#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:33:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181251 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232908.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232908_Fobs loop_ _publ_author_name 'Cheng, Xiao-Chun' _publ_section_title ; Tetraaquabis{5-[4-(imidazol-1-yl-\kN^3^)phenyl]tetrazolido}manganese(II) ; _journal_coeditor_code PV2481 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1757 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 80.758 _cell_angle_beta 75.880 _cell_angle_gamma 88.791 _cell_length_a 8.4150 _cell_length_b 8.4580 _cell_length_c 8.7220 _exptl_crystal_F_000 283.00 _reflns_d_resolution_high 0.8225 _cod_data_source_file pv2481Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 709.55 681.20 10.83 o 2 0 0 577.92 603.52 14.16 o 3 0 0 203.17 207.60 5.57 o 4 0 0 2799.33 2891.79 65.55 o 5 0 0 190.57 181.95 5.49 o 6 0 0 97.93 99.49 3.82 o 7 0 0 133.18 117.19 4.44 o 8 0 0 49.55 42.35 2.59 o 9 0 0 7.89 7.57 1.50 o -9 1 0 10.07 9.81 1.64 o -8 1 0 71.50 75.28 3.60 o -7 1 0 0.56 0.58 0.53 o -6 1 0 21.66 17.64 1.51 o -5 1 0 34.50 29.95 1.61 o -4 1 0 1275.60 1236.06 22.28 o -3 1 0 823.36 827.80 18.23 o -2 1 0 0.49 0.67 0.13 o -1 1 0 2.76 1.14 0.15 o 0 1 0 717.30 784.04 18.16 o 1 1 0 123.55 122.65 3.02 o 2 1 0 38.58 39.83 1.40 o 3 1 0 2519.76 2764.17 62.41 o 4 1 0 785.71 813.74 19.39 o 5 1 0 167.16 166.12 5.12 o 6 1 0 133.07 128.19 3.07 o 7 1 0 42.19 48.56 2.66 o 8 1 0 150.58 143.28 5.30 o 9 1 0 113.08 114.12 4.98 o -9 2 0 105.08 107.46 4.87 o -8 2 0 337.77 333.30 10.01 o -7 2 0 59.76 62.35 2.11 o -6 2 0 38.43 38.46 1.50 o -5 2 0 33.88 23.89 1.79 o -4 2 0 300.26 279.67 5.24 o -3 2 0 529.48 513.75 11.72 o -2 2 0 427.77 415.37 5.68 o -1 2 0 54.73 42.36 0.79 o 0 2 0 2137.09 2133.26 48.78 o 1 2 0 3518.01 3472.07 55.63 o 2 2 0 200.24 176.83 3.30 o 3 2 0 1036.25 1064.01 19.74 o 4 2 0 241.29 223.90 4.39 o 5 2 0 881.96 945.41 16.06 o 6 2 0 217.99 215.40 4.59 o 7 2 0 71.37 68.38 2.17 o 8 2 0 159.78 137.57 5.13 o 9 2 0 29.99 33.47 2.52 o -9 3 0 1.39 1.60 0.84 o -8 3 0 97.76 99.69 3.05 o -7 3 0 200.70 190.25 6.79 o -6 3 0 468.68 476.68 8.78 o -5 3 0 333.40 324.90 6.16 o -4 3 0 346.11 368.21 15.14 o -3 3 0 114.99 107.54 1.85 o -1 3 0 734.04 707.29 9.42 o 0 3 0 679.41 675.79 16.08 o 1 3 0 1110.95 1082.87 35.09 o 2 3 0 59.02 51.04 1.30 o 3 3 0 350.04 325.73 5.94 o 4 3 0 34.64 33.18 1.22 o 5 3 0 30.22 25.81 1.15 o 6 3 0 105.28 109.69 2.87 o 7 3 0 38.23 37.52 1.58 o 8 3 0 13.93 10.02 1.07 o 9 3 0 34.16 32.32 2.52 o -9 4 0 21.86 21.04 1.55 o -8 4 0 64.35 67.84 2.45 o -7 4 0 96.58 103.81 2.99 o -6 4 0 4.23 4.43 0.67 o -5 4 0 199.75 204.52 4.35 o -4 4 0 50.27 41.61 1.94 o -3 4 0 704.57 749.31 11.03 o -2 4 0 378.00 373.51 5.39 o -1 4 0 653.26 619.80 10.27 o 0 4 0 650.61 667.39 16.18 o 1 4 0 703.69 714.94 17.38 o 2 4 0 357.81 372.42 26.38 o 3 4 0 1036.05 1102.24 18.35 o 4 4 0 194.11 198.36 4.12 o 5 4 0 128.74 125.64 3.28 o 6 4 0 325.52 314.44 6.33 o 7 4 0 264.50 254.23 6.38 o 8 4 0 7.72 5.43 1.02 o 9 4 0 35.81 32.86 2.57 o -8 5 0 37.03 34.53 1.74 o -7 5 0 2.46 1.70 0.54 o -6 5 0 226.67 226.43 7.19 o -5 5 0 219.64 227.76 5.95 o -4 5 0 3.29 4.47 0.43 o -3 5 0 87.86 82.92 1.66 o -2 5 0 51.04 57.79 1.66 o -1 5 0 184.28 168.12 4.92 o 0 5 0 2.50 1.26 0.48 o 1 5 0 10.57 9.77 1.03 o 2 5 0 712.13 734.12 18.27 o 3 5 0 796.38 770.66 19.28 o 4 5 0 124.62 142.98 5.10 o 5 5 0 15.27 21.36 1.15 o 6 5 0 135.39 147.88 5.67 o 7 5 0 100.03 105.45 4.72 o 8 5 0 3.65 4.36 1.25 o -8 6 0 28.71 32.60 2.68 o -7 6 0 76.37 74.96 3.75 o -6 6 0 50.46 53.75 3.02 o -5 6 0 84.35 85.29 3.70 o -4 6 0 8.71 6.99 1.10 o -3 6 0 10.41 11.13 0.80 o -2 6 0 391.94 401.07 7.46 o -1 6 0 221.18 228.02 6.56 o 0 6 0 51.93 48.76 2.34 o 1 6 0 140.54 139.65 4.73 o 2 6 0 4.79 5.40 0.98 o 3 6 0 58.51 54.90 2.76 o 4 6 0 0.94 -0.34 0.46 o 5 6 0 217.76 226.00 7.48 o 6 6 0 73.01 69.01 3.59 o 7 6 0 68.72 74.56 3.94 o -7 7 0 28.18 32.42 2.58 o -6 7 0 33.07 37.32 2.61 o -5 7 0 59.18 64.04 3.33 o -4 7 0 34.48 31.98 2.27 o -3 7 0 18.11 15.11 1.54 o -2 7 0 36.88 35.23 1.51 o -1 7 0 3.41 4.18 0.62 o 0 7 0 12.32 11.37 1.25 o 1 7 0 72.13 72.38 3.25 o 2 7 0 39.64 37.58 2.29 o 3 7 0 78.25 71.31 3.40 o 4 7 0 39.00 44.03 2.70 o 5 7 0 0.15 0.76 0.72 o 6 7 0 0.12 1.87 0.94 o 7 7 0 39.90 35.83 2.87 o -6 8 0 17.45 20.32 2.20 o -5 8 0 3.10 3.41 1.12 o -4 8 0 6.80 5.20 1.26 o -3 8 0 67.82 70.46 3.47 o -2 8 0 345.46 347.60 7.02 o -1 8 0 54.17 50.17 1.93 o 0 8 0 24.22 26.38 1.90 o 1 8 0 73.91 75.70 3.54 o 2 8 0 132.81 124.48 4.96 o 3 8 0 56.28 56.27 3.21 o 4 8 0 71.43 64.65 3.58 o 5 8 0 1.54 2.88 1.10 o -4 9 0 0.67 1.09 0.99 o -3 9 0 0.97 1.09 0.91 o -2 9 0 2.16 3.53 1.14 o -1 9 0 21.56 20.69 1.40 o 0 9 0 1.05 0.87 0.78 o 1 9 0 6.42 4.85 1.18 o 2 9 0 4.46 2.02 0.97 o 3 9 0 0.08 -0.28 0.63 o 4 9 0 15.31 16.34 2.13 o -1 10 0 29.19 26.36 1.69 o 0 10 0 0.62 0.58 0.90 o 1 10 0 2.76 2.01 1.07 o -3 -9 1 6.24 5.28 1.42 o -2 -9 1 44.55 43.95 2.94 o -1 -9 1 14.18 10.08 1.57 o 0 -9 1 24.43 20.38 1.88 o 1 -9 1 28.78 23.62 1.44 o 2 -9 1 29.75 31.45 2.44 o 3 -9 1 1.11 0.92 0.96 o 4 -9 1 52.17 53.13 3.38 o -5 -8 1 32.02 39.63 3.02 o -4 -8 1 33.00 32.03 2.60 o -3 -8 1 26.40 29.68 2.37 o -2 -8 1 51.90 49.78 2.91 o -1 -8 1 11.00 12.62 1.55 o 0 -8 1 77.11 77.67 3.53 o 1 -8 1 371.94 323.56 15.30 o 2 -8 1 101.10 102.17 4.40 o 3 -8 1 0.17 1.31 0.86 o 4 -8 1 16.05 13.87 1.81 o 5 -8 1 33.41 30.09 2.51 o 6 -8 1 10.70 10.22 1.76 o -6 -7 1 36.69 36.07 2.79 o -5 -7 1 40.86 39.44 2.83 o -4 -7 1 62.44 59.90 3.32 o -3 -7 1 89.46 86.99 3.96 o -2 -7 1 342.74 324.37 9.54 o -1 -7 1 104.17 98.99 3.95 o 0 -7 1 59.91 62.37 2.90 o 1 -7 1 149.94 142.42 4.81 o 2 -7 1 51.08 45.00 1.69 o 3 -7 1 68.25 68.27 3.29 o 4 -7 1 183.31 177.97 6.15 o 5 -7 1 131.14 138.21 5.33 o 6 -7 1 1.30 3.80 1.15 o 7 -7 1 0.15 -0.96 0.64 o -7 -6 1 19.54 25.19 2.60 o -6 -6 1 175.45 199.76 7.48 o -5 -6 1 27.81 24.32 2.28 o -4 -6 1 43.12 50.40 2.99 o -3 -6 1 0.38 0.45 0.56 o -2 -6 1 211.11 223.94 6.95 o -1 -6 1 13.40 14.56 1.37 o 0 -6 1 73.95 78.70 3.13 o 1 -6 1 359.14 382.85 10.18 o 2 -6 1 229.69 240.67 4.90 o 3 -6 1 0.83 0.86 0.35 o 4 -6 1 136.62 134.97 4.89 o 5 -6 1 244.84 248.10 7.69 o 6 -6 1 339.39 319.13 9.50 o 7 -6 1 39.72 35.53 2.54 o 8 -6 1 15.01 12.71 1.93 o -8 -5 1 38.90 41.61 3.04 o -7 -5 1 13.07 10.87 1.70 o -6 -5 1 0.68 0.73 0.65 o -5 -5 1 149.97 146.14 5.47 o -4 -5 1 496.89 506.69 13.71 o -3 -5 1 190.26 188.49 6.10 o -2 -5 1 79.91 72.95 3.11 o -1 -5 1 89.22 81.70 3.18 o 0 -5 1 105.27 102.06 3.51 o 1 -5 1 409.24 387.89 10.01 o 2 -5 1 948.15 963.39 16.07 o 3 -5 1 46.43 51.23 1.20 o 4 -5 1 22.02 23.14 1.06 o 5 -5 1 24.12 26.75 1.24 o 6 -5 1 56.94 57.87 2.01 o 7 -5 1 39.21 37.60 1.90 o 8 -5 1 0.20 0.33 0.61 o -8 -4 1 34.49 33.06 1.74 o -7 -4 1 116.98 122.58 3.67 o -6 -4 1 40.33 38.01 1.65 o -5 -4 1 106.48 116.69 4.67 o -4 -4 1 64.88 76.64 2.15 o -3 -4 1 621.08 665.98 11.53 o -2 -4 1 604.47 630.40 10.79 o -1 -4 1 1446.51 1586.14 25.79 o 0 -4 1 151.41 143.71 2.75 o 1 -4 1 676.23 668.45 11.09 o 2 -4 1 690.92 712.40 9.67 o 3 -4 1 31.67 41.34 1.12 o 4 -4 1 326.24 324.04 6.09 o 5 -4 1 312.56 311.83 6.04 o 6 -4 1 237.13 228.67 7.15 o 7 -4 1 38.50 35.15 1.57 o 8 -4 1 27.25 32.61 1.65 o 9 -4 1 37.65 45.38 2.09 o -9 -3 1 3.50 2.93 1.08 o -8 -3 1 25.37 27.28 1.59 o -7 -3 1 189.78 203.44 4.79 o -6 -3 1 20.53 24.44 1.31 o -5 -3 1 36.85 36.76 1.48 o -4 -3 1 354.27 361.21 6.77 o -3 -3 1 491.14 475.63 8.40 o -2 -3 1 185.32 172.80 3.39 o -1 -3 1 8.84 12.61 0.55 o 0 -3 1 1156.29 1185.91 19.26 o 1 -3 1 3006.16 3176.78 72.45 o 2 -3 1 341.50 322.66 5.34 o 3 -3 1 1665.44 1816.75 23.77 o 4 -3 1 766.27 821.07 11.12 o 5 -3 1 1402.54 1444.06 23.60 o 6 -3 1 116.46 117.00 2.98 o 7 -3 1 464.61 450.11 12.02 o 8 -3 1 51.45 52.02 2.08 o 9 -3 1 31.42 31.03 2.39 o -9 -2 1 5.97 2.62 1.14 o -8 -2 1 1.84 1.96 0.87 o -7 -2 1 171.57 170.34 5.44 o -6 -2 1 0.99 1.95 0.50 o -5 -2 1 60.85 71.99 2.95 o -4 -2 1 107.42 105.91 3.51 o -3 -2 1 1012.89 1035.11 24.03 o -2 -2 1 4.17 3.66 0.47 o -1 -2 1 292.41 301.97 7.25 o 0 -2 1 522.54 499.32 8.26 o 1 -2 1 3503.36 2938.10 143.70 o 2 -2 1 562.43 558.11 7.50 o 3 -2 1 210.62 207.97 3.07 o 4 -2 1 86.22 78.21 1.98 o 5 -2 1 733.37 767.04 13.01 o 6 -2 1 191.46 186.48 4.09 o 7 -2 1 701.89 694.10 12.35 o 8 -2 1 127.39 120.91 4.77 o 9 -2 1 19.66 21.84 2.10 o -9 -1 1 15.12 15.74 1.95 o -8 -1 1 0.38 -0.03 0.72 o -7 -1 1 479.68 474.21 12.98 o -6 -1 1 113.62 134.45 4.83 o -5 -1 1 9.44 9.25 1.07 o -4 -1 1 685.55 784.75 18.79 o -3 -1 1 753.18 805.32 18.93 o -2 -1 1 84.33 76.33 2.34 o -1 -1 1 9.35 7.20 0.49 o 0 -1 1 15.97 19.24 0.70 o 1 -1 1 196.89 217.46 2.99 o 2 -1 1 381.82 382.73 6.41 o 3 -1 1 391.22 403.59 6.91 o 4 -1 1 311.35 275.69 5.10 o 5 -1 1 377.71 372.55 6.82 o 6 -1 1 25.38 23.34 1.13 o 7 -1 1 4.00 5.70 1.08 o 8 -1 1 522.58 472.92 13.00 o 9 -1 1 52.68 47.63 2.90 o 10 -1 1 57.13 57.25 3.51 o -9 0 1 4.46 5.07 1.37 o -8 0 1 51.24 42.34 2.78 o -7 0 1 50.34 60.89 3.14 o -6 0 1 51.74 53.07 2.72 o -5 0 1 38.39 42.14 2.15 o -4 0 1 237.86 289.94 7.76 o -3 0 1 616.48 679.05 16.12 o -2 0 1 303.61 311.16 7.66 o -1 0 1 11178.97 9682.38 217.41 o 0 0 1 19.80 23.54 0.54 o 1 0 1 657.43 660.35 13.94 o 2 0 1 1703.46 1775.50 23.04 o 3 0 1 1695.08 1789.66 23.31 o 4 0 1 975.70 1034.84 21.12 o 5 0 1 619.16 661.89 11.30 o 6 0 1 232.40 259.14 7.49 o 7 0 1 74.73 89.18 3.69 o 8 0 1 178.64 165.48 5.83 o 9 0 1 7.71 7.70 1.40 o 10 0 1 1.89 3.01 1.14 o -9 1 1 25.35 22.49 2.20 o -8 1 1 8.98 10.07 1.58 o -7 1 1 1.52 4.25 1.00 o -6 1 1 72.05 75.88 3.41 o -5 1 1 131.45 122.43 4.23 o -4 1 1 321.70 318.03 8.39 o -3 1 1 271.27 283.70 5.08 o -2 1 1 372.47 377.66 5.21 o -1 1 1 142.36 152.40 2.19 o 0 1 1 770.43 765.75 15.11 o 1 1 1 1693.07 1607.42 25.79 o 2 1 1 1267.92 1361.81 21.99 o 3 1 1 511.77 541.37 9.14 o 4 1 1 217.85 217.00 4.14 o 5 1 1 37.20 41.93 1.32 o 6 1 1 145.46 144.15 3.24 o 7 1 1 194.47 194.72 6.26 o 8 1 1 396.79 349.32 10.13 o 9 1 1 5.84 6.29 1.33 o 10 1 1 12.84 13.42 1.90 o -8 2 1 61.08 56.17 3.21 o -7 2 1 15.77 14.98 1.61 o -6 2 1 0.84 0.76 0.40 o -5 2 1 5.06 4.96 0.80 o -4 2 1 219.24 216.90 3.43 o -3 2 1 207.56 257.70 5.03 o -2 2 1 60.57 60.06 1.14 o -1 2 1 60.57 59.66 1.94 o 0 2 1 5306.29 5137.73 82.58 o 1 2 1 9513.58 9113.55 179.68 o 2 2 1 433.62 449.65 7.60 o 3 2 1 900.88 970.46 21.11 o 4 2 1 2752.42 3133.21 50.45 o 5 2 1 32.47 32.41 1.21 o 6 2 1 205.49 208.24 4.38 o 7 2 1 352.21 332.69 6.57 o 8 2 1 140.17 136.85 5.08 o 9 2 1 45.17 45.47 2.86 o -7 3 1 121.60 122.75 5.98 o -6 3 1 92.96 96.09 2.69 o -5 3 1 49.00 49.68 2.14 o -4 3 1 343.55 356.85 5.31 o -3 3 1 29.60 30.57 0.82 o -2 3 1 13.69 13.67 0.55 o -1 3 1 725.37 673.75 9.01 o 0 3 1 1130.96 1128.60 18.36 o 1 3 1 401.00 394.15 6.69 o 2 3 1 2.13 2.69 0.68 o 3 3 1 542.14 516.61 8.90 o 4 3 1 20.88 15.35 1.54 o 5 3 1 2.64 2.53 0.52 o 6 3 1 3.15 6.37 0.72 o 7 3 1 4.33 8.34 1.06 o 8 3 1 97.85 98.25 4.10 o 9 3 1 17.04 11.47 1.61 o -8 4 1 38.15 33.38 2.41 o -7 4 1 3.28 2.88 0.65 o -6 4 1 17.40 19.23 1.67 o -5 4 1 145.73 149.76 2.75 o -4 4 1 611.32 626.85 8.82 o -3 4 1 114.38 114.00 2.54 o -2 4 1 6.06 6.50 0.39 o -1 4 1 195.41 180.95 3.54 o 0 4 1 1192.88 1160.16 27.29 o 2 4 1 0.90 1.33 0.26 o 3 4 1 194.92 191.65 5.64 o 4 4 1 123.62 125.73 2.85 o 5 4 1 233.21 235.55 5.68 o 6 4 1 56.87 50.34 1.77 o 7 4 1 71.88 71.69 2.29 o 8 4 1 121.92 113.00 3.19 o 9 4 1 1.66 3.39 1.07 o -8 5 1 42.25 49.85 3.41 o -7 5 1 50.11 42.92 1.86 o -6 5 1 422.87 435.30 8.27 o -5 5 1 8.03 10.70 1.31 o -4 5 1 27.92 26.79 1.12 o -3 5 1 27.38 25.41 1.57 o -2 5 1 17.53 16.93 0.61 o -1 5 1 1.91 1.77 0.36 o 0 5 1 77.81 71.70 2.73 o 1 5 1 330.76 363.37 9.70 o 2 5 1 55.74 61.43 2.65 o 3 5 1 264.88 268.58 5.07 o 4 5 1 26.75 30.19 1.17 o 5 5 1 116.52 125.86 3.06 o 6 5 1 34.06 34.60 1.50 o 7 5 1 19.64 22.20 1.98 o 8 5 1 20.33 17.52 1.89 o -7 6 1 18.03 18.91 2.02 o -6 6 1 9.81 8.17 1.41 o -5 6 1 22.29 22.99 1.83 o -4 6 1 5.56 6.31 1.07 o -3 6 1 200.54 213.84 4.46 o -2 6 1 33.01 32.81 1.27 o -1 6 1 84.18 82.10 2.34 o 0 6 1 37.69 41.95 2.13 o 1 6 1 17.71 18.66 1.46 o 2 6 1 0.50 0.72 0.52 o 3 6 1 80.37 81.06 3.46 o 4 6 1 68.27 72.36 3.31 o 5 6 1 41.14 39.22 2.41 o 6 6 1 32.14 38.00 2.52 o 7 6 1 8.57 6.97 1.37 o 8 6 1 6.16 6.71 1.39 o -7 7 1 16.44 17.21 2.04 o -6 7 1 47.92 52.37 3.11 o -5 7 1 364.87 390.74 11.06 o -4 7 1 11.34 12.44 1.50 o -3 7 1 28.25 30.12 1.72 o -2 7 1 13.18 11.82 0.91 o -1 7 1 125.51 121.99 3.09 o 0 7 1 11.79 12.26 1.30 o 1 7 1 10.03 13.21 1.37 o 2 7 1 58.27 62.55 3.05 o 3 7 1 0.17 0.35 0.57 o 4 7 1 46.67 46.35 2.76 o 5 7 1 2.67 3.91 1.04 o 6 7 1 128.52 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86.87 4.32 o -3 4 8 0.12 0.29 0.55 o -2 4 8 21.86 20.02 1.43 o -1 4 8 7.63 5.09 0.82 o 0 4 8 179.35 184.63 4.58 o 1 4 8 48.25 46.85 1.90 o 2 4 8 57.51 55.52 2.05 o 3 4 8 84.44 84.69 2.61 o 4 4 8 3.24 3.93 0.70 o 5 4 8 19.03 20.01 1.83 o 6 4 8 60.62 62.49 3.30 o 7 4 8 97.15 103.71 4.60 o -3 5 8 2.46 1.69 0.69 o -2 5 8 69.98 70.42 3.05 o -1 5 8 1.49 2.70 0.71 o 0 5 8 26.59 30.29 1.66 o 1 5 8 0.83 0.18 0.44 o 2 5 8 28.96 30.01 1.50 o 3 5 8 72.68 73.77 2.43 o 4 5 8 27.89 29.68 3.02 o 5 5 8 33.99 32.74 1.60 o 6 5 8 42.48 46.24 2.76 o 7 5 8 9.30 12.05 1.71 o -2 6 8 4.80 2.97 1.21 o -1 6 8 30.30 26.83 2.39 o 0 6 8 44.13 34.89 2.55 o 1 6 8 64.03 62.59 3.42 o 2 6 8 0.65 0.46 0.69 o 3 6 8 24.19 28.04 2.31 o 4 6 8 28.90 26.01 2.26 o 5 6 8 0.71 0.05 0.77 o -1 7 8 9.03 8.52 1.64 o 0 7 8 0.88 0.44 0.85 o 1 7 8 38.30 39.68 2.87 o 2 7 8 7.58 7.71 1.51 o 3 7 8 46.96 48.75 3.19 o 4 7 8 22.13 25.26 2.37 o 5 7 8 8.74 7.60 1.57 o 0 -3 9 10.33 14.84 2.29 o 1 -3 9 52.10 61.00 3.94 o 2 -3 9 23.41 20.48 2.07 o 3 -3 9 13.17 13.35 1.70 o 4 -3 9 84.40 80.75 4.00 o 5 -3 9 43.57 39.83 2.85 o -1 -2 9 21.76 26.40 2.79 o 0 -2 9 49.42 62.54 3.98 o 1 -2 9 165.56 146.50 5.68 o 2 -2 9 196.91 172.62 6.30 o 3 -2 9 1.01 1.45 0.76 o 4 -2 9 43.35 41.83 2.74 o 5 -2 9 39.25 47.75 3.06 o 6 -2 9 33.37 32.20 2.53 o -2 -1 9 119.30 131.00 5.95 o -1 -1 9 42.55 50.97 3.57 o 0 -1 9 1.58 3.81 1.42 o 1 -1 9 58.88 58.27 3.23 o 2 -1 9 202.45 182.99 6.52 o 3 -1 9 71.51 65.71 3.45 o 4 -1 9 33.74 34.59 2.51 o 5 -1 9 111.24 114.98 4.96 o 6 -1 9 8.11 7.67 1.54 o -2 0 9 81.60 83.33 4.52 o -1 0 9 6.05 8.45 1.73 o 0 0 9 40.46 48.37 3.31 o 1 0 9 79.48 77.20 3.82 o 2 0 9 427.84 378.98 11.07 o 3 0 9 0.71 0.61 0.68 o 4 0 9 72.78 74.66 3.73 o 5 0 9 303.51 286.09 9.13 o 6 0 9 98.10 88.48 4.28 o 7 0 9 66.45 68.18 3.87 o -3 1 9 10.32 9.35 1.79 o -2 1 9 7.76 7.34 1.61 o -1 1 9 48.42 55.85 3.57 o 0 1 9 0.36 -0.57 0.60 o 1 1 9 27.35 27.78 2.24 o 2 1 9 7.64 7.68 1.37 o 3 1 9 105.70 94.71 4.21 o 4 1 9 13.02 14.34 1.74 o 5 1 9 100.60 101.73 4.53 o 6 1 9 0.18 1.91 0.93 o 7 1 9 43.35 44.59 3.13 o -3 2 9 20.03 18.15 2.19 o -2 2 9 1.93 1.76 1.09 o -1 2 9 89.95 100.67 4.84 o 0 2 9 1.48 1.31 0.62 o 1 2 9 30.45 31.32 1.64 o 2 2 9 12.60 12.14 1.13 o 3 2 9 186.71 175.29 6.36 o 4 2 9 4.80 3.57 1.07 o 5 2 9 69.51 70.15 3.63 o 6 2 9 5.23 5.31 1.24 o 7 2 9 87.28 96.03 4.67 o -2 3 9 2.79 3.44 1.18 o -1 3 9 60.02 63.70 2.57 o 0 3 9 53.23 54.39 2.32 o 1 3 9 11.66 13.58 1.19 o 2 3 9 3.45 4.66 0.82 o 3 3 9 60.97 61.56 2.30 o 4 3 9 125.98 122.40 4.97 o 5 3 9 46.59 48.42 2.95 o 6 3 9 2.24 2.53 1.09 o 7 3 9 0.74 0.10 0.78 o -2 4 9 5.37 4.61 0.91 o -1 4 9 27.66 26.72 1.73 o 0 4 9 57.47 59.10 4.51 o 1 4 9 8.50 7.77 1.03 o 2 4 9 10.58 11.21 1.10 o 3 4 9 0.59 0.22 0.51 o 4 4 9 63.63 62.75 2.33 o 5 4 9 23.81 25.60 2.19 o 6 4 9 40.75 45.47 2.94 o -1 5 9 1.70 1.08 0.66 o 0 5 9 5.10 5.33 1.33 o 1 5 9 2.27 2.12 0.69 o 2 5 9 4.89 3.78 0.78 o 3 5 9 0.98 0.71 0.53 o 4 5 9 53.80 57.55 2.25 o 5 5 9 5.94 4.67 1.20 o 0 6 9 58.75 53.00 3.41 o 1 6 9 1.20 1.13 0.90 o 2 6 9 3.20 2.82 1.10 o 3 6 9 4.16 3.56 1.19 o 4 6 9 0.73 0.69 0.92 o 1 -1 10 44.22 50.12 3.65 o 2 -1 10 32.75 32.16 2.59 o 3 -1 10 5.52 6.95 1.50 o 4 -1 10 24.94 23.14 2.30 o 0 0 10 16.17 23.43 2.71 o 1 0 10 47.94 58.68 3.84 o 2 0 10 0.14 0.09 0.82 o 3 0 10 3.15 2.44 1.10 o 4 0 10 134.15 124.66 5.33 o 5 0 10 45.29 44.75 3.07 o 0 1 10 1.09 -0.37 1.01 o 1 1 10 55.33 60.55 3.83 o 2 1 10 32.40 25.90 2.39 o 3 1 10 1.94 1.19 0.84 o 4 1 10 9.52 7.42 1.48 o 5 1 10 18.49 13.53 1.84 o 0 2 10 6.96 8.88 1.79 o 1 2 10 23.39 24.10 1.70 o 2 2 10 32.66 34.20 1.82 o 3 2 10 105.38 97.38 4.52 o 4 2 10 34.57 36.56 2.65 o 5 2 10 26.09 28.56 2.48 o 0 3 10 0.16 0.39 0.63 o 1 3 10 28.89 31.75 1.80 o 2 3 10 17.99 19.98 1.52 o 3 3 10 18.93 17.62 1.65 o 4 3 10 2.88 3.30 1.16 o 5 3 10 15.64 11.32 1.73 o 1 4 10 33.04 35.50 1.95 o 2 4 10 3.80 3.78 0.90 o 3 4 10 18.64 19.09 1.48 o 4 4 10 1.56 1.30 0.94 o