#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/28/2232892.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232892_Fobs loop_ _publ_author_name 'Koen, Renier' 'Roodt, Andreas' 'Visser, Hendrik G.' 'Muller, Theunis J.' _publ_section_title ; 1,1,1,5,5,5-Hexafluoro-2,4-dimethoxypentane-2,4-diol ; _journal_coeditor_code PV2464 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3155 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.509 _cell_angle_gamma 90.000 _cell_length_a 17.8290 _cell_length_b 6.7130 _cell_length_c 9.3470 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file pv2464Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I C2/c R = 0.04' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 18517.56 17895.40 151.39 o 6 0 0 2636.96 2274.24 22.82 o 8 0 0 1892.95 1992.76 21.67 o 10 0 0 494.52 504.38 27.03 o 12 0 0 12.41 10.31 4.97 o 14 0 0 748.26 730.49 17.37 o 16 0 0 176.46 173.28 10.72 o 18 0 0 0.90 0.56 6.25 o 20 0 0 136.45 151.74 18.94 o 22 0 0 305.92 284.75 40.04 o 3 1 0 6747.44 6655.50 42.45 o 5 1 0 1065.90 1147.97 8.32 o 7 1 0 919.55 976.03 8.40 o 9 1 0 126.92 136.31 4.33 o 11 1 0 1386.72 1295.94 16.33 o 13 1 0 684.25 693.39 13.75 o 15 1 0 17.35 11.71 3.83 o 17 1 0 1514.59 1467.80 26.41 o 19 1 0 16.90 17.12 7.25 o 21 1 0 126.90 136.16 20.03 o 0 2 0 2251.95 2074.69 52.28 o 2 2 0 3263.88 3244.01 31.45 o 4 2 0 7683.58 7583.85 51.06 o 6 2 0 5076.02 5234.69 38.80 o 8 2 0 4383.81 4327.92 38.80 o 10 2 0 61.56 61.02 3.52 o 12 2 0 526.14 541.55 11.05 o 14 2 0 16.79 15.32 4.11 o 16 2 0 57.61 66.14 7.95 o 18 2 0 273.33 266.04 14.06 o 20 2 0 76.70 59.77 18.30 o 1 3 0 3566.17 3541.49 48.42 o 3 3 0 689.65 685.24 8.13 o 5 3 0 1261.63 1402.27 13.89 o 7 3 0 0.04 -0.18 1.80 o 9 3 0 19.76 6.91 1.79 o 11 3 0 93.85 84.42 4.86 o 13 3 0 52.72 40.67 5.83 o 15 3 0 2232.39 2125.54 42.48 o 17 3 0 15.02 34.82 7.07 o 19 3 0 47.34 26.01 7.17 o 0 4 0 229.29 219.79 19.80 o 2 4 0 773.45 810.29 14.19 o 4 4 0 18.51 22.94 1.73 o 6 4 0 1546.50 1649.85 19.64 o 8 4 0 680.46 699.92 10.01 o 10 4 0 1066.00 1117.14 14.82 o 12 4 0 46.14 50.98 8.92 o 14 4 0 3.00 2.26 5.37 o 16 4 0 21.91 23.59 7.04 o 18 4 0 126.62 119.97 12.27 o 1 5 0 315.06 308.90 10.53 o 3 5 0 789.53 751.24 15.13 o 5 5 0 1021.33 1009.11 12.65 o 7 5 0 1031.12 1033.49 13.51 o 9 5 0 765.76 710.81 20.47 o 11 5 0 1193.64 1153.23 30.00 o 13 5 0 0.00 1.05 4.91 o 15 5 0 14.27 8.10 6.11 o 17 5 0 201.30 225.90 24.72 o 0 6 0 851.77 861.15 41.38 o 2 6 0 197.90 199.96 6.37 o 4 6 0 5.20 5.49 6.69 o 6 6 0 281.55 291.84 8.35 o 8 6 0 1485.42 1483.46 46.28 o 10 6 0 32.48 32.63 6.65 o 12 6 0 137.19 135.27 10.26 o 14 6 0 332.78 355.07 16.14 o 16 6 0 218.14 252.48 20.55 o 1 7 0 995.20 922.55 46.72 o 3 7 0 38.24 41.97 6.84 o 5 7 0 994.96 984.70 35.01 o 7 7 0 5.16 4.72 4.98 o 9 7 0 332.97 338.96 23.25 o 11 7 0 0.02 7.37 6.10 o 13 7 0 79.17 61.61 9.35 o 2 8 0 67.61 64.85 8.40 o 4 8 0 5.57 3.49 6.58 o 6 8 0 56.80 47.34 9.19 o 8 8 0 10.08 18.27 6.01 o -21 1 1 451.99 452.00 27.17 o -19 1 1 4.94 13.06 6.09 o -17 1 1 31.35 37.54 6.17 o -15 1 1 1436.76 1389.13 21.44 o -13 1 1 169.51 147.72 7.53 o -11 1 1 563.43 580.01 9.40 o -9 1 1 2352.25 2360.27 20.81 o -7 1 1 16402.96 16546.13 100.41 o -5 1 1 1.46 -0.32 0.98 o -3 1 1 16.83 10.12 1.40 o -1 1 1 12414.15 11069.23 260.85 o 1 1 1 17562.01 17390.90 107.91 o 3 1 1 621.66 584.68 5.15 o 5 1 1 2681.44 2734.99 18.81 o 7 1 1 299.54 267.27 4.85 o 9 1 1 37.47 35.98 3.12 o 11 1 1 266.59 254.11 7.37 o 13 1 1 534.34 515.74 11.34 o 15 1 1 15.79 11.26 3.82 o 17 1 1 1.79 2.01 5.61 o 19 1 1 196.30 198.55 12.22 o 21 1 1 113.01 121.53 16.45 o -22 2 1 0.53 14.04 10.41 o -20 2 1 9.17 14.56 7.56 o -18 2 1 278.62 280.74 18.88 o -16 2 1 282.26 234.73 11.42 o -14 2 1 205.05 165.84 6.57 o -12 2 1 86.62 89.79 5.01 o -10 2 1 393.55 407.11 7.49 o -8 2 1 92.06 128.74 3.89 o -6 2 1 5210.66 5112.49 30.35 o -4 2 1 2964.94 2943.16 34.21 o -2 2 1 1620.87 1626.56 14.83 o 0 2 1 108.81 105.92 2.70 o 2 2 1 2535.87 2510.31 18.66 o 4 2 1 8.44 5.11 0.97 o 6 2 1 4464.90 4411.99 42.80 o 8 2 1 1020.60 983.55 11.01 o 10 2 1 1119.51 1059.00 12.59 o 12 2 1 12.82 11.95 2.65 o 14 2 1 1346.26 1257.55 25.28 o 16 2 1 2434.02 2396.90 46.89 o 18 2 1 39.83 41.42 7.80 o 20 2 1 74.23 63.46 12.67 o -21 3 1 200.16 235.72 21.62 o -19 3 1 42.19 39.58 8.46 o -17 3 1 292.74 321.60 15.70 o -15 3 1 31.53 33.89 5.35 o -13 3 1 897.59 840.20 17.56 o -11 3 1 326.38 310.09 6.40 o -9 3 1 16.17 13.38 2.14 o -7 3 1 521.14 542.42 9.83 o -5 3 1 989.71 1089.87 11.41 o -3 3 1 1849.94 1912.80 19.90 o -1 3 1 116.64 127.64 3.23 o 1 3 1 2175.77 2195.46 24.38 o 3 3 1 552.73 529.39 5.69 o 5 3 1 113.84 124.75 3.57 o 7 3 1 1487.52 1440.43 13.18 o 9 3 1 219.34 213.81 6.83 o 11 3 1 222.83 228.19 6.79 o 13 3 1 116.62 132.55 10.38 o 15 3 1 269.30 245.70 15.13 o 17 3 1 1.76 -6.56 6.76 o 19 3 1 35.76 39.35 9.54 o -20 4 1 57.35 55.48 10.93 o -18 4 1 4.72 13.40 7.43 o -16 4 1 153.13 129.45 11.71 o -14 4 1 162.08 194.43 9.72 o -12 4 1 634.69 678.59 16.18 o -10 4 1 886.97 915.21 12.05 o -8 4 1 53.92 52.39 3.00 o -6 4 1 647.53 631.06 7.45 o -4 4 1 48.97 60.38 3.71 o -2 4 1 3717.17 3733.82 42.00 o 0 4 1 123.81 147.95 4.65 o 2 4 1 2.21 -1.90 1.38 o 4 4 1 410.81 385.25 5.91 o 6 4 1 996.44 1001.76 13.05 o 8 4 1 3502.20 3491.09 32.85 o 10 4 1 173.35 182.00 13.31 o 12 4 1 333.51 336.84 19.46 o 14 4 1 71.13 71.43 10.77 o 16 4 1 251.91 213.87 47.72 o 18 4 1 199.31 181.07 14.59 o -17 5 1 9.70 9.25 7.10 o -15 5 1 3.52 -1.83 5.99 o -13 5 1 135.50 137.46 10.40 o -11 5 1 14.66 14.67 5.01 o -9 5 1 72.49 81.07 5.54 o -7 5 1 326.38 319.32 6.33 o -5 5 1 206.05 206.21 9.63 o -3 5 1 220.96 213.97 9.15 o -1 5 1 153.53 183.98 5.79 o 1 5 1 980.23 1054.25 15.75 o 3 5 1 191.84 197.79 5.24 o 5 5 1 358.68 364.27 7.32 o 7 5 1 1.76 0.71 3.06 o 9 5 1 333.43 316.20 14.05 o 11 5 1 560.37 568.13 22.47 o 13 5 1 234.85 192.46 14.86 o 15 5 1 842.60 873.86 30.51 o 17 5 1 92.46 97.82 11.67 o -16 6 1 6.87 1.94 7.17 o -14 6 1 64.61 64.90 8.79 o -12 6 1 150.51 165.56 10.14 o -10 6 1 168.05 167.32 9.07 o -8 6 1 429.69 392.76 18.12 o -6 6 1 129.65 126.56 11.35 o -4 6 1 137.84 143.45 13.15 o -2 6 1 117.74 118.52 6.53 o 0 6 1 227.25 206.23 6.73 o 2 6 1 215.13 219.19 5.78 o 4 6 1 249.12 229.08 7.35 o 6 6 1 45.69 43.51 5.60 o 8 6 1 316.78 310.59 12.57 o 10 6 1 3.34 -4.29 7.23 o 12 6 1 1.73 -1.74 5.98 o 14 6 1 93.75 54.81 10.77 o -13 7 1 83.73 95.41 9.13 o -11 7 1 54.30 34.91 6.26 o -9 7 1 128.26 113.31 7.54 o -7 7 1 776.44 791.36 18.58 o -5 7 1 0.04 0.78 5.61 o -3 7 1 37.04 34.63 13.90 o -1 7 1 1.91 -0.77 4.91 o 1 7 1 18.94 21.41 12.57 o 3 7 1 17.88 14.52 4.05 o 5 7 1 262.53 257.40 11.85 o 7 7 1 8.46 8.10 4.96 o 9 7 1 12.87 15.36 5.91 o 11 7 1 68.25 69.03 9.16 o -10 8 1 17.96 25.82 7.16 o -8 8 1 34.26 40.51 6.62 o -6 8 1 80.06 71.84 10.87 o -4 8 1 3.75 12.31 7.01 o -2 8 1 285.20 298.77 17.13 o 0 8 1 451.55 460.72 20.02 o 2 8 1 67.08 56.00 5.93 o 4 8 1 56.34 43.41 6.07 o 6 8 1 14.99 11.47 4.79 o 8 8 1 34.30 25.89 5.71 o -22 0 2 36.95 18.36 12.96 o -20 0 2 2.62 7.01 10.54 o -18 0 2 293.19 295.00 16.91 o -16 0 2 1920.19 1795.87 36.39 o -14 0 2 9929.17 9418.35 187.65 o -12 0 2 23.39 17.04 4.61 o -10 0 2 1556.46 1412.76 22.03 o -8 0 2 18.68 19.98 3.06 o -6 0 2 97.97 118.83 4.38 o -4 0 2 14121.00 13085.70 103.47 o -2 0 2 189.56 175.04 3.81 o 0 0 2 22572.97 21554.11 181.90 o 2 0 2 500.78 493.27 12.56 o 4 0 2 128.51 126.04 4.24 o 6 0 2 2497.61 2400.03 25.19 o 8 0 2 767.02 672.55 22.22 o 10 0 2 4518.99 4379.29 63.34 o 12 0 2 832.26 791.45 28.28 o 14 0 2 987.31 1021.97 27.63 o 16 0 2 178.69 182.10 13.07 o 18 0 2 37.15 56.51 19.13 o 20 0 2 0.07 -2.67 17.57 o -23 1 2 3.92 15.20 11.13 o -21 1 2 49.17 45.38 11.23 o -19 1 2 161.88 165.90 10.86 o -17 1 2 3.40 -1.37 4.25 o -15 1 2 24.75 13.16 5.00 o -13 1 2 46.85 47.57 4.05 o -11 1 2 1505.73 1502.82 24.71 o -9 1 2 4.82 6.27 1.72 o -7 1 2 14043.76 13712.73 84.07 o -5 1 2 4409.84 4215.98 27.52 o -3 1 2 7015.10 6691.31 41.46 o -1 1 2 16.72 14.39 1.20 o 1 1 2 9427.37 8910.68 56.95 o 3 1 2 3373.74 3501.51 23.26 o 5 1 2 88.38 91.99 2.81 o 7 1 2 4599.47 4743.07 37.27 o 9 1 2 65.23 68.20 4.04 o 11 1 2 827.43 854.26 15.60 o 13 1 2 206.31 226.57 12.73 o 15 1 2 512.54 487.66 13.41 o 17 1 2 202.91 217.81 19.69 o 19 1 2 268.14 235.29 27.14 o -22 2 2 97.65 130.41 15.65 o -20 2 2 32.32 13.54 7.32 o -18 2 2 18.46 23.57 6.68 o -16 2 2 352.44 362.67 12.86 o -14 2 2 17.25 14.54 3.30 o -12 2 2 197.72 200.99 7.10 o -10 2 2 4397.81 4449.27 38.40 o -8 2 2 14412.32 14719.36 104.80 o -6 2 2 11954.33 12290.04 82.39 o -4 2 2 6306.92 6158.16 40.47 o -2 2 2 4571.56 4492.42 31.30 o 0 2 2 26.82 28.05 1.34 o 2 2 2 1663.49 1638.83 12.39 o 4 2 2 3274.17 3310.41 29.64 o 6 2 2 1263.35 1320.14 13.12 o 8 2 2 957.48 1016.68 11.72 o 10 2 2 310.54 314.99 7.49 o 12 2 2 7.83 11.29 3.45 o 14 2 2 8.72 10.73 3.98 o 16 2 2 23.35 24.10 7.59 o 18 2 2 0.35 -0.08 7.51 o 20 2 2 52.37 56.06 21.80 o -21 3 2 218.26 254.53 19.98 o -19 3 2 53.10 34.52 7.91 o -17 3 2 115.99 119.16 10.08 o -15 3 2 259.69 204.86 12.31 o -13 3 2 3465.27 3413.23 38.21 o -11 3 2 1.72 2.06 1.92 o -9 3 2 3232.93 3153.47 25.39 o -7 3 2 909.34 881.51 11.29 o -5 3 2 2766.17 2670.23 21.55 o -3 3 2 103.34 84.54 3.24 o -1 3 2 349.21 332.21 6.37 o 1 3 2 5851.85 6496.12 52.74 o 3 3 2 350.26 344.44 5.15 o 5 3 2 8.86 11.09 1.80 o 7 3 2 10.73 9.50 1.85 o 9 3 2 5079.50 4967.28 40.21 o 11 3 2 209.07 191.96 7.98 o 13 3 2 587.20 535.11 22.96 o 15 3 2 154.08 119.03 16.26 o 17 3 2 139.08 119.81 15.16 o 19 3 2 32.31 29.63 11.37 o -20 4 2 0.20 1.09 7.88 o -18 4 2 91.16 82.03 12.52 o -16 4 2 94.73 82.76 9.50 o -14 4 2 2.93 14.84 5.91 o -12 4 2 0.56 -3.44 3.70 o -10 4 2 494.21 539.26 8.52 o -8 4 2 643.93 648.83 9.54 o -6 4 2 0.10 1.68 1.45 o -4 4 2 2557.97 2655.11 31.13 o -2 4 2 589.76 536.65 9.49 o 0 4 2 2.19 3.69 1.67 o 2 4 2 710.53 801.72 9.34 o 4 4 2 2212.16 2319.26 22.30 o 6 4 2 5.58 4.56 1.82 o 8 4 2 2584.82 2651.89 22.17 o 10 4 2 18.35 16.58 4.44 o 12 4 2 10.63 12.53 4.97 o 14 4 2 0.25 7.57 6.75 o 16 4 2 133.15 145.75 15.78 o 18 4 2 0.23 5.82 9.61 o -19 5 2 31.41 38.90 9.72 o -17 5 2 181.01 184.79 14.24 o -15 5 2 301.50 317.99 16.30 o -13 5 2 0.02 2.31 4.82 o -11 5 2 76.71 66.67 6.22 o -9 5 2 165.05 150.67 6.58 o -7 5 2 691.27 699.89 10.75 o -5 5 2 180.08 180.53 6.55 o -3 5 2 427.02 445.04 14.25 o -1 5 2 427.29 422.64 10.06 o 1 5 2 4.17 3.96 1.56 o 3 5 2 288.18 276.41 5.81 o 5 5 2 32.68 35.31 3.37 o 7 5 2 1511.84 1484.97 29.21 o 9 5 2 755.21 741.83 25.46 o 11 5 2 8.24 10.26 6.33 o 13 5 2 545.80 590.37 23.66 o 15 5 2 66.62 68.31 11.97 o -16 6 2 102.74 108.30 12.11 o -14 6 2 74.17 68.93 8.02 o -12 6 2 108.50 102.07 8.18 o -10 6 2 10.35 3.24 4.07 o -8 6 2 483.73 483.43 11.66 o -6 6 2 1049.59 1021.94 28.22 o -4 6 2 32.37 41.43 7.28 o -2 6 2 431.66 420.96 12.82 o 0 6 2 38.03 39.03 5.22 o 2 6 2 2850.69 2918.16 33.13 o 4 6 2 0.29 0.25 5.08 o 6 6 2 882.72 872.80 20.27 o 8 6 2 46.24 47.73 11.35 o 10 6 2 217.32 217.76 19.35 o 12 6 2 1.50 4.63 7.37 o 14 6 2 768.59 817.42 29.71 o -13 7 2 30.26 31.26 6.75 o -11 7 2 93.72 107.34 8.10 o -9 7 2 0.01 0.97 4.96 o -7 7 2 23.31 14.47 7.28 o -5 7 2 11.58 14.68 6.80 o -3 7 2 3.23 0.89 6.45 o -1 7 2 125.80 128.17 22.69 o 1 7 2 905.45 923.51 26.43 o 3 7 2 3.58 4.04 4.08 o 5 7 2 241.79 221.36 10.64 o 7 7 2 4.45 10.74 5.36 o 9 7 2 6.52 -2.60 5.48 o 11 7 2 0.01 -0.85 7.15 o -10 8 2 57.36 79.24 8.96 o -8 8 2 37.78 39.37 10.45 o -6 8 2 4.43 -7.79 8.45 o -4 8 2 7.24 8.01 8.01 o -2 8 2 1207.24 1203.30 39.38 o 0 8 2 0.48 -3.08 6.63 o 2 8 2 544.58 546.34 20.09 o 4 8 2 21.01 20.34 5.46 o 6 8 2 12.13 10.14 6.03 o -23 1 3 349.19 358.65 26.07 o -21 1 3 122.17 116.10 14.07 o -19 1 3 33.65 27.52 6.14 o -17 1 3 164.44 165.01 10.47 o -15 1 3 2773.21 2693.61 33.09 o -13 1 3 1601.36 1501.51 19.26 o -11 1 3 400.15 411.94 8.89 o -9 1 3 647.48 630.86 9.21 o -7 1 3 4038.61 3887.57 29.37 o -5 1 3 0.09 -2.24 1.14 o -3 1 3 17.23 31.87 2.60 o -1 1 3 346.41 346.80 4.48 o 1 1 3 532.90 526.45 5.64 o 3 1 3 6366.68 6381.81 45.04 o 5 1 3 247.69 255.41 5.16 o 7 1 3 2617.43 2648.73 24.99 o 9 1 3 66.59 68.61 4.60 o 11 1 3 111.67 107.59 6.18 o 13 1 3 28.36 25.65 4.34 o 15 1 3 177.73 165.29 9.89 o 17 1 3 736.54 766.80 21.26 o 19 1 3 0.57 6.23 18.46 o -22 2 3 32.74 23.72 10.57 o -20 2 3 1016.59 1077.07 27.20 o -18 2 3 16.70 25.81 5.86 o -16 2 3 141.43 157.51 9.48 o -14 2 3 89.54 101.91 5.64 o -12 2 3 732.64 752.85 12.22 o -10 2 3 1640.50 1629.43 17.55 o -8 2 3 579.61 598.48 8.75 o -6 2 3 925.11 1026.70 9.49 o -4 2 3 11.36 19.15 1.64 o -2 2 3 3.76 5.47 0.93 o 0 2 3 12811.67 13691.89 86.99 o 2 2 3 5648.06 5990.63 44.50 o 4 2 3 687.09 695.92 9.06 o 6 2 3 195.04 191.96 4.98 o 8 2 3 17.45 16.86 2.45 o 10 2 3 332.63 322.30 8.70 o 12 2 3 37.67 26.24 4.06 o 14 2 3 6.04 5.03 5.72 o 16 2 3 330.51 319.87 15.18 o 18 2 3 0.18 11.76 8.91 o -21 3 3 314.35 348.05 20.87 o -19 3 3 91.95 92.81 10.10 o -17 3 3 2.05 2.48 5.18 o -15 3 3 221.13 273.56 12.13 o -13 3 3 0.04 -3.26 3.48 o -11 3 3 5.92 3.06 2.09 o -9 3 3 3.89 1.45 1.99 o -7 3 3 712.66 782.29 10.62 o -5 3 3 78.00 82.90 2.98 o -3 3 3 317.23 348.42 5.20 o -1 3 3 3575.77 3675.28 30.05 o 1 3 3 19.96 21.49 1.88 o 3 3 3 813.17 814.60 9.02 o 5 3 3 332.73 344.43 5.91 o 7 3 3 1701.90 1707.14 18.24 o 9 3 3 1987.47 1967.27 29.97 o 11 3 3 314.27 315.27 19.62 o 13 3 3 332.58 322.20 12.04 o 15 3 3 22.87 19.03 6.94 o 17 3 3 10.65 11.17 9.88 o -20 4 3 66.41 49.73 15.28 o -18 4 3 83.16 69.32 11.20 o -16 4 3 1.14 1.29 5.14 o -14 4 3 1.43 -5.49 4.13 o -12 4 3 1512.58 1506.22 26.05 o -10 4 3 58.80 58.44 3.76 o -8 4 3 542.39 541.79 8.10 o -6 4 3 173.27 172.26 4.20 o -4 4 3 1179.98 1168.90 11.48 o -2 4 3 1036.34 1050.09 11.21 o 0 4 3 102.46 126.43 4.02 o 2 4 3 3342.31 3460.00 29.17 o 4 4 3 720.22 753.62 9.44 o 6 4 3 10.85 13.65 2.14 o 8 4 3 4273.93 4314.25 48.67 o 10 4 3 554.50 515.41 30.30 o 12 4 3 330.65 337.73 24.32 o 14 4 3 179.36 189.92 13.38 o 16 4 3 38.85 28.31 10.64 o -19 5 3 163.77 139.29 13.85 o -17 5 3 21.95 18.88 7.60 o -15 5 3 382.55 316.91 14.20 o -13 5 3 21.34 12.07 4.92 o -11 5 3 69.83 76.19 6.59 o -9 5 3 119.83 112.50 6.55 o -7 5 3 189.13 188.02 5.71 o -5 5 3 1090.83 1095.43 25.11 o -3 5 3 195.56 199.88 8.71 o -1 5 3 1360.13 1401.99 15.33 o 1 5 3 713.89 655.64 8.77 o 3 5 3 307.24 309.87 7.48 o 5 5 3 134.40 123.33 15.03 o 7 5 3 141.54 131.36 8.60 o 9 5 3 13.95 3.06 4.51 o 11 5 3 234.42 240.07 13.37 o 13 5 3 1.91 -4.98 6.73 o 15 5 3 261.16 250.81 29.70 o -16 6 3 11.41 10.83 7.69 o -14 6 3 10.44 15.51 5.93 o -12 6 3 46.46 59.94 6.76 o -10 6 3 3.37 10.46 4.18 o -8 6 3 283.28 286.38 9.20 o -6 6 3 524.71 521.68 26.47 o -4 6 3 29.72 16.87 6.37 o -2 6 3 241.39 259.01 14.11 o 0 6 3 588.87 589.16 11.57 o 2 6 3 18.12 19.98 3.49 o 4 6 3 136.15 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