#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232935.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232935_Fobs loop_ _publ_author_name 'Ru, Jing' 'Zhang, Rufen' _publ_section_title ; catena-Poly[[triphenyltin(IV)]-\m-3-methylphenylseleninato-\k^2^O:O'] ; _journal_coeditor_code RZ2663 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1809 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.324 _cell_angle_gamma 90.000 _cell_length_a 12.3293 _cell_length_b 14.3519 _cell_length_c 12.2865 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file rz2663Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 110508g in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 12645.07 13479.89 484.51 o 4 0 0 16480.04 17889.86 664.35 o 5 0 0 8698.49 9259.03 386.26 o 6 0 0 150.17 140.20 65.27 o 7 0 0 1588.86 1482.74 137.64 o 8 0 0 4940.64 4549.21 264.08 o 9 0 0 249.15 222.72 62.57 o 10 0 0 3830.20 4080.25 279.72 o 11 0 0 1650.21 2002.62 230.59 o 12 0 0 5056.79 5224.49 355.50 o 13 0 0 3793.46 3669.47 305.35 o 14 0 0 1082.84 1113.66 230.68 o 2 1 0 1439.54 1593.39 45.96 o 3 1 0 50790.31 55237.04 2205.21 o 4 1 0 10504.53 11049.00 348.97 o 5 1 0 7296.81 7414.44 160.80 o 6 1 0 12786.52 12976.29 293.07 o 7 1 0 1576.85 1434.34 71.67 o 8 1 0 1041.31 993.61 70.83 o 9 1 0 5704.28 5591.22 224.78 o 10 1 0 70.90 -7.98 65.81 o 11 1 0 2687.75 2765.36 176.21 o 12 1 0 3659.88 3756.09 208.71 o 13 1 0 2897.58 3203.12 201.86 o 14 1 0 2543.27 2980.75 218.65 o 0 2 0 32356.91 33268.25 800.72 o 1 2 0 3451.54 3707.92 75.03 o 2 2 0 741.14 766.51 28.67 o 3 2 0 3696.06 3730.99 76.81 o 4 2 0 12581.30 12897.33 249.17 o 5 2 0 17255.68 17566.07 602.54 o 6 2 0 21.36 -35.22 23.48 o 7 2 0 4661.89 4580.12 135.57 o 8 2 0 2839.67 2455.81 106.38 o 9 2 0 187.40 134.62 69.59 o 10 2 0 2229.51 2045.43 141.98 o 11 2 0 883.55 871.69 123.82 o 12 2 0 3089.55 3307.85 198.36 o 13 2 0 1829.13 2273.70 201.09 o 14 2 0 617.83 620.24 166.64 o 1 3 0 17142.23 17888.78 316.98 o 2 3 0 1265.52 1265.85 39.35 o 3 3 0 286.89 240.16 23.02 o 4 3 0 4675.28 4171.62 114.75 o 5 3 0 98.00 51.64 26.25 o 6 3 0 6815.24 6419.79 205.41 o 7 3 0 4244.99 4519.22 136.03 o 8 3 0 2982.18 2886.75 108.46 o 9 3 0 2924.81 2685.84 237.81 o 10 3 0 77.74 -6.57 68.61 o 11 3 0 1284.04 1301.56 142.60 o 12 3 0 75.60 -17.04 85.83 o 13 3 0 394.96 329.40 183.13 o 14 3 0 321.06 326.80 125.53 o 0 4 0 703.04 594.10 46.12 o 1 4 0 5850.68 6017.16 122.70 o 2 4 0 4241.60 4474.90 136.48 o 3 4 0 287.06 244.11 25.90 o 4 4 0 2004.20 2065.28 61.10 o 5 4 0 6110.10 6098.99 143.77 o 6 4 0 3941.49 3992.95 113.27 o 7 4 0 4235.03 3815.29 188.49 o 8 4 0 1437.91 1513.63 86.53 o 9 4 0 4427.46 4381.03 197.61 o 10 4 0 181.12 140.84 81.13 o 11 4 0 1712.51 1569.54 151.14 o 12 4 0 67.06 41.80 90.85 o 13 4 0 96.92 67.20 98.19 o 14 4 0 113.58 -26.83 110.09 o 1 5 0 3388.86 3111.71 69.41 o 2 5 0 2886.99 3037.95 72.36 o 3 5 0 14787.44 15052.72 257.92 o 4 5 0 6626.52 6679.94 135.58 o 5 5 0 1073.63 1080.03 54.17 o 6 5 0 2207.14 2200.76 79.65 o 7 5 0 411.17 373.82 51.76 o 8 5 0 3074.41 3093.21 119.18 o 9 5 0 87.01 66.24 65.73 o 10 5 0 2264.57 2096.69 147.11 o 11 5 0 293.16 274.42 100.60 o 12 5 0 2479.41 2463.88 310.30 o 13 5 0 20.36 5.33 108.46 o 0 6 0 7821.27 7020.65 214.61 o 1 6 0 3.67 -3.16 16.91 o 2 6 0 11932.90 11739.84 207.83 o 3 6 0 8.63 -8.01 22.20 o 4 6 0 460.30 264.88 45.92 o 5 6 0 1606.53 1641.85 64.94 o 6 6 0 72.04 -21.31 28.67 o 7 6 0 478.68 385.78 73.11 o 8 6 0 23.57 -66.03 51.62 o 9 6 0 1022.03 1149.94 118.16 o 10 6 0 563.26 461.60 101.16 o 11 6 0 1131.35 1499.60 148.59 o 12 6 0 354.79 365.54 122.30 o 13 6 0 469.85 384.07 128.59 o 1 7 0 12084.69 11866.75 210.99 o 2 7 0 549.35 550.53 40.03 o 3 7 0 11903.95 11754.29 243.23 o 4 7 0 898.02 794.46 51.24 o 5 7 0 404.17 323.71 40.99 o 6 7 0 1124.56 1156.48 69.77 o 7 7 0 57.23 9.57 37.24 o 8 7 0 2.60 -58.36 61.55 o 9 7 0 430.28 560.24 101.27 o 10 7 0 60.95 -9.21 73.67 o 11 7 0 1238.77 1505.08 157.04 o 12 7 0 273.81 261.15 106.15 o 13 7 0 273.72 194.90 119.35 o 0 8 0 4581.78 4557.72 232.34 o 1 8 0 1402.06 1410.33 55.05 o 2 8 0 5658.94 5390.72 147.81 o 3 8 0 6668.71 6358.66 139.24 o 4 8 0 226.31 178.34 38.02 o 5 8 0 5088.21 4861.91 136.18 o 6 8 0 168.68 111.21 49.45 o 7 8 0 4186.81 4112.44 129.17 o 8 8 0 472.33 528.06 102.53 o 9 8 0 1334.85 1533.07 149.75 o 10 8 0 1953.59 2005.02 158.73 o 11 8 0 0.38 -102.76 82.30 o 12 8 0 741.48 697.71 147.33 o 1 9 0 99.72 37.33 34.23 o 2 9 0 4753.92 4724.99 130.72 o 3 9 0 17.69 -7.33 31.10 o 4 9 0 10474.37 10244.37 339.06 o 5 9 0 245.33 116.34 45.77 o 6 9 0 12618.20 13486.61 291.91 o 7 9 0 1406.77 1489.28 91.37 o 8 9 0 4421.79 4425.21 169.44 o 9 9 0 2860.44 3141.02 191.29 o 10 9 0 1109.21 1088.81 142.32 o 11 9 0 1594.62 1857.13 179.19 o 12 9 0 21.90 -43.74 107.46 o 0 10 0 45.58 -64.43 86.20 o 1 10 0 148.83 74.51 42.62 o 2 10 0 203.15 100.67 45.21 o 3 10 0 6829.78 6837.31 225.77 o 4 10 0 10.65 5.49 41.30 o 5 10 0 9679.32 10380.94 251.63 o 6 10 0 2004.12 2120.24 122.67 o 7 10 0 7086.48 7546.46 249.69 o 8 10 0 3202.27 3428.61 155.88 o 9 10 0 3628.13 3899.40 215.22 o 10 10 0 3393.33 3552.46 211.37 o 11 10 0 419.80 470.68 235.12 o 1 11 0 573.03 529.32 74.23 o 2 11 0 2932.26 2871.20 109.65 o 3 11 0 12.03 -62.65 41.77 o 4 11 0 6268.18 6252.70 176.55 o 5 11 0 1618.33 1660.27 98.81 o 6 11 0 7560.60 7903.50 210.02 o 7 11 0 1926.80 2076.49 150.92 o 8 11 0 3563.76 3881.51 246.32 o 9 11 0 1887.67 2345.26 206.24 o 10 11 0 1313.24 1510.30 199.88 o 11 11 0 932.04 718.21 141.35 o 0 12 0 868.09 867.81 113.27 o 1 12 0 801.34 800.73 88.22 o 2 12 0 457.00 412.95 62.32 o 3 12 0 5163.08 4971.91 154.90 o 4 12 0 40.39 -32.86 50.64 o 5 12 0 4730.69 4943.40 160.64 o 6 12 0 498.59 477.72 74.96 o 7 12 0 2669.87 2643.59 141.98 o 8 12 0 275.28 287.46 87.69 o 9 12 0 1081.08 967.94 178.85 o 10 12 0 744.44 719.71 151.59 o 1 13 0 1872.44 1719.73 104.77 o 2 13 0 393.83 305.76 65.38 o 3 13 0 1709.06 1718.17 104.60 o 4 13 0 662.29 619.11 77.09 o 5 13 0 86.94 68.19 63.35 o 6 13 0 579.13 567.04 79.71 o 7 13 0 31.82 -26.04 89.39 o 8 13 0 239.11 202.13 113.01 o 9 13 0 161.45 -9.08 87.43 o 0 14 0 670.19 527.95 112.72 o 1 14 0 114.61 69.06 60.19 o 2 14 0 1548.07 1606.80 107.00 o 3 14 0 661.46 565.16 78.64 o 4 14 0 407.64 418.24 92.39 o 5 14 0 84.81 22.31 63.75 o 6 14 0 37.10 -64.30 60.77 o 7 14 0 16.21 -114.10 76.07 o 8 14 0 5.72 -77.11 80.60 o 1 15 0 292.87 179.70 72.55 o 2 15 0 465.57 257.17 74.13 o 3 15 0 199.07 162.88 70.24 o 4 15 0 690.95 609.53 111.23 o 5 15 0 97.25 38.69 71.82 o 6 15 0 936.21 936.82 100.68 o 0 16 0 29.98 -62.37 135.25 o 1 16 0 108.76 87.63 104.43 o 2 16 0 94.40 39.72 96.64 o 3 16 0 815.05 900.71 152.27 o 4 16 0 13.11 -100.63 94.03 o 5 16 0 1509.26 1587.67 179.82 o 1 17 0 262.52 199.79 118.12 o -14 1 1 238.43 244.64 114.12 o -13 1 1 584.93 546.33 134.96 o -12 1 1 3.57 5.54 103.08 o -11 1 1 1451.86 1517.03 145.48 o -10 1 1 460.54 390.70 97.61 o -9 1 1 1497.54 1650.23 127.01 o -8 1 1 356.21 347.88 43.60 o -7 1 1 4016.45 3869.01 101.58 o -6 1 1 566.92 524.38 42.99 o -5 1 1 1655.34 1829.67 55.83 o -4 1 1 50.69 113.66 24.95 o -3 1 1 1465.48 1644.77 109.17 o -2 1 1 1385.62 1514.37 114.34 o -1 1 1 1752.10 2304.03 311.97 o 1 1 1 4238.65 4781.09 359.43 o 2 1 1 2704.15 2774.01 88.30 o 3 1 1 10757.61 10378.81 226.12 o 4 1 1 3537.25 3316.28 117.12 o 5 1 1 10430.57 10549.46 242.13 o 6 1 1 3428.26 3220.31 104.49 o 7 1 1 1999.21 1952.82 84.28 o 8 1 1 2043.07 2025.27 92.88 o 9 1 1 244.80 220.15 51.81 o 10 1 1 104.58 9.12 67.65 o 11 1 1 32.06 -13.34 74.19 o 12 1 1 121.43 -5.47 94.46 o 13 1 1 8.68 -121.59 96.60 o 14 1 1 246.55 58.76 113.87 o -14 2 1 653.56 690.82 142.02 o -13 2 1 930.01 1258.43 157.07 o -12 2 1 3586.27 3361.46 198.03 o -11 2 1 2562.98 2885.51 258.44 o -10 2 1 10864.79 10707.22 366.41 o -9 2 1 2105.15 2084.44 135.12 o -8 2 1 10231.85 9698.96 270.65 o -7 2 1 504.87 485.36 44.41 o -6 2 1 4015.98 4238.17 101.76 o -5 2 1 676.13 1095.76 68.40 o -4 2 1 796.28 1256.43 253.51 o -3 2 1 982.64 1033.77 108.00 o -2 2 1 24693.73 30648.18 2402.07 o -1 2 1 24.75 22.92 11.08 o 0 2 1 9458.63 10584.68 601.61 o 1 2 1 4706.05 5326.80 118.54 o 2 2 1 77419.88 82351.90 1614.36 o 3 2 1 13768.44 13552.67 289.48 o 4 2 1 37225.62 36796.96 744.38 o 5 2 1 15697.48 15142.37 553.27 o 6 2 1 9967.81 9335.10 226.32 o 7 2 1 6205.60 5993.48 207.77 o 8 2 1 1599.43 1664.27 85.51 o 9 2 1 222.60 215.33 68.08 o 10 2 1 86.76 310.13 184.63 o 11 2 1 3.29 -17.31 74.28 o 12 2 1 48.37 97.86 130.93 o 13 2 1 843.17 668.43 206.07 o 14 2 1 36.43 -59.05 101.75 o -14 3 1 1123.30 1024.56 281.81 o -13 3 1 1841.22 1898.14 182.47 o -12 3 1 1208.20 1330.29 159.72 o -11 3 1 8433.60 7894.78 307.55 o -10 3 1 3593.51 3563.20 189.50 o -9 3 1 13459.25 13208.12 350.75 o -8 3 1 375.97 315.37 64.93 o -7 3 1 12442.22 12374.16 312.51 o -6 3 1 16.50 -3.65 25.10 o -5 3 1 1687.02 1828.31 92.18 o -4 3 1 4495.42 5425.09 154.47 o -3 3 1 907.97 1130.18 152.37 o -2 3 1 13127.63 14537.69 448.83 o -1 3 1 14601.96 15797.20 252.47 o 0 3 1 4119.21 4004.58 116.82 o 1 3 1 60251.79 64061.93 1247.07 o 2 3 1 30029.84 31804.49 553.39 o 3 3 1 25575.29 25741.88 455.81 o 4 3 1 16232.62 15901.77 344.61 o 5 3 1 18182.54 17699.12 526.93 o 6 3 1 2292.07 1791.80 119.26 o 7 3 1 6174.33 6142.06 172.00 o 8 3 1 3971.94 3595.14 127.34 o 9 3 1 616.61 783.22 74.29 o 10 3 1 306.18 242.66 78.22 o 11 3 1 221.17 92.21 79.32 o 12 3 1 65.05 62.39 89.75 o 13 3 1 444.47 328.26 114.07 o 14 3 1 1027.44 1187.44 167.84 o -14 4 1 175.38 210.45 119.65 o -13 4 1 1727.60 2237.06 216.15 o -12 4 1 2189.84 2512.62 191.56 o -11 4 1 2397.41 2332.05 240.84 o -10 4 1 8816.98 8568.82 313.31 o -9 4 1 477.93 498.09 79.76 o -8 4 1 12835.70 12232.53 323.03 o -7 4 1 118.53 172.77 38.36 o -6 4 1 6451.73 6275.07 148.06 o -5 4 1 5080.12 5583.72 190.15 o -4 4 1 1453.46 2016.51 135.17 o -3 4 1 5941.79 6035.17 232.39 o -2 4 1 4668.91 4823.95 94.23 o -1 4 1 483.86 450.87 24.98 o 0 4 1 3818.41 3596.03 83.23 o 1 4 1 2131.83 2242.35 61.72 o 2 4 1 36039.57 38422.93 668.55 o 3 4 1 8807.95 9183.91 185.34 o 4 4 1 28701.23 29201.01 521.62 o 5 4 1 14615.61 14445.77 395.03 o 6 4 1 11426.57 11108.19 326.30 o 7 4 1 7737.94 7253.84 207.34 o 8 4 1 546.65 612.09 148.52 o 9 4 1 982.00 1011.84 111.86 o 10 4 1 430.81 355.10 87.64 o 11 4 1 359.33 327.53 104.02 o 12 4 1 1000.95 1070.05 140.48 o 13 4 1 315.20 291.74 110.90 o 14 4 1 1132.63 1365.12 174.39 o -14 5 1 1270.97 1490.48 178.34 o -13 5 1 317.84 307.78 171.94 o -12 5 1 1350.73 1536.28 162.27 o -11 5 1 1780.91 1934.80 186.76 o -10 5 1 1315.37 1241.12 135.83 o -9 5 1 5689.68 5196.82 322.62 o -8 5 1 58.73 94.73 56.05 o -7 5 1 6908.73 6842.06 262.64 o -6 5 1 1756.93 1564.47 74.79 o -5 5 1 4416.69 4384.68 199.22 o -4 5 1 17828.48 17561.51 297.40 o -3 5 1 14.60 28.63 20.12 o -2 5 1 13877.52 14400.56 242.42 o -1 5 1 8196.21 7941.03 143.18 o 0 5 1 1133.84 955.74 42.93 o 1 5 1 24928.04 25231.45 451.02 o 2 5 1 10.39 2.84 24.31 o 3 5 1 19226.28 19761.27 365.80 o 4 5 1 5424.22 5325.91 128.42 o 5 5 1 10034.44 10472.36 509.42 o 6 5 1 7160.52 6831.80 186.92 o 7 5 1 716.06 804.25 67.01 o 8 5 1 6963.61 6792.01 233.72 o 9 5 1 2383.41 2252.16 168.65 o 10 5 1 2332.50 2393.07 234.91 o 11 5 1 2543.49 2428.01 163.99 o 12 5 1 33.31 23.79 146.48 o 13 5 1 1537.88 1462.95 172.56 o -13 6 1 535.41 428.40 132.20 o -12 6 1 34.00 -19.25 87.15 o -11 6 1 760.19 747.91 187.40 o -10 6 1 1071.20 1172.40 132.06 o -9 6 1 30.16 25.62 63.15 o -8 6 1 2652.20 2555.62 127.13 o -7 6 1 3468.05 3612.85 170.88 o -6 6 1 1481.84 1489.52 84.22 o -5 6 1 10647.62 10649.16 396.08 o -4 6 1 140.61 134.22 29.56 o -3 6 1 26285.95 26201.53 427.63 o -2 6 1 625.13 662.35 37.54 o -1 6 1 16300.29 16313.38 306.04 o 0 6 1 3618.59 3512.82 92.52 o 1 6 1 7296.25 7247.55 222.13 o 2 6 1 9467.48 9107.16 190.00 o 3 6 1 474.38 470.41 70.44 o 4 6 1 1039.39 1048.46 59.49 o 5 6 1 1166.17 1148.95 75.00 o 6 6 1 12.72 -23.18 38.89 o 7 6 1 6950.24 6844.67 204.00 o 8 6 1 1873.95 1802.66 96.95 o 9 6 1 4354.66 4394.71 295.44 o 10 6 1 2853.05 2821.32 170.62 o 11 6 1 1843.10 1867.79 165.45 o 12 6 1 2109.65 2449.98 279.08 o 13 6 1 111.15 113.71 107.64 o -13 7 1 201.42 111.20 108.46 o -12 7 1 263.97 235.79 146.91 o -11 7 1 44.87 -23.22 85.15 o -10 7 1 12.78 -38.08 81.11 o -9 7 1 286.34 396.50 95.75 o -8 7 1 2897.70 2625.46 109.10 o -7 7 1 295.15 213.32 44.66 o -6 7 1 10722.94 11302.49 291.85 o -5 7 1 1134.78 1075.78 65.96 o -4 7 1 20483.18 20235.58 346.87 o -3 7 1 63.08 44.37 26.23 o -2 7 1 22707.15 22738.91 376.64 o -1 7 1 224.60 190.95 27.31 o 0 7 1 16705.67 16449.51 315.57 o 1 7 1 130.80 105.31 30.44 o 2 7 1 7567.89 7583.15 172.79 o 3 7 1 1082.55 1022.20 81.56 o 4 7 1 314.74 407.22 54.77 o 5 7 1 51.94 13.89 32.97 o 6 7 1 3412.06 3190.75 105.30 o 7 7 1 677.95 713.75 74.13 o 8 7 1 3672.30 3572.28 140.35 o 9 7 1 2922.47 2986.90 171.39 o 10 7 1 2507.37 2177.59 158.39 o 11 7 1 3085.30 3157.20 198.41 o 12 7 1 716.03 804.98 140.71 o 13 7 1 1352.46 1757.16 185.03 o -12 8 1 192.20 192.66 115.35 o -11 8 1 48.75 -9.69 121.28 o -10 8 1 15.26 -114.16 91.42 o -9 8 1 504.69 575.40 103.31 o -8 8 1 3.11 -3.94 49.75 o -7 8 1 4951.66 4882.15 225.06 o -6 8 1 145.01 129.19 42.26 o -5 8 1 10674.96 10409.66 258.78 o -4 8 1 203.70 160.84 36.31 o -3 8 1 19752.30 20023.45 344.19 o -2 8 1 144.58 146.67 31.17 o -1 8 1 14614.84 14805.58 260.23 o 0 8 1 8.31 -31.67 21.12 o 1 8 1 3648.21 3671.64 107.24 o 2 8 1 2343.24 2390.13 85.44 o 3 8 1 247.59 332.72 106.54 o 4 8 1 163.54 105.81 38.89 o 5 8 1 1.08 34.66 38.63 o 6 8 1 903.22 828.46 69.87 o 7 8 1 1240.22 1356.52 107.10 o 8 8 1 2644.22 2664.73 126.08 o 9 8 1 976.16 1127.30 135.63 o 10 8 1 2105.32 2244.17 170.19 o 11 8 1 1355.61 1275.09 156.45 o 12 8 1 1404.36 1436.05 174.66 o -12 9 1 1.85 -137.71 91.80 o -11 9 1 7.84 -5.08 91.35 o -10 9 1 38.72 -5.08 89.45 o -9 9 1 108.85 41.35 67.56 o -8 9 1 1710.85 1672.05 125.75 o -7 9 1 221.44 176.12 64.30 o -6 9 1 4133.97 4152.42 121.62 o -5 9 1 147.46 101.74 42.24 o -4 9 1 4293.66 3832.00 106.85 o -3 9 1 144.85 74.11 34.57 o -2 9 1 3774.15 3601.57 95.83 o -1 9 1 52.71 20.79 29.46 o 0 9 1 932.82 773.16 62.24 o 1 9 1 200.08 156.85 39.89 o 2 9 1 421.29 393.58 48.67 o 3 9 1 154.49 87.85 41.47 o 4 9 1 135.58 109.23 44.30 o 5 9 1 1999.53 1831.59 89.65 o 6 9 1 6.91 4.40 43.25 o 7 9 1 1460.80 1479.20 101.91 o 8 9 1 91.09 65.29 75.50 o 9 9 1 964.97 788.06 130.42 o 10 9 1 408.18 353.65 111.99 o 11 9 1 913.24 665.64 138.90 o 12 9 1 334.69 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