#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/30/2233009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233009_Fobs loop_ _publ_author_name 'Han, Li-Jun' 'Yang, Shu-Ping' 'Fu, Lin-Lin' 'Gao, Hai-Lei' _publ_section_title ; Hexaaquacobalt(II) bis(5-acetyl-2-hydroxybenzoate) dihydrate ; _journal_coeditor_code XU5375 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1733 _journal_volume 67 _journal_year 2011 _space_group_IT_number 73 _symmetry_space_group_name_Hall '-I 2b 2c' _symmetry_space_group_name_H-M 'I b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.6238 _cell_length_b 13.6271 _cell_length_c 33.3180 _exptl_crystal_F_000 2344.00 _reflns_d_resolution_high 0.7458 _[local]_cod_data_source_file xu5375Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hanhongse_0m in I b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 742.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z' 'x, -y, -z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1, z+1/2' 'x+1/2, -y+1/2, -z+1' '-x+1/2, y+1, -z+1' '-x, -y, -z' 'x, y-1/2, -z' '-x, y, z-1/2' 'x, -y-1/2, z-1/2' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y, -z+1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 255.40 195.85 15.46 o 4 0 0 77186.06 80606.66 1140.55 o 6 0 0 75357.34 75983.14 1082.10 o 8 0 0 2182.06 2211.07 92.77 o 10 0 0 16728.73 15214.65 381.40 o 12 0 0 32.62 139.16 51.54 o 14 0 0 1409.88 1515.28 113.39 o 0 2 0 78812.79 79517.32 1667.32 o 2 2 0 33243.95 35661.78 291.72 o 4 2 0 36571.13 36128.66 325.12 o 6 2 0 17621.11 18239.49 181.88 o 8 2 0 5408.14 5058.68 112.98 o 10 2 0 4496.06 4648.52 116.62 o 12 2 0 1383.54 1224.83 126.27 o 14 2 0 619.85 629.85 58.31 o 0 4 0 551387.75 477246.69 27313.77 o 2 4 0 97.80 95.25 4.99 o 4 4 0 1868.90 2473.79 30.03 o 6 4 0 10177.52 9812.74 92.66 o 8 4 0 1163.31 1067.56 33.67 o 10 4 0 865.03 863.13 52.75 o 12 4 0 3262.17 3339.93 102.04 o 0 6 0 301.72 286.26 18.22 o 2 6 0 7545.80 7089.18 67.91 o 4 6 0 9787.59 10235.77 104.57 o 6 6 0 1440.70 1260.98 23.36 o 8 6 0 3990.76 4107.32 65.52 o 10 6 0 3264.61 3230.56 92.88 o 12 6 0 299.75 252.55 38.14 o 0 8 0 188557.92 192763.39 2203.78 o 2 8 0 20077.50 17711.42 156.98 o 4 8 0 10274.88 9899.04 105.44 o 6 8 0 3979.41 4048.62 63.10 o 8 8 0 2979.12 2936.30 50.16 o 10 8 0 2568.22 2544.22 141.74 o 12 8 0 300.61 328.50 41.79 o 0 10 0 10365.47 9781.30 201.01 o 2 10 0 8068.69 7720.45 103.03 o 4 10 0 5832.75 5431.24 80.44 o 6 10 0 4433.49 4010.69 79.31 o 8 10 0 404.49 451.31 31.64 o 0 12 0 1070.63 1032.06 49.10 o 2 12 0 8.52 14.32 16.00 o 4 12 0 1604.38 1581.11 42.81 o 6 12 0 3119.52 3024.57 72.37 o 8 12 0 239.81 203.98 29.76 o 0 14 0 390.34 423.14 41.79 o 2 14 0 158.22 215.13 25.05 o 4 14 0 101.61 69.58 20.62 o 6 14 0 248.61 271.23 32.73 o 8 14 0 896.26 1021.52 51.52 o 0 16 0 548.05 385.93 45.45 o 2 16 0 1884.20 1665.68 93.73 o 4 16 0 11.15 -11.96 25.67 o 6 16 0 41.37 8.18 28.65 o 0 18 0 19.17 11.12 34.48 o 2 18 0 280.30 287.14 43.38 o 2 1 1 7185.32 7911.86 52.76 o 4 1 1 2421.71 2278.55 22.57 o 6 1 1 890.87 1029.76 18.36 o 8 1 1 4563.21 4044.72 67.62 o 10 1 1 21.48 58.58 19.20 o 12 1 1 18.13 15.46 21.18 o 14 1 1 57.48 91.77 27.63 o 1 2 1 8.08 121.68 5.39 o 3 2 1 3563.11 3583.41 26.29 o 5 2 1 443.13 597.33 9.69 o 7 2 1 1786.08 1890.76 30.00 o 9 2 1 211.22 124.45 19.87 o 11 2 1 27.52 0.83 18.59 o 13 2 1 550.91 626.15 43.89 o 2 3 1 18346.65 19601.86 133.78 o 4 3 1 2841.34 2791.53 22.19 o 6 3 1 261.43 263.59 11.16 o 8 3 1 1066.83 956.99 24.06 o 10 3 1 264.16 223.00 23.76 o 12 3 1 6.25 35.93 21.79 o 14 3 1 121.88 162.02 33.48 o 1 4 1 37289.05 40877.95 236.80 o 3 4 1 68.63 130.21 5.01 o 5 4 1 702.92 693.33 10.88 o 7 4 1 1708.74 1662.40 26.92 o 9 4 1 0.35 -10.56 10.56 o 11 4 1 6.88 17.95 19.87 o 13 4 1 27.22 42.42 28.27 o 2 5 1 208.57 266.66 6.24 o 4 5 1 1468.98 1598.38 17.27 o 6 5 1 2971.71 3124.85 29.20 o 8 5 1 5458.04 4951.85 59.52 o 10 5 1 6.52 1.24 17.28 o 12 5 1 20.84 74.67 23.76 o 1 6 1 11720.86 12715.11 79.41 o 3 6 1 505.41 441.91 9.25 o 5 6 1 544.43 587.50 12.21 o 7 6 1 4249.96 4016.05 39.52 o 9 6 1 425.96 360.61 19.44 o 11 6 1 576.98 539.10 32.14 o 13 6 1 528.03 629.54 41.66 o 2 7 1 928.76 1132.05 14.17 o 4 7 1 257.04 210.94 8.12 o 6 7 1 1887.41 1975.32 27.52 o 8 7 1 420.40 425.55 14.61 o 10 7 1 226.32 216.72 25.05 o 12 7 1 3.15 -20.92 20.92 o 1 8 1 19924.36 20669.42 127.61 o 3 8 1 139.61 196.65 8.05 o 5 8 1 287.78 404.47 11.43 o 7 8 1 3436.15 3327.78 36.48 o 9 8 1 4.01 32.30 12.69 o 11 8 1 824.40 919.36 39.12 o 2 9 1 121.96 127.02 8.45 o 4 9 1 70.67 90.00 7.99 o 6 9 1 1685.62 1716.00 26.38 o 8 9 1 2588.11 2683.01 36.60 o 10 9 1 121.61 140.44 30.92 o 12 9 1 45.09 59.27 32.80 o 1 10 1 2645.80 2743.47 36.44 o 3 10 1 11.92 113.56 20.15 o 5 10 1 497.61 488.18 20.66 o 7 10 1 757.29 697.55 22.77 o 9 10 1 164.29 294.76 25.05 o 2 11 1 658.93 615.94 23.87 o 4 11 1 99.96 94.01 12.29 o 6 11 1 383.75 437.16 21.68 o 8 11 1 143.25 167.69 18.53 o 1 12 1 2355.86 2163.83 35.01 o 3 12 1 24.35 35.21 12.13 o 5 12 1 2.94 18.29 12.69 o 7 12 1 99.30 157.53 30.01 o 9 12 1 15.46 30.01 24.55 o 2 13 1 208.28 180.51 15.41 o 4 13 1 24.04 28.55 12.95 o 6 13 1 51.82 39.06 15.68 o 8 13 1 646.42 699.47 34.19 o 1 14 1 53.36 45.08 13.81 o 3 14 1 4.43 -2.58 12.76 o 5 14 1 33.85 28.49 17.14 o 7 14 1 22.35 45.10 18.82 o 9 14 1 53.80 45.83 25.05 o 2 15 1 195.74 190.21 17.65 o 4 15 1 56.19 35.93 15.41 o 6 15 1 205.00 201.10 22.02 o 8 15 1 68.39 80.05 21.68 o 1 16 1 224.50 161.71 18.99 o 3 16 1 16.50 75.48 17.09 o 5 16 1 68.52 111.94 21.68 o 2 17 1 39.70 50.55 17.96 o 4 17 1 7.86 17.62 20.54 o 1 18 1 20.35 57.11 18.99 o 2 0 2 28237.30 28040.26 333.50 o 4 0 2 66134.41 69484.34 696.33 o 6 0 2 73304.38 74649.27 751.60 o 8 0 2 66.24 69.58 23.19 o 10 0 2 2464.00 2253.06 76.53 o 12 0 2 2168.67 2339.02 85.59 o 14 0 2 275.52 173.49 41.79 o 1 1 2 1808.48 2054.34 27.66 o 3 1 2 7507.95 7579.66 63.89 o 5 1 2 32255.62 34878.93 252.70 o 7 1 2 992.63 1021.01 18.78 o 9 1 2 8757.82 8470.93 163.01 o 11 1 2 178.43 182.96 24.38 o 13 1 2 112.66 102.04 25.58 o 0 2 2 67156.78 67889.84 602.40 o 2 2 2 37095.52 39632.22 264.72 o 4 2 2 30158.78 29973.30 185.29 o 6 2 2 14771.25 15460.29 104.39 o 8 2 2 6121.80 5745.79 73.66 o 10 2 2 3951.60 4204.52 92.58 o 12 2 2 1033.00 907.71 41.23 o 14 2 2 559.75 597.24 41.66 o 1 3 2 37706.82 40724.39 245.80 o 3 3 2 3596.43 3461.03 24.96 o 5 3 2 416.49 657.96 10.83 o 7 3 2 5074.06 5035.85 53.06 o 9 3 2 184.22 141.19 20.37 o 11 3 2 693.04 666.01 33.50 o 13 3 2 418.12 426.83 34.09 o 0 4 2 208283.78 212657.36 1881.57 o 2 4 2 3852.21 4948.01 37.29 o 4 4 2 1738.87 1807.13 17.25 o 6 4 2 3571.24 3163.34 32.15 o 8 4 2 4256.25 4266.27 49.70 o 10 4 2 6021.56 5666.78 79.80 o 12 4 2 430.72 441.77 32.14 o 1 5 2 22329.05 24436.17 145.05 o 3 5 2 922.34 865.80 11.65 o 5 5 2 414.48 331.09 8.71 o 7 5 2 1570.19 1602.93 24.73 o 9 5 2 477.37 442.71 28.29 o 11 5 2 1103.37 1115.47 41.83 o 13 5 2 466.89 501.62 35.25 o 2 6 2 2099.57 1860.24 19.67 o 4 6 2 9251.72 9309.00 68.42 o 6 6 2 890.38 736.32 14.44 o 8 6 2 864.44 980.32 25.81 o 10 6 2 2733.59 2801.07 62.49 o 12 6 2 419.05 404.17 35.71 o 1 7 2 34.04 39.48 7.38 o 3 7 2 491.75 555.87 11.10 o 5 7 2 9127.91 9376.21 68.82 o 7 7 2 357.05 385.71 13.18 o 9 7 2 672.28 668.18 28.81 o 11 7 2 414.89 404.71 29.55 o 13 7 2 53.48 79.89 25.77 o 0 8 2 595.77 711.30 40.72 o 2 8 2 11708.06 11021.17 72.88 o 4 8 2 10976.41 11459.49 80.47 o 6 8 2 8907.10 8923.12 67.61 o 8 8 2 447.57 437.23 15.26 o 10 8 2 674.62 735.42 34.72 o 12 8 2 812.89 928.20 47.42 o 1 9 2 82.28 176.63 9.12 o 3 9 2 5275.63 5139.47 46.18 o 5 9 2 169.74 214.00 10.66 o 7 9 2 2464.42 2356.88 32.41 o 9 9 2 955.67 1050.21 30.46 o 11 9 2 1.11 69.58 29.16 o 0 10 2 13710.50 13071.76 155.89 o 2 10 2 8762.44 8492.50 78.09 o 4 10 2 3764.99 3567.08 43.00 o 6 10 2 4832.64 4440.16 54.45 o 8 10 2 2272.69 2446.01 40.57 o 10 10 2 500.95 386.55 56.69 o 1 11 2 3195.82 3039.98 40.30 o 3 11 2 781.53 754.55 21.36 o 5 11 2 15.83 11.28 11.21 o 7 11 2 137.35 165.04 17.45 o 9 11 2 54.35 51.60 20.92 o 0 12 2 6126.57 5738.46 88.24 o 2 12 2 1405.95 1427.89 28.39 o 4 12 2 250.95 249.54 17.78 o 6 12 2 509.96 558.07 24.13 o 8 12 2 989.03 938.49 31.81 o 1 13 2 660.96 612.32 21.36 o 3 13 2 155.53 180.75 15.19 o 5 13 2 170.92 145.70 15.82 o 7 13 2 388.65 367.52 24.13 o 9 13 2 44.88 56.83 23.76 o 0 14 2 5.58 -1.29 18.04 o 2 14 2 159.33 166.33 19.48 o 4 14 2 151.75 173.35 18.26 o 6 14 2 48.56 82.92 22.80 o 8 14 2 66.71 77.31 20.26 o 1 15 2 105.00 83.72 16.32 o 3 15 2 17.36 6.08 13.68 o 5 15 2 129.48 116.95 19.91 o 7 15 2 60.34 65.97 20.64 o 0 16 2 115.74 103.01 37.20 o 2 16 2 213.89 249.11 20.67 o 4 16 2 243.44 209.26 21.35 o 6 16 2 101.72 101.49 21.68 o 1 17 2 12.29 23.61 17.18 o 3 17 2 10.22 23.43 17.02 o 5 17 2 4.03 13.35 20.26 o 0 18 2 250.90 212.38 30.92 o 2 18 2 104.67 146.23 26.66 o 2 1 3 202.94 294.16 5.34 o 4 1 3 7140.32 7941.84 68.06 o 6 1 3 1460.18 1690.24 29.14 o 8 1 3 136.95 106.56 17.85 o 10 1 3 685.76 498.49 29.76 o 12 1 3 2.92 34.02 21.18 o 14 1 3 14.96 -12.89 23.19 o 1 2 3 459.84 451.52 7.73 o 3 2 3 21648.78 22633.10 154.93 o 5 2 3 2046.51 2265.36 23.18 o 7 2 3 34.58 82.84 6.99 o 9 2 3 7183.70 6625.90 97.93 o 11 2 3 29.90 22.61 18.59 o 13 2 3 129.96 180.73 27.63 o 2 3 3 13699.04 13625.81 82.30 o 4 3 3 19379.36 20320.59 127.46 o 6 3 3 3508.59 3720.35 34.76 o 8 3 3 968.68 992.82 24.10 o 10 3 3 2304.51 2258.15 55.25 o 12 3 3 12.44 -18.13 19.87 o 14 3 3 14.78 60.19 31.64 o 1 4 3 24801.07 23926.50 147.33 o 3 4 3 4826.92 4771.29 35.39 o 5 4 3 40.90 70.94 11.37 o 7 4 3 102.48 130.90 10.91 o 9 4 3 486.83 511.69 27.69 o 11 4 3 391.39 375.11 28.35 o 13 4 3 70.94 105.99 25.58 o 2 5 3 88.47 102.55 5.97 o 4 5 3 3711.31 3907.72 33.66 o 6 5 3 15.35 15.57 5.16 o 8 5 3 1198.82 1046.18 23.41 o 10 5 3 136.84 180.26 19.27 o 12 5 3 1.51 -3.94 20.83 o 1 6 3 5954.41 6959.86 46.72 o 3 6 3 791.48 633.92 11.41 o 5 6 3 758.04 905.61 14.58 o 7 6 3 2225.98 2036.96 27.41 o 9 6 3 2422.76 2596.33 46.48 o 11 6 3 433.97 388.35 28.93 o 13 6 3 24.12 -10.31 23.19 o 2 7 3 2292.30 2306.99 21.34 o 4 7 3 228.98 230.90 8.51 o 6 7 3 6895.50 6743.31 56.15 o 8 7 3 218.24 214.06 11.61 o 10 7 3 1530.95 1349.64 37.22 o 12 7 3 235.12 270.58 29.55 o 1 8 3 12450.82 12601.83 85.60 o 3 8 3 2005.43 1789.17 19.64 o 5 8 3 506.19 597.67 14.99 o 7 8 3 102.93 135.74 10.80 o 9 8 3 431.72 407.86 20.64 o 11 8 3 35.94 88.03 25.67 o 2 9 3 66.37 104.09 10.61 o 4 9 3 142.54 175.26 10.41 o 6 9 3 645.84 632.87 17.64 o 8 9 3 846.30 976.13 23.81 o 10 9 3 197.91 263.23 24.22 o 12 9 3 103.42 139.16 51.54 o 1 10 3 840.37 881.59 21.36 o 3 10 3 230.22 266.48 12.79 o 5 10 3 79.65 117.45 11.38 o 7 10 3 113.53 97.70 13.30 o 9 10 3 1055.42 973.37 37.30 o 11 10 3 36.05 20.62 41.23 o 2 11 3 157.25 187.18 13.36 o 4 11 3 0.08 -0.98 10.38 o 6 11 3 115.69 122.42 16.03 o 8 11 3 43.02 63.34 15.68 o 1 12 3 2991.38 2793.67 52.86 o 3 12 3 131.22 138.42 13.04 o 5 12 3 1.11 -11.55 11.55 o 7 12 3 30.98 31.35 16.13 o 9 12 3 23.86 -6.25 20.37 o 2 13 3 295.91 275.04 16.72 o 4 13 3 61.37 55.95 13.15 o 6 13 3 110.69 86.79 17.79 o 8 13 3 216.00 200.29 21.56 o 1 14 3 225.25 194.95 17.02 o 3 14 3 3.13 20.73 13.73 o 5 14 3 34.65 35.84 16.42 o 7 14 3 386.12 421.24 26.59 o 9 14 3 176.89 221.28 29.21 o 2 15 3 157.11 129.65 17.24 o 4 15 3 8.62 2.16 15.48 o 6 15 3 70.71 47.93 19.12 o 8 15 3 25.60 42.07 25.05 o 1 16 3 473.87 419.02 22.72 o 3 16 3 2.21 32.99 16.25 o 5 16 3 28.29 48.47 19.91 o 2 17 3 9.35 37.43 17.24 o 4 17 3 4.76 11.76 19.16 o 1 18 3 2.24 1.72 17.83 o 0 0 4 26768.01 28943.44 520.56 o 2 0 4 98935.27 100512.52 1157.48 o 4 0 4 28209.74 31221.72 371.89 o 6 0 4 17565.94 18937.17 201.78 o 8 0 4 19295.01 18250.46 298.84 o 10 0 4 2844.47 2398.21 78.29 o 12 0 4 2568.08 2634.35 91.11 o 14 0 4 59.79 -4.61 38.66 o 1 1 4 105432.70 105364.17 736.51 o 3 1 4 24494.57 25171.59 181.69 o 5 1 4 29390.21 29288.49 229.99 o 7 1 4 452.30 408.93 15.00 o 9 1 4 7138.27 6952.23 103.08 o 11 1 4 1811.42 1703.06 49.57 o 13 1 4 128.72 120.96 26.78 o 0 2 4 11689.92 11691.90 107.83 o 2 2 4 14428.40 15761.10 102.79 o 4 2 4 22253.13 21905.77 143.13 o 6 2 4 4111.88 4265.32 38.27 o 8 2 4 2872.08 2757.16 46.75 o 10 2 4 2620.05 2630.42 58.59 o 12 2 4 356.94 315.96 33.48 o 14 2 4 325.63 367.44 35.38 o 1 3 4 413.22 552.08 12.75 o 3 3 4 3341.86 2963.89 63.16 o 5 3 4 14545.08 15275.30 104.16 o 7 3 4 2185.46 2323.82 26.65 o 9 3 4 893.22 732.53 32.14 o 11 3 4 1791.54 1710.92 49.57 o 13 3 4 246.38 252.18 30.21 o 0 4 4 227541.13 236108.73 2328.40 o 2 4 4 12138.40 15548.59 94.46 o 4 4 4 1745.46 1770.39 20.09 o 6 4 4 4811.02 4398.08 36.40 o 8 4 4 2521.66 2430.46 39.31 o 10 4 4 1379.24 1350.13 37.01 o 12 4 4 20.48 16.71 19.87 o 1 5 4 1303.12 1089.67 12.84 o 3 5 4 117.02 72.46 7.80 o 5 5 4 8033.71 8141.67 59.08 o 7 5 4 6161.91 5960.57 53.84 o 9 5 4 546.08 566.73 21.90 o 11 5 4 1350.23 1439.52 45.04 o 13 5 4 310.69 307.05 31.82 o 0 6 4 9410.55 9185.15 93.52 o 2 6 4 4230.06 3932.62 31.46 o 4 6 4 955.09 929.32 13.45 o 6 6 4 4021.97 3775.43 34.81 o 8 6 4 558.92 668.68 18.57 o 10 6 4 955.46 961.51 32.17 o 12 6 4 615.04 695.31 38.08 o 1 7 4 45469.30 46748.96 286.63 o 3 7 4 128.57 144.60 8.91 o 5 7 4 8471.58 8093.25 60.26 o 7 7 4 4782.73 4824.14 45.56 o 9 7 4 987.66 1024.78 31.50 o 11 7 4 937.26 887.24 37.96 o 13 7 4 370.73 487.84 34.72 o 0 8 4 324.46 306.91 48.78 o 2 8 4 2988.14 2880.63 29.35 o 4 8 4 4639.34 4827.59 40.37 o 6 8 4 6220.03 6159.94 51.08 o 8 8 4 3211.71 3262.37 47.41 o 10 8 4 1524.75 1433.83 43.70 o 12 8 4 517.42 634.43 42.58 o 1 9 4 7109.70 7401.71 59.37 o 3 9 4 8633.05 8770.60 68.86 o 5 9 4 946.85 884.84 23.22 o 7 9 4 605.33 599.47 17.88 o 9 9 4 1104.77 1148.31 49.94 o 11 9 4 220.60 216.96 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11 0.97 -1.03 19.20 o 13 4 11 73.35 58.37 25.05 o 2 5 11 862.07 1131.81 14.48 o 4 5 11 6340.64 6486.33 44.88 o 6 5 11 490.42 521.18 19.72 o 8 5 11 182.45 180.30 12.74 o 10 5 11 14.05 44.54 16.53 o 12 5 11 28.76 60.53 20.34 o 1 6 11 2097.36 2143.11 21.45 o 3 6 11 410.27 412.10 10.50 o 5 6 11 2212.88 2455.03 25.28 o 7 6 11 22.06 28.30 8.35 o 9 6 11 766.18 721.07 26.24 o 11 6 11 30.87 58.95 20.07 o 2 7 11 1061.55 924.68 15.88 o 4 7 11 404.47 498.82 18.97 o 6 7 11 1.64 34.51 9.48 o 8 7 11 400.08 428.16 22.27 o 10 7 11 110.12 121.91 19.27 o 12 7 11 2.49 18.80 21.79 o 1 8 11 931.49 893.70 16.69 o 3 8 11 1638.81 1553.21 24.02 o 5 8 11 741.69 722.63 21.57 o 7 8 11 3.33 8.00 10.72 o 9 8 11 699.24 702.24 33.35 o 11 8 11 328.61 428.28 43.85 o 2 9 11 309.69 269.12 10.95 o 4 9 11 1345.98 1170.49 21.48 o 6 9 11 116.54 98.44 12.42 o 8 9 11 301.44 213.46 20.59 o 10 9 11 16.18 8.53 19.87 o 1 10 11 1153.91 1139.62 20.54 o 3 10 11 167.69 167.10 10.95 o 5 10 11 663.72 695.99 18.92 o 7 10 11 766.75 752.82 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43.81 o 1 1 12 4805.04 5212.61 42.16 o 3 1 12 1484.35 1405.12 21.56 o 5 1 12 748.37 745.47 17.23 o 7 1 12 2333.29 2106.25 35.33 o 9 1 12 9.44 1.27 10.85 o 11 1 12 887.94 977.02 61.84 o 13 1 12 271.50 312.15 31.51 o 0 2 12 9560.11 8820.62 164.81 o 2 2 12 3869.82 4139.07 31.52 o 4 2 12 19580.15 18508.50 140.30 o 6 2 12 3238.61 3280.05 48.72 o 8 2 12 1298.66 1291.46 28.70 o 10 2 12 3839.99 3809.78 87.78 o 12 2 12 394.85 394.04 30.92 o 1 3 12 8693.82 8266.11 52.05 o 3 3 12 5476.03 5010.37 44.32 o 5 3 12 6858.93 6884.11 57.27 o 7 3 12 2115.65 2147.06 32.42 o 9 3 12 4112.15 3896.02 62.18 o 11 3 12 494.57 438.15 54.31 o 13 3 12 265.66 262.40 30.92 o 0 4 12 25382.76 25031.27 210.00 o 2 4 12 29201.24 28676.17 164.00 o 4 4 12 739.57 610.71 11.04 o 6 4 12 19327.14 18945.69 148.16 o 8 4 12 5442.34 5199.07 72.26 o 10 4 12 187.06 208.81 23.76 o 12 4 12 1888.34 2117.69 58.59 o 1 5 12 14821.03 14089.53 88.56 o 3 5 12 4199.58 4054.09 32.06 o 5 5 12 17620.09 17973.22 113.80 o 7 5 12 1195.09 1079.53 21.75 o 9 5 12 3991.11 3678.16 60.97 o 11 5 12 882.10 901.44 34.83 o 13 5 12 19.42 -8.59 22.46 o 0 6 12 19677.80 19995.91 192.17 o 2 6 12 20723.33 20925.98 134.40 o 4 6 12 5063.56 5141.20 38.40 o 6 6 12 6700.73 6212.66 57.01 o 8 6 12 3584.11 3599.98 52.81 o 10 6 12 856.42 891.46 48.02 o 12 6 12 533.94 508.06 33.94 o 1 7 12 7882.57 8310.79 66.65 o 3 7 12 1209.10 1241.68 19.69 o 5 7 12 6015.34 5689.88 60.13 o 7 7 12 1141.72 1215.73 29.79 o 9 7 12 5.19 54.63 16.13 o 11 7 12 817.07 914.79 46.87 o 0 8 12 11540.72 11525.63 121.22 o 2 8 12 472.12 678.25 15.11 o 4 8 12 4364.65 4344.44 47.29 o 6 8 12 2133.74 2145.65 35.28 o 8 8 12 139.03 154.73 21.18 o 10 8 12 880.38 765.13 35.38 o 12 8 12 195.57 218.01 33.64 o 1 9 12 210.18 258.32 10.84 o 3 9 12 2840.43 2918.21 36.59 o 5 9 12 431.79 395.84 16.06 o 7 9 12 564.34 580.76 25.15 o 9 9 12 6.08 1.04 18.29 o 11 9 12 33.12 43.36 27.67 o 0 10 12 531.27 679.21 23.31 o 2 10 12 8.11 6.46 8.28 o 4 10 12 913.83 923.99 24.55 o 6 10 12 674.66 650.36 28.01 o 8 10 12 135.37 178.30 20.59 o 10 10 12 323.99 302.71 28.93 o 1 11 12 119.76 113.82 10.68 o 3 11 12 24.58 8.97 9.16 o 5 11 12 185.07 172.97 13.31 o 7 11 12 65.31 102.16 17.31 o 9 11 12 731.61 719.88 79.36 o 0 12 12 661.17 607.14 31.99 o 2 12 12 471.65 566.44 22.45 o 4 12 12 312.99 337.61 19.40 o 6 12 12 624.49 692.89 31.19 o 8 12 12 515.54 534.15 40.59 o 10 12 12 346.61 424.64 49.10 o 1 13 12 233.37 231.26 17.02 o 3 13 12 231.34 244.46 17.15 o 5 13 12 704.49 742.55 26.91 o 7 13 12 506.15 494.37 48.35 o 9 13 12 206.72 206.03 35.71 o 0 14 12 229.64 218.37 25.77 o 2 14 12 2033.02 2114.15 38.70 o 4 14 12 600.19 620.58 26.38 o 6 14 12 104.03 91.01 22.91 o 8 14 12 388.85 481.13 44.64 o 1 15 12 439.80 441.06 22.66 o 3 15 12 348.75 406.34 26.40 o 5 15 12 179.05 135.20 20.25 o 7 15 12 249.82 279.06 33.50 o 0 16 12 6.79 46.87 27.66 o 2 16 12 709.50 729.11 32.14 o 4 16 12 196.28 189.35 21.17 o 1 17 12 134.66 122.46 19.85 o 3 17 12 48.09 6.33 18.57 o 2 1 13 4196.49 4508.48 35.75 o 4 1 13 860.61 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13 344.10 297.44 20.58 o 11 6 13 85.80 88.50 21.18 o 2 7 13 496.32 491.63 15.94 o 4 7 13 200.59 256.27 11.42 o 6 7 13 3.81 13.49 9.29 o 8 7 13 24.25 45.17 14.21 o 10 7 13 185.82 244.07 22.91 o 12 7 13 15.57 13.12 22.46 o 1 8 13 638.73 593.23 14.48 o 3 8 13 1389.87 1316.87 21.58 o 5 8 13 21.43 23.56 8.22 o 7 8 13 129.72 131.88 14.38 o 9 8 13 1220.20 1311.16 49.10 o 11 8 13 816.74 824.84 50.98 o 2 9 13 47.04 34.72 7.74 o 4 9 13 1257.60 1248.78 22.37 o 6 9 13 112.28 100.81 13.18 o 8 9 13 135.72 124.95 20.62 o 10 9 13 1.88 -4.98 19.87 o 1 10 13 53.56 87.38 9.38 o 3 10 13 334.99 311.12 13.76 o 5 10 13 319.64 362.18 15.56 o 7 10 13 922.59 842.91 25.98 o 9 10 13 5.47 9.95 19.87 o 11 10 13 85.27 59.46 28.66 o 2 11 13 17.32 1.83 8.95 o 4 11 13 183.65 231.53 14.30 o 6 11 13 28.63 42.08 13.87 o 8 11 13 50.48 63.08 19.72 o 10 11 13 180.87 182.95 33.41 o 1 12 13 0.28 40.91 13.88 o 3 12 13 129.84 140.20 13.60 o 5 12 13 391.00 519.25 20.44 o 7 12 13 61.39 61.32 18.47 o 9 12 13 276.10 310.22 56.69 o 2 13 13 25.30 22.89 13.81 o 4 13 13 564.22 527.54 24.08 o 6 13 13 178.35 177.84 22.91 o 8 13 13 10.05 30.37 28.66 o 1 14 13 524.36 472.63 21.75 o 3 14 13 43.92 56.15 16.82 o 5 14 13 57.12 91.52 22.91 o 7 14 13 45.24 115.53 33.48 o 2 15 13 6.36 27.09 15.47 o 4 15 13 0.06 6.27 16.34 o 6 15 13 0.24 7.85 24.87 o 1 16 13 34.53 22.99 16.72 o 3 16 13 0.05 36.03 17.76 o 5 16 13 14.51 -0.51 22.40 o 2 17 13 9.60 7.97 18.67 o 0 0 14 4217.44 2925.41 60.05 o 2 0 14 5739.84 5987.76 65.13 o 4 0 14 494.33 732.16 19.75 o 6 0 14 11629.20 10835.07 152.73 o 8 0 14 486.71 392.91 27.01 o 10 0 14 7775.75 7194.89 154.86 o 12 0 14 764.24 832.32 157.20 o 1 1 14 243.00 259.76 11.35 o 3 1 14 3554.22 3815.74 37.30 o 5 1 14 1062.66 1088.31 19.24 o 7 1 14 222.22 229.99 14.16 o 9 1 14 537.97 463.86 21.04 o 11 1 14 73.10 59.27 20.62 o 13 1 14 131.14 190.55 28.93 o 0 2 14 11568.42 10528.84 118.50 o 2 2 14 16979.19 18196.36 112.80 o 4 2 14 16775.26 15631.36 121.89 o 6 2 14 5903.60 5990.60 68.68 o 8 2 14 4172.29 3865.62 53.94 o 10 2 14 3491.85 3719.26 80.34 o 12 2 14 983.55 960.03 43.12 o 1 3 14 51.51 81.26 7.20 o 3 3 14 488.89 353.21 9.28 o 5 3 14 3209.34 3149.91 35.54 o 7 3 14 1569.09 1512.24 28.22 o 9 3 14 34.90 0.58 13.59 o 11 3 14 231.57 277.70 26.97 o 13 3 14 269.88 305.94 30.92 o 0 4 14 153374.45 155139.88 1154.75 o 2 4 14 23043.13 23546.10 136.93 o 4 4 14 46984.92 47563.19 291.42 o 6 4 14 16610.65 16845.01 134.48 o 8 4 14 1692.17 1740.36 31.63 o 10 4 14 1730.02 1705.06 42.22 o 12 4 14 891.38 974.73 43.15 o 1 5 14 837.90 881.06 12.31 o 3 5 14 796.02 846.56 17.20 o 5 5 14 2057.16 2176.00 27.74 o 7 5 14 2114.74 2023.72 32.77 o 9 5 14 32.55 28.25 20.39 o 11 5 14 49.23 68.11 19.07 o 0 6 14 28729.69 29407.69 250.27 o 2 6 14 6331.72 6052.45 52.10 o 4 6 14 10370.79 10422.51 71.25 o 6 6 14 7468.67 7144.51 63.64 o 8 6 14 945.66 995.73 24.00 o 10 6 14 2200.21 2198.15 48.34 o 12 6 14 275.04 292.83 30.06 o 1 7 14 3272.56 3431.64 33.88 o 3 7 14 27.43 25.19 5.83 o 5 7 14 92.22 60.82 10.20 o 7 7 14 11.64 1.91 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14 14 217.69 229.97 26.35 o 2 14 14 1428.81 1453.96 32.69 o 4 14 14 338.69 388.80 23.17 o 6 14 14 253.29 188.68 25.77 o 1 15 14 126.24 107.87 17.65 o 3 15 14 183.64 258.83 21.85 o 5 15 14 18.58 33.05 22.91 o 0 16 14 11.62 5.15 22.46 o 2 16 14 101.14 127.91 19.64 o 4 16 14 13.51 9.07 18.01 o 1 17 14 41.93 36.49 17.81 o 2 1 15 1662.13 1628.86 17.85 o 4 1 15 179.11 183.75 7.12 o 6 1 15 33.35 44.52 12.68 o 8 1 15 0.02 2.21 10.80 o 10 1 15 41.67 47.67 18.04 o 12 1 15 774.53 803.10 39.88 o 1 2 15 45642.35 49447.48 314.89 o 3 2 15 5103.02 4666.76 42.84 o 5 2 15 195.42 202.69 10.49 o 7 2 15 1033.72 1025.42 25.90 o 9 2 15 165.66 132.35 13.40 o 11 2 15 937.80 926.45 39.25 o 13 2 15 4.79 -11.56 22.46 o 2 3 15 193.14 211.17 12.43 o 4 3 15 10.94 -1.56 6.87 o 6 3 15 118.19 68.29 10.20 o 8 3 15 21.26 27.06 10.20 o 10 3 15 40.07 70.66 16.95 o 12 3 15 851.14 931.48 42.46 o 1 4 15 2797.26 2159.78 22.01 o 3 4 15 88.47 60.79 7.74 o 5 4 15 873.47 812.92 22.18 o 7 4 15 54.38 66.12 10.45 o 9 4 15 11.57 7.77 13.37 o 11 4 15 484.44 533.23 32.14 o 13 4 15 0.72 21.81 36.16 o 2 5 15 4009.85 4140.85 33.40 o 4 5 15 554.01 633.98 12.46 o 6 5 15 941.55 885.27 21.71 o 8 5 15 409.04 309.97 16.34 o 10 5 15 7.20 28.01 15.34 o 12 5 15 123.61 122.57 21.47 o 1 6 15 729.34 886.08 14.40 o 3 6 15 1.10 20.56 5.80 o 5 6 15 6.06 17.69 8.07 o 7 6 15 766.30 644.36 20.81 o 9 6 15 25.26 7.09 15.08 o 11 6 15 5.22 8.79 21.79 o 2 7 15 286.26 277.09 10.83 o 4 7 15 605.88 526.38 14.81 o 6 7 15 826.10 837.81 24.49 o 8 7 15 175.51 148.13 16.70 o 10 7 15 98.32 146.26 22.98 o 12 7 15 199.56 241.18 37.41 o 1 8 15 746.42 698.56 16.06 o 3 8 15 1.23 8.32 7.36 o 5 8 15 45.48 59.77 11.55 o 7 8 15 155.07 158.14 17.40 o 9 8 15 2.38 -5.89 18.60 o 11 8 15 0.70 9.69 28.09 o 2 9 15 855.66 878.78 18.08 o 4 9 15 56.74 59.02 8.77 o 6 9 15 602.04 706.07 26.75 o 8 9 15 129.72 135.06 22.46 o 10 9 15 8.29 21.90 20.62 o 1 10 15 2008.47 1896.39 27.10 o 3 10 15 0.11 12.04 8.64 o 5 10 15 69.12 66.54 14.76 o 7 10 15 84.08 65.86 14.56 o 9 10 15 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5 20 226.22 216.68 19.04 o 11 5 20 529.34 559.70 34.72 o 0 6 20 1468.77 1367.70 34.21 o 2 6 20 4534.56 4545.16 42.51 o 4 6 20 1237.15 1214.53 25.77 o 6 6 20 35.08 58.19 13.92 o 8 6 20 420.75 388.81 21.81 o 10 6 20 185.14 192.53 24.87 o 1 7 20 4929.54 4798.11 45.55 o 3 7 20 635.70 712.60 18.99 o 5 7 20 4095.13 4110.10 52.41 o 7 7 20 6046.99 5804.66 110.64 o 9 7 20 727.76 769.10 36.67 o 11 7 20 341.33 306.38 30.76 o 0 8 20 299.78 266.51 19.22 o 2 8 20 3617.57 3693.55 39.62 o 4 8 20 1134.36 1068.30 26.83 o 6 8 20 2502.80 2533.71 45.82 o 8 8 20 327.75 305.73 22.91 o 10 8 20 259.47 234.20 29.55 o 1 9 20 2748.63 2754.77 34.01 o 3 9 20 1148.95 1192.93 31.67 o 5 9 20 6944.88 6914.68 78.40 o 7 9 20 1292.59 1255.12 38.53 o 9 9 20 941.07 905.04 41.71 o 0 10 20 5847.44 5515.20 76.47 o 2 10 20 7.20 9.64 10.10 o 4 10 20 400.59 363.55 20.25 o 6 10 20 1280.79 1276.69 33.02 o 8 10 20 179.50 188.49 25.48 o 10 10 20 192.87 175.96 28.17 o 1 11 20 1909.91 1870.84 34.71 o 3 11 20 1512.38 1584.99 34.05 o 5 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