 6 1 6623.18 6743.38 45.75 o -10 6 1 1675.99 1643.77 20.01 o -8 6 1 6783.58 6759.75 77.27 o -6 6 1 78395.69 86478.24 545.06 o -4 6 1 6621.80 5808.52 35.64 o -2 6 1 5122.80 4929.85 49.26 o 0 6 1 27722.54 26268.33 151.25 o 2 6 1 27554.38 27510.38 150.17 o 4 6 1 6961.63 7199.12 51.24 o 6 6 1 19460.34 19773.99 117.60 o 8 6 1 46156.90 50261.95 301.10 o 10 6 1 5658.85 5325.15 41.30 o 12 6 1 151.66 190.08 13.10 o 14 6 1 8392.14 8390.97 56.11 o 16 6 1 5094.14 5075.07 37.49 o 18 6 1 95.02 90.82 13.60 o 20 6 1 1699.58 1716.61 22.60 o 22 6 1 4816.58 4807.99 47.04 o 24 6 1 8.92 11.92 19.32 o -25 7 1 444.08 527.41 34.59 o -23 7 1 422.45 392.72 86.98 o -21 7 1 204.66 180.78 16.53 o -19 7 1 3.73 -0.84 8.75 o -17 7 1 2380.41 2375.07 25.90 o -15 7 1 1524.07 1432.69 18.61 o -13 7 1 2121.50 1906.10 27.76 o -11 7 1 1736.18 1658.36 26.84 o -9 7 1 8842.96 8809.26 54.98 o -7 7 1 4227.37 4671.49 37.81 o -5 7 1 8464.84 8189.92 51.95 o -3 7 1 24190.60 24995.50 140.07 o -1 7 1 7263.95 7523.69 51.58 o 1 7 1 241.67 211.26 12.71 o 3 7 1 180.93 230.27 12.74 o 5 7 1 23701.01 23536.11 132.01 o 7 7 1 54.61 37.41 14.47 o 9 7 1 17.61 27.93 11.30 o 11 7 1 9073.47 8889.14 60.40 o 13 7 1 5709.46 5794.54 36.41 o 15 7 1 999.53 956.58 17.78 o 17 7 1 1829.34 1687.34 22.55 o 19 7 1 2867.64 2872.71 28.53 o 21 7 1 194.24 192.94 17.47 o 23 7 1 136.18 124.14 20.27 o -24 8 1 618.24 665.77 45.50 o -22 8 1 277.06 219.72 37.19 o -20 8 1 2735.06 2605.02 54.12 o -18 8 1 13901.90 13019.34 91.45 o -16 8 1 2796.22 2412.52 29.93 o -14 8 1 13.20 32.31 20.53 o -12 8 1 17913.43 17753.49 114.95 o -10 8 1 4987.45 5144.67 47.16 o -8 8 1 4831.54 4231.52 34.03 o -6 8 1 497.80 561.34 17.64 o -4 8 1 7984.60 6505.22 42.86 o -2 8 1 2303.16 2026.16 23.75 o 0 8 1 29032.26 28118.40 160.05 o 2 8 1 7495.67 7809.51 48.51 o 4 8 1 7963.37 7486.40 47.72 o 6 8 1 14576.30 13669.97 83.79 o 8 8 1 1266.25 1286.70 20.24 o 10 8 1 9824.79 9333.15 61.95 o 12 8 1 243.19 395.25 20.79 o 14 8 1 13218.53 12931.38 71.21 o 16 8 1 1061.29 1037.49 20.61 o 18 8 1 639.54 637.48 36.25 o 20 8 1 3715.34 3505.72 49.25 o 22 8 1 1545.38 1401.37 30.21 o 24 8 1 1.10 27.45 21.28 o -23 9 1 426.74 358.75 35.11 o -21 9 1 78.93 54.23 16.03 o -19 9 1 17.77 14.96 17.10 o -17 9 1 242.95 274.80 13.65 o -15 9 1 1363.25 1225.30 27.53 o -13 9 1 1301.73 1219.15 26.61 o -11 9 1 1642.23 1611.03 29.14 o -9 9 1 88.20 64.74 15.38 o -7 9 1 2232.19 2244.82 26.89 o -5 9 1 7823.72 7718.55 55.24 o -3 9 1 928.96 793.69 20.73 o -1 9 1 2340.76 2353.76 26.20 o 1 9 1 299.34 256.79 15.50 o 3 9 1 668.70 594.01 18.95 o 5 9 1 93.28 162.24 17.98 o 7 9 1 154.22 152.24 16.86 o 9 9 1 3853.21 3817.26 41.86 o 11 9 1 2446.20 2409.16 32.80 o 13 9 1 32.03 34.62 17.03 o 15 9 1 486.85 422.52 18.67 o 17 9 1 238.93 272.60 17.62 o 19 9 1 483.76 454.57 17.84 o 21 9 1 8.68 28.03 13.71 o 23 9 1 164.33 146.26 23.56 o -22 10 1 0.35 -11.92 21.64 o -20 10 1 561.97 565.02 21.18 o -18 10 1 3258.59 2956.05 53.56 o -16 10 1 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