#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232937.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232937_Fobs loop_ _publ_author_name 'Hossaini Sadr, Moayad' 'Soltani, Behzad' _publ_section_title ; Dichloridobis(4-methyl-3,5-diphenyl-1H-pyrazole-\kN^2^)copper(II) ; _journal_coeditor_code RZ2665 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1894 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.385 _cell_angle_gamma 90.000 _cell_length_a 19.1052 _cell_length_b 8.5062 _cell_length_c 17.3991 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7265 _[local]_cod_data_source_file rz2665Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KH191-2H IN C2/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 312.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6196.90 7017.11 205.90 o 4 0 0 74.83 280.92 174.44 o 6 0 0 1372.27 1540.43 120.70 o 8 0 0 54.28 -107.27 107.27 o 10 0 0 23497.91 22132.09 552.61 o 12 0 0 9665.03 8398.96 128.94 o 14 0 0 4272.12 3646.07 268.55 o 16 0 0 164.52 228.51 77.10 o 18 0 0 4449.69 3912.13 99.37 o 20 0 0 4282.08 4011.89 78.04 o 22 0 0 1533.58 1453.14 119.73 o 24 0 0 3028.27 3205.47 128.46 o 1 1 0 38.14 117.06 171.28 o 3 1 0 3429.12 3310.92 128.04 o 5 1 0 40.15 105.04 87.24 o 7 1 0 19620.69 18372.15 2827.08 o 9 1 0 8928.37 7643.25 1178.56 o 11 1 0 15349.83 14929.57 500.12 o 13 1 0 5155.27 5283.68 59.41 o 15 1 0 338.07 491.22 55.04 o 17 1 0 54.76 88.95 63.67 o 19 1 0 676.08 547.05 38.08 o 21 1 0 6466.18 6093.17 145.81 o 23 1 0 1809.42 1613.75 77.38 o 25 1 0 2343.43 2164.50 66.89 o 0 2 0 32437.92 49323.46 370.34 o 2 2 0 294.55 151.69 164.87 o 4 2 0 3159.57 2841.29 81.88 o 6 2 0 437.12 420.76 88.30 o 8 2 0 652.60 1035.40 65.18 o 10 2 0 4895.03 4571.33 135.94 o 12 2 0 7724.56 7391.57 126.15 o 14 2 0 15132.34 14671.23 345.91 o 16 2 0 1015.13 1063.98 65.77 o 18 2 0 167.89 216.31 92.50 o 20 2 0 1008.42 1091.99 47.02 o 22 2 0 374.46 415.82 78.08 o 24 2 0 963.63 1019.32 63.95 o 1 3 0 787.32 669.91 173.54 o 3 3 0 1519.26 894.67 330.59 o 5 3 0 1026.24 979.57 178.83 o 7 3 0 5077.97 5198.21 655.35 o 9 3 0 9.25 44.07 52.47 o 11 3 0 18.67 114.97 117.96 o 13 3 0 603.41 650.74 52.30 o 15 3 0 3217.76 2681.86 303.23 o 17 3 0 46.94 89.40 53.51 o 19 3 0 253.53 283.20 65.91 o 21 3 0 19.76 172.54 93.89 o 23 3 0 260.44 213.82 61.84 o 0 4 0 3687.90 4478.05 150.27 o 2 4 0 4103.17 3974.88 142.51 o 4 4 0 2952.33 3331.93 253.46 o 6 4 0 121.57 169.36 95.59 o 8 4 0 33.89 -16.75 67.14 o 10 4 0 556.21 531.57 67.11 o 12 4 0 4352.20 4334.48 141.91 o 14 4 0 3157.71 3577.75 427.88 o 16 4 0 1316.99 1289.63 133.78 o 18 4 0 553.41 553.12 52.75 o 20 4 0 99.98 171.07 73.46 o 22 4 0 663.90 652.68 85.56 o 24 4 0 601.32 564.63 42.60 o 1 5 0 4412.94 4391.78 91.52 o 3 5 0 575.65 551.58 84.97 o 5 5 0 148.26 210.22 92.58 o 7 5 0 271.67 449.44 102.51 o 9 5 0 6000.49 5929.45 261.85 o 11 5 0 19557.69 19519.41 144.83 o 13 5 0 3922.00 3805.47 250.85 o 15 5 0 1479.69 1353.01 85.14 o 17 5 0 39.77 194.64 41.29 o 19 5 0 14.23 119.14 55.27 o 21 5 0 2331.04 2370.00 191.01 o 23 5 0 3538.49 4209.46 807.82 o 0 6 0 28394.28 15432.24 130.88 o 2 6 0 11444.75 8409.28 4114.00 o 4 6 0 47.86 275.88 90.16 o 6 6 0 12.84 -37.70 63.99 o 8 6 0 402.64 404.75 62.78 o 10 6 0 12441.07 11838.69 68.65 o 12 6 0 1012.14 1038.88 182.48 o 14 6 0 669.76 873.65 177.13 o 16 6 0 249.98 246.43 45.57 o 18 6 0 952.64 1105.80 48.23 o 20 6 0 2769.93 3088.08 140.14 o 22 6 0 987.83 1031.69 176.60 o 1 7 0 9233.95 8546.77 355.80 o 3 7 0 10305.13 10886.59 683.97 o 5 7 0 91.54 191.94 60.99 o 7 7 0 1367.57 1322.31 184.69 o 9 7 0 5845.11 7022.36 483.39 o 11 7 0 2887.68 3221.56 397.60 o 13 7 0 2487.87 2693.36 158.78 o 15 7 0 739.99 1079.09 159.28 o 17 7 0 96.82 125.21 52.68 o 19 7 0 627.87 631.66 63.17 o 0 8 0 106.17 153.18 98.89 o 2 8 0 41.73 6.83 71.29 o 4 8 0 2247.49 1984.90 223.95 o 6 8 0 1218.50 1228.22 127.94 o 8 8 0 196.93 200.68 44.11 o 10 8 0 3052.91 3159.81 186.63 o 12 8 0 1911.60 1973.49 325.99 o 14 8 0 1720.94 1948.97 189.74 o 16 8 0 53.41 -60.77 60.77 o 18 8 0 13.68 3.17 54.67 o 1 9 0 265.40 469.94 68.89 o 3 9 0 155.43 174.60 56.65 o 5 9 0 772.84 697.18 108.06 o 7 9 0 82.50 109.63 72.23 o 9 9 0 1348.25 1357.69 51.09 o 11 9 0 193.42 331.57 53.90 o 13 9 0 1.87 -8.34 54.29 o 15 9 0 1152.89 1224.50 68.87 o 0 10 0 98.44 187.11 93.07 o 2 10 0 90.79 112.56 136.21 o 4 10 0 132.83 193.99 80.23 o 6 10 0 477.80 588.33 59.61 o 8 10 0 532.68 427.82 83.70 o 10 10 0 527.37 468.53 124.25 o 12 10 0 285.51 333.59 54.81 o 1 11 0 2894.78 2871.67 188.08 o 3 11 0 304.63 371.25 109.44 o 5 11 0 1000.81 909.00 117.59 o 7 11 0 376.88 300.76 54.47 o -25 1 1 264.64 331.00 42.17 o -23 1 1 367.46 458.75 64.51 o -21 1 1 60.36 236.92 42.12 o -19 1 1 1567.98 1537.74 130.98 o -17 1 1 4427.24 3774.94 132.94 o -15 1 1 2676.39 2153.54 202.53 o -13 1 1 892.90 1038.06 48.94 o -11 1 1 51.70 60.41 80.46 o -9 1 1 16418.77 16790.41 262.37 o -7 1 1 3668.71 3406.88 86.04 o -5 1 1 3181.67 2931.82 100.73 o -3 1 1 487.64 558.78 114.12 o -1 1 1 38610.30 39731.47 2681.11 o 1 1 1 10755.00 15758.76 2932.69 o 3 1 1 3963.31 3991.98 120.39 o 5 1 1 12378.30 12331.64 365.31 o 7 1 1 5487.10 5359.40 79.14 o 9 1 1 152.91 305.25 59.07 o 11 1 1 233.15 365.81 55.11 o 13 1 1 2100.49 2349.40 209.76 o 15 1 1 3650.41 3779.66 140.49 o 17 1 1 2735.00 2601.32 54.16 o 19 1 1 1105.01 1053.09 88.86 o 21 1 1 39.27 41.45 46.86 o 23 1 1 112.77 234.10 46.88 o 25 1 1 4.33 147.14 60.87 o -24 2 1 89.81 -16.15 83.58 o -22 2 1 712.80 668.60 88.90 o -20 2 1 1323.59 1180.78 95.43 o -18 2 1 6392.81 6281.12 109.15 o -16 2 1 39.09 62.33 54.71 o -14 2 1 1301.59 1350.11 107.64 o -12 2 1 290.63 342.53 47.78 o -10 2 1 1390.52 1852.18 275.10 o -8 2 1 13406.11 13464.93 228.23 o -6 2 1 31220.16 30401.65 659.90 o -4 2 1 11284.45 11061.14 104.94 o -2 2 1 9049.44 7628.39 2653.48 o 0 2 1 21304.44 26086.15 12645.95 o 2 2 1 5835.62 5880.65 1098.43 o 4 2 1 7476.51 7210.07 1032.71 o 6 2 1 17720.56 16701.00 1057.33 o 8 2 1 738.47 729.30 63.24 o 10 2 1 797.48 809.37 72.91 o 12 2 1 2845.33 2452.99 141.75 o 14 2 1 900.05 811.62 61.71 o 16 2 1 12272.72 12968.38 1040.29 o 18 2 1 3112.42 2883.57 424.70 o 20 2 1 651.31 587.20 45.67 o 22 2 1 19.45 111.43 90.96 o 24 2 1 459.53 560.17 107.13 o -25 3 1 219.28 211.83 57.37 o -23 3 1 68.52 51.74 38.16 o -21 3 1 51.57 -43.35 43.35 o -19 3 1 2292.54 3226.44 630.54 o -17 3 1 7519.93 6925.56 380.34 o -15 3 1 23554.53 23505.98 71.31 o -13 3 1 8590.85 8090.78 298.91 o -11 3 1 366.52 443.93 50.07 o -9 3 1 5909.90 7040.60 870.86 o -7 3 1 14018.50 13283.21 197.17 o -5 3 1 16484.55 15393.47 105.57 o -3 3 1 14635.25 13832.17 1064.98 o -1 3 1 820.02 835.13 117.82 o 1 3 1 3723.22 4953.06 447.42 o 3 3 1 28488.72 38524.39 4291.42 o 5 3 1 75311.74 79474.02 3323.39 o 7 3 1 9134.67 8019.65 159.52 o 9 3 1 2652.11 2422.27 58.90 o 11 3 1 12.35 -33.78 51.35 o 13 3 1 2615.64 2451.95 106.39 o 15 3 1 19234.64 18117.91 332.90 o 17 3 1 2007.51 2176.82 92.50 o 19 3 1 833.91 949.39 40.35 o 21 3 1 81.05 152.69 38.29 o 23 3 1 54.41 51.07 62.22 o -24 4 1 399.96 353.63 78.99 o -22 4 1 452.82 485.13 42.64 o -20 4 1 588.76 630.16 88.44 o -18 4 1 3993.43 3780.61 103.69 o -16 4 1 4984.60 4999.97 111.81 o -14 4 1 748.21 626.20 85.33 o -12 4 1 2361.29 2089.90 52.91 o -10 4 1 646.05 485.95 49.41 o -8 4 1 17518.13 18298.13 527.15 o -6 4 1 16124.48 14557.82 776.46 o -4 4 1 8709.32 7980.30 203.03 o -2 4 1 24.86 22.78 91.86 o 0 4 1 437.54 196.00 94.54 o 2 4 1 9024.54 9396.83 1327.71 o 4 4 1 7344.98 8657.73 673.82 o 6 4 1 27930.89 34393.79 5857.25 o 8 4 1 3044.19 2576.27 532.57 o 10 4 1 220.90 357.04 71.59 o 12 4 1 5947.71 6126.57 137.16 o 14 4 1 240.46 503.06 73.32 o 16 4 1 6542.35 6230.13 223.47 o 18 4 1 3112.56 3019.69 151.41 o 20 4 1 176.85 103.14 45.48 o 22 4 1 279.43 178.02 123.70 o 24 4 1 45.40 129.06 41.45 o -23 5 1 4.69 0.72 95.43 o -21 5 1 416.62 461.37 57.40 o -19 5 1 809.93 830.61 39.27 o -17 5 1 2432.94 2531.36 48.98 o -15 5 1 741.87 672.54 50.15 o -13 5 1 427.55 350.29 41.89 o -11 5 1 551.15 583.95 49.86 o -9 5 1 1411.36 1268.97 133.93 o -7 5 1 1385.16 1264.93 190.29 o -5 5 1 5179.20 5512.52 230.33 o -3 5 1 11029.37 9229.43 2195.88 o -1 5 1 757.58 843.79 201.17 o 1 5 1 6923.25 6434.63 2040.28 o 3 5 1 127.04 259.54 177.42 o 5 5 1 2797.98 3963.93 450.92 o 7 5 1 98.92 105.16 100.21 o 9 5 1 2515.18 3673.59 996.12 o 11 5 1 517.73 519.07 66.32 o 13 5 1 127.07 85.79 50.13 o 15 5 1 2165.29 2320.03 171.85 o 17 5 1 4003.69 4223.29 266.49 o 19 5 1 1444.96 1599.78 102.89 o 21 5 1 6.92 57.29 48.27 o 23 5 1 65.63 82.41 72.35 o -22 6 1 276.20 229.20 169.69 o -20 6 1 107.69 220.35 92.61 o -18 6 1 0.91 -46.74 93.05 o -16 6 1 0.81 -66.01 66.01 o -14 6 1 449.00 653.02 57.00 o -12 6 1 3616.74 3383.53 55.13 o -10 6 1 2154.51 1956.69 69.18 o -8 6 1 1011.85 1160.21 113.74 o -6 6 1 499.25 681.43 69.21 o -4 6 1 213.62 233.65 114.40 o -2 6 1 1761.75 2176.50 844.42 o 0 6 1 4690.99 4641.98 339.80 o 2 6 1 1837.45 1700.45 114.40 o 4 6 1 343.31 414.53 66.06 o 6 6 1 1972.91 2230.14 70.51 o 8 6 1 201.21 295.18 52.75 o 10 6 1 577.94 705.23 57.45 o 12 6 1 419.04 433.85 61.35 o 14 6 1 35.29 94.46 77.82 o 16 6 1 337.51 652.78 136.49 o 18 6 1 26.70 10.38 61.31 o 20 6 1 434.99 769.29 129.68 o -19 7 1 702.91 781.43 42.70 o -17 7 1 972.45 1075.23 107.84 o -15 7 1 20.16 175.38 54.18 o -13 7 1 676.94 785.94 73.74 o -11 7 1 625.46 592.59 125.17 o -9 7 1 507.00 659.95 99.57 o -7 7 1 1761.58 2182.98 123.78 o -5 7 1 111.27 154.48 60.82 o -3 7 1 1411.14 1422.77 127.00 o -1 7 1 1023.98 1145.98 80.17 o 1 7 1 203.75 220.37 106.64 o 3 7 1 1332.37 1252.42 64.54 o 5 7 1 2471.90 2288.22 259.53 o 7 7 1 1023.50 1199.42 59.83 o 9 7 1 117.08 221.61 55.90 o 11 7 1 5232.05 6088.84 519.97 o 13 7 1 148.34 174.35 118.56 o 15 7 1 96.03 172.52 125.21 o 17 7 1 1386.77 1767.91 341.29 o 19 7 1 415.85 587.84 74.80 o -18 8 1 2196.57 2946.43 475.57 o -16 8 1 2480.42 2581.75 225.77 o -14 8 1 89.29 86.79 45.84 o -12 8 1 54.03 17.53 76.34 o -10 8 1 1984.77 1950.09 166.92 o -8 8 1 3192.10 3067.94 222.00 o -6 8 1 5894.16 6187.33 192.61 o -4 8 1 11883.58 11483.69 142.51 o -2 8 1 1321.95 1123.98 227.83 o 0 8 1 1004.70 1142.78 59.88 o 2 8 1 525.84 583.25 155.12 o 4 8 1 3494.21 3828.11 373.74 o 6 8 1 2826.19 3539.78 213.25 o 8 8 1 1339.71 1452.72 166.46 o 10 8 1 276.76 363.09 59.18 o 12 8 1 455.75 521.32 154.15 o 14 8 1 2514.50 2326.07 554.30 o 16 8 1 4033.76 5151.98 585.93 o 18 8 1 545.71 415.70 63.12 o -15 9 1 1655.35 1306.40 375.55 o -13 9 1 97.54 92.79 75.13 o -11 9 1 1093.30 1059.88 93.97 o -9 9 1 15.70 12.99 53.85 o -7 9 1 2002.23 2195.01 196.04 o -5 9 1 8885.40 7978.63 982.42 o -3 9 1 153.93 222.11 56.13 o -1 9 1 479.33 549.38 87.25 o 1 9 1 96.49 61.80 68.89 o 3 9 1 2759.42 2838.04 109.07 o 5 9 1 7122.76 6337.99 891.53 o 7 9 1 1446.09 1235.13 255.70 o 9 9 1 719.34 874.02 160.76 o 11 9 1 15.81 127.21 56.90 o 13 9 1 2519.31 2462.75 97.86 o 15 9 1 1590.99 1531.84 56.20 o -12 10 1 671.95 647.78 56.34 o -10 10 1 425.30 400.97 114.39 o -8 10 1 1800.73 2068.63 208.69 o -6 10 1 2884.61 2741.33 462.13 o -4 10 1 2100.49 2119.90 56.13 o -2 10 1 259.53 66.86 152.69 o 0 10 1 277.27 333.16 93.07 o 2 10 1 2588.13 2671.38 114.40 o 4 10 1 1375.62 1399.13 173.86 o 6 10 1 5491.91 5066.71 409.30 o 8 10 1 1942.32 1949.68 51.86 o 10 10 1 23.29 233.34 120.58 o 12 10 1 495.68 503.61 163.05 o -7 11 1 456.57 622.34 151.03 o -5 11 1 1993.90 1828.58 275.09 o -3 11 1 526.34 606.12 62.11 o -1 11 1 1667.22 1517.65 242.37 o 1 11 1 871.56 907.47 50.03 o 3 11 1 836.54 910.20 57.39 o 5 11 1 11.50 39.10 88.81 o 7 11 1 473.01 376.08 63.35 o -26 0 2 1029.37 805.15 141.54 o -24 0 2 3798.21 3499.80 103.73 o -22 0 2 5466.83 5358.44 196.32 o -20 0 2 2539.98 2413.42 120.70 o -18 0 2 31.82 4.43 88.22 o -16 0 2 3180.38 2963.66 184.20 o -14 0 2 606.68 690.46 80.95 o -12 0 2 22259.41 19805.52 183.72 o -10 0 2 47674.26 48917.92 154.59 o -8 0 2 6405.47 6286.91 177.90 o -6 0 2 95.94 167.22 115.82 o -4 0 2 23843.75 23052.69 193.54 o -2 0 2 97430.40 96353.84 592.35 o 0 0 2 38804.75 41593.77 483.77 o 2 0 2 41176.89 47221.66 4765.98 o 4 0 2 19709.46 15587.82 6557.59 o 6 0 2 282.53 444.09 85.33 o 8 0 2 5977.88 4998.00 129.91 o 10 0 2 8758.42 6854.27 833.76 o 12 0 2 17606.48 16734.20 1117.82 o 14 0 2 1639.67 1615.22 476.50 o 16 0 2 781.53 635.91 61.16 o 18 0 2 905.56 738.66 70.24 o 20 0 2 2763.17 2363.16 72.23 o 22 0 2 6305.05 5472.20 1384.91 o 24 0 2 1080.95 992.61 226.37 o -25 1 2 271.33 351.61 114.24 o -23 1 2 3452.00 2864.57 424.77 o -21 1 2 2826.54 2403.40 98.09 o -19 1 2 213.34 248.90 40.23 o -17 1 2 13.53 40.28 37.95 o -15 1 2 3931.25 3472.32 89.52 o -13 1 2 7802.88 7669.80 115.24 o -11 1 2 8121.46 7116.26 83.68 o -9 1 2 3772.47 3586.09 114.75 o -7 1 2 781.05 883.04 73.87 o -5 1 2 342.19 376.11 88.03 o -3 1 2 49044.55 49222.28 589.99 o -1 1 2 8563.44 8454.14 217.99 o 3 1 2 26073.14 28839.95 1785.96 o 5 1 2 12.53 94.59 76.87 o 7 1 2 1182.92 1099.60 76.31 o 9 1 2 33256.96 33751.10 1292.98 o 11 1 2 5224.52 4184.64 118.14 o 13 1 2 1287.95 1182.77 113.07 o 15 1 2 655.83 610.24 50.87 o 17 1 2 3495.60 3434.55 240.73 o 19 1 2 1679.63 1850.67 116.87 o 21 1 2 5863.64 5820.06 269.72 o 23 1 2 2437.94 3087.29 749.19 o 25 1 2 105.26 46.77 71.23 o -24 2 2 987.42 1163.73 94.31 o -22 2 2 2370.80 2563.00 91.01 o -20 2 2 482.66 443.52 73.74 o -18 2 2 590.46 546.10 79.00 o -16 2 2 732.81 802.14 68.71 o -14 2 2 507.96 622.86 57.40 o -12 2 2 10358.51 8547.57 1123.63 o -10 2 2 1779.29 1708.46 110.90 o -8 2 2 155.09 123.87 51.71 o -6 2 2 651.49 654.21 65.42 o -4 2 2 585.02 775.54 87.03 o -2 2 2 14643.08 15715.03 167.92 o 0 2 2 184.85 213.71 154.49 o 2 2 2 10843.33 20361.85 4166.36 o 4 2 2 1964.80 1732.14 78.70 o 6 2 2 121.72 143.55 76.90 o 8 2 2 9020.80 9095.61 279.59 o 10 2 2 9464.55 9120.75 458.46 o 12 2 2 10544.91 10600.67 353.15 o 14 2 2 397.00 450.12 55.39 o 16 2 2 4.60 143.38 93.34 o 18 2 2 247.07 251.91 55.41 o 20 2 2 730.47 696.72 112.97 o 22 2 2 773.43 686.22 56.95 o 24 2 2 985.46 866.58 87.60 o -25 3 2 347.61 398.84 110.02 o -23 3 2 1.17 128.27 41.02 o -21 3 2 19.07 47.10 52.19 o -19 3 2 213.65 268.04 66.19 o -17 3 2 2153.99 2101.44 125.38 o -15 3 2 562.78 597.18 98.09 o -13 3 2 832.36 916.45 47.19 o -11 3 2 28.93 100.73 52.62 o -9 3 2 3932.80 3843.75 104.53 o -7 3 2 525.10 748.93 59.24 o -5 3 2 2428.88 2248.10 91.83 o -3 3 2 10.66 11.79 91.63 o -1 3 2 244.16 191.61 92.71 o 1 3 2 5848.81 7538.08 355.32 o 3 3 2 4391.78 2854.16 159.00 o 5 3 2 2414.63 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