#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:32:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181250 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/28/2232897.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232897_Fobs loop_ _publ_author_name 'Al-Mohammed, Nassir N.' 'Alias, Yatimah' 'Abdullah, Zanariah' 'Khaledi, Hamid' _publ_section_title ; 1,1'-{[1,4-Phenylenebis(methylene)]bis(oxy)bis(4,1-phenylene)}diethanone ; _journal_coeditor_code PV2469 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3164 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 116.164 _cell_angle_beta 106.328 _cell_angle_gamma 100.196 _cell_length_a 8.1286 _cell_length_b 8.1610 _cell_length_c 8.4878 _exptl_crystal_F_000 198.00 _reflns_d_resolution_high 0.8257 _cod_data_source_file pv2469Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 103.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 77.10 74.04 2.47 o 2 0 0 6.77 10.78 0.62 o 3 0 0 1484.04 1544.26 48.95 o 4 0 0 7.11 7.59 0.53 o 5 0 0 120.80 125.24 3.31 o 6 0 0 1.29 1.20 0.66 o 7 0 0 0.40 0.64 0.34 o 8 0 0 0.06 -0.27 0.44 o -9 1 0 45.83 51.33 2.92 o -8 1 0 19.43 19.44 1.50 o -7 1 0 0.10 0.04 0.25 o -6 1 0 99.83 112.01 3.09 o -5 1 0 7.49 8.79 0.71 o -4 1 0 25.30 28.49 0.97 o -3 1 0 277.37 287.75 5.28 o -2 1 0 960.28 857.77 15.09 o -1 1 0 110.20 93.01 1.70 o 0 1 0 42.64 36.84 1.24 o 1 1 0 267.03 266.85 5.85 o 2 1 0 76.86 72.10 2.65 o 3 1 0 39.49 29.95 1.41 o 4 1 0 25.64 32.69 1.68 o 5 1 0 50.58 51.41 1.72 o 6 1 0 0.16 0.22 0.23 o 7 1 0 0.06 0.09 0.29 o 8 1 0 60.00 65.82 3.53 o -9 2 0 1.31 0.44 0.53 o -8 2 0 3.59 4.24 0.80 o -7 2 0 13.58 11.76 0.84 o -6 2 0 102.84 102.15 3.84 o -5 2 0 43.18 41.42 1.34 o -4 2 0 90.48 89.65 2.28 o -3 2 0 13.45 10.04 0.37 o -2 2 0 40.96 46.89 0.97 o -1 2 0 258.28 230.77 5.06 o 0 2 0 170.01 183.60 6.18 o 1 2 0 227.53 221.07 7.33 o 2 2 0 425.03 433.52 9.52 o 3 2 0 84.49 90.03 3.53 o 6 2 0 165.22 172.93 4.68 o 7 2 0 53.43 49.95 1.93 o -9 3 0 8.68 9.10 1.15 o -8 3 0 4.94 5.12 0.88 o -7 3 0 6.21 7.74 0.84 o -6 3 0 0.22 0.00 0.15 o -5 3 0 1.39 1.19 0.28 o -4 3 0 152.05 156.51 3.03 o -3 3 0 85.86 91.76 1.82 o -2 3 0 189.06 202.72 3.72 o -1 3 0 67.65 64.85 2.30 o 0 3 0 7.31 5.29 0.40 o 1 3 0 678.88 753.71 16.41 o 2 3 0 19.80 22.35 0.78 o 3 3 0 38.09 39.41 1.25 o 4 3 0 629.92 635.44 14.02 o 5 3 0 7.79 9.98 1.15 o 6 3 0 26.69 24.57 1.50 o 7 3 0 1.64 2.01 0.53 o -9 4 0 1.42 2.74 0.71 o -8 4 0 222.71 241.38 8.66 o -7 4 0 53.75 50.68 1.39 o -6 4 0 60.31 60.12 1.84 o -5 4 0 220.44 242.93 5.93 o -4 4 0 22.46 23.31 0.69 o -3 4 0 3.28 4.04 0.27 o -2 4 0 1.75 1.33 0.21 o -1 4 0 2.31 4.59 0.53 o 0 4 0 0.65 0.68 0.21 o 1 4 0 2.34 1.98 0.29 o 2 4 0 77.63 73.23 2.04 o 3 4 0 114.02 114.58 2.93 o 4 4 0 0.87 0.71 0.53 o 5 4 0 8.03 8.39 1.24 o 6 4 0 5.21 4.83 0.69 o -7 5 0 52.63 49.57 2.47 o -6 5 0 9.75 11.33 0.75 o -5 5 0 13.11 15.16 0.63 o -4 5 0 40.95 40.07 0.99 o -3 5 0 122.00 117.14 2.87 o -2 5 0 79.29 82.43 3.09 o -1 5 0 28.92 31.90 1.50 o 0 5 0 16.48 14.68 0.74 o 1 5 0 11.34 12.27 0.75 o 2 5 0 56.00 68.76 2.02 o 3 5 0 213.52 183.60 7.07 o 4 5 0 7.29 7.33 1.15 o 5 5 0 46.51 54.08 2.12 o -8 6 0 33.23 34.72 2.12 o -7 6 0 6.56 6.63 0.97 o -6 6 0 3.96 3.18 0.71 o -5 6 0 14.96 12.55 1.33 o -4 6 0 152.56 160.27 5.65 o -3 6 0 181.54 202.60 6.80 o -2 6 0 5.68 5.57 0.80 o -1 6 0 314.86 327.53 10.34 o 0 6 0 69.28 66.88 2.65 o 1 6 0 73.61 69.80 2.92 o 2 6 0 51.98 47.36 2.74 o 3 6 0 0.38 -0.09 0.53 o 4 6 0 4.52 4.95 1.06 o -8 7 0 10.09 9.54 1.33 o -7 7 0 128.59 129.97 5.21 o -6 7 0 19.28 22.53 1.68 o -5 7 0 19.05 19.17 1.68 o -4 7 0 385.50 409.43 13.08 o -3 7 0 204.14 205.78 7.07 o -2 7 0 0.77 0.80 0.44 o -1 7 0 21.93 22.18 1.41 o 0 7 0 7.93 7.25 0.88 o 1 7 0 1.66 2.12 0.80 o 2 7 0 21.79 24.56 2.03 o -6 8 0 2.50 2.83 0.80 o -5 8 0 18.53 17.41 1.68 o -4 8 0 0.40 0.62 0.44 o -3 8 0 4.55 3.71 0.80 o -2 8 0 38.89 37.64 2.03 o -1 8 0 12.96 12.72 1.33 o 2 -9 1 37.14 40.82 2.21 o 3 -9 1 0.02 -0.18 0.44 o 4 -9 1 1.82 2.30 0.71 o 5 -9 1 26.94 28.98 2.03 o -1 -8 1 4.19 0.97 0.62 o 1 -8 1 9.36 12.10 1.24 o 2 -8 1 0.02 0.00 0.35 o 3 -8 1 9.45 9.98 1.15 o 4 -8 1 24.77 26.59 1.77 o 5 -8 1 3.98 4.77 0.97 o 6 -8 1 11.10 9.63 1.33 o 7 -8 1 33.84 37.29 2.39 o -3 -7 1 0.01 0.00 0.62 o -2 -7 1 1.15 0.44 0.53 o -1 -7 1 8.80 5.12 0.97 o 0 -7 1 21.71 20.58 1.50 o 1 -7 1 17.38 18.29 1.24 o 2 -7 1 577.83 584.73 17.94 o 3 -7 1 21.62 26.51 1.59 o 4 -7 1 32.67 32.16 1.86 o 5 -7 1 116.58 114.42 4.51 o 6 -7 1 5.34 5.57 0.97 o 7 -7 1 8.10 8.31 1.24 o -5 -6 1 0.18 0.09 0.53 o -4 -6 1 17.91 21.56 2.03 o -3 -6 1 13.70 10.69 1.41 o -2 -6 1 398.84 390.79 13.69 o -1 -6 1 212.90 227.86 5.51 o 0 -6 1 305.86 305.91 7.25 o 1 -6 1 726.95 748.98 22.44 o 2 -6 1 1.80 1.81 0.88 o 3 -6 1 51.56 54.20 1.31 o 4 -6 1 0.51 0.79 0.21 o 5 -6 1 1.23 1.25 0.25 o 6 -6 1 8.66 9.63 1.15 o -6 -5 1 28.02 31.54 2.30 o -5 -5 1 0.13 -0.18 0.44 o -4 -5 1 11.84 9.19 1.24 o -3 -5 1 11.82 11.93 1.33 o -2 -5 1 26.17 29.34 1.03 o -1 -5 1 0.03 0.21 0.21 o 0 -5 1 17.82 16.73 0.76 o 1 -5 1 0.19 0.27 0.19 o 2 -5 1 15.44 13.85 0.65 o 3 -5 1 27.56 25.68 0.74 o 4 -5 1 9.52 9.80 0.56 o 5 -5 1 0.54 0.56 0.20 o 6 -5 1 59.38 57.34 1.49 o 7 -5 1 65.49 68.39 3.09 o 8 -5 1 11.58 10.34 1.24 o -6 -4 1 4.56 3.98 0.88 o -5 -4 1 0.00 -0.27 0.35 o -4 -4 1 25.66 14.58 1.41 o -3 -4 1 1.07 1.72 0.24 o -2 -4 1 258.81 254.88 5.82 o -1 -4 1 28.32 27.39 0.91 o 0 -4 1 25.88 28.16 0.95 o 1 -4 1 43.47 41.16 1.24 o 2 -4 1 62.06 63.08 1.38 o 3 -4 1 740.97 811.94 18.02 o 4 -4 1 78.49 85.20 1.85 o 5 -4 1 6.61 7.70 0.47 o 6 -4 1 552.93 551.15 18.11 o 7 -4 1 58.48 53.90 2.65 o 8 -4 1 47.25 46.47 2.47 o 9 -4 1 13.36 14.58 1.59 o -7 -3 1 0.00 -0.13 0.34 o -6 -3 1 18.01 19.53 1.50 o -3 -3 1 93.70 108.13 2.61 o -2 -3 1 558.76 620.78 13.53 o -1 -3 1 503.54 532.67 11.61 o 0 -3 1 100.57 112.39 2.64 o 1 -3 1 3.68 3.76 0.26 o 2 -3 1 889.50 889.71 15.71 o 3 -3 1 530.54 526.45 9.46 o 4 -3 1 35.05 34.04 1.12 o 5 -3 1 31.98 28.69 0.86 o 6 -3 1 36.22 33.38 1.22 o 7 -3 1 0.67 0.09 0.35 o 8 -3 1 75.94 72.63 3.45 o 9 -3 1 0.48 0.80 0.62 o -8 -2 1 7.65 8.48 0.89 o -7 -2 1 480.80 504.41 17.23 o -6 -2 1 14.98 19.00 1.41 o -5 -2 1 62.75 65.12 2.92 o -4 -2 1 142.30 142.16 5.30 o -3 -2 1 37.45 41.61 1.94 o -2 -2 1 28.99 22.12 0.65 o -1 -2 1 918.40 923.35 19.88 o 0 -2 1 258.27 260.43 5.70 o 1 -2 1 326.48 326.44 5.84 o 2 -2 1 1476.48 1384.91 24.34 o 3 -2 1 1.89 1.04 0.21 o 4 -2 1 3.77 2.51 0.28 o 5 -2 1 7.07 7.99 0.51 o 6 -2 1 11.12 12.87 0.97 o 7 -2 1 15.85 17.58 1.33 o 8 -2 1 38.32 37.82 2.21 o -8 -1 1 39.13 39.83 1.72 o -7 -1 1 61.22 62.74 2.15 o -6 -1 1 3.48 3.45 0.71 o -5 -1 1 3.74 4.24 0.71 o -4 -1 1 216.90 240.85 8.31 o -3 -1 1 317.57 330.80 10.96 o -2 -1 1 156.51 142.96 4.86 o -1 -1 1 126.21 122.02 4.06 o 0 -1 1 0.13 -0.04 0.06 o 1 -1 1 5506.49 4484.00 98.69 o 2 -1 1 438.73 429.09 7.87 o 3 -1 1 441.66 441.25 12.45 o 4 -1 1 1098.29 1214.13 27.27 o 5 -1 1 1.13 1.20 0.28 o 6 -1 1 1.75 2.25 0.80 o 7 -1 1 48.40 44.44 2.47 o 8 -1 1 1.20 1.06 0.53 o -9 0 1 6.37 5.65 1.06 o -8 0 1 6.36 6.62 0.72 o -7 0 1 0.78 0.88 0.49 o -6 0 1 56.69 58.85 2.12 o -5 0 1 294.24 307.74 10.43 o -4 0 1 3.07 3.53 0.53 o -3 0 1 20.91 20.57 0.68 o -2 0 1 3305.53 2972.31 64.25 o -1 0 1 347.19 301.82 9.28 o 0 0 1 174.82 150.99 3.40 o 1 0 1 180.84 149.69 2.82 o 2 0 1 119.31 145.15 10.51 o 3 0 1 11.67 13.95 0.59 o 4 0 1 50.74 42.76 1.86 o 5 0 1 4.27 4.72 0.49 o 6 0 1 5.45 6.22 0.75 o 7 0 1 1.78 1.33 0.62 o 8 0 1 0.82 0.27 0.53 o -9 1 1 24.68 26.27 1.41 o -8 1 1 1.86 3.40 0.50 o -7 1 1 30.74 35.55 1.40 o -6 1 1 303.38 306.59 7.40 o -5 1 1 160.52 160.42 3.19 o -4 1 1 7.95 6.31 0.36 o -3 1 1 1121.42 1051.15 30.75 o -2 1 1 921.04 780.43 22.88 o -1 1 1 19.09 17.05 0.80 o 0 1 1 0.19 -0.22 0.22 o 1 1 1 147.83 143.59 3.44 o 2 1 1 101.77 95.71 5.26 o 3 1 1 27.78 25.42 0.97 o 4 1 1 13.31 13.77 1.06 o 5 1 1 109.54 109.80 5.17 o 6 1 1 85.85 91.65 4.46 o 7 1 1 30.42 28.54 2.03 o -9 2 1 4.04 3.50 0.56 o -8 2 1 0.59 0.40 0.31 o -7 2 1 19.44 17.48 0.90 o -6 2 1 6.03 5.05 0.67 o -5 2 1 1.53 0.81 0.22 o -4 2 1 90.07 94.36 2.34 o -3 2 1 41.67 35.61 0.99 o -2 2 1 80.95 72.62 1.71 o -1 2 1 356.44 344.94 10.43 o 0 2 1 85.22 82.49 2.09 o 1 2 1 123.24 148.79 3.48 o 2 2 1 392.55 411.83 9.15 o 3 2 1 16.93 17.01 0.61 o 4 2 1 3.31 4.42 0.50 o 5 2 1 877.82 935.43 54.91 o 6 2 1 6.49 6.50 0.72 o 7 2 1 1.23 0.88 0.71 o -9 3 1 0.14 0.22 0.34 o -8 3 1 9.19 8.65 0.72 o -7 3 1 29.98 28.67 0.95 o -6 3 1 1.04 1.14 0.28 o -5 3 1 73.86 67.28 1.84 o -4 3 1 356.65 380.16 8.43 o -3 3 1 15.53 13.03 0.84 o -2 3 1 7.99 4.72 0.35 o -1 3 1 1519.85 1792.71 52.39 o 0 3 1 110.85 115.03 5.52 o 1 3 1 30.44 33.80 1.14 o 2 3 1 357.96 349.41 7.93 o 3 3 1 0.88 1.29 0.24 o 4 3 1 45.65 43.37 1.23 o 5 3 1 5.81 5.08 0.62 o 6 3 1 2.30 1.59 0.50 o -9 4 1 50.78 53.90 2.83 o -8 4 1 272.15 274.28 8.53 o -7 4 1 49.39 47.36 2.30 o -6 4 1 95.29 102.55 2.75 o -5 4 1 271.49 279.52 6.40 o -4 4 1 35.57 37.69 1.10 o -3 4 1 0.25 0.18 0.08 o -2 4 1 23.41 21.38 1.24 o -1 4 1 86.04 104.26 3.71 o 0 4 1 141.41 148.61 4.95 o 1 4 1 108.63 107.61 2.86 o 2 4 1 16.91 14.52 0.78 o 3 4 1 60.09 63.02 1.60 o 4 4 1 8.08 9.68 0.87 o 5 4 1 35.44 38.93 1.69 o -9 5 1 0.55 0.53 0.37 o -8 5 1 4.14 5.39 0.97 o -7 5 1 3.34 2.12 0.62 o -6 5 1 0.10 -0.27 0.27 o -5 5 1 42.59 41.35 2.12 o -4 5 1 0.38 0.27 0.35 o -3 5 1 65.50 64.85 2.74 o -2 5 1 96.57 92.15 3.45 o -1 5 1 8.62 9.54 0.97 o 0 5 1 39.71 37.90 1.77 o 1 5 1 78.55 66.16 2.04 o 2 5 1 3.90 5.56 1.19 o 3 5 1 0.85 0.47 0.34 o 4 5 1 13.11 17.58 1.24 o -8 6 1 10.75 14.14 1.50 o -7 6 1 0.01 0.44 0.44 o -6 6 1 10.03 9.19 1.15 o -5 6 1 0.78 1.33 0.53 o -4 6 1 45.88 42.68 2.21 o -3 6 1 646.41 635.62 19.44 o -2 6 1 40.77 44.62 2.12 o -1 6 1 9.56 9.98 0.97 o 0 6 1 232.05 204.72 6.89 o 1 6 1 29.52 25.98 1.50 o 2 6 1 0.85 0.80 0.62 o 3 6 1 11.40 15.62 1.33 o -7 7 1 44.37 47.80 2.65 o -6 7 1 52.16 49.57 2.65 o -5 7 1 6.11 6.27 0.97 o -4 7 1 211.56 215.05 7.51 o -3 7 1 16.26 15.55 1.41 o -2 7 1 9.01 7.51 0.97 o -1 7 1 13.27 11.22 1.15 o 0 7 1 1.33 2.56 0.62 o -6 8 1 18.88 16.61 1.77 o -5 8 1 13.76 15.46 1.59 o -4 8 1 3.27 4.33 0.88 o -3 8 1 1.02 1.59 0.62 o -2 8 1 2.40 2.12 0.62 o -1 8 1 0.35 0.35 0.44 o 2 -9 2 82.48 83.67 3.53 o 3 -9 2 1.49 1.86 0.62 o 4 -9 2 6.38 5.30 0.97 o 5 -9 2 11.79 12.28 1.50 o -2 -8 2 0.83 0.35 0.62 o -1 -8 2 3.97 3.80 0.97 o 0 -8 2 123.03 131.65 5.65 o 1 -8 2 7.78 9.81 1.06 o 2 -8 2 8.81 9.90 1.06 o 3 -8 2 34.33 31.37 1.86 o 4 -8 2 0.09 0.18 0.35 o 5 -8 2 0.02 -0.09 0.44 o 6 -8 2 71.56 57.34 3.00 o -4 -7 2 64.76 73.86 3.89 o -3 -7 2 1.35 1.59 0.71 o -2 -7 2 0.89 1.50 0.62 o -1 -7 2 159.09 166.02 6.63 o 0 -7 2 182.29 206.36 5.08 o 1 -7 2 436.04 472.17 14.49 o 2 -7 2 466.37 500.44 11.15 o 3 -7 2 6.12 6.10 0.47 o 4 -7 2 133.15 126.21 2.97 o 5 -7 2 101.08 94.89 2.75 o -5 -6 2 13.09 12.46 1.59 o -4 -6 2 101.73 92.86 4.33 o -3 -6 2 0.10 -0.27 0.35 o -2 -6 2 53.57 63.17 3.09 o -1 -6 2 125.38 138.30 4.46 o 0 -6 2 0.65 0.44 0.35 o 1 -6 2 0.22 0.34 0.21 o 2 -6 2 44.53 48.72 1.24 o 3 -6 2 0.04 0.02 0.17 o 4 -6 2 22.68 19.91 0.83 o 5 -6 2 16.30 16.50 0.84 o 6 -6 2 32.55 34.03 1.86 o 7 -6 2 0.03 -0.10 0.49 o 8 -6 2 12.03 10.87 1.33 o -6 -5 2 10.60 10.96 1.50 o -5 -5 2 81.11 68.30 3.45 o -4 -5 2 3.17 1.24 0.53 o -3 -5 2 23.74 24.47 1.68 o -2 -5 2 0.13 0.14 0.27 o -1 -5 2 0.08 0.09 0.15 o 0 -5 2 1.65 2.74 0.57 o 1 -5 2 79.21 66.47 1.84 o 2 -5 2 107.61 111.45 2.74 o 3 -5 2 16.05 18.25 0.84 o 4 -5 2 22.65 26.35 1.86 o 5 -5 2 66.77 65.86 2.03 o 6 -5 2 63.28 68.68 2.15 o 7 -5 2 530.13 549.56 18.38 o 8 -5 2 30.62 28.19 1.94 o -7 -4 2 18.74 18.64 1.94 o -6 -4 2 14.63 14.40 1.59 o -5 -4 2 8.04 8.31 1.15 o -4 -4 2 2.59 3.00 0.71 o -3 -4 2 0.03 0.35 0.35 o -2 -4 2 26.84 36.70 1.03 o -1 -4 2 138.57 163.50 3.81 o 0 -4 2 138.53 138.66 3.30 o 1 -4 2 337.30 355.87 6.57 o 2 -4 2 126.37 124.33 2.54 o 3 -4 2 666.29 701.13 18.02 o 4 -4 2 540.68 538.08 17.54 o 5 -4 2 161.50 164.28 8.39 o 6 -4 2 199.07 203.19 5.12 o 7 -4 2 34.38 32.60 2.03 o 8 -4 2 11.68 12.19 1.41 o -8 -3 2 31.36 32.87 2.30 o -7 -3 2 3.89 4.68 0.97 o -6 -3 2 350.33 327.09 11.57 o -5 -3 2 16.04 11.84 1.24 o -4 -3 2 110.33 140.22 5.30 o -3 -3 2 220.21 243.77 8.48 o -1 -3 2 1.32 2.12 0.35 o 0 -3 2 226.56 221.54 5.22 o 1 -3 2 29.04 26.01 0.70 o 2 -3 2 49.23 54.67 1.53 o 3 -3 2 261.73 269.77 6.31 o 4 -3 2 9.21 9.59 0.46 o 5 -3 2 6.27 5.83 0.71 o 6 -3 2 23.28 23.94 1.59 o 7 -3 2 6.05 5.04 0.88 o 8 -3 2 3.33 3.80 0.88 o -8 -2 2 129.82 138.94 4.12 o -7 -2 2 143.74 150.91 6.10 o -6 -2 2 3.78 3.00 0.71 o -5 -2 2 26.04 26.42 1.59 o -4 -2 2 238.17 289.89 9.98 o -3 -2 2 0.20 0.80 0.35 o -2 -2 2 321.65 323.02 10.69 o -1 -2 2 307.60 293.95 9.63 o 0 -2 2 322.43 279.36 19.39 o 1 -2 2 1001.10 989.13 17.95 o 2 -2 2 47.56 42.54 1.25 o 3 -2 2 84.25 81.65 1.72 o 4 -2 2 49.09 49.78 1.21 o 5 -2 2 0.01 0.85 0.21 o 6 -2 2 15.37 14.84 1.24 o 7 -2 2 0.68 0.00 0.35 o 8 -2 2 70.34 60.35 3.18 o -9 -1 2 20.71 22.44 1.40 o -8 -1 2 1.01 1.30 0.49 o -7 -1 2 18.73 18.82 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