#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:33:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181251 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232983_Fobs loop_ _publ_author_name 'Diop, Tidiane' 'Diop, Libasse' 'Diop, Cheikh A. K.' 'Molloy, Kieran C.' 'Kociok-K\"ohn, Gabriele' _publ_section_title ; Dicyclohexylammonium trimethylbis(hydrogen phenylphosphonato)stannate(IV) ; _journal_coeditor_code VN2021 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1872 _journal_page_last m1873 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.625 _cell_angle_beta 103.687 _cell_angle_gamma 111.996 _cell_length_a 10.8718 _cell_length_b 12.7103 _cell_length_c 13.3218 _exptl_crystal_F_000 684.00 _reflns_d_resolution_high 0.7686 _cod_data_source_file vn2021Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' h09kcm10' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k 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585.10 35.37 o 11 1 0 753.86 689.44 65.79 o -12 2 0 757.17 801.42 36.11 o -11 2 0 961.80 1043.14 32.63 o -10 2 0 26.51 39.51 12.79 o -9 2 0 1326.99 1633.96 56.57 o -8 2 0 18.58 -16.80 19.03 o -7 2 0 5264.41 6240.07 157.31 o -6 2 0 87.24 85.61 8.73 o -5 2 0 0.89 5.10 6.21 o -4 2 0 3173.35 3310.45 90.03 o -3 2 0 4142.67 4567.84 101.43 o -2 2 0 408.18 373.04 84.67 o 1 2 0 399.26 398.41 10.98 o 2 2 0 16072.45 14152.87 610.76 o 3 2 0 6119.68 7150.17 481.52 o 4 2 0 30.18 14.23 9.40 o 5 2 0 2386.38 2547.54 234.45 o 6 2 0 771.28 806.45 44.97 o 7 2 0 985.80 943.67 29.90 o 8 2 0 1254.60 1267.66 52.24 o 9 2 0 10.43 3.19 18.04 o 10 2 0 613.26 501.60 70.65 o 11 2 0 774.93 691.97 35.33 o -13 3 0 440.59 419.26 51.22 o -12 3 0 799.57 914.85 86.40 o -11 3 0 577.18 668.46 34.46 o -10 3 0 536.43 628.82 30.08 o -9 3 0 208.78 229.98 17.19 o -8 3 0 305.88 323.77 14.53 o -7 3 0 6989.81 8408.46 166.31 o -6 3 0 2144.36 2565.22 63.04 o -5 3 0 10.54 23.03 6.29 o -4 3 0 4664.85 5324.99 125.59 o -3 3 0 2767.22 2972.30 80.88 o -2 3 0 2908.72 3124.68 87.03 o -1 3 0 6434.07 5460.77 315.67 o 0 3 0 23146.53 20088.69 1043.25 o 1 3 0 695.96 646.49 28.10 o 2 3 0 10001.50 9436.51 423.44 o 3 3 0 4555.83 5217.99 273.60 o 4 3 0 473.45 515.63 23.89 o 5 3 0 70.54 87.62 13.01 o 6 3 0 127.35 148.78 17.16 o 7 3 0 3150.54 3286.04 176.86 o 8 3 0 944.08 889.69 82.91 o 9 3 0 39.60 47.23 32.50 o 10 3 0 94.67 55.16 17.62 o 11 3 0 371.65 291.23 52.11 o -13 4 0 283.46 264.94 24.18 o -12 4 0 10.64 20.48 21.42 o -11 4 0 1355.26 1518.69 93.43 o -10 4 0 982.81 1135.76 57.87 o -9 4 0 138.42 155.52 13.20 o -8 4 0 85.03 90.19 20.27 o -7 4 0 4293.56 5053.78 104.43 o -6 4 0 1875.93 1979.18 61.41 o -5 4 0 2506.63 2476.30 77.56 o -4 4 0 795.28 822.65 27.34 o -3 4 0 16.43 29.16 8.99 o -2 4 0 9760.05 8941.76 217.43 o -1 4 0 7.11 43.09 6.04 o 0 4 0 8663.88 7680.78 188.81 o 1 4 0 275.00 283.13 26.28 o 2 4 0 4893.95 5187.92 342.34 o 3 4 0 628.32 542.59 20.98 o 4 4 0 2595.28 2867.04 115.38 o 5 4 0 82.88 90.44 28.98 o 6 4 0 24.20 9.22 15.23 o 7 4 0 2977.01 3080.48 93.84 o 8 4 0 869.61 765.13 37.05 o 9 4 0 23.98 6.08 21.84 o 10 4 0 160.97 150.42 40.48 o -13 5 0 285.16 319.23 43.67 o -12 5 0 50.23 125.28 21.00 o -11 5 0 1161.32 1405.20 52.08 o -10 5 0 575.75 662.66 31.23 o -9 5 0 2157.15 2532.01 79.28 o -8 5 0 217.12 230.98 13.10 o -7 5 0 551.34 584.77 18.77 o -6 5 0 1554.27 1598.82 47.22 o -5 5 0 3317.71 3019.84 83.41 o -4 5 0 3896.65 3968.03 443.23 o -3 5 0 324.86 383.82 21.41 o -2 5 0 3403.70 2924.56 80.62 o -1 5 0 1245.36 1034.63 25.74 o 0 5 0 4157.33 3586.24 74.73 o 1 5 0 41.35 28.82 9.23 o 2 5 0 2249.05 2392.61 56.71 o 3 5 0 1621.92 1527.43 40.09 o 4 5 0 2655.75 2722.11 138.53 o 5 5 0 118.81 145.53 49.24 o 6 5 0 499.01 489.63 28.76 o 7 5 0 25.22 35.89 10.88 o 8 5 0 261.59 229.77 15.42 o 9 5 0 146.67 134.02 16.00 o -13 6 0 362.11 403.14 32.82 o -12 6 0 233.28 254.93 26.05 o -11 6 0 228.48 244.54 18.19 o -10 6 0 160.67 181.51 14.14 o -9 6 0 3737.38 4220.26 97.78 o -8 6 0 1329.89 1348.61 34.96 o -7 6 0 1715.58 1840.56 58.51 o -6 6 0 1791.57 1610.76 111.23 o -5 6 0 16911.52 18454.77 1232.23 o -4 6 0 3020.28 2994.84 212.54 o -3 6 0 4659.43 4836.33 129.97 o -2 6 0 393.59 413.41 12.96 o -1 6 0 231.18 175.65 10.37 o 0 6 0 2790.40 2541.72 65.23 o 1 6 0 4109.36 4309.12 119.30 o 2 6 0 3.31 -3.25 11.63 o 3 6 0 340.01 315.56 20.03 o 4 6 0 432.75 434.80 42.03 o 5 6 0 518.00 525.50 68.92 o 6 6 0 1473.61 1445.39 38.15 o 7 6 0 11.70 15.52 30.35 o 8 6 0 20.78 38.18 22.80 o 9 6 0 560.04 464.22 58.38 o -13 7 0 309.39 346.20 30.81 o -12 7 0 405.48 380.38 22.82 o -11 7 0 0.67 -11.92 11.92 o -10 7 0 31.40 13.55 19.16 o -9 7 0 3650.52 3999.70 135.51 o -8 7 0 1155.73 1156.84 30.41 o -7 7 0 832.44 858.36 23.96 o -6 7 0 14.71 103.95 28.83 o -5 7 0 54.28 54.44 15.63 o -4 7 0 4315.39 4289.14 135.53 o -3 7 0 6328.09 6281.98 200.38 o -2 7 0 279.98 218.98 10.25 o -1 7 0 6.24 12.20 7.55 o 0 7 0 3962.56 3954.51 86.66 o 1 7 0 2133.61 2213.02 54.43 o 2 7 0 1154.36 1205.01 33.25 o 3 7 0 27.91 36.78 10.57 o 4 7 0 172.11 137.22 11.71 o 5 7 0 755.51 753.85 34.71 o 6 7 0 1662.79 1790.85 69.78 o 7 7 0 288.85 259.22 33.25 o 8 7 0 9.86 -12.98 35.13 o -13 8 0 241.57 245.88 23.18 o -12 8 0 772.20 695.27 52.26 o -11 8 0 321.70 323.13 21.00 o -10 8 0 100.97 84.09 13.77 o -9 8 0 1901.30 1825.32 59.63 o -8 8 0 16.27 10.79 8.62 o -7 8 0 1294.44 1218.51 47.14 o -6 8 0 1390.92 1345.90 73.46 o -5 8 0 1.44 9.59 6.99 o -4 8 0 1095.45 1037.48 36.17 o -3 8 0 4684.57 4546.69 206.83 o -2 8 0 950.03 890.92 24.10 o -1 8 0 439.42 423.08 15.01 o 0 8 0 58.54 70.90 20.55 o 1 8 0 696.24 684.40 22.28 o 2 8 0 666.77 696.54 30.16 o 3 8 0 2919.37 3128.31 78.26 o 4 8 0 6.37 -6.82 13.54 o 5 8 0 251.64 220.62 25.72 o 6 8 0 459.19 486.66 34.73 o 7 8 0 36.68 25.51 28.34 o -13 9 0 162.26 148.45 25.02 o -12 9 0 346.98 350.12 24.69 o -11 9 0 823.44 797.03 36.36 o -10 9 0 335.34 317.98 17.40 o -9 9 0 8.75 21.94 8.89 o -8 9 0 5.19 26.70 11.25 o -7 9 0 2522.03 2486.85 71.48 o -6 9 0 3156.73 3145.97 168.49 o -5 9 0 1516.35 1530.91 46.78 o -4 9 0 67.91 143.14 42.39 o -3 9 0 1526.68 1576.54 104.14 o -2 9 0 393.95 450.06 20.36 o -1 9 0 2409.44 2466.18 57.16 o 0 9 0 344.49 308.26 19.92 o 1 9 0 295.47 299.07 14.94 o 2 9 0 1125.29 1226.27 47.61 o 3 9 0 488.58 529.80 21.90 o 4 9 0 24.82 14.83 21.72 o 5 9 0 19.41 44.17 23.80 o 6 9 0 59.95 30.94 28.38 o -13 10 0 16.08 21.79 40.17 o -12 10 0 31.16 28.56 29.60 o -11 10 0 323.40 275.06 15.58 o -10 10 0 1878.00 1717.28 49.13 o -9 10 0 353.87 392.67 36.24 o -8 10 0 0.14 -0.96 5.88 o -7 10 0 1367.50 1362.96 107.24 o -6 10 0 811.48 772.60 34.28 o -5 10 0 794.97 843.12 23.33 o -4 10 0 265.00 281.76 20.10 o -3 10 0 36.45 80.68 42.89 o -2 10 0 216.86 285.49 38.97 o -1 10 0 4010.61 4329.71 99.97 o 0 10 0 87.95 106.35 15.39 o 1 10 0 6.30 -4.32 15.58 o 2 10 0 503.83 534.13 23.64 o 3 10 0 709.16 745.22 27.48 o 4 10 0 169.39 150.10 24.30 o 5 10 0 496.97 536.23 52.39 o -13 11 0 143.91 82.90 52.51 o -12 11 0 74.99 61.45 24.60 o -11 11 0 262.02 296.81 109.05 o -10 11 0 1178.86 1087.19 65.85 o -9 11 0 403.16 398.47 40.50 o -8 11 0 208.28 257.21 25.27 o -7 11 0 129.54 220.65 96.65 o -6 11 0 89.84 117.14 26.42 o -5 11 0 415.48 396.97 26.47 o -4 11 0 1675.09 1615.10 42.75 o -3 11 0 683.34 707.61 27.29 o -2 11 0 539.41 597.30 36.53 o -1 11 0 672.98 752.88 34.86 o 0 11 0 70.17 52.13 12.86 o 1 11 0 464.82 488.28 22.78 o 2 11 0 23.53 12.48 15.01 o 3 11 0 16.14 -13.00 15.14 o 4 11 0 486.90 491.66 38.77 o -12 12 0 352.68 338.18 49.51 o -11 12 0 66.87 86.24 32.27 o -10 12 0 294.98 328.03 39.98 o -9 12 0 552.46 505.91 31.39 o -8 12 0 1367.82 1358.09 53.42 o -7 12 0 176.92 187.57 24.29 o -6 12 0 24.22 49.78 16.03 o -5 12 0 497.05 618.94 70.02 o -4 12 0 1030.23 1042.08 31.90 o -3 12 0 196.91 242.47 15.98 o -2 12 0 245.56 250.08 21.53 o -1 12 0 76.18 81.63 15.38 o 0 12 0 29.20 42.30 13.46 o 1 12 0 1052.00 1133.95 38.29 o 2 12 0 96.14 115.04 19.70 o 3 12 0 0.50 -19.27 19.27 o -12 13 0 58.38 -4.89 40.62 o -11 13 0 131.14 191.74 55.33 o -10 13 0 57.71 149.93 28.49 o -9 13 0 427.80 430.56 41.22 o -8 13 0 1761.46 1722.35 61.96 o -7 13 0 405.38 394.75 16.13 o -6 13 0 54.46 88.84 16.15 o -5 13 0 210.99 348.38 86.08 o -4 13 0 220.24 243.62 15.73 o -3 13 0 1209.15 1312.76 38.98 o -2 13 0 76.54 84.41 14.57 o -1 13 0 18.67 -4.77 21.03 o 0 13 0 90.79 66.72 19.18 o 1 13 0 782.91 837.63 44.26 o 2 13 0 132.99 137.25 22.27 o -11 14 0 203.04 176.51 46.89 o -10 14 0 82.65 73.25 70.56 o -9 14 0 95.64 291.17 32.44 o -8 14 0 495.35 671.82 67.86 o -7 14 0 121.85 139.24 15.06 o -6 14 0 307.92 331.24 17.76 o -5 14 0 8.09 21.79 13.13 o -4 14 0 3.09 5.90 17.27 o -3 14 0 571.53 604.97 25.81 o -2 14 0 382.25 367.76 32.73 o -1 14 0 94.39 64.74 17.90 o 0 14 0 0.71 3.30 19.84 o 1 14 0 130.98 137.66 47.03 o -10 15 0 310.67 242.05 37.51 o -9 15 0 3.50 45.92 30.01 o -8 15 0 0.94 57.03 35.51 o -7 15 0 104.77 119.37 14.44 o -6 15 0 701.19 799.03 33.82 o -5 15 0 34.10 48.81 16.97 o -4 15 0 5.28 22.05 16.58 o -3 15 0 169.58 193.53 22.98 o -2 15 0 6.48 -25.28 25.28 o -1 15 0 282.25 303.75 44.87 o -8 16 0 75.19 184.36 68.56 o -7 16 0 96.31 132.71 31.23 o -6 16 0 450.02 441.56 36.34 o -5 16 0 24.81 117.34 50.55 o -4 16 0 154.67 149.10 24.19 o 3 -16 1 3.16 -27.14 46.75 o 4 -16 1 549.71 580.25 62.36 o 5 -16 1 5.27 16.85 24.34 o 6 -16 1 32.54 67.91 27.71 o 7 -16 1 79.07 61.08 28.70 o 8 -16 1 78.39 101.19 39.49 o 1 -15 1 130.76 130.85 21.35 o 2 -15 1 1.67 -1.26 17.79 o 3 -15 1 46.81 53.31 15.91 o 4 -15 1 465.26 541.49 36.68 o 5 -15 1 177.09 167.69 23.56 o 6 -15 1 593.01 766.69 42.42 o 7 -15 1 37.56 75.49 26.92 o 8 -15 1 73.39 86.54 25.51 o 9 -15 1 472.89 402.44 76.54 o 10 -15 1 391.95 370.66 40.37 o -1 -14 1 5.74 5.36 46.73 o 0 -14 1 535.96 626.75 31.72 o 1 -14 1 100.87 139.59 19.54 o 2 -14 1 186.66 236.07 15.16 o 3 -14 1 163.69 219.58 20.06 o 4 -14 1 343.16 308.87 35.90 o 5 -14 1 578.96 656.23 24.90 o 6 -14 1 868.65 962.72 84.03 o 7 -14 1 0.46 46.71 30.31 o 8 -14 1 2.14 99.06 23.83 o 9 -14 1 431.56 459.18 38.54 o 10 -14 1 271.27 247.23 31.37 o 11 -14 1 261.75 236.54 58.98 o -2 -13 1 56.72 42.66 29.73 o -1 -13 1 295.73 284.78 26.48 o 0 -13 1 295.48 319.88 22.66 o 1 -13 1 106.68 176.20 22.46 o 2 -13 1 494.16 556.58 30.59 o 3 -13 1 112.84 301.62 52.09 o 4 -13 1 52.76 74.34 28.24 o 5 -13 1 183.22 226.62 14.49 o 6 -13 1 589.67 588.62 30.91 o 7 -13 1 403.96 441.70 26.42 o 8 -13 1 506.19 683.80 84.19 o 9 -13 1 28.20 71.18 22.83 o 10 -13 1 302.59 270.00 30.83 o 11 -13 1 805.05 668.92 46.77 o 12 -13 1 123.65 36.95 42.91 o -4 -12 1 5.92 46.70 44.73 o -3 -12 1 187.13 206.43 22.15 o -2 -12 1 263.68 282.03 36.64 o -1 -12 1 454.92 573.49 50.72 o 0 -12 1 2.43 14.90 16.59 o 1 -12 1 362.81 411.13 65.57 o 2 -12 1 1725.58 1894.53 47.55 o 3 -12 1 85.70 127.57 12.34 o 4 -12 1 620.14 800.54 66.17 o 5 -12 1 21.83 49.83 28.79 o 6 -12 1 621.36 671.10 31.54 o 7 -12 1 1587.95 1587.50 82.57 o 8 -12 1 1212.52 1231.00 81.39 o 9 -12 1 3.43 -30.10 35.68 o 10 -12 1 5.56 -28.94 31.55 o 11 -12 1 361.63 301.72 44.60 o 12 -12 1 409.05 283.22 53.93 o -5 -11 1 146.62 67.09 41.53 o -4 -11 1 130.34 106.30 26.81 o -3 -11 1 46.49 26.40 18.93 o -2 -11 1 923.02 1027.80 35.77 o -1 -11 1 901.75 998.34 72.20 o 0 -11 1 25.04 12.18 15.28 o 1 -11 1 4.61 76.12 35.92 o 2 -11 1 60.04 141.02 27.06 o 3 -11 1 1097.72 1201.86 31.23 o 4 -11 1 1908.59 2101.62 56.50 o 5 -11 1 10.31 36.50 12.70 o 6 -11 1 33.32 -11.94 29.12 o 7 -11 1 1412.54 1362.32 76.05 o 8 -11 1 1214.65 1153.55 66.83 o 9 -11 1 15.67 -9.60 26.94 o 10 -11 1 323.16 320.48 78.82 o 11 -11 1 261.57 257.58 33.18 o 12 -11 1 650.08 498.13 40.99 o -6 -10 1 58.44 50.60 38.28 o -5 -10 1 935.39 1000.98 52.46 o -4 -10 1 102.98 108.55 23.10 o -3 -10 1 3.33 6.70 13.29 o -2 -10 1 17.41 26.44 15.91 o -1 -10 1 99.42 134.02 30.41 o 0 -10 1 445.14 493.34 62.77 o 1 -10 1 1591.77 2133.48 197.47 o 2 -10 1 170.79 187.32 11.03 o 3 -10 1 547.74 567.86 15.59 o 4 -10 1 3602.90 3675.15 100.37 o 5 -10 1 191.51 194.44 42.13 o 6 -10 1 160.36 173.40 30.10 o 7 -10 1 160.21 129.94 29.92 o 8 -10 1 259.10 300.70 34.26 o 9 -10 1 634.31 563.58 32.30 o 10 -10 1 1641.73 1595.33 152.35 o 11 -10 1 78.82 86.13 76.74 o 12 -10 1 175.03 169.44 27.06 o 13 -10 1 250.84 94.70 42.15 o -7 -9 1 47.54 -28.52 39.79 o -6 -9 1 169.08 145.37 35.97 o -5 -9 1 1190.28 1242.20 55.25 o -4 -9 1 152.36 135.23 12.67 o -3 -9 1 725.50 823.00 44.03 o -2 -9 1 454.09 507.16 43.14 o -1 -9 1 1.14 -5.37 12.23 o 0 -9 1 3366.08 3783.88 142.11 o 1 -9 1 3593.07 3835.58 85.55 o 2 -9 1 68.95 62.01 8.03 o 3 -9 1 242.19 263.34 28.96 o 4 -9 1 424.14 428.41 38.06 o 5 -9 1 333.26 338.93 25.34 o 6 -9 1 4285.08 4527.20 173.76 o 7 -9 1 1492.50 1428.38 59.42 o 8 -9 1 222.00 194.78 38.09 o 9 -9 1 678.70 682.06 24.20 o 10 -9 1 1453.62 1404.84 48.56 o 11 -9 1 85.99 92.44 12.98 o 12 -9 1 32.47 23.76 16.11 o 13 -9 1 196.13 155.55 32.97 o -8 -8 1 470.67 488.88 52.75 o -7 -8 1 68.25 44.80 35.01 o -6 -8 1 0.04 -40.97 40.97 o -5 -8 1 668.56 741.20 36.19 o -4 -8 1 223.74 204.41 25.47 o -3 -8 1 2548.58 2868.56 96.38 o -2 -8 1 899.48 937.14 27.52 o -1 -8 1 275.81 290.37 17.96 o 0 -8 1 2562.69 2561.60 58.94 o 1 -8 1 3421.78 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