#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:33:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181251 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232988.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232988_Fobs loop_ _publ_author_name 'Pourayoubi, Mehrdad' 'Rheingold, Arnold L.' 'Chen, Chao' 'Karimi Ahmadabad, Fatemeh' 'Tarahhomi, Atekeh' _publ_section_title ; O-Phenyl (tert-butylamido)(p-tolylamido)phosphinate ; _journal_coeditor_code WM2550 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3405 _journal_page_last o3406 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.332 _cell_angle_gamma 90.000 _cell_length_a 11.4116 _cell_length_b 9.5189 _cell_length_c 15.7682 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.7504 _cod_data_source_file wm2550Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21n in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 201.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 40721.14 44448.78 1004.99 o 4 0 0 7.94 27.20 8.12 o 6 0 0 3.30 0.00 66.40 o 8 0 0 769.17 758.28 44.21 o 10 0 0 267.04 214.11 31.09 o 12 0 0 39.88 81.23 24.72 o 14 0 0 80.74 88.65 20.84 o 1 1 0 10.17 13.42 2.12 o 2 1 0 747.14 582.95 13.48 o 3 1 0 1604.62 1525.60 37.70 o 4 1 0 103.02 232.82 10.60 o 5 1 0 1111.34 1045.49 25.86 o 6 1 0 34.95 40.27 9.18 o 7 1 0 2178.40 2159.09 57.83 o 8 1 0 2447.83 2365.15 66.34 o 9 1 0 1448.42 1382.08 49.56 o 10 1 0 2172.08 2164.57 80.08 o 11 1 0 178.46 194.29 20.49 o 12 1 0 20.49 43.44 14.48 o 13 1 0 0.48 12.01 13.77 o 14 1 0 13.12 19.42 11.30 o 0 2 0 11070.72 10432.42 406.30 o 1 2 0 40373.87 40647.21 724.21 o 2 2 0 146.85 169.64 9.54 o 3 2 0 2491.94 2239.55 98.75 o 4 2 0 253.45 305.38 11.31 o 5 2 0 272.61 261.54 10.96 o 6 2 0 209.72 167.13 12.37 o 7 2 0 476.30 469.11 23.69 o 8 2 0 1799.78 1644.69 50.67 o 9 2 0 210.15 223.28 26.14 o 10 2 0 278.30 255.10 24.03 o 11 2 0 7.09 9.54 7.06 o 12 2 0 62.59 82.30 17.66 o 13 2 0 2.22 15.89 14.13 o 14 2 0 0.05 9.89 11.65 o 1 3 0 400.41 795.91 27.95 o 2 3 0 188.41 148.43 9.90 o 3 3 0 26.92 40.27 4.24 o 4 3 0 1067.69 1155.77 27.63 o 5 3 0 26.72 60.75 5.65 o 6 3 0 495.30 515.11 30.40 o 7 3 0 1317.25 1357.08 49.92 o 8 3 0 402.08 364.02 21.20 o 9 3 0 307.35 279.49 32.51 o 10 3 0 51.28 98.19 17.31 o 11 3 0 251.07 207.38 21.20 o 12 3 0 0.02 22.25 14.48 o 13 3 0 9.29 1.77 13.07 o 0 4 0 1404.42 1270.24 68.11 o 1 4 0 9.65 65.34 5.30 o 2 4 0 512.89 478.55 16.27 o 3 4 0 770.63 823.15 49.19 o 4 4 0 192.15 221.19 11.66 o 5 4 0 440.44 387.80 14.14 o 6 4 0 191.88 187.96 12.37 o 7 4 0 2809.40 2828.75 83.76 o 8 4 0 5.15 62.16 12.71 o 9 4 0 1063.04 1218.62 57.31 o 10 4 0 0.05 14.48 12.36 o 11 4 0 120.37 107.03 18.37 o 12 4 0 1.60 37.44 15.89 o 13 4 0 150.22 200.64 22.61 o 1 5 0 154.85 291.48 16.25 o 2 5 0 313.71 232.21 16.26 o 3 5 0 204.08 175.25 19.08 o 4 5 0 24.97 25.08 5.65 o 5 5 0 229.13 239.56 16.25 o 6 5 0 145.99 134.95 15.54 o 7 5 0 37.19 10.60 10.60 o 8 5 0 0.04 3.53 6.71 o 9 5 0 124.09 121.87 20.84 o 10 5 0 232.50 249.06 24.73 o 11 5 0 33.59 47.68 10.24 o 12 5 0 133.65 161.78 20.84 o 13 5 0 5.93 2.47 294.55 o 0 6 0 239.05 198.23 25.09 o 1 6 0 33.46 23.31 4.59 o 2 6 0 4.12 3.18 4.24 o 3 6 0 159.17 220.80 27.91 o 4 6 0 112.37 100.32 14.48 o 5 6 0 126.05 95.73 10.24 o 6 6 0 624.73 702.82 44.19 o 7 6 0 56.78 34.61 21.55 o 8 6 0 763.16 759.45 48.44 o 9 6 0 20.10 27.55 17.31 o 10 6 0 86.58 64.28 21.19 o 11 6 0 29.27 13.07 10.24 o 12 6 0 43.46 42.74 21.19 o 1 7 0 144.57 139.54 14.13 o 2 7 0 290.53 319.79 20.85 o 3 7 0 22.44 32.85 9.54 o 4 7 0 16.02 13.07 9.54 o 5 7 0 64.29 32.85 8.12 o 6 7 0 326.04 313.77 29.68 o 7 7 0 136.40 136.70 21.90 o 8 7 0 7.47 18.72 9.18 o 9 7 0 13.71 32.14 18.37 o 10 7 0 247.78 282.27 32.15 o 11 7 0 5.86 14.13 13.42 o 0 8 0 1968.75 2391.13 248.71 o 1 8 0 16.86 23.31 10.60 o 2 8 0 256.04 176.66 28.27 o 3 8 0 10.33 0.00 12.01 o 4 8 0 336.18 357.59 28.62 o 5 8 0 0.02 7.06 7.06 o 6 8 0 134.48 136.70 20.13 o 7 8 0 110.62 107.38 21.55 o 8 8 0 8.36 13.07 9.89 o 9 8 0 69.15 97.48 21.55 o 10 8 0 1.43 7.77 19.78 o 1 9 0 31.82 81.94 21.19 o 2 9 0 61.03 44.15 16.25 o 3 9 0 52.45 64.28 12.72 o 4 9 0 134.15 141.65 20.49 o 5 9 0 20.55 18.37 16.25 o 6 9 0 0.60 0.00 12.71 o 7 9 0 11.51 27.90 17.31 o 8 9 0 31.79 16.25 11.30 o 9 9 0 17.77 18.72 20.13 o 0 10 0 166.68 121.17 38.86 o 1 10 0 324.93 306.69 35.33 o 2 10 0 31.85 19.78 13.42 o 3 10 0 265.32 264.62 30.74 o 4 10 0 61.63 56.87 16.95 o 5 10 0 114.10 110.91 27.55 o 6 10 0 4.95 9.18 16.95 o 7 10 0 17.21 5.65 22.60 o 8 10 0 27.20 3.53 25.78 o 1 11 0 12.94 8.12 13.77 o 2 11 0 15.99 1.41 13.42 o 3 11 0 44.36 51.21 16.60 o 4 11 0 19.01 40.97 16.95 o 5 11 0 31.75 12.36 21.90 o 6 11 0 22.13 17.66 27.55 o 7 11 0 74.07 97.13 375.10 o 0 12 0 72.85 58.28 23.66 o 1 12 0 6.81 7.77 30.73 o 2 12 0 37.65 0.00 23.31 o 3 12 0 101.54 110.91 38.50 o 4 12 0 4.79 33.90 1098.38 o -13 0 1 120.26 138.11 24.73 o -11 0 1 55.86 46.98 14.13 o -9 0 1 299.49 334.98 60.07 o -7 0 1 287.68 295.44 25.09 o -5 0 1 263.34 370.77 23.33 o -3 0 1 3876.44 3292.18 151.15 o -1 0 1 13988.43 13870.64 318.01 o 1 0 1 4118.22 3916.39 87.23 o 3 0 1 5498.53 4989.76 155.51 o 5 0 1 775.32 885.19 33.62 o 7 0 1 170.90 202.79 21.90 o 9 0 1 203.25 223.63 40.28 o 11 0 1 125.27 98.20 19.78 o 13 0 1 73.80 96.07 21.90 o -14 1 1 0.86 18.01 9.54 o -13 1 1 121.65 126.81 20.13 o -12 1 1 29.10 53.33 14.83 o -11 1 1 91.41 103.49 16.25 o -10 1 1 70.36 91.13 14.83 o -9 1 1 127.44 161.08 19.78 o -8 1 1 592.06 635.00 28.64 o -7 1 1 1380.70 1382.80 46.75 o -6 1 1 2780.92 2925.57 61.87 o -5 1 1 5258.62 5291.62 98.23 o -4 1 1 2127.62 2038.25 43.06 o -3 1 1 3.89 10.24 4.24 o -2 1 1 178.41 158.40 6.36 o -1 1 1 734.27 623.92 16.00 o 0 1 1 101.74 123.04 7.78 o 1 1 1 4008.26 3490.61 73.59 o 2 1 1 1080.23 1049.92 22.03 o 3 1 1 131.20 181.28 18.02 o 4 1 1 1703.13 1739.16 36.23 o 5 1 1 2096.47 1990.77 45.11 o 6 1 1 2348.57 2371.97 52.20 o 7 1 1 2344.79 2215.97 58.19 o 8 1 1 408.75 428.71 22.62 o 9 1 1 1251.22 1235.77 53.79 o 10 1 1 75.03 122.92 24.37 o 11 1 1 132.74 148.71 18.37 o 12 1 1 57.89 74.17 16.95 o 13 1 1 56.33 73.47 15.19 o 14 1 1 7.74 31.79 13.42 o -14 2 1 52.59 49.80 13.77 o -13 2 1 18.32 43.79 15.54 o -12 2 1 6.99 12.01 19.78 o -11 2 1 137.31 177.33 18.72 o -10 2 1 3.08 7.42 10.24 o -9 2 1 507.17 492.03 37.47 o -8 2 1 31.70 43.09 9.18 o -7 2 1 3.56 7.06 5.65 o -6 2 1 317.85 403.98 30.75 o -5 2 1 136.59 184.42 7.77 o -4 2 1 2134.87 2188.57 44.80 o -3 2 1 62.37 90.79 7.42 o -2 2 1 4274.81 4198.09 79.62 o -1 2 1 239.27 235.18 12.73 o 0 2 1 1285.40 1161.47 50.53 o 1 2 1 132.29 153.39 11.31 o 2 2 1 4711.40 4460.82 91.19 o 3 2 1 405.28 434.69 15.21 o 4 2 1 1648.42 1606.34 38.69 o 5 2 1 219.35 231.81 10.95 o 6 2 1 245.64 242.76 26.15 o 7 2 1 92.41 97.85 11.30 o 8 2 1 300.29 276.68 18.37 o 9 2 1 429.74 462.62 39.23 o 10 2 1 113.75 111.97 21.19 o 11 2 1 29.84 12.01 8.83 o 12 2 1 10.37 52.27 16.25 o 13 2 1 23.69 21.90 14.83 o 14 2 1 8.01 42.03 70.28 o -14 3 1 349.38 463.90 46.28 o -13 3 1 30.84 53.33 15.89 o -12 3 1 233.86 264.25 27.20 o -11 3 1 42.80 41.32 11.66 o -10 3 1 70.88 81.94 14.13 o -9 3 1 4.33 21.19 10.24 o -8 3 1 619.06 619.78 25.81 o -7 3 1 259.35 281.27 15.90 o -6 3 1 378.79 469.40 17.32 o -5 3 1 1067.76 1140.17 25.85 o -4 3 1 193.97 217.32 10.25 o -3 3 1 1381.78 1413.94 52.50 o -2 3 1 7042.98 6449.20 122.37 o -1 3 1 46.29 17.66 3.53 o 0 3 1 4673.84 4637.38 166.58 o 1 3 1 3202.20 2685.19 64.35 o 2 3 1 801.59 795.07 26.92 o 3 3 1 1744.97 1852.60 52.90 o 4 3 1 2.51 52.62 5.65 o 5 3 1 93.20 135.29 8.83 o 6 3 1 253.31 292.58 16.25 o 7 3 1 70.25 84.77 9.89 o 8 3 1 482.94 494.84 27.92 o 9 3 1 154.88 89.02 16.60 o 10 3 1 482.82 515.63 37.11 o 11 3 1 0.51 10.95 8.12 o 12 3 1 131.22 152.24 20.13 o 13 3 1 9.54 24.02 14.83 o -13 4 1 9.76 17.66 18.01 o -12 4 1 112.27 139.88 20.84 o -11 4 1 0.27 12.36 7.77 o -10 4 1 338.73 353.70 31.80 o -9 4 1 5.40 5.30 10.95 o -8 4 1 369.46 390.49 22.62 o -7 4 1 132.30 172.74 25.79 o -6 4 1 82.83 63.58 15.90 o -5 4 1 353.53 379.60 16.61 o -4 4 1 123.79 92.91 7.77 o -3 4 1 979.28 1109.01 44.26 o -2 4 1 152.32 174.90 9.89 o -1 4 1 54.97 106.68 9.18 o 0 4 1 224.77 429.76 21.91 o 1 4 1 68.96 80.19 6.01 o 2 4 1 62.78 58.28 8.12 o 3 4 1 466.72 518.37 21.22 o 4 4 1 143.16 113.41 9.19 o 5 4 1 600.99 640.05 21.22 o 6 4 1 670.92 672.24 44.20 o 7 4 1 0.25 10.24 14.48 o 8 4 1 214.85 244.48 20.49 o 9 4 1 194.73 221.15 21.20 o 10 4 1 150.51 209.12 25.08 o 11 4 1 34.77 18.72 9.54 o 12 4 1 18.22 23.66 19.42 o 13 4 1 38.43 15.89 19.43 o -13 5 1 192.36 219.72 45.92 o -12 5 1 70.83 95.01 18.01 o -11 5 1 110.21 99.96 16.25 o -10 5 1 17.97 25.78 14.48 o -9 5 1 5.75 26.84 16.25 o -8 5 1 210.22 195.72 19.08 o -7 5 1 85.38 80.54 13.07 o -6 5 1 102.44 103.85 18.72 o -5 5 1 39.68 33.91 6.00 o -4 5 1 220.40 242.39 14.13 o -3 5 1 147.28 163.57 11.66 o -2 5 1 1230.22 1422.14 36.84 o -1 5 1 246.76 296.85 12.02 o 0 5 1 147.27 173.12 12.01 o 1 5 1 410.58 431.66 14.85 o 2 5 1 967.95 1059.09 43.89 o 3 5 1 35.10 61.10 7.77 o 4 5 1 33.86 24.72 6.71 o 5 5 1 195.78 190.08 17.31 o 6 5 1 83.67 105.97 15.54 o 7 5 1 3.26 7.06 19.42 o 8 5 1 5.31 40.97 8.83 o 9 5 1 200.16 233.51 23.32 o 10 5 1 64.25 23.66 15.89 o 11 5 1 132.73 136.35 16.60 o 12 5 1 41.67 33.20 16.60 o -12 6 1 9.15 0.00 21.19 o -11 6 1 23.43 33.91 12.01 o -10 6 1 30.73 49.80 16.60 o -9 6 1 86.00 69.94 22.96 o -8 6 1 173.75 158.61 16.25 o -7 6 1 63.78 97.84 19.43 o -6 6 1 183.30 172.40 27.20 o -5 6 1 269.36 235.68 18.02 o -4 6 1 306.24 331.47 22.26 o -3 6 1 96.73 86.54 10.24 o -2 6 1 229.07 240.98 13.78 o -1 6 1 55.93 54.75 6.71 o 0 6 1 45.83 69.23 8.48 o 1 6 1 366.84 365.81 23.33 o 2 6 1 52.77 50.86 8.48 o 3 6 1 5.56 0.00 19.78 o 4 6 1 91.01 92.19 12.01 o 5 6 1 386.10 382.74 23.32 o 6 6 1 1.63 0.00 12.01 o 7 6 1 172.75 231.39 22.26 o 8 6 1 11.77 3.18 7.06 o 9 6 1 66.49 128.57 23.66 o 10 6 1 10.01 14.83 14.13 o 11 6 1 13.59 9.54 10.60 o 12 6 1 24.24 17.31 28.96 o -11 7 1 153.27 140.59 23.67 o -10 7 1 1.05 32.85 16.95 o -9 7 1 0.97 1.77 17.66 o -8 7 1 146.99 163.91 17.66 o -7 7 1 14.44 1.77 13.07 o -6 7 1 198.65 231.75 23.32 o -5 7 1 0.70 3.53 5.65 o -4 7 1 16.82 18.37 9.89 o -3 7 1 0.34 12.36 7.77 o -2 7 1 11.64 12.71 5.65 o -1 7 1 195.40 224.70 16.96 o 0 7 1 101.01 132.82 16.25 o 1 7 1 336.32 374.24 22.97 o 2 7 1 51.91 45.21 10.24 o 3 7 1 347.46 368.58 28.98 o 4 7 1 201.19 203.85 16.60 o 5 7 1 180.41 168.16 15.19 o 6 7 1 316.06 312.35 29.68 o 7 7 1 75.30 203.10 40.62 o 8 7 1 0.06 0.35 9.18 o 9 7 1 37.85 26.14 18.37 o 10 7 1 32.04 8.48 16.95 o 11 7 1 21.21 26.14 14.83 o -10 8 1 42.38 13.42 22.60 o -9 8 1 3.43 55.45 19.42 o -8 8 1 20.03 6.36 8.48 o -7 8 1 87.19 77.35 19.07 o -6 8 1 1.08 0.00 20.48 o -5 8 1 289.55 244.15 19.79 o -4 8 1 46.55 40.97 12.01 o -3 8 1 921.12 945.03 67.55 o -2 8 1 0.25 4.94 8.83 o -1 8 1 250.00 304.56 26.15 o 0 8 1 8.57 7.42 14.13 o 1 8 1 39.58 35.67 12.01 o 2 8 1 54.25 31.08 10.24 o 3 8 1 24.81 19.78 21.90 o 4 8 1 14.69 18.72 10.60 o 5 8 1 1.46 2.47 8.12 o 6 8 1 44.55 22.25 13.77 o 7 8 1 134.06 164.96 23.67 o 8 8 1 4.51 26.14 10.24 o 9 8 1 55.36 148.34 35.67 o 10 8 1 0.04 20.48 19.78 o -10 9 1 15.87 0.00 103.48 o -9 9 1 17.77 84.76 23.66 o -8 9 1 0.79 12.71 11.30 o -7 9 1 38.76 5.30 19.43 o -6 9 1 19.53 10.95 14.13 o -5 9 1 132.46 125.40 22.96 o -4 9 1 38.05 28.61 13.07 o -3 9 1 19.68 21.90 10.95 o -2 9 1 5.80 12.71 13.77 o -1 9 1 289.70 221.18 26.15 o 0 9 1 17.65 21.19 12.01 o 1 9 1 149.97 286.13 32.50 o 2 9 1 38.44 37.44 12.71 o 3 9 1 190.35 180.52 24.73 o 4 9 1 97.05 97.14 15.54 o 5 9 1 196.53 172.04 22.96 o 6 9 1 137.58 226.78 26.49 o 7 9 1 55.62 24.72 22.25 o 8 9 1 42.47 34.61 12.36 o 9 9 1 49.78 88.65 23.31 o -8 10 1 21.72 13.07 25.43 o -7 10 1 4.45 24.02 34.26 o -6 10 1 12.04 0.00 21.90 o -5 10 1 17.98 17.31 17.31 o -4 10 1 190.78 198.53 24.37 o -3 10 1 2.25 1.06 13.07 o -2 10 1 262.36 224.70 30.03 o -1 10 1 1.34 13.77 14.83 o 0 10 1 100.32 94.66 22.25 o 1 10 1 5.69 10.60 14.48 o 2 10 1 93.08 69.58 19.07 o 3 10 1 5.70 27.90 11.30 o 4 10 1 67.07 123.62 24.72 o 5 10 1 3.80 3.53 16.95 o 6 10 1 62.54 78.76 21.90 o 7 10 1 0.49 0.00 19.78 o 8 10 1 0.54 0.00 25.08 o -6 11 1 15.18 22.96 19.78 o -5 11 1 16.52 10.95 23.31 o -4 11 1 3.49 34.26 21.54 o -3 11 1 4.60 7.42 14.83 o -2 11 1 18.96 18.72 14.83 o -1 11 1 0.08 21.90 13.77 o 0 11 1 0.80 5.65 12.71 o 1 11 1 1.33 0.00 13.77 o 2 11 1 0.04 8.48 14.13 o 3 11 1 1.71 19.42 14.13 o 4 11 1 69.64 55.45 22.60 o 5 11 1 21.51 39.56 23.66 o 6 11 1 54.06 49.45 345.07 o -3 12 1 44.24 36.03 27.20 o -2 12 1 0.15 0.00 24.02 o -1 12 1 33.22 0.00 20.84 o 0 12 1 17.43 0.00 16.95 o 1 12 1 16.54 8.48 24.02 o 2 12 1 50.91 66.75 27.90 o 3 12 1 26.63 54.39 27.55 o 4 12 1 19.89 110.90 1247.08 o -14 0 2 5.69 2.12 12.01 o -12 0 2 15.06 25.43 31.08 o -10 0 2 550.91 496.28 42.42 o -8 0 2 218.50 307.39 30.03 o -6 0 2 11.97 22.25 5.30 o -4 0 2 3643.01 3096.18 81.96 o -2 0 2 328.84 319.26 12.03 o 0 0 2 7108.62 7251.02 278.75 o 2 0 2 2816.83 2469.00 62.35 o 4 0 2 3308.42 3240.17 84.93 o 6 0 2 1253.88 1260.13 55.25 o 8 0 2 0.21 7.06 7.77 o 10 0 2 55.47 43.44 18.72 o 12 0 2 3.11 24.02 30.73 o -14 1 2 121.87 159.66 23.31 o -13 1 2 9.81 20.13 13.07 o -12 1 2 48.31 44.50 15.19 o -11 1 2 2.16 7.77 6.36 o -10 1 2 330.38 369.61 27.21 o -9 1 2 76.66 109.85 14.13 o -8 1 2 278.27 320.50 20.14 o -7 1 2 240.54 244.87 14.13 o -6 1 2 61.40 63.93 7.77 o -5 1 2 41.36 234.89 10.95 o -4 1 2 77.76 184.41 8.83 o -3 1 2 226.86 284.95 19.44 o -2 1 2 42.13 40.98 4.59 o -1 1 2 55.81 68.54 4.59 o 0 1 2 3105.25 2955.64 107.02 o 1 1 2 404.09 315.48 11.68 o 2 1 2 193.30 244.62 9.90 o 3 1 2 934.14 880.02 25.87 o 4 1 2 931.78 861.37 21.25 o 5 1 2 414.68 364.16 12.37 o 6 1 2 115.00 112.34 19.43 o 7 1 2 16.54 28.25 9.54 o 8 1 2 213.31 286.88 20.49 o 9 1 2 12.85 53.68 15.89 o 10 1 2 247.56 282.64 23.32 o 11 1 2 8.04 19.78 8.12 o 12 1 2 116.70 148.71 20.84 o 13 1 2 96.79 129.98 18.37 o 14 1 2 160.89 242.32 640.42 o -14 2 2 6.80 8.48 10.60 o -13 2 2 5.84 3.53 13.77 o -12 2 2 66.02 84.77 18.72 o -11 2 2 8.31 9.89 5.65 o -10 2 2 479.55 456.63 33.22 o -9 2 2 7.04 0.00 13.07 o -8 2 2 784.98 713.37 28.65 o -7 2 2 644.29 677.57 28.29 o -6 2 2 0.20 5.30 2.47 o -5 2 2 3192.10 2964.71 52.36 o -4 2 2 13.57 19.07 3.53 o -3 2 2 5023.78 5122.69 129.55 o -2 2 2 888.44 759.90 21.98 o -1 2 2 234.27 259.90 12.73 o 0 2 2 3864.59 3538.90 128.25 o 1 2 2 156.05 151.27 11.31 o 2 2 2 223.49 200.43 10.25 o 3 2 2 2317.01 1946.07 62.99 o 4 2 2 3.92 5.65 2.83 o 5 2 2 1758.00 2097.21 45.40 o 6 2 2 110.97 123.64 12.72 o 7 2 2 28.10 21.90 6.71 o 8 2 2 853.63 825.15 35.37 o 9 2 2 47.01 123.62 18.37 o 10 2 2 33.48 27.20 13.42 o 11 2 2 0.14 5.30 7.42 o 12 2 2 0.95 14.48 17.66 o 13 2 2 10.26 9.18 13.42 o -14 3 2 8.25 21.19 17.31 o -13 3 2 76.73 86.54 15.89 o -12 3 2 2.02 26.13 15.19 o -11 3 2 137.28 144.12 18.02 o -10 3 2 20.96 6.36 12.71 o -9 3 2 27.51 70.99 11.30 o -8 3 2 36.37 51.57 7.77 o -7 3 2 172.92 184.42 16.96 o -6 3 2 1.04 84.41 6.36 o -5 3 2 237.97 394.37 15.55 o -4 3 2 1071.34 1501.90 41.80 o -3 3 2 0.69 4.24 3.88 o -2 3 2 83.99 82.31 6.36 o -1 3 2 687.10 1081.04 37.53 o 0 3 2 901.49 778.95 51.03 o 1 3 2 479.47 429.14 23.00 o 2 3 2 1663.94 1530.41 49.71 o 3 3 2 1055.48 1109.14 62.35 o 4 3 2 561.20 580.38 19.10 o 5 3 2 818.60 829.71 24.41 o 6 3 2 270.14 242.05 16.61 o 7 3 2 1673.29 1704.57 62.70 o 8 3 2 600.48 539.47 28.99 o 9 3 2 18.22 0.00 24.37 o 10 3 2 43.28 37.09 12.36 o 11 3 2 90.89 111.62 17.31 o 12 3 2 0.00 22.25 15.89 o 13 3 2 212.35 261.77 23.67 o -14 4 2 12.71 33.55 19.07 o -13 4 2 63.61 72.05 16.95 o -12 4 2 0.25 0.00 15.54 o -11 4 2 97.27 97.84 18.72 o -10 4 2 20.70 47.33 16.25 o -9 4 2 19.97 27.20 13.07 o -8 4 2 61.21 77.00 10.95 o -7 4 2 2133.56 2035.01 54.95 o -6 4 2 209.73 264.64 15.19 o -5 4 2 733.54 736.84 23.35 o -4 4 2 1032.93 993.82 30.09 o -3 4 2 2629.62 3071.40 82.15 o -2 4 2 34.04 29.67 6.00 o -1 4 2 0.09 7.42 2.83 o 0 4 2 1529.52 1472.33 74.50 o 1 4 2 190.47 301.78 18.73 o 2 4 2 52.61 35.68 6.71 o 3 4 2 1101.51 976.35 84.64 o 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