#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:32:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181250 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/28/2232887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232887_Fobs loop_ _publ_author_name 'Tong, Shao-Wei' 'Li, Shi-Jie' 'Song, Wen-Dong' 'Miao, Dong-Liang' 'An, Jing-Bo' _publ_section_title ; Diaquabis(5-carboxy-2-propyl-1H-imidazole-4-carboxylato-\k^2^N^3^,O^4^)cadmium N,N-dimethylformamide disolvate ; _journal_coeditor_code PK2369 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1870 _journal_page_last m1871 _journal_volume 67 _journal_year 2011 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.6040 _cell_length_b 9.8516 _cell_length_c 18.4154 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.8036 _cod_data_source_file pk2369Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2 in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 414.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -22 341.51 431.61 107.42 o 2 0 -22 34.14 -9.62 42.94 o 4 0 -22 152.27 99.80 53.04 o 1 1 -22 114.19 172.14 40.13 o 2 1 -22 1.47 10.17 29.15 o 3 1 -22 18.99 -2.06 30.97 o 4 1 -22 8.71 49.36 33.03 o 5 1 -22 51.37 60.90 35.73 o 0 2 -22 4.28 -27.14 36.84 o 1 2 -22 1.31 15.16 30.00 o 2 2 -22 0.06 17.90 31.36 o 3 2 -22 1.32 12.22 31.84 o 4 2 -22 131.09 67.20 35.49 o 1 3 -22 80.55 111.99 38.27 o 2 3 -22 0.72 -21.95 31.45 o 2 0 -21 459.16 377.59 68.55 o 4 0 -21 44.82 50.40 40.91 o 6 0 -21 113.92 86.82 62.19 o 8 0 -21 28.22 6.79 41.81 o 0 1 -21 28.66 7.99 39.45 o 1 1 -21 101.11 114.82 32.82 o 2 1 -21 5.17 -11.25 26.28 o 3 1 -21 112.78 120.18 34.49 o 4 1 -21 0.41 0.24 27.03 o 5 1 -21 6.16 30.83 29.71 o 6 1 -21 3.81 17.27 28.49 o 7 1 -21 90.01 94.20 34.40 o 8 1 -21 38.30 6.99 30.87 o 1 2 -21 24.54 69.26 59.94 o 2 2 -21 11.23 -8.99 26.98 o 3 2 -21 5.52 20.43 27.86 o 4 2 -21 35.10 8.31 26.47 o 5 2 -21 9.24 -5.75 27.04 o 6 2 -21 99.03 86.80 33.45 o 7 2 -21 10.16 0.83 30.32 o 0 3 -21 31.05 13.60 38.68 o 1 3 -21 127.68 123.36 35.65 o 2 3 -21 26.64 -0.36 26.07 o 3 3 -21 199.06 151.25 36.11 o 4 3 -21 1.98 12.16 29.26 o 5 3 -21 32.22 17.11 29.48 o 6 3 -21 17.67 28.89 31.25 o 1 4 -21 3.90 7.83 29.36 o 2 4 -21 146.56 154.60 67.67 o 3 4 -21 9.51 -23.31 26.79 o 4 4 -21 8.12 -10.60 29.22 o 0 0 -20 600.86 435.93 95.81 o 2 0 -20 12.00 5.66 34.28 o 4 0 -20 340.35 278.16 66.21 o 6 0 -20 145.20 68.38 39.93 o 8 0 -20 89.44 28.70 40.94 o 10 0 -20 41.22 52.55 47.87 o 1 1 -20 312.64 308.75 43.41 o 2 1 -20 239.70 208.60 38.28 o 3 1 -20 71.78 34.95 28.68 o 4 1 -20 6.79 -7.23 24.63 o 5 1 -20 161.10 170.94 35.02 o 6 1 -20 4.90 -24.98 24.98 o 7 1 -20 5.61 -0.16 24.85 o 8 1 -20 27.70 11.43 26.67 o 9 1 -20 66.41 102.46 36.41 o 0 2 -20 10.48 19.00 36.31 o 1 2 -20 52.01 79.93 32.61 o 2 2 -20 2.89 27.15 25.37 o 3 2 -20 4.21 -17.93 23.37 o 4 2 -20 168.77 120.48 32.63 o 5 2 -20 30.62 -6.87 23.81 o 6 2 -20 60.51 68.32 29.99 o 7 2 -20 14.34 35.97 29.11 o 8 2 -20 90.10 35.48 29.20 o 9 2 -20 0.16 6.23 25.84 o 1 3 -20 98.75 107.58 32.78 o 2 3 -20 7.27 -22.09 23.43 o 3 3 -20 74.47 51.38 29.09 o 4 3 -20 2.40 10.93 26.04 o 5 3 -20 173.15 144.59 63.18 o 6 3 -20 13.37 -8.47 25.85 o 7 3 -20 14.69 30.34 29.60 o 8 3 -20 6.25 17.00 25.19 o 0 4 -20 482.86 383.41 67.33 o 1 4 -20 9.30 0.01 25.39 o 2 4 -20 29.28 46.02 29.98 o 3 4 -20 1.66 18.98 28.27 o 4 4 -20 130.89 121.02 34.45 o 5 4 -20 20.92 4.74 38.16 o 6 4 -20 43.85 83.12 40.35 o 7 4 -20 0.65 26.47 38.24 o 1 5 -20 89.15 62.87 31.92 o 2 5 -20 6.28 -26.83 26.83 o 3 5 -20 51.55 85.91 37.99 o 4 5 -20 3.50 -4.33 33.39 o 5 5 -20 119.46 128.47 42.65 o 2 0 -19 209.96 190.89 49.62 o 4 0 -19 69.97 82.18 50.81 o 6 0 -19 290.81 276.52 80.12 o 8 0 -19 115.83 177.27 57.73 o 10 0 -19 102.34 54.73 34.04 o 0 1 -19 304.36 275.58 89.71 o 1 1 -19 258.14 154.72 32.15 o 2 1 -19 58.52 42.04 30.69 o 3 1 -19 251.11 119.20 45.69 o 4 1 -19 29.17 46.35 25.81 o 5 1 -19 58.62 43.68 26.37 o 6 1 -19 51.35 68.89 27.13 o 7 1 -19 212.93 233.13 47.59 o 8 1 -19 40.20 27.23 24.44 o 9 1 -19 1.80 -6.69 21.38 o 10 1 -19 31.27 32.50 23.44 o 11 1 -19 132.29 132.15 31.47 o 1 2 -19 79.30 54.99 25.60 o 2 2 -19 380.66 377.81 44.10 o 3 2 -19 4.60 -20.89 20.89 o 4 2 -19 82.72 72.60 27.83 o 5 2 -19 2.92 -6.03 22.45 o 6 2 -19 321.58 286.33 47.93 o 7 2 -19 54.99 -11.63 20.93 o 8 2 -19 111.75 93.54 27.41 o 9 2 -19 5.89 -17.60 22.08 o 10 2 -19 77.13 86.97 30.28 o 11 2 -19 12.85 36.99 24.43 o 0 3 -19 35.25 60.34 77.07 o 1 3 -19 119.09 48.16 26.46 o 2 3 -19 69.38 94.91 29.53 o 3 3 -19 327.68 322.54 58.87 o 4 3 -19 50.51 6.35 23.97 o 5 3 -19 41.14 17.27 26.10 o 6 3 -19 3.40 -18.45 21.20 o 7 3 -19 326.30 363.12 40.51 o 8 3 -19 5.92 -7.51 24.71 o 9 3 -19 2.85 -22.18 22.18 o 10 3 -19 17.17 -6.97 27.98 o 1 4 -19 39.08 66.18 32.75 o 2 4 -19 364.99 372.77 43.84 o 3 4 -19 28.98 56.98 28.86 o 4 4 -19 29.03 49.75 28.24 o 5 4 -19 57.52 47.33 27.86 o 6 4 -19 129.46 114.92 34.60 o 7 4 -19 0.48 7.28 25.76 o 8 4 -19 66.68 53.21 32.43 o 9 4 -19 1.62 -27.79 27.79 o 0 5 -19 30.10 51.47 80.49 o 1 5 -19 115.13 201.17 38.02 o 2 5 -19 2.12 -14.21 29.45 o 3 5 -19 169.97 210.65 62.04 o 4 5 -19 41.13 44.56 33.25 o 5 5 -19 22.84 47.51 29.96 o 6 5 -19 12.60 -7.08 27.40 o 7 5 -19 65.71 126.34 43.42 o 1 6 -19 20.29 55.66 49.32 o 2 6 -19 195.00 183.36 55.81 o 3 6 -19 9.34 -6.96 31.29 o 4 6 -19 18.09 -6.25 27.21 o 5 6 -19 3.27 1.28 28.09 o 0 0 -18 393.95 449.76 91.50 o 2 0 -18 25.61 26.82 29.77 o 4 0 -18 634.29 703.27 77.29 o 6 0 -18 130.70 67.03 70.00 o 8 0 -18 238.84 136.41 43.07 o 10 0 -18 209.47 273.29 85.01 o 12 0 -18 111.82 82.33 40.29 o 1 1 -18 376.13 308.15 38.90 o 2 1 -18 142.17 69.22 26.58 o 3 1 -18 109.48 69.41 25.44 o 4 1 -18 63.51 50.83 24.56 o 5 1 -18 309.56 393.23 44.81 o 6 1 -18 41.92 21.71 21.88 o 7 1 -18 7.20 20.46 20.15 o 8 1 -18 21.27 16.25 21.44 o 9 1 -18 217.55 167.60 29.15 o 10 1 -18 14.48 22.76 21.96 o 11 1 -18 12.03 7.72 25.41 o 12 1 -18 0.31 -3.86 25.19 o 0 2 -18 216.33 119.40 43.50 o 1 2 -18 30.50 49.39 24.96 o 2 2 -18 33.22 28.18 23.04 o 3 2 -18 14.12 63.28 24.75 o 4 2 -18 462.71 477.78 46.94 o 5 2 -18 1.90 -4.60 21.89 o 6 2 -18 306.01 282.38 42.24 o 7 2 -18 2.10 2.28 20.75 o 8 2 -18 182.03 128.71 28.97 o 9 2 -18 28.28 8.41 20.07 o 10 2 -18 162.16 122.87 30.03 o 11 2 -18 13.13 40.26 27.13 o 12 2 -18 34.50 25.17 27.15 o 1 3 -18 147.50 105.24 34.77 o 2 3 -18 0.08 2.85 22.29 o 3 3 -18 280.68 224.27 34.60 o 4 3 -18 30.44 -4.10 21.85 o 5 3 -18 336.41 290.24 43.74 o 6 3 -18 2.08 -9.65 18.91 o 7 3 -18 55.14 61.13 24.14 o 8 3 -18 8.79 10.99 22.43 o 9 3 -18 261.25 281.33 37.75 o 10 3 -18 11.83 2.21 27.60 o 11 3 -18 13.30 1.15 28.18 o 0 4 -18 1039.07 1232.38 98.52 o 1 4 -18 19.06 14.34 23.58 o 2 4 -18 101.00 77.86 27.76 o 3 4 -18 25.09 13.09 24.71 o 4 4 -18 106.79 108.76 25.92 o 5 4 -18 9.71 3.10 21.64 o 6 4 -18 123.30 101.30 30.52 o 7 4 -18 28.66 9.18 26.80 o 8 4 -18 68.25 18.71 27.12 o 9 4 -18 1.64 -12.55 30.12 o 10 4 -18 109.01 114.53 36.04 o 1 5 -18 337.55 286.64 38.86 o 2 5 -18 17.51 36.61 30.89 o 3 5 -18 103.86 87.66 29.76 o 4 5 -18 79.13 62.88 28.60 o 5 5 -18 363.77 412.31 60.10 o 6 5 -18 25.81 -2.97 24.45 o 7 5 -18 46.34 12.53 28.33 o 8 5 -18 2.64 6.87 26.22 o 9 5 -18 140.13 125.16 45.48 o 0 6 -18 358.81 249.65 80.64 o 1 6 -18 39.88 -6.32 35.70 o 2 6 -18 28.85 17.04 31.97 o 3 6 -18 26.30 25.79 26.87 o 4 6 -18 202.94 168.37 45.72 o 5 6 -18 6.52 -14.11 25.90 o 6 6 -18 37.92 18.73 44.39 o 7 6 -18 5.17 24.63 34.08 o 1 7 -18 161.56 251.29 57.81 o 2 7 -18 11.88 51.32 42.38 o 3 7 -18 79.32 78.84 48.64 o 4 7 -18 2.05 3.17 42.12 o 2 0 -17 639.13 513.20 63.63 o 4 0 -17 162.81 164.43 43.52 o 6 0 -17 479.54 421.70 49.11 o 8 0 -17 191.99 134.92 35.49 o 10 0 -17 168.36 159.45 38.85 o 12 0 -17 275.92 286.93 63.38 o 0 1 -17 117.44 21.59 30.06 o 1 1 -17 297.89 266.66 34.90 o 2 1 -17 7.92 -14.06 17.98 o 3 1 -17 530.63 600.73 49.46 o 4 1 -17 198.12 247.40 35.20 o 5 1 -17 87.41 71.49 22.13 o 6 1 -17 72.99 37.16 20.76 o 7 1 -17 675.13 718.03 45.62 o 8 1 -17 25.68 13.41 18.49 o 9 1 -17 37.47 49.23 21.03 o 10 1 -17 0.04 -20.04 20.04 o 11 1 -17 342.70 339.90 40.87 o 12 1 -17 3.98 21.48 23.95 o 13 1 -17 21.03 46.69 33.94 o 1 2 -17 34.13 27.06 21.02 o 2 2 -17 1377.99 1512.79 72.38 o 3 2 -17 320.57 421.46 43.24 o 4 2 -17 214.70 210.49 38.93 o 5 2 -17 4.18 15.47 22.05 o 6 2 -17 754.93 834.91 78.29 o 7 2 -17 11.79 1.87 18.82 o 8 2 -17 233.87 270.66 36.77 o 9 2 -17 8.56 7.82 22.02 o 10 2 -17 143.95 152.07 30.75 o 11 2 -17 16.91 17.43 24.35 o 12 2 -17 57.38 3.62 24.07 o 13 2 -17 18.53 -14.43 27.27 o 0 3 -17 2.43 28.46 29.19 o 1 3 -17 167.41 159.49 29.80 o 2 3 -17 175.20 134.96 29.48 o 3 3 -17 379.42 398.46 37.74 o 4 3 -17 200.31 226.32 30.05 o 5 3 -17 52.24 29.14 20.79 o 6 3 -17 4.91 16.28 19.85 o 7 3 -17 433.36 381.22 38.27 o 8 3 -17 22.81 23.46 24.06 o 9 3 -17 16.81 -6.99 21.96 o 10 3 -17 10.49 21.36 27.77 o 11 3 -17 254.43 320.28 41.23 o 12 3 -17 11.18 -23.54 27.11 o 1 4 -17 1.11 -19.75 20.01 o 2 4 -17 960.87 880.55 51.75 o 3 4 -17 15.94 14.37 19.19 o 4 4 -17 51.31 60.10 23.13 o 5 4 -17 26.58 51.44 22.22 o 6 4 -17 409.72 498.19 42.12 o 7 4 -17 4.52 6.99 23.95 o 8 4 -17 107.27 80.84 34.06 o 9 4 -17 9.71 48.73 31.72 o 10 4 -17 113.36 74.13 29.27 o 11 4 -17 33.67 19.25 26.83 o 12 4 -17 170.37 201.72 38.62 o 0 5 -17 86.80 46.89 33.90 o 1 5 -17 417.40 510.54 76.94 o 2 5 -17 11.76 26.39 21.79 o 3 5 -17 580.26 564.44 50.56 o 4 5 -17 17.56 19.61 25.17 o 5 5 -17 53.10 56.96 25.47 o 6 5 -17 48.45 5.46 33.09 o 7 5 -17 264.83 241.28 37.81 o 8 5 -17 34.95 14.80 32.18 o 9 5 -17 1.89 -22.49 28.69 o 10 5 -17 2.61 -2.74 30.04 o 11 5 -17 137.15 151.03 41.66 o 1 6 -17 38.22 34.71 30.04 o 2 6 -17 429.20 463.55 46.80 o 3 6 -17 24.48 10.35 23.88 o 4 6 -17 80.02 84.02 30.87 o 5 6 -17 6.11 -14.24 25.72 o 6 6 -17 102.48 87.26 36.10 o 7 6 -17 6.07 13.05 30.93 o 8 6 -17 121.42 60.33 36.94 o 9 6 -17 29.79 58.67 38.66 o 0 7 -17 7.28 -15.88 36.60 o 1 7 -17 92.14 131.89 38.50 o 2 7 -17 8.51 1.54 48.06 o 3 7 -17 289.52 185.59 53.03 o 4 7 -17 4.43 -17.92 33.09 o 5 7 -17 56.60 45.02 42.87 o 6 7 -17 24.75 -9.82 35.70 o 7 7 -17 431.37 404.26 109.97 o 1 8 -17 20.36 -2.68 58.92 o 2 8 -17 77.97 224.21 80.19 o 3 8 -17 13.54 69.37 45.86 o 0 0 -16 258.31 140.00 55.64 o 2 0 -16 6.15 26.01 27.37 o 4 0 -16 543.60 605.76 52.63 o 6 0 -16 403.40 344.43 57.93 o 8 0 -16 298.14 347.16 67.03 o 10 0 -16 331.97 395.18 65.36 o 12 0 -16 106.19 40.47 84.88 o 14 0 -16 279.51 270.22 69.35 o 1 1 -16 691.72 617.65 47.42 o 2 1 -16 18.68 -10.34 16.71 o 3 1 -16 197.75 202.23 26.55 o 4 1 -16 88.33 30.24 18.73 o 5 1 -16 509.01 551.05 36.92 o 6 1 -16 176.19 197.31 24.57 o 7 1 -16 36.56 13.63 17.66 o 8 1 -16 31.74 8.76 18.17 o 9 1 -16 684.49 711.21 49.60 o 10 1 -16 15.14 -10.59 19.34 o 11 1 -16 36.39 41.79 27.73 o 12 1 -16 9.64 7.77 27.65 o 13 1 -16 291.25 355.10 54.65 o 14 1 -16 0.72 -20.92 28.31 o 0 2 -16 2134.37 2068.65 256.57 o 1 2 -16 55.28 25.38 21.28 o 2 2 -16 92.89 89.22 21.47 o 3 2 -16 336.76 407.75 51.76 o 4 2 -16 1475.99 1525.86 95.04 o 5 2 -16 84.02 42.46 19.88 o 6 2 -16 561.57 592.43 39.28 o 7 2 -16 21.65 18.28 28.19 o 8 2 -16 391.41 415.12 39.16 o 9 2 -16 22.13 28.41 22.09 o 10 2 -16 367.43 397.00 46.07 o 11 2 -16 5.17 -18.48 21.31 o 12 2 -16 24.76 9.20 22.22 o 13 2 -16 24.53 70.12 33.69 o 14 2 -16 122.85 117.11 37.74 o 1 3 -16 382.64 291.93 35.23 o 2 3 -16 54.78 26.78 18.02 o 3 3 -16 484.08 505.07 51.47 o 4 3 -16 259.75 223.44 33.81 o 5 3 -16 1168.95 1276.35 58.41 o 6 3 -16 2.76 7.60 17.11 o 7 3 -16 117.64 118.15 25.18 o 8 3 -16 29.20 37.26 21.95 o 9 3 -16 437.83 431.44 40.99 o 10 3 -16 7.91 -14.96 20.25 o 11 3 -16 10.61 6.23 23.45 o 12 3 -16 32.61 42.56 27.34 o 13 3 -16 87.80 104.73 32.62 o 0 4 -16 895.05 1046.69 101.77 o 1 4 -16 20.86 14.74 17.58 o 2 4 -16 218.41 265.14 31.00 o 3 4 -16 15.22 -10.20 17.04 o 4 4 -16 213.86 177.25 37.34 o 5 4 -16 4.60 3.24 17.48 o 6 4 -16 155.31 168.96 33.47 o 7 4 -16 66.61 100.08 34.32 o 8 4 -16 143.41 99.63 31.37 o 9 4 -16 17.44 28.10 27.49 o 10 4 -16 226.82 254.57 37.55 o 11 4 -16 1.08 15.89 25.17 o 12 4 -16 103.29 175.98 36.30 o 13 4 -16 33.69 16.75 34.41 o 1 5 -16 609.90 641.16 71.20 o 2 5 -16 130.69 118.16 25.06 o 3 5 -16 316.02 291.15 54.52 o 4 5 -16 47.58 51.16 24.34 o 5 5 -16 528.93 511.35 48.26 o 6 5 -16 8.84 65.19 27.21 o 7 5 -16 96.06 97.37 46.13 o 8 5 -16 79.10 14.06 27.55 o 9 5 -16 117.05 80.98 32.16 o 10 5 -16 2.38 -3.02 26.32 o 11 5 -16 20.44 37.35 31.56 o 12 5 -16 1.28 -8.39 32.39 o 0 6 -16 1181.66 1242.78 142.23 o 1 6 -16 16.89 27.90 24.87 o 2 6 -16 58.37 57.53 25.37 o 3 6 -16 15.13 0.73 23.01 o 4 6 -16 434.02 396.10 44.16 o 5 6 -16 9.43 -21.53 21.94 o 6 6 -16 120.30 118.41 58.57 o 7 6 -16 4.22 -12.69 27.13 o 8 6 -16 254.68 294.40 53.33 o 9 6 -16 33.71 37.52 33.97 o 10 6 -16 258.12 307.41 51.78 o 1 7 -16 126.83 82.49 29.13 o 2 7 -16 25.14 26.50 28.77 o 3 7 -16 63.40 48.74 39.92 o 4 7 -16 1.00 32.51 35.23 o 5 7 -16 562.50 446.28 57.75 o 6 7 -16 6.05 25.23 27.39 o 7 7 -16 26.72 60.60 37.54 o 8 7 -16 37.51 40.39 37.37 o 0 8 -16 60.78 148.93 75.43 o 1 8 -16 3.79 -31.69 31.69 o 2 8 -16 3.50 -35.66 35.66 o 3 8 -16 13.77 25.50 42.74 o 4 8 -16 329.03 271.41 50.31 o 5 8 -16 2.65 17.44 35.20 o 6 8 -16 101.73 33.11 36.58 o 2 0 -15 3277.64 3078.99 201.90 o 4 0 -15 538.02 412.04 44.24 o 6 0 -15 687.80 574.92 89.45 o 8 0 -15 340.69 320.07 93.14 o 10 0 -15 385.34 403.30 64.21 o 12 0 -15 620.63 613.91 79.57 o 14 0 -15 105.36 139.10 51.00 o 0 1 -15 171.34 175.14 41.44 o 1 1 -15 691.81 778.00 67.56 o 2 1 -15 130.14 133.28 22.72 o 3 1 -15 706.15 704.93 42.36 o 4 1 -15 28.91 38.44 18.25 o 5 1 -15 42.72 32.08 15.52 o 6 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693.90 743.82 33.64 o 3 5 1 3638.21 3277.76 67.20 o 4 5 1 179.89 164.32 15.57 o 5 5 1 1256.62 1263.06 36.71 o 6 5 1 90.00 168.52 22.06 o 7 5 1 8263.73 8223.80 161.06 o 8 5 1 196.01 168.18 28.25 o 9 5 1 279.99 252.36 29.19 o 10 5 1 541.10 497.07 40.27 o 11 5 1 2911.96 2852.84 105.03 o 12 5 1 517.06 530.09 43.32 o 13 5 1 771.19 719.98 70.36 o 14 5 1 167.63 158.19 33.72 o 15 5 1 1877.04 2041.78 123.35 o 16 5 1 434.29 339.62 50.82 o 17 5 1 393.47 353.71 52.95 o 18 5 1 1.23 -7.26 34.53 o 1 6 1 955.14 881.87 40.80 o 2 6 1 5841.98 5931.66 120.84 o 3 6 1 257.73 186.56 22.05 o 4 6 1 2654.54 2595.98 60.74 o 5 6 1 51.91 48.08 16.98 o 6 6 1 5258.53 5111.06 116.72 o 7 6 1 231.59 162.58 24.37 o 8 6 1 1579.34 1625.25 63.69 o 9 6 1 342.68 375.12 63.46 o 10 6 1 496.53 560.42 43.89 o 11 6 1 694.87 700.14 50.19 o 12 6 1 2129.79 2093.06 84.33 o 13 6 1 47.63 47.06 24.21 o 14 6 1 133.67 100.71 31.98 o 15 6 1 113.91 133.99 56.37 o 16 6 1 1862.30 1933.71 149.11 o 17 6 1 11.79 15.72 32.34 o 0 7 1 52.58 26.09 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469.33 233.14 85.25 o 4 11 8 1.31 32.29 61.60 o 5 11 8 1206.93 1441.54 171.54 o 1 4 9 463.58 563.07 41.01 o 2 4 9 7121.07 7261.97 186.11 o 0 5 9 34.29 -0.30 29.46 o 1 5 9 4136.21 4132.33 129.12 o 2 5 9 697.16 717.12 80.64 o 3 5 9 4869.70 5184.26 227.93 o 4 5 9 907.12 1075.53 102.51 o 1 6 9 15.03 -0.69 23.89 o 2 6 9 2216.00 2170.11 138.37 o 3 6 9 956.06 1039.08 104.30 o 4 6 9 206.01 246.98 63.23 o 5 6 9 192.01 220.64 64.87 o 6 6 9 1139.61 1202.44 125.27 o 0 7 9 27.88 79.60 43.00 o 1 7 9 1379.77 1486.02 124.08 o 2 7 9 107.30 93.14 48.65 o 3 7 9 2489.37 2681.03 166.49 o 4 7 9 133.65 110.40 54.16 o 5 7 9 1140.04 1085.06 122.45 o 6 7 9 108.15 45.82 46.57 o 7 7 9 2967.95 2722.39 191.93 o 8 7 9 12.72 -12.35 41.21 o 1 8 9 124.13 37.94 42.25 o 2 8 9 2353.78 2137.68 152.80 o 3 8 9 659.28 516.42 89.86 o 4 8 9 524.92 568.79 96.11 o 5 8 9 30.38 -9.52 43.44 o 6 8 9 1275.91 1216.58 140.90 o 7 8 9 108.10 123.49 61.45 o 8 8 9 543.33 508.09 106.82 o 9 8 9 6.36 9.22 55.64 o 2 9 9 31.86 95.22 54.90 o 3 9 9 1785.59 1799.20 162.77 o 4 9 9 26.53 -18.90 44.49 o 5 9 9 294.39 327.47 81.83 o 6 9 9 35.35 -38.09 46.42 o 7 9 9 1301.51 1374.14 158.45 o 8 9 9 54.76 5.21 56.69 o 9 9 9 136.73 195.20 77.66 o 10 9 9 7.14 45.97 62.19 o 3 10 9 22.70 44.93 59.07 o 4 10 9 32.45 -18.45 46.27 o 5 10 9 24.27 22.17 56.39 o 6 10 9 532.50 606.13 122.00 o 7 10 9 13.63 -4.31 56.98 o 8 10 9 327.35 464.05 107.27 o 4 11 9 15.99 49.40 69.93 o 1 5 10 3648.87 3950.72 183.00 o 2 5 10 19.07 -25.14 29.76 o 3 5 10 1476.74 1512.50 113.52 o 1 6 10 155.17 153.54 51.33 o 2 6 10 45.66 99.83 43.89 o 3 6 10 459.36 396.80 74.09 o 4 6 10 1779.02 1723.92 134.94 o 5 6 10 212.32 123.04 56.83 o 2 7 10 85.88 35.41 42.40 o 3 7 10 559.90 337.14 75.88 o 4 7 10 60.40 32.58 46.27 o 5 7 10 3085.43 3166.35 195.05 o 6 7 10 105.85 115.75 59.07 o 2 8 10 39.00 51.78 46.72 o 3 8 10 397.11 503.92 92.10 o 4 8 10 2642.16 2560.07 179.43 o 5 8 10 157.45 166.93 65.31 o 6 8 10 390.22 411.23 91.05 o 7 8 10 49.67 79.00 61.60 o 8 8 10 480.38 442.47 101.17 o 4 9 10 26.19 51.33 57.73 o 5 9 10 787.79 885.54 128.99 o 6 9 10 9.18 81.68 57.73 o 7 9 10 35.78 81.53 63.23 o 8 9 10 65.95 28.57 63.68 o 5 10 10 7.72 14.28 57.28 o 6 10 10 188.06 49.54 65.91 o 7 10 10 43.81 109.65 76.92 o 2 6 11 1236.50 1227.89 109.50 o 3 6 11 354.58 368.83 72.16 o 3 7 11 1584.98 1787.90 137.03 o 4 7 11 89.25 61.00 52.07 o 5 7 11 188.64 247.57 73.05 o 4 8 11 331.62 177.79 70.52 o 5 8 11 138.59 54.45 57.88 o 6 8 11 952.28 902.50 129.59 o 5 9 11 139.92 83.47 61.89 o 6 9 11 17.21 -28.57 52.07 o 7 9 11 633.70 704.33 126.02 o