#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/30/2233037.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233037_Fobs loop_ _publ_author_name 'Singh, Shailja' 'Singh, Manavendra K.' 'Agarwal, Alka' 'Awasthi, Satish K.' _publ_section_title ; 2-(4-Chlorophenyl)chromen-4-one ; _journal_coeditor_code ZJ2023 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3163 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.524 _cell_angle_gamma 90.000 _cell_length_a 22.1564 _cell_length_b 3.8745 _cell_length_c 26.7728 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file zj2023Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sflo-1 in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5032.08 5174.03 53.44 o 6 0 0 855.62 812.96 30.12 o 8 0 0 1839.49 1792.14 35.61 o 10 0 0 2355.35 2179.18 38.29 o 12 0 0 1618.24 1662.94 37.07 o 14 0 0 6415.81 6143.29 77.12 o 16 0 0 1597.80 1510.50 41.04 o 18 0 0 771.86 720.20 30.56 o 20 0 0 328.69 312.91 26.46 o 22 0 0 432.19 367.76 30.87 o 24 0 0 432.08 433.32 34.10 o 26 0 0 13.22 29.87 10.51 o 1 1 0 1827.38 1890.03 26.95 o 3 1 0 15137.24 15142.09 216.46 o 5 1 0 1492.13 1416.87 28.22 o 7 1 0 771.08 740.91 25.02 o 9 1 0 115.49 148.29 14.01 o 11 1 0 304.22 294.90 14.12 o 13 1 0 724.05 707.13 26.77 o 15 1 0 556.61 562.57 26.61 o 17 1 0 5233.59 5049.33 82.39 o 19 1 0 29.05 53.20 12.83 o 21 1 0 328.72 357.56 26.53 o 23 1 0 1174.37 1111.50 42.30 o 25 1 0 8.67 5.01 4.81 o 0 2 0 248.35 255.46 21.14 o 2 2 0 190.68 186.13 11.99 o 4 2 0 241.86 222.33 36.59 o 6 2 0 5409.75 5430.15 129.05 o 8 2 0 18.79 7.63 4.15 o 10 2 0 36.47 26.24 3.27 o 12 2 0 1263.66 1235.59 32.42 o 14 2 0 178.96 153.96 32.42 o 16 2 0 0.94 4.94 5.18 o 18 2 0 10.95 27.05 10.65 o 20 2 0 67.26 104.80 15.45 o 22 2 0 15.90 50.13 22.38 o 24 2 0 737.68 762.72 57.79 o 1 3 0 22.41 18.74 4.08 o 3 3 0 0.39 0.00 4.35 o 5 3 0 1114.12 1067.69 47.94 o 7 3 0 3195.54 2916.36 81.75 o 9 3 0 2370.73 2177.23 84.30 o 11 3 0 214.91 241.18 21.44 o 13 3 0 125.50 154.45 17.27 o 15 3 0 0.04 10.15 7.24 o 17 3 0 83.41 72.48 35.71 o 19 3 0 198.41 175.70 24.30 o 21 3 0 9.60 11.72 6.34 o 0 4 0 91.20 94.92 34.63 o 2 4 0 574.98 550.32 52.25 o 4 4 0 15.54 22.46 10.37 o 6 4 0 1.97 13.33 7.42 o 8 4 0 565.85 598.42 36.79 o 10 4 0 15.72 28.37 9.29 o 12 4 0 5.56 23.88 9.64 o 14 4 0 0.04 12.29 8.44 o -25 1 1 3.32 4.45 5.57 o -23 1 1 0.12 33.59 10.02 o -21 1 1 9.30 33.57 10.77 o -19 1 1 90.30 113.28 13.99 o -17 1 1 1254.47 1326.86 42.52 o -15 1 1 3681.27 3595.91 64.61 o -13 1 1 272.34 308.86 17.97 o -11 1 1 259.76 204.87 12.19 o -9 1 1 604.79 567.21 32.96 o -7 1 1 901.97 885.61 27.79 o -5 1 1 12349.90 12319.30 78.99 o -3 1 1 49594.64 48765.07 1077.87 o -1 1 1 22.82 32.84 3.35 o 1 1 1 5675.43 6210.94 80.40 o 3 1 1 14858.81 15281.76 99.93 o 5 1 1 2015.08 1929.45 32.47 o 7 1 1 1842.72 1729.50 31.89 o 9 1 1 8101.01 8327.67 64.17 o 11 1 1 174.04 141.90 8.18 o 13 1 1 825.40 702.27 21.77 o 15 1 1 734.66 730.47 31.59 o 17 1 1 294.27 321.31 22.44 o 19 1 1 8.33 21.23 6.53 o 21 1 1 3295.49 3340.18 69.25 o 23 1 1 0.68 27.11 8.81 o 25 1 1 56.54 56.25 10.19 o -24 2 1 1337.03 1488.01 64.51 o -22 2 1 34.62 84.43 33.75 o -20 2 1 292.44 294.93 24.02 o -18 2 1 84.58 105.78 15.62 o -16 2 1 30.06 29.08 12.85 o -14 2 1 400.32 396.95 31.18 o -12 2 1 2801.37 2627.87 42.25 o -10 2 1 867.56 795.96 45.73 o -8 2 1 1413.60 1306.96 50.86 o -6 2 1 25.36 11.61 3.86 o -4 2 1 209.01 171.54 10.89 o -2 2 1 51.43 67.87 6.40 o 0 2 1 0.49 0.97 2.23 o 2 2 1 4943.13 4953.45 59.01 o 4 2 1 29674.86 28970.34 716.54 o 6 2 1 303.77 289.89 21.82 o 8 2 1 1618.04 1762.37 46.41 o 10 2 1 801.42 721.81 26.09 o 12 2 1 2564.42 2482.39 48.86 o 14 2 1 152.59 147.81 18.83 o 16 2 1 61.17 64.82 11.54 o 18 2 1 788.65 830.57 32.78 o 20 2 1 394.02 399.46 28.85 o 22 2 1 30.72 70.02 26.63 o 24 2 1 237.09 309.78 52.53 o -21 3 1 26.85 44.34 10.64 o -19 3 1 67.50 40.76 23.91 o -17 3 1 77.97 65.60 41.35 o -15 3 1 74.90 82.96 12.41 o -13 3 1 445.82 421.12 28.22 o -11 3 1 572.98 535.86 31.92 o -9 3 1 209.05 220.42 20.27 o -7 3 1 1154.04 1139.84 51.30 o -5 3 1 262.65 257.92 18.28 o -3 3 1 2.53 4.76 4.78 o -1 3 1 1.92 -0.85 3.53 o 1 3 1 174.95 150.06 14.14 o 3 3 1 1.00 12.75 5.48 o 5 3 1 301.41 343.98 27.88 o 7 3 1 1025.26 940.91 46.47 o 9 3 1 269.05 288.39 22.93 o 11 3 1 147.83 100.07 13.83 o 13 3 1 281.74 290.13 23.18 o 15 3 1 0.65 -0.06 9.78 o 17 3 1 33.59 16.40 24.05 o 19 3 1 9.21 10.96 14.31 o 21 3 1 15.59 29.26 9.21 o -14 4 1 40.96 24.52 11.96 o -12 4 1 144.19 118.56 17.20 o -10 4 1 76.63 39.94 10.82 o -8 4 1 232.87 248.58 24.09 o -6 4 1 58.15 78.82 15.52 o -4 4 1 0.02 12.13 6.93 o -2 4 1 225.38 231.40 34.36 o 0 4 1 185.89 178.27 30.92 o 2 4 1 227.83 258.59 36.46 o 4 4 1 156.11 184.90 31.59 o 6 4 1 10.16 20.98 9.20 o 8 4 1 144.34 170.30 20.46 o 10 4 1 59.70 82.01 15.22 o 12 4 1 158.52 170.98 19.96 o 14 4 1 0.89 -0.66 6.82 o -26 0 2 194.84 195.34 33.78 o -24 0 2 116.18 129.29 18.72 o -22 0 2 22.82 20.35 7.47 o -20 0 2 22236.04 22965.46 221.72 o -18 0 2 1038.32 1011.90 36.11 o -16 0 2 4640.65 4429.06 70.65 o -14 0 2 6.05 10.81 4.59 o -12 0 2 18.75 11.12 7.35 o -10 0 2 149.80 122.00 13.64 o -8 0 2 8673.03 7728.44 134.73 o -6 0 2 27322.26 25972.40 123.58 o -4 0 2 3075.71 2885.88 43.26 o 4 0 2 4228.14 4327.00 57.38 o 6 0 2 9394.86 9371.92 72.00 o 8 0 2 6451.09 6573.30 60.75 o 10 0 2 596.06 679.69 21.98 o 12 0 2 9960.57 10830.02 95.18 o 14 0 2 2484.75 2490.07 49.30 o 16 0 2 2993.36 2775.66 56.34 o 18 0 2 2784.89 2641.38 58.77 o 20 0 2 111.40 87.61 13.40 o 22 0 2 212.02 202.22 36.07 o 24 0 2 218.15 220.44 27.40 o 26 0 2 157.36 149.66 24.88 o -25 1 2 12.92 19.17 6.58 o -23 1 2 116.76 151.42 17.42 o -21 1 2 702.90 721.90 35.85 o -19 1 2 46.87 63.12 11.12 o -17 1 2 915.09 934.68 32.50 o -15 1 2 0.74 10.56 5.70 o -13 1 2 917.55 916.75 27.28 o -11 1 2 55.55 50.75 5.59 o -9 1 2 97.38 84.17 16.65 o -7 1 2 511.50 513.50 16.17 o -5 1 2 173.11 209.89 8.76 o -3 1 2 68136.49 68077.31 497.67 o -1 1 2 572.82 608.85 15.96 o 1 1 2 34533.80 34909.78 173.06 o 3 1 2 29039.33 29837.43 141.18 o 5 1 2 1752.38 1883.50 29.83 o 7 1 2 547.73 590.20 15.33 o 9 1 2 1998.23 1987.59 32.78 o 11 1 2 1255.66 1159.55 21.21 o 13 1 2 2109.73 2046.79 41.47 o 15 1 2 790.55 833.47 31.29 o 17 1 2 403.37 376.51 20.89 o 19 1 2 91.41 94.18 10.64 o 21 1 2 338.34 405.07 25.42 o 23 1 2 30.33 49.21 10.00 o 25 1 2 163.94 176.44 17.76 o -24 2 2 12.69 98.48 28.81 o -22 2 2 122.48 153.17 20.17 o -20 2 2 45.91 90.83 18.35 o -18 2 2 0.44 17.82 8.50 o -16 2 2 292.61 283.18 22.69 o -14 2 2 1722.35 1696.82 41.07 o -12 2 2 2.79 7.50 10.38 o -10 2 2 119.39 120.05 10.16 o -8 2 2 1810.17 1746.27 36.34 o -6 2 2 692.39 745.43 23.29 o -4 2 2 6.68 8.83 3.09 o -2 2 2 149.80 176.85 10.27 o 0 2 2 27.59 10.94 2.62 o 2 2 2 1.19 1.91 2.08 o 4 2 2 16468.84 16807.94 306.92 o 6 2 2 8484.69 8700.01 285.37 o 8 2 2 102.50 103.87 10.13 o 10 2 2 1007.40 971.23 34.53 o 12 2 2 427.42 401.17 21.00 o 14 2 2 372.27 326.17 27.69 o 16 2 2 619.31 621.33 33.47 o 18 2 2 1.54 19.27 6.88 o 20 2 2 416.82 421.25 30.27 o 22 2 2 3.53 56.77 28.22 o 24 2 2 197.32 232.09 27.40 o -21 3 2 124.79 126.72 17.39 o -19 3 2 131.64 128.25 19.02 o -17 3 2 1.36 9.96 10.10 o -15 3 2 10.70 15.48 8.18 o -13 3 2 497.19 469.96 30.43 o -11 3 2 2492.40 2479.50 67.69 o -9 3 2 147.78 169.10 17.85 o -7 3 2 922.76 870.48 38.92 o -5 3 2 558.02 567.32 25.15 o -3 3 2 450.69 421.05 22.34 o -1 3 2 146.49 150.09 13.85 o 1 3 2 124.24 127.85 13.10 o 3 3 2 1257.92 1268.09 50.21 o 5 3 2 782.53 776.03 40.63 o 7 3 2 363.60 421.82 31.10 o 9 3 2 657.80 675.72 34.81 o 11 3 2 10.17 10.39 4.42 o 13 3 2 2.40 11.10 5.63 o 15 3 2 135.15 172.74 22.74 o 17 3 2 304.89 266.35 36.36 o 19 3 2 192.32 161.57 40.32 o -14 4 2 1.42 8.51 7.21 o -12 4 2 275.12 245.15 24.67 o -10 4 2 370.56 300.36 27.15 o -8 4 2 258.84 268.02 25.27 o -6 4 2 1.72 4.89 7.27 o -4 4 2 30.33 33.67 11.16 o -2 4 2 4.15 5.54 7.52 o 0 4 2 9.45 14.11 13.75 o 2 4 2 90.11 100.84 24.33 o 4 4 2 12.93 31.80 16.16 o 6 4 2 337.12 308.13 39.29 o 8 4 2 314.38 304.76 26.29 o 10 4 2 1132.74 981.88 47.39 o 12 4 2 16.64 22.96 8.19 o 14 4 2 12.59 19.33 8.90 o -25 1 3 18.81 17.71 7.33 o -23 1 3 2127.04 2220.60 73.86 o -21 1 3 7.18 38.19 9.56 o -19 1 3 556.59 583.98 27.90 o -17 1 3 3588.86 3704.06 63.57 o -15 1 3 795.99 817.64 27.90 o -13 1 3 163.89 184.86 13.74 o -11 1 3 879.01 979.62 32.12 o -9 1 3 4358.03 4200.56 42.55 o -7 1 3 2601.38 2463.15 61.50 o -5 1 3 0.39 0.24 2.15 o -3 1 3 21945.44 21311.58 199.35 o -1 1 3 1712.58 1650.79 32.68 o 1 1 3 80114.55 81231.99 1033.49 o 3 1 3 2772.53 2923.62 45.70 o 5 1 3 13854.97 14341.08 336.15 o 7 1 3 1471.39 1433.67 23.74 o 9 1 3 3127.54 3647.94 58.46 o 11 1 3 90.43 81.27 6.34 o 13 1 3 732.80 676.58 24.22 o 15 1 3 570.58 598.35 24.68 o 17 1 3 78.01 76.34 9.39 o 19 1 3 529.39 548.00 24.04 o 21 1 3 340.64 380.97 23.97 o 23 1 3 38.63 52.77 10.24 o 25 1 3 4.74 3.51 5.04 o -24 2 3 67.66 89.02 18.79 o -22 2 3 199.61 242.42 45.42 o -20 2 3 169.78 194.90 21.09 o -18 2 3 384.30 388.17 28.68 o -16 2 3 2651.89 2649.91 66.24 o -14 2 3 1606.68 1522.65 45.32 o -12 2 3 2422.03 2366.46 48.68 o -10 2 3 96.11 102.81 9.74 o -8 2 3 370.39 389.22 15.01 o -6 2 3 5284.65 5391.15 184.02 o -4 2 3 1253.00 1191.99 22.36 o -2 2 3 914.11 879.14 23.42 o 0 2 3 664.24 627.60 22.70 o 2 2 3 440.76 377.71 16.31 o 4 2 3 3166.49 3197.44 74.22 o 6 2 3 5277.60 5412.69 209.93 o 8 2 3 192.56 205.35 14.27 o 10 2 3 1743.56 1683.04 40.03 o 12 2 3 172.99 156.98 11.94 o 14 2 3 429.97 436.89 29.42 o 16 2 3 264.34 285.85 31.33 o 18 2 3 304.66 305.53 20.08 o 20 2 3 127.07 150.24 17.73 o 22 2 3 125.36 158.90 23.16 o 24 2 3 5.39 88.87 18.95 o -21 3 3 17.14 38.20 10.34 o -19 3 3 37.13 31.08 12.02 o -17 3 3 100.13 56.42 34.93 o -15 3 3 157.36 161.44 18.29 o -13 3 3 128.84 166.53 18.56 o -11 3 3 21.89 47.86 12.47 o -9 3 3 20.92 10.90 4.95 o -7 3 3 149.41 146.62 16.98 o -5 3 3 184.66 176.54 13.20 o -3 3 3 211.55 203.58 15.01 o -1 3 3 608.01 586.33 26.62 o 1 3 3 116.84 140.64 14.20 o 3 3 3 820.91 820.56 40.99 o 5 3 3 80.75 111.48 16.48 o 7 3 3 769.38 786.91 42.46 o 9 3 3 425.39 421.17 27.86 o 11 3 3 9.23 10.48 6.12 o 13 3 3 0.04 6.56 7.93 o 15 3 3 286.92 278.93 28.97 o 17 3 3 349.93 242.09 55.92 o 19 3 3 7.56 7.31 18.10 o -14 4 3 3.02 12.36 9.29 o -12 4 3 44.32 56.86 12.17 o -10 4 3 33.17 100.56 17.05 o -8 4 3 116.69 107.31 16.24 o -6 4 3 7.09 14.18 8.30 o -4 4 3 49.82 50.02 12.86 o -2 4 3 15.69 3.91 9.10 o 0 4 3 66.57 77.59 21.27 o 2 4 3 28.56 25.55 15.58 o 4 4 3 114.35 112.46 24.89 o 6 4 3 1.30 6.01 9.89 o 8 4 3 254.29 203.35 21.90 o 10 4 3 115.57 102.25 17.15 o 12 4 3 0.42 14.13 11.29 o 14 4 3 3.78 28.94 11.91 o -26 0 4 21.84 28.60 14.88 o -24 0 4 12.98 45.94 16.67 o -22 0 4 5.07 8.49 7.21 o -20 0 4 218.52 228.65 32.13 o -18 0 4 20.47 14.46 6.96 o -16 0 4 74.19 54.72 17.01 o -14 0 4 944.62 942.55 35.58 o -12 0 4 624.66 574.30 25.77 o -10 0 4 1434.07 1203.03 33.29 o -8 0 4 22727.21 22202.78 171.02 o -6 0 4 43.19 41.48 5.64 o -4 0 4 4046.22 4009.42 75.14 o -2 0 4 76775.89 73922.52 242.98 o 2 0 4 19235.05 19300.32 339.92 o 4 0 4 5996.53 6581.47 91.28 o 6 0 4 10365.41 10551.51 99.62 o 8 0 4 1425.41 1509.80 29.86 o 10 0 4 17493.46 18690.29 143.17 o 12 0 4 2941.97 2901.45 50.30 o 14 0 4 3270.03 3187.79 72.03 o 16 0 4 12.86 12.78 4.29 o 18 0 4 1015.98 959.18 35.91 o 20 0 4 62.56 63.42 13.88 o 22 0 4 296.95 299.38 31.75 o 24 0 4 189.96 204.15 28.42 o 26 0 4 113.10 146.89 39.50 o -25 1 4 14.61 16.91 6.27 o -23 1 4 1226.35 1328.58 51.33 o -21 1 4 3.81 24.26 8.48 o -19 1 4 3060.67 3132.72 68.57 o -17 1 4 2419.47 2521.96 57.66 o -15 1 4 1626.33 1690.84 43.45 o -13 1 4 770.26 832.35 28.48 o -11 1 4 1296.05 1261.83 27.74 o -9 1 4 56.78 55.79 9.05 o -7 1 4 384.94 423.59 13.92 o -5 1 4 8422.68 8331.37 284.62 o -3 1 4 7.15 11.46 3.27 o -1 1 4 1652.53 1669.58 35.54 o 1 1 4 24394.31 25095.88 340.47 o 3 1 4 6342.21 6509.38 89.89 o 5 1 4 262.68 243.63 8.92 o 7 1 4 3820.31 4174.11 71.18 o 9 1 4 10579.65 11845.08 141.13 o 11 1 4 2217.74 2309.28 47.58 o 13 1 4 262.09 329.40 17.22 o 15 1 4 199.21 207.51 16.25 o 17 1 4 85.11 88.45 9.50 o 19 1 4 337.28 364.62 19.65 o 21 1 4 181.82 187.42 17.24 o 23 1 4 230.22 247.89 20.27 o 25 1 4 80.00 72.68 11.50 o -24 2 4 2.71 41.17 22.82 o -22 2 4 9.83 49.26 25.91 o -20 2 4 2.80 48.72 22.88 o -18 2 4 12.78 32.90 7.71 o -16 2 4 2747.08 2654.77 66.47 o -14 2 4 2206.60 2148.17 49.09 o -12 2 4 267.71 294.67 19.19 o -10 2 4 940.09 913.87 29.78 o -8 2 4 718.81 707.09 29.23 o -6 2 4 2533.23 2770.96 73.28 o -4 2 4 1437.03 1471.57 59.35 o -2 2 4 366.43 377.71 14.95 o 0 2 4 2058.58 2009.52 44.08 o 2 2 4 163.53 152.50 9.04 o 4 2 4 4780.87 5018.95 148.45 o 6 2 4 1894.95 2060.47 48.56 o 8 2 4 42.43 46.67 7.31 o 10 2 4 0.02 7.43 4.45 o 12 2 4 26.82 34.98 6.07 o 14 2 4 153.27 110.07 20.59 o 16 2 4 413.02 408.99 28.40 o 18 2 4 23.85 44.62 8.46 o 20 2 4 0.30 22.75 11.85 o 22 2 4 56.48 118.53 19.11 o 24 2 4 549.38 612.86 37.57 o -21 3 4 22.36 36.74 10.32 o -19 3 4 49.65 55.13 16.04 o -17 3 4 179.77 176.19 26.48 o -15 3 4 546.97 498.54 31.14 o -13 3 4 641.91 648.78 40.00 o -11 3 4 514.52 486.19 33.71 o -9 3 4 45.94 34.70 9.60 o -7 3 4 224.45 207.93 19.68 o -5 3 4 909.50 914.57 46.41 o -3 3 4 153.98 141.40 13.89 o -1 3 4 1.80 5.41 4.16 o 1 3 4 218.15 236.55 18.15 o 3 3 4 2801.71 2974.83 79.26 o 5 3 4 1395.96 1433.82 55.01 o 7 3 4 4311.55 4210.90 97.21 o 9 3 4 1433.43 1388.74 65.26 o 11 3 4 49.44 38.84 8.81 o 13 3 4 261.76 221.27 20.25 o 15 3 4 34.65 60.23 14.37 o 17 3 4 242.70 199.10 56.12 o 19 3 4 135.53 115.27 30.36 o -14 4 4 45.47 46.36 10.86 o -12 4 4 46.82 57.67 13.65 o -10 4 4 1469.90 1344.98 56.98 o -8 4 4 2.15 9.79 6.24 o -6 4 4 16.42 15.20 6.28 o -4 4 4 69.38 55.66 12.91 o -2 4 4 0.10 4.16 6.89 o 0 4 4 236.97 235.88 26.34 o 2 4 4 1.95 5.54 7.92 o 4 4 4 208.84 177.64 30.99 o 6 4 4 229.45 240.21 35.17 o 8 4 4 562.92 441.40 37.82 o 10 4 4 12.41 24.79 9.01 o 12 4 4 155.97 160.67 19.30 o 14 4 4 141.77 147.71 22.81 o -25 1 5 22.48 48.77 10.96 o -23 1 5 1053.18 1165.51 47.97 o -21 1 5 204.36 233.72 20.54 o -19 1 5 2680.99 2738.72 64.03 o -17 1 5 1175.94 1204.81 40.03 o -15 1 5 3131.30 3224.30 59.81 o -13 1 5 158.64 184.81 17.24 o -11 1 5 6077.28 6479.55 60.28 o -9 1 5 603.08 536.66 24.98 o -7 1 5 343.19 345.27 12.48 o -5 1 5 556.32 505.42 11.55 o -3 1 5 4213.23 3948.63 71.03 o -1 1 5 7554.33 7416.86 174.80 o 1 1 5 188.71 176.97 7.51 o 3 1 5 15.57 15.13 3.07 o 5 1 5 51.73 31.46 3.29 o 7 1 5 11341.48 12183.48 218.54 o 9 1 5 363.03 443.35 24.35 o 11 1 5 2425.33 2548.40 49.80 o 13 1 5 8413.46 8785.71 161.85 o 15 1 5 51.61 56.92 8.60 o 17 1 5 2.97 15.25 4.93 o 19 1 5 759.52 763.23 32.08 o 21 1 5 528.50 568.29 29.11 o 23 1 5 75.21 97.91 13.34 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