#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:33:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181251 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232989.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232989_Fobs loop_ _publ_author_name 'Guo, Jing-Ke' 'Wen, Yi-Hang' _publ_section_title ; Tetrakis[\m-3-(3-hydroxyphenyl)propenoato]bis{aqua(2,2'-bipyridine)[3-(3-hydroxyphenyl)propenoato]neodymium(III)} 2,2'-bipyridine disolvate dihydrate ; _journal_coeditor_code WM2552 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1907 _journal_page_last m1908 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.274 _cell_angle_gamma 90.000 _cell_length_a 10.7333 _cell_length_b 28.9077 _cell_length_c 14.3276 _exptl_crystal_F_000 1956.00 _reflns_d_resolution_high 0.7671 _cod_data_source_file wm2552Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' T in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 38011.77 37714.97 1584.78 o 3 0 0 42614.90 38755.61 1679.63 o 4 0 0 21699.50 20071.61 993.63 o 5 0 0 53677.36 55410.14 2446.54 o 6 0 0 28356.91 27474.94 969.92 o 7 0 0 1629.18 1894.83 182.25 o 8 0 0 1648.52 1846.55 186.51 o 9 0 0 3857.56 3771.20 287.19 o 10 0 0 1693.85 2163.37 481.42 o 11 0 0 648.44 557.04 245.24 o 12 0 0 1706.11 1819.93 414.34 o 2 1 0 508.43 172.75 215.39 o 3 1 0 142.68 104.32 44.53 o 4 1 0 84.42 55.74 50.67 o 5 1 0 1413.79 1583.92 144.23 o 6 1 0 2869.46 3060.69 228.12 o 7 1 0 148.74 26.65 80.76 o 8 1 0 0.92 15.48 63.32 o 9 1 0 92.68 78.05 72.92 o 10 1 0 1040.21 715.48 156.28 o 11 1 0 141.69 50.23 131.40 o 12 1 0 0.03 288.29 237.86 o 0 2 0 72471.46 65425.09 2522.98 o 1 2 0 5357.58 5523.90 106.98 o 2 2 0 18704.28 20536.53 648.39 o 3 2 0 41622.04 40716.41 1241.81 o 4 2 0 10452.34 10431.53 749.46 o 5 2 0 13308.37 13754.83 381.37 o 6 2 0 15905.15 16046.30 450.75 o 7 2 0 1038.44 1179.77 127.29 o 8 2 0 1299.48 1272.99 216.66 o 9 2 0 5168.42 5324.60 236.69 o 10 2 0 1482.84 1037.66 135.62 o 11 2 0 1411.27 1416.79 222.34 o 12 2 0 2423.54 2350.78 537.38 o 1 3 0 8136.93 8096.96 134.20 o 2 3 0 2526.02 2475.79 61.22 o 3 3 0 1995.77 2113.76 71.98 o 4 3 0 3546.77 3603.05 179.91 o 5 3 0 23.78 12.06 48.26 o 6 3 0 245.31 180.26 65.44 o 7 3 0 18.15 91.85 73.49 o 8 3 0 373.49 244.54 91.60 o 9 3 0 414.82 445.38 96.64 o 10 3 0 1026.04 763.46 135.12 o 11 3 0 341.86 188.62 105.99 o 12 3 0 135.38 16.64 206.73 o 13 3 0 61.73 -153.51 308.99 o 0 4 0 66924.08 65595.47 1441.84 o 1 4 0 28706.73 29127.03 376.09 o 2 4 0 53465.77 53755.95 889.77 o 3 4 0 24436.59 24575.51 375.65 o 4 4 0 2643.15 2480.65 97.47 o 5 4 0 18638.07 17722.72 441.24 o 6 4 0 24573.86 24738.32 595.41 o 7 4 0 1407.67 1223.60 224.18 o 8 4 0 4820.44 4897.19 240.92 o 9 4 0 6171.94 6194.38 322.51 o 10 4 0 189.15 234.96 78.35 o 11 4 0 1241.31 1154.96 253.62 o 12 4 0 1966.80 2262.21 183.90 o 13 4 0 168.09 -83.11 253.29 o 1 5 0 4236.02 4234.57 79.78 o 2 5 0 6362.27 6847.19 117.40 o 3 5 0 2245.93 2375.26 66.72 o 4 5 0 4419.09 4283.88 120.84 o 5 5 0 1461.24 1327.39 69.54 o 6 5 0 1633.96 1942.93 104.40 o 7 5 0 1566.92 1493.71 203.79 o 8 5 0 2179.04 2121.93 244.50 o 9 5 0 48.97 47.17 94.29 o 10 5 0 3067.27 2760.05 361.55 o 11 5 0 558.49 656.47 132.22 o 12 5 0 109.71 78.92 123.57 o 13 5 0 341.86 428.90 284.42 o 0 6 0 28749.12 27910.78 682.45 o 1 6 0 63155.68 63536.97 848.63 o 2 6 0 15849.84 15379.25 211.92 o 3 6 0 48019.93 46808.47 650.04 o 4 6 0 2084.53 1970.12 66.61 o 5 6 0 10235.67 10609.71 209.91 o 6 6 0 27944.67 30055.14 511.20 o 7 6 0 2185.78 2298.74 96.31 o 8 6 0 662.81 713.42 108.73 o 9 6 0 5085.92 5198.41 196.13 o 10 6 0 193.52 147.15 67.35 o 11 6 0 477.37 411.51 69.44 o 12 6 0 1417.58 1241.34 136.84 o 13 6 0 286.64 46.70 249.57 o 1 7 0 1087.14 1227.80 56.89 o 2 7 0 29559.20 28437.01 338.49 o 3 7 0 1869.65 1897.92 56.01 o 4 7 0 32131.88 31616.29 437.13 o 5 7 0 1600.06 1581.67 67.41 o 6 7 0 1712.14 1798.08 97.31 o 7 7 0 6073.53 6301.27 161.99 o 8 7 0 6444.23 6593.54 237.41 o 9 7 0 925.37 802.95 101.81 o 10 7 0 1800.05 1997.63 114.34 o 11 7 0 305.22 370.80 74.40 o 12 7 0 38.07 -21.96 118.55 o 13 7 0 820.50 1047.93 623.59 o 0 8 0 13241.13 13540.64 326.30 o 1 8 0 848.93 994.68 44.40 o 2 8 0 905.84 968.05 42.35 o 3 8 0 21704.45 22285.88 318.61 o 4 8 0 10327.20 10424.78 168.06 o 5 8 0 4816.13 4656.58 100.44 o 6 8 0 15211.05 15104.01 283.47 o 7 8 0 1855.33 1921.28 75.95 o 8 8 0 1073.71 1147.23 132.91 o 9 8 0 2109.62 2182.94 247.80 o 10 8 0 16.80 64.94 62.34 o 11 8 0 890.08 678.37 98.64 o 12 8 0 1125.53 1253.02 198.78 o 1 9 0 1931.45 1829.61 61.35 o 2 9 0 16955.68 16508.03 227.45 o 3 9 0 3689.73 4031.89 90.11 o 4 9 0 3942.50 3657.78 92.46 o 5 9 0 10494.32 10093.13 171.48 o 6 9 0 9.14 36.09 30.92 o 7 9 0 7382.67 7317.83 192.96 o 8 9 0 2841.43 2740.42 163.98 o 9 9 0 26.09 -40.96 53.66 o 10 9 0 2337.98 2480.83 206.41 o 11 9 0 828.30 856.09 101.94 o 12 9 0 65.24 41.73 150.07 o 0 10 0 11568.36 11410.57 299.84 o 1 10 0 2789.80 2701.33 77.17 o 2 10 0 823.07 804.57 47.46 o 3 10 0 9920.66 10252.84 170.96 o 4 10 0 211.13 254.49 32.33 o 5 10 0 2611.57 2707.83 84.18 o 6 10 0 4350.77 4241.34 139.00 o 7 10 0 1075.67 1247.23 92.82 o 8 10 0 2863.35 2942.52 220.53 o 9 10 0 2054.50 1876.72 127.39 o 10 10 0 9.06 15.78 70.66 o 11 10 0 751.24 786.37 116.52 o 12 10 0 1026.64 1133.39 226.87 o 1 11 0 8498.28 8288.07 160.88 o 2 11 0 44113.29 45147.93 643.61 o 3 11 0 6.58 40.28 23.59 o 4 11 0 13782.49 13712.05 220.08 o 5 11 0 12215.78 11701.65 220.19 o 6 11 0 3.28 -13.57 37.45 o 7 11 0 12665.06 12767.67 307.84 o 8 11 0 3372.55 3428.30 177.48 o 9 11 0 1395.26 1262.02 150.10 o 10 11 0 2845.32 3185.90 235.79 o 11 11 0 1613.90 1608.88 138.40 o 12 11 0 79.42 -52.74 230.30 o 0 12 0 233.46 72.25 50.79 o 1 12 0 2695.54 2654.95 89.47 o 2 12 0 721.82 831.74 54.88 o 3 12 0 6968.70 7243.14 145.32 o 4 12 0 830.83 865.22 52.66 o 5 12 0 1964.00 2117.98 98.34 o 6 12 0 1326.79 1260.96 90.31 o 7 12 0 2406.09 2383.88 131.53 o 8 12 0 169.83 129.67 67.24 o 9 12 0 470.06 499.94 90.40 o 10 12 0 1.05 -46.28 73.62 o 11 12 0 592.57 539.27 148.45 o 12 12 0 184.95 -32.31 245.42 o 1 13 0 23277.94 22466.44 358.53 o 2 13 0 24966.50 25080.31 393.53 o 3 13 0 335.02 362.19 44.73 o 4 13 0 9289.69 9285.33 206.92 o 5 13 0 9997.73 9839.35 221.62 o 6 13 0 55.94 24.67 45.19 o 7 13 0 6599.23 7040.67 275.06 o 8 13 0 2096.69 2414.38 295.74 o 9 13 0 198.18 30.90 76.13 o 10 13 0 2766.43 2814.74 175.26 o 11 13 0 2114.13 2085.85 299.55 o 12 13 0 8.29 41.15 248.43 o 0 14 0 694.06 733.64 75.65 o 1 14 0 4539.69 4802.71 121.91 o 2 14 0 100.91 91.64 42.38 o 3 14 0 506.21 429.35 55.46 o 4 14 0 31.68 65.44 41.49 o 5 14 0 250.79 229.16 53.95 o 6 14 0 1968.33 1914.49 116.37 o 7 14 0 1061.37 1020.44 102.49 o 8 14 0 9.51 -2.23 62.15 o 9 14 0 19.87 33.97 75.15 o 10 14 0 3.03 11.95 85.63 o 11 14 0 139.05 -168.99 244.99 o 12 14 0 0.94 -119.08 255.12 o 1 15 0 21953.76 21614.78 357.08 o 2 15 0 24957.46 25107.81 402.99 o 3 15 0 240.54 226.58 49.77 o 4 15 0 11011.57 11448.18 260.26 o 5 15 0 9362.25 9081.30 250.46 o 6 15 0 15.65 -13.05 52.84 o 7 15 0 10611.13 10889.16 305.42 o 8 15 0 3718.41 3574.25 195.96 o 9 15 0 119.50 177.19 86.18 o 10 15 0 3633.49 3844.60 216.40 o 11 15 0 2271.19 2257.17 392.76 o 12 15 0 70.87 242.43 345.70 o 0 16 0 837.02 924.50 108.63 o 1 16 0 5.36 52.57 32.25 o 2 16 0 2980.62 3016.73 123.71 o 3 16 0 9.53 -7.30 40.93 o 4 16 0 316.39 222.33 59.65 o 5 16 0 37.82 1.90 52.20 o 6 16 0 5.57 34.10 62.24 o 7 16 0 177.33 374.97 83.00 o 8 16 0 97.60 39.26 69.02 o 9 16 0 11.88 -48.10 73.51 o 10 16 0 0.27 -0.54 92.27 o 11 16 0 8.92 -70.72 296.09 o 1 17 0 21003.34 21043.42 359.88 o 2 17 0 7775.86 7809.57 204.59 o 3 17 0 40.18 -14.83 43.59 o 4 17 0 12281.72 12954.40 337.72 o 5 17 0 9134.86 9229.47 265.79 o 6 17 0 737.90 623.53 91.59 o 7 17 0 5538.75 5279.86 236.10 o 8 17 0 4143.93 4239.28 268.19 o 9 17 0 0.41 -82.29 82.29 o 10 17 0 3021.19 2899.96 333.70 o 11 17 0 1284.25 1330.70 432.96 o 0 18 0 261.82 186.49 63.92 o 1 18 0 266.36 305.39 49.17 o 2 18 0 1.52 -40.90 46.57 o 3 18 0 221.45 135.64 74.48 o 4 18 0 250.30 185.44 63.05 o 5 18 0 590.45 580.68 87.19 o 6 18 0 525.30 511.14 96.30 o 7 18 0 3.05 80.64 73.20 o 8 18 0 44.12 50.76 81.31 o 9 18 0 558.00 606.55 118.03 o 10 18 0 194.95 59.92 166.35 o 11 18 0 249.10 894.62 385.74 o 1 19 0 16294.20 16096.20 322.23 o 2 19 0 4609.56 4672.03 169.89 o 3 19 0 1024.58 1124.91 120.66 o 4 19 0 9408.11 9350.17 274.53 o 5 19 0 2825.74 2915.27 226.17 o 6 19 0 656.63 512.42 100.11 o 7 19 0 4906.87 4823.92 288.82 o 8 19 0 3195.72 2962.13 197.10 o 9 19 0 71.41 8.48 89.17 o 10 19 0 1946.25 1474.88 260.40 o 11 19 0 1093.11 959.73 402.17 o 0 20 0 240.39 95.75 67.86 o 1 20 0 20.69 116.38 52.29 o 2 20 0 1906.71 2008.00 150.50 o 3 20 0 3850.84 3954.06 189.24 o 4 20 0 1893.27 2164.77 145.10 o 5 20 0 1153.25 1135.42 109.93 o 6 20 0 1085.81 1012.88 123.05 o 7 20 0 665.24 639.48 116.41 o 8 20 0 17.44 8.12 83.38 o 9 20 0 1259.80 1200.12 204.00 o 10 20 0 3.74 91.24 161.24 o 11 20 0 85.52 447.94 319.39 o 1 21 0 6555.31 6669.61 211.10 o 2 21 0 6146.48 6155.17 253.19 o 3 21 0 227.24 112.07 70.81 o 4 21 0 6894.13 6882.46 251.90 o 5 21 0 4165.46 3975.35 220.70 o 6 21 0 180.59 54.70 79.46 o 7 21 0 2694.70 2820.22 240.16 o 8 21 0 3511.63 3674.02 233.64 o 9 21 0 68.04 311.99 209.69 o 10 21 0 2014.33 1477.97 447.21 o 0 22 0 204.64 208.37 145.60 o 1 22 0 109.23 147.04 62.53 o 2 22 0 2874.30 3209.84 175.94 o 3 22 0 3622.51 3901.03 194.80 o 4 22 0 2040.58 2189.66 152.37 o 5 22 0 280.97 285.52 91.55 o 6 22 0 2948.44 2890.41 200.27 o 7 22 0 301.75 163.25 98.19 o 8 22 0 263.21 175.79 107.98 o 9 22 0 1126.21 1013.83 352.15 o 10 22 0 90.40 92.46 289.54 o 1 23 0 4578.22 5072.65 267.30 o 2 23 0 5713.01 5367.19 226.74 o 3 23 0 51.17 51.17 69.60 o 4 23 0 4443.70 4632.90 281.52 o 5 23 0 3635.81 3656.81 222.29 o 6 23 0 4.66 -59.34 86.38 o 7 23 0 1032.32 1065.60 166.25 o 8 23 0 891.04 1019.04 147.16 o 9 23 0 12.42 49.09 157.79 o 10 23 0 1348.38 1527.68 492.55 o 0 24 0 10726.14 11856.48 561.25 o 1 24 0 1283.78 1298.02 172.61 o 2 24 0 172.48 143.57 76.72 o 3 24 0 3180.59 3155.97 187.48 o 4 24 0 201.29 52.42 79.19 o 5 24 0 1853.98 1667.41 164.74 o 6 24 0 1949.32 1976.74 178.51 o 7 24 0 452.39 371.54 125.73 o 8 24 0 1258.57 1356.45 194.71 o 9 24 0 1931.53 1835.86 260.14 o 10 24 0 51.76 62.51 318.25 o 1 25 0 2639.91 2817.55 246.31 o 2 25 0 660.50 644.04 199.77 o 3 25 0 403.88 404.06 99.39 o 4 25 0 2134.61 1988.75 175.39 o 5 25 0 2167.73 2112.10 209.81 o 6 25 0 1.24 1.77 95.60 o 7 25 0 347.86 353.13 119.27 o 8 25 0 336.49 329.62 179.93 o 9 25 0 94.30 -96.28 204.92 o 0 26 0 8851.64 7788.90 727.18 o 1 26 0 308.04 282.70 156.97 o 2 26 0 2116.19 2358.19 330.75 o 3 26 0 5758.63 5590.77 338.51 o 4 26 0 1506.52 1299.23 154.30 o 5 26 0 1033.31 922.20 174.91 o 6 26 0 3062.02 2649.49 246.13 o 7 26 0 23.77 -102.39 106.30 o 8 26 0 1190.81 1386.25 246.13 o 9 26 0 1101.60 1601.40 583.14 o 1 27 0 10.32 72.84 106.87 o 2 27 0 1319.07 1363.75 193.90 o 3 27 0 14.06 -100.86 100.86 o 4 27 0 1133.20 1081.66 248.56 o 5 27 0 913.68 935.09 146.91 o 6 27 0 1.55 77.00 112.61 o 7 27 0 256.92 313.91 145.14 o 8 27 0 209.78 247.91 177.02 o 9 27 0 14.22 125.58 227.31 o 0 28 0 10909.92 11997.01 899.61 o 1 28 0 2838.98 3479.77 481.06 o 2 28 0 1723.27 1734.47 218.38 o 3 28 0 3786.87 3831.80 545.48 o 4 28 0 162.88 152.89 140.78 o 5 28 0 1502.65 1467.96 167.25 o 6 28 0 2992.37 3626.63 259.94 o 7 28 0 348.01 254.72 181.74 o 8 28 0 995.79 801.06 235.74 o 1 29 0 840.68 744.19 204.59 o 2 29 0 3.25 66.67 124.92 o 3 29 0 2.76 183.10 138.87 o 4 29 0 508.87 411.46 265.67 o 5 29 0 123.21 226.76 153.32 o 6 29 0 3.94 154.76 131.03 o 7 29 0 161.98 104.93 179.78 o 8 29 0 86.75 251.89 252.03 o 0 30 0 3149.36 3709.53 581.99 o 1 30 0 2872.78 3378.25 374.33 o 2 30 0 1835.99 1356.73 264.58 o 3 30 0 3553.37 3935.62 413.65 o 4 30 0 55.80 -64.47 175.92 o 5 30 0 1669.22 1812.13 421.53 o 6 30 0 3849.30 4064.43 322.41 o 7 30 0 297.50 130.52 175.51 o 8 30 0 787.75 1147.04 468.22 o 1 31 0 30.41 188.92 267.34 o 2 31 0 0.13 190.59 181.38 o 3 31 0 194.55 -48.73 181.96 o 4 31 0 6.22 45.41 182.95 o 5 31 0 3.77 18.23 155.44 o 6 31 0 42.55 -95.07 200.23 o 7 31 0 0.16 52.97 165.28 o 0 32 0 2971.84 2412.63 495.15 o 1 32 0 991.61 1088.61 256.03 o 2 32 0 1672.55 1175.55 267.11 o 3 32 0 3951.68 4032.67 647.93 o 4 32 0 275.66 296.17 343.93 o 5 32 0 935.52 328.56 235.99 o 6 32 0 2415.95 1826.11 1152.08 o 7 32 0 87.52 319.49 363.07 o 1 33 0 60.48 259.79 209.28 o 2 33 0 148.60 428.69 235.94 o 3 33 0 34.23 271.24 326.36 o 4 33 0 136.28 53.77 313.88 o 5 33 0 78.63 79.67 221.29 o 6 33 0 118.80 230.15 351.53 o 0 34 0 3011.40 3323.79 561.92 o 1 34 0 784.89 738.64 248.65 o 2 34 0 446.39 369.83 374.93 o 3 34 0 2650.01 2319.13 547.88 o 4 34 0 689.85 780.22 389.49 o 5 34 0 293.89 283.74 325.37 o 1 35 0 132.38 33.21 216.44 o 2 35 0 242.32 94.95 326.98 o 3 35 0 1.75 -34.94 266.04 o 4 35 0 347.48 642.52 397.49 o 0 36 0 2635.45 2091.27 486.00 o 1 36 0 184.82 55.76 256.68 o 2 36 0 291.48 336.86 332.08 o 3 36 0 1861.61 1936.82 525.52 o 1 37 0 619.06 612.78 385.12 o 2 37 0 157.82 367.96 346.95 o -12 1 1 1937.92 2177.38 445.02 o -11 1 1 0.69 79.27 133.39 o -10 1 1 5665.67 5979.68 313.75 o -9 1 1 6566.32 6756.32 261.69 o -8 1 1 122.33 104.08 61.55 o -7 1 1 4429.21 4624.96 191.31 o -6 1 1 18652.65 17612.39 385.60 o -5 1 1 848.74 627.74 120.84 o -4 1 1 6183.04 5680.53 186.12 o -3 1 1 30509.89 30240.20 588.33 o -2 1 1 1221.13 1260.88 94.47 o -1 1 1 86297.96 83593.67 1883.92 o 0 1 1 48843.84 44649.57 1241.80 o 1 1 1 317.19 395.02 18.13 o 2 1 1 1940.91 1948.95 47.01 o 3 1 1 17502.10 17266.52 685.37 o 4 1 1 68.42 206.74 83.88 o 5 1 1 20628.38 19439.13 583.49 o 6 1 1 6946.52 6888.67 315.30 o 7 1 1 23.40 43.27 90.12 o 8 1 1 9973.83 10099.73 610.86 o 9 1 1 4297.04 5367.16 370.28 o 10 1 1 595.14 680.29 162.26 o 11 1 1 5310.40 5850.19 582.23 o 12 1 1 652.04 774.10 208.01 o -12 2 1 18.54 -164.56 184.26 o -11 2 1 501.36 203.39 161.97 o -10 2 1 736.99 824.28 120.27 o -9 2 1 70.35 140.97 76.87 o -8 2 1 335.44 323.78 77.26 o -7 2 1 40.87 69.10 56.56 o -6 2 1 500.44 296.80 129.94 o -5 2 1 2053.01 1827.38 264.14 o -4 2 1 1741.66 1718.63 219.92 o -3 2 1 413.05 426.07 52.53 o -2 2 1 2184.78 2156.36 58.52 o -1 2 1 58.42 163.16 45.99 o 0 2 1 3083.66 2620.47 62.76 o 1 2 1 562.66 519.44 24.04 o 2 2 1 10875.24 10685.53 177.76 o 3 2 1 1174.76 1202.72 47.67 o 4 2 1 3017.64 3308.17 178.24 o 5 2 1 686.69 850.90 184.92 o 6 2 1 112.50 66.57 76.78 o 7 2 1 33.16 66.13 85.14 o 8 2 1 124.46 -4.50 84.55 o 9 2 1 2449.46 2373.02 150.33 o 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