#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/30/2233044.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233044_Fobs loop_ _publ_author_name 'Semenaka, Valentyna V.' 'Nesterova, Oksana V.' 'Kokozay, Volodymyr N.' 'Zubatyuk, Roman I.' 'Shishkin, Oleg V.' _publ_section_title ; Bis{\m~2~-2-[(2-hydroxyethyl)(methyl)amino]ethanolato}bis(\m~3~-N-methyl-2,2'-azanediyldiethanolato)tetrakis(thiocyanatato-\kN)dichromium(III)dimanganese(II) dimethylformamide tetrasolvate ; _journal_coeditor_code ZK2033 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1864 _journal_page_last m1865 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.123 _cell_angle_gamma 90.000 _cell_length_a 11.5207 _cell_length_b 13.5261 _cell_length_c 18.5825 _exptl_crystal_F_000 1263.73 _reflns_d_resolution_high 0.7107 _[local]_cod_data_source_file zk2033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' koko233 R = 0.03' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4383.56 4375.12 57.32 o 4 0 0 6285.45 6280.88 96.46 o 6 0 0 216.74 155.10 46.48 o 8 0 0 14314.58 14358.15 211.47 o 10 0 0 13.74 0.00 69.58 o 12 0 0 369.68 320.10 87.06 o 14 0 0 26.14 10.79 90.98 o 2 1 0 14.62 45.40 26.59 o 3 1 0 3989.59 4130.99 61.20 o 4 1 0 1293.24 1378.99 41.29 o 5 1 0 5069.48 5148.97 73.29 o 6 1 0 221.52 274.93 31.98 o 7 1 0 45.09 34.08 34.29 o 8 1 0 97.12 82.60 42.89 o 9 1 0 775.66 842.00 55.54 o 10 1 0 114.53 73.13 45.70 o 11 1 0 41.88 42.86 47.21 o 12 1 0 95.09 62.39 56.02 o 13 1 0 760.00 806.31 72.82 o 14 1 0 26.00 27.33 66.87 o 15 1 0 105.58 115.16 68.97 o 2 2 0 44860.99 45183.94 360.54 o 3 2 0 23157.82 24429.55 158.21 o 4 2 0 18962.52 18647.47 77.23 o 5 2 0 888.59 1042.52 27.30 o 6 2 0 5284.13 5054.95 87.06 o 7 2 0 685.37 691.69 48.72 o 8 2 0 2.26 0.34 24.09 o 9 2 0 437.07 394.93 26.31 o 10 2 0 959.25 985.08 65.02 o 11 2 0 1417.05 1471.49 76.46 o 12 2 0 1862.63 1958.57 104.23 o 13 2 0 1058.89 1102.79 81.45 o 14 2 0 521.33 409.68 69.93 o 15 2 0 15.92 46.84 73.66 o 1 3 0 8552.08 8321.66 105.46 o 2 3 0 2978.35 3010.79 40.31 o 3 3 0 15183.68 15229.11 101.35 o 4 3 0 2936.54 3111.52 40.86 o 6 3 0 1532.65 1722.67 43.36 o 7 3 0 124.95 125.88 19.28 o 8 3 0 144.83 116.30 20.75 o 9 3 0 249.88 250.91 31.51 o 10 3 0 513.15 571.34 57.37 o 11 3 0 122.84 97.62 50.23 o 12 3 0 185.55 107.24 54.87 o 13 3 0 1194.32 1310.32 82.99 o 14 3 0 6.11 2.68 62.79 o 15 3 0 128.19 118.58 98.52 o 0 4 0 3308.59 3568.12 36.77 o 1 4 0 24.41 43.74 15.15 o 2 4 0 32972.52 33373.24 194.46 o 3 4 0 239.00 252.79 22.31 o 4 4 0 1906.02 2106.72 38.14 o 5 4 0 1769.08 1758.04 43.56 o 6 4 0 1810.37 1783.27 58.69 o 7 4 0 84.25 101.31 22.62 o 8 4 0 546.64 500.95 28.06 o 9 4 0 148.75 108.69 33.94 o 10 4 0 3901.23 4162.78 145.43 o 11 4 0 15.92 5.88 75.19 o 12 4 0 936.93 891.33 94.71 o 13 4 0 405.72 343.63 87.88 o 14 4 0 123.34 162.52 92.55 o 15 4 0 96.66 123.36 92.84 o 1 5 0 7945.18 7578.34 68.65 o 2 5 0 22.49 10.73 24.48 o 3 5 0 795.56 761.84 30.76 o 4 5 0 443.62 481.86 25.87 o 5 5 0 39.39 40.50 33.05 o 6 5 0 920.92 957.97 33.71 o 7 5 0 7236.65 7430.51 121.92 o 8 5 0 701.03 744.25 44.85 o 9 5 0 1597.44 1602.66 59.93 o 10 5 0 34.31 22.95 38.45 o 11 5 0 165.08 163.58 80.28 o 12 5 0 234.40 199.84 79.00 o 13 5 0 59.16 11.86 84.65 o 14 5 0 7.46 1.81 100.89 o 15 5 0 80.50 62.84 109.19 o 0 6 0 2928.64 3003.89 45.53 o 1 6 0 2871.54 2823.35 31.76 o 2 6 0 119.86 125.78 14.99 o 3 6 0 2886.88 3041.07 54.11 o 4 6 0 12680.87 12291.72 101.41 o 5 6 0 2445.76 2451.88 48.99 o 6 6 0 1128.94 1095.66 61.87 o 7 6 0 152.62 131.66 42.99 o 8 6 0 269.93 160.19 44.72 o 9 6 0 221.90 191.49 39.38 o 10 6 0 1363.57 1324.41 64.15 o 11 6 0 1305.98 1417.93 112.32 o 12 6 0 1272.84 1332.61 109.14 o 13 6 0 12.88 90.36 96.65 o 14 6 0 295.48 326.01 99.80 o 1 7 0 226.50 260.66 17.41 o 2 7 0 323.96 286.02 16.56 o 3 7 0 10979.55 10656.36 104.46 o 4 7 0 1574.69 1568.16 46.54 o 5 7 0 17060.92 16974.93 128.53 o 6 7 0 29.95 16.85 42.29 o 7 7 0 4.19 15.76 44.24 o 8 7 0 632.35 563.41 58.26 o 9 7 0 11.45 22.55 35.16 o 10 7 0 3.52 0.00 44.20 o 11 7 0 388.15 339.97 90.51 o 12 7 0 220.46 206.20 93.15 o 13 7 0 676.70 609.80 100.45 o 14 7 0 1.81 4.14 105.24 o 0 8 0 9792.62 9525.39 94.02 o 1 8 0 596.43 564.96 23.74 o 2 8 0 255.96 206.27 17.31 o 3 8 0 38.68 49.22 14.32 o 4 8 0 2142.97 2094.81 46.86 o 5 8 0 260.81 237.06 27.83 o 6 8 0 935.31 875.99 52.66 o 7 8 0 64.28 36.51 34.13 o 8 8 0 2052.32 2216.68 72.23 o 9 8 0 4.05 0.00 37.09 o 10 8 0 327.03 268.29 64.37 o 11 8 0 14.56 21.63 73.47 o 12 8 0 12.53 0.00 75.25 o 13 8 0 50.53 79.62 91.70 o 14 8 0 38.08 39.11 106.15 o 1 9 0 5554.76 5643.09 116.52 o 2 9 0 1911.37 1826.76 33.41 o 3 9 0 1309.78 1239.66 46.68 o 4 9 0 28.45 27.34 25.79 o 5 9 0 95.54 119.66 29.09 o 6 9 0 95.53 50.58 28.60 o 7 9 0 2527.27 2547.09 115.62 o 8 9 0 183.22 88.91 39.82 o 9 9 0 4533.92 4637.74 100.42 o 10 9 0 16.92 27.69 64.43 o 11 9 0 274.77 266.20 54.76 o 12 9 0 10.71 0.00 79.49 o 13 9 0 82.50 45.57 94.11 o 0 10 0 1675.95 1585.73 86.89 o 1 10 0 506.04 435.63 44.69 o 2 10 0 16.72 5.21 37.71 o 3 10 0 165.89 157.18 31.33 o 4 10 0 720.65 747.29 40.35 o 5 10 0 22.14 19.63 29.49 o 6 10 0 65.21 61.95 30.12 o 7 10 0 598.01 566.77 50.40 o 8 10 0 1198.45 1260.99 64.53 o 9 10 0 507.26 441.53 52.16 o 10 10 0 179.74 170.50 68.15 o 11 10 0 19.71 20.98 52.14 o 12 10 0 32.80 18.45 89.31 o 13 10 0 0.89 25.16 90.18 o 1 11 0 1238.85 1199.32 58.40 o 2 11 0 54.47 32.81 41.22 o 3 11 0 1838.75 1758.61 65.90 o 4 11 0 0.36 1.42 33.31 o 5 11 0 4296.40 4333.43 81.15 o 6 11 0 6.82 0.00 32.67 o 7 11 0 1684.59 1732.73 71.62 o 8 11 0 25.58 22.03 44.83 o 9 11 0 402.37 362.77 53.63 o 10 11 0 45.62 38.12 70.37 o 11 11 0 1331.93 1299.80 112.06 o 12 11 0 2.53 0.00 102.02 o 0 12 0 7.62 36.25 61.92 o 1 12 0 170.98 167.21 46.40 o 2 12 0 36.51 28.37 41.61 o 3 12 0 64.17 36.37 40.28 o 4 12 0 732.81 699.49 54.31 o 5 12 0 4.69 6.59 41.23 o 6 12 0 0.88 0.00 35.35 o 7 12 0 206.78 170.76 48.55 o 8 12 0 93.82 76.56 50.17 o 9 12 0 36.32 33.80 50.69 o 10 12 0 4.83 0.76 80.54 o 11 12 0 16.65 39.58 77.51 o 12 12 0 415.49 483.54 118.26 o 1 13 0 1820.58 1871.74 73.80 o 2 13 0 9.54 0.00 43.35 o 3 13 0 487.60 463.00 53.04 o 4 13 0 145.61 170.06 46.15 o 5 13 0 240.59 216.94 48.43 o 6 13 0 198.80 154.89 78.93 o 7 13 0 644.60 602.36 91.43 o 8 13 0 254.41 189.06 81.59 o 9 13 0 1959.18 2353.58 137.48 o 10 13 0 153.11 165.66 82.04 o 11 13 0 423.66 381.91 101.03 o 0 14 0 1377.51 1282.22 96.33 o 1 14 0 90.63 17.01 46.31 o 2 14 0 386.47 332.98 54.98 o 3 14 0 395.05 373.08 50.26 o 4 14 0 409.66 397.50 53.62 o 5 14 0 8.29 7.09 47.40 o 6 14 0 7.74 5.80 80.64 o 7 14 0 45.77 34.29 84.39 o 8 14 0 1317.62 1391.99 117.06 o 9 14 0 78.17 163.62 89.49 o 10 14 0 268.47 274.53 93.08 o 1 15 0 0.04 0.00 47.43 o 2 15 0 552.93 488.37 57.39 o 3 15 0 1436.51 1497.17 77.09 o 4 15 0 123.62 77.14 48.71 o 5 15 0 529.73 493.55 62.94 o 6 15 0 93.03 135.08 90.38 o 7 15 0 113.22 100.56 92.76 o 8 15 0 32.13 6.55 81.24 o 9 15 0 140.47 118.72 98.08 o 0 16 0 186.87 168.41 83.41 o 1 16 0 19.77 9.60 56.04 o 2 16 0 136.78 82.59 52.01 o 3 16 0 432.16 351.64 61.93 o 4 16 0 855.33 919.20 73.37 o 5 16 0 66.82 90.62 92.50 o 6 16 0 689.10 864.53 114.45 o 7 16 0 30.34 24.75 94.49 o 8 16 0 9.76 19.42 95.40 o 1 17 0 773.69 826.56 77.44 o 2 17 0 451.39 427.88 64.15 o 3 17 0 46.22 70.44 57.70 o 4 17 0 10.79 3.93 57.10 o 5 17 0 103.83 134.97 97.61 o 6 17 0 327.11 302.97 98.65 o 7 17 0 79.32 191.91 100.03 o 0 18 0 1447.27 1450.11 125.31 o 1 18 0 143.47 92.35 59.56 o 2 18 0 194.10 162.65 66.94 o 3 18 0 52.35 50.76 65.77 o 4 18 0 0.91 0.00 88.93 o 5 18 0 83.46 75.38 103.19 o -15 0 1 545.44 438.92 115.13 o -13 0 1 829.06 799.71 109.15 o -11 0 1 888.71 892.66 95.50 o -9 0 1 13752.34 14478.95 228.21 o -7 0 1 7876.34 8238.87 149.08 o -5 0 1 374.61 359.51 45.87 o -3 0 1 13167.04 13313.63 117.04 o 3 0 1 15241.48 15929.74 130.98 o 5 0 1 2637.49 2525.91 75.04 o 7 0 1 29399.04 29546.20 273.24 o 9 0 1 2182.94 2231.72 102.97 o 11 0 1 2747.14 2792.55 126.33 o 13 0 1 122.00 92.24 74.92 o 15 0 1 285.69 227.80 111.24 o -15 1 1 2.66 15.41 70.01 o -14 1 1 2.24 0.00 56.11 o -13 1 1 13.55 6.40 57.33 o -12 1 1 113.25 78.41 57.25 o -11 1 1 84.49 68.59 48.09 o -10 1 1 157.56 183.40 50.89 o -9 1 1 109.00 112.69 44.37 o -8 1 1 4956.90 4964.89 93.65 o -7 1 1 543.32 589.74 42.71 o -6 1 1 153.30 149.97 28.94 o -5 1 1 3865.67 3926.73 63.73 o -4 1 1 3990.14 4065.57 246.70 o -3 1 1 2052.80 2221.67 27.17 o -2 1 1 4886.18 4990.64 28.75 o 1 1 1 87.15 69.15 13.65 o 2 1 1 712.18 754.77 33.81 o 3 1 1 5702.42 5926.09 63.58 o 4 1 1 2732.16 2789.72 52.09 o 5 1 1 332.38 358.61 35.02 o 6 1 1 500.48 493.47 36.95 o 7 1 1 1104.34 1181.84 62.29 o 8 1 1 11.63 13.88 36.19 o 9 1 1 807.17 799.09 57.68 o 10 1 1 511.25 472.23 54.63 o 11 1 1 176.37 143.53 54.42 o 12 1 1 195.85 180.90 89.20 o 13 1 1 27.94 62.29 60.49 o 14 1 1 14.75 26.39 65.64 o 15 1 1 13.68 0.00 72.12 o -15 2 1 28.72 26.62 70.87 o -14 2 1 0.41 0.00 64.76 o -13 2 1 3442.77 3804.28 115.66 o -12 2 1 6.42 7.21 56.99 o -11 2 1 1081.24 1016.35 65.80 o -10 2 1 960.72 930.31 62.14 o -9 2 1 239.02 175.80 29.60 o -8 2 1 61.68 35.90 22.32 o -7 2 1 2059.18 2113.68 52.32 o -6 2 1 7995.42 7944.65 65.99 o -5 2 1 11389.77 11129.38 117.99 o -4 2 1 5479.74 5680.06 52.14 o -2 2 1 13.72 38.77 11.07 o -1 2 1 1172.24 1241.38 16.28 o 0 2 1 480.70 542.29 17.75 o 1 2 1 1985.62 1952.44 22.65 o 2 2 1 658.24 655.52 24.42 o 3 2 1 15017.42 14953.00 85.20 o 4 2 1 315.74 403.37 43.50 o 5 2 1 28505.62 28625.09 120.05 o 6 2 1 2686.92 2679.73 52.42 o 7 2 1 2074.88 2126.99 44.71 o 8 2 1 1256.48 1226.48 40.93 o 9 2 1 869.24 735.37 39.93 o 10 2 1 243.11 237.85 52.23 o 11 2 1 775.51 774.50 64.96 o 12 2 1 27.39 48.70 54.10 o 13 2 1 1578.97 1734.66 89.21 o 14 2 1 1.26 60.07 98.27 o 15 2 1 306.67 345.77 73.13 o -15 3 1 6.07 13.68 106.22 o -14 3 1 765.87 793.46 79.28 o -13 3 1 2.14 0.00 53.11 o -12 3 1 2882.28 3065.03 100.35 o -11 3 1 4.10 30.76 46.60 o -10 3 1 118.15 156.46 47.21 o -9 3 1 680.14 645.61 37.15 o -8 3 1 605.10 515.54 23.23 o -7 3 1 763.96 812.24 24.27 o -6 3 1 3161.81 3294.02 36.50 o -5 3 1 40.16 56.72 14.43 o -4 3 1 17110.00 16695.48 172.14 o -3 3 1 5263.26 5209.75 45.71 o -2 3 1 3475.00 3293.00 30.73 o -1 3 1 141.37 130.35 15.60 o 0 3 1 17470.47 17660.21 136.34 o 1 3 1 26123.20 26869.24 155.12 o 2 3 1 300.15 281.91 20.48 o 3 3 1 1025.63 1015.26 30.52 o 4 3 1 6312.96 6070.27 59.95 o 5 3 1 3112.07 3266.64 47.98 o 6 3 1 399.73 323.96 21.51 o 7 3 1 97.78 57.92 19.91 o 8 3 1 1102.80 1129.41 32.48 o 9 3 1 36.59 44.52 23.32 o 10 3 1 4.32 13.37 51.28 o 11 3 1 2.22 0.00 52.80 o 12 3 1 1268.14 1322.20 79.53 o 13 3 1 4.42 6.35 63.63 o 14 3 1 452.12 458.79 75.89 o 15 3 1 187.80 173.30 103.55 o -15 4 1 259.90 272.51 107.92 o -14 4 1 83.86 51.04 90.23 o -13 4 1 140.06 168.52 85.23 o -12 4 1 29.66 19.58 79.23 o -11 4 1 230.64 189.20 83.14 o -10 4 1 179.76 129.00 60.28 o -9 4 1 2096.50 2003.12 47.27 o -8 4 1 2099.15 2163.89 138.38 o -7 4 1 8818.08 7925.14 911.36 o -6 4 1 181.34 151.57 18.98 o -5 4 1 1758.24 1636.00 32.87 o -4 4 1 5343.83 5340.06 52.19 o -3 4 1 1863.79 1946.43 59.76 o -2 4 1 2419.41 2551.93 31.53 o -1 4 1 4355.41 4169.24 43.78 o 0 4 1 11817.04 11918.94 122.42 o 1 4 1 14273.43 13730.53 91.61 o 2 4 1 1165.95 1197.69 35.09 o 3 4 1 613.88 640.44 22.01 o 4 4 1 423.48 342.60 24.01 o 5 4 1 9135.82 9266.75 100.79 o 6 4 1 120.90 140.06 25.14 o 7 4 1 1129.30 1103.77 34.23 o 8 4 1 1081.73 1088.25 36.36 o 9 4 1 5809.72 6188.49 98.44 o 10 4 1 176.43 188.66 77.72 o 11 4 1 15.56 1.49 63.78 o 12 4 1 64.44 71.14 83.56 o 13 4 1 23.67 0.00 90.51 o 14 4 1 12.08 0.00 99.30 o 15 4 1 18.12 10.80 105.13 o -15 5 1 48.89 13.32 97.82 o -14 5 1 0.83 8.40 82.66 o -13 5 1 148.46 112.58 80.97 o -12 5 1 717.36 633.77 100.04 o -11 5 1 25.42 0.00 66.25 o -10 5 1 4166.44 4263.86 91.28 o -9 5 1 712.81 669.49 50.99 o -8 5 1 3545.07 3532.44 87.19 o -7 5 1 12.67 10.82 20.46 o -6 5 1 149.56 131.45 36.61 o -5 5 1 1520.13 1576.36 61.08 o -4 5 1 4868.78 5127.89 50.91 o -3 5 1 829.73 873.86 27.14 o -2 5 1 1239.09 1208.65 26.69 o -1 5 1 695.42 706.71 23.07 o 0 5 1 12702.80 11940.38 70.10 o 1 5 1 2300.25 2411.47 34.41 o 2 5 1 2512.38 2224.28 44.95 o 3 5 1 58.94 81.25 22.82 o 4 5 1 1796.94 1802.97 42.06 o 5 5 1 529.33 546.98 29.43 o 6 5 1 889.43 914.90 36.14 o 7 5 1 20.64 5.94 25.36 o 8 5 1 6288.88 6473.09 73.70 o 9 5 1 3.11 21.44 33.88 o 10 5 1 776.54 852.10 84.23 o 11 5 1 30.92 0.00 77.24 o 12 5 1 224.24 182.02 85.15 o 13 5 1 556.31 470.31 104.58 o 14 5 1 73.66 23.14 90.63 o -14 6 1 125.88 102.96 103.50 o -13 6 1 676.65 726.97 104.51 o -12 6 1 657.42 582.85 98.72 o -11 6 1 1684.04 1532.36 106.99 o -10 6 1 419.41 352.02 45.62 o -9 6 1 35.66 44.67 27.78 o -8 6 1 230.95 154.28 31.80 o -7 6 1 3447.13 3266.91 67.46 o -6 6 1 340.17 343.90 33.38 o -5 6 1 4526.00 4334.88 71.36 o -4 6 1 4097.42 4047.18 53.80 o -3 6 1 10649.01 10669.33 79.67 o -2 6 1 169.62 159.63 18.63 o -1 6 1 4868.27 4941.31 52.61 o 0 6 1 977.27 1060.34 31.35 o 1 6 1 958.12 942.30 26.05 o 2 6 1 4893.21 4882.08 68.53 o 3 6 1 7944.89 8080.13 85.40 o 4 6 1 1798.01 1752.73 44.42 o 5 6 1 5981.12 5986.84 118.55 o 6 6 1 1543.80 1578.42 45.81 o 7 6 1 1104.06 1127.33 42.88 o 8 6 1 3465.58 3438.94 103.61 o 9 6 1 108.79 90.55 39.56 o 10 6 1 307.74 342.83 80.98 o 11 6 1 322.13 357.39 87.05 o 12 6 1 418.29 393.62 97.68 o 13 6 1 907.64 822.34 105.12 o 14 6 1 205.07 103.25 100.42 o -14 7 1 548.65 374.60 104.22 o -13 7 1 3.28 0.00 92.76 o -12 7 1 2496.54 2613.30 140.90 o -11 7 1 50.75 63.26 81.14 o -10 7 1 9.99 34.56 42.36 o -9 7 1 444.78 389.89 40.18 o -8 7 1 149.56 139.98 34.75 o -7 7 1 141.45 109.37 33.48 o -6 7 1 2701.11 2663.83 46.65 o -5 7 1 71.13 43.99 22.07 o -4 7 1 13040.47 12829.64 97.14 o -3 7 1 186.97 158.76 23.89 o -2 7 1 6882.25 6699.52 67.52 o -1 7 1 865.44 849.61 29.54 o 0 7 1 189.64 177.92 18.56 o 1 7 1 2856.63 2962.84 41.99 o 2 7 1 1022.93 1030.29 33.89 o 3 7 1 3511.01 3624.00 69.64 o 4 7 1 3417.11 3140.63 61.99 o 5 7 1 14.27 0.00 46.63 o 6 7 1 2455.05 2416.69 88.54 o 7 7 1 1652.85 1562.25 79.49 o 8 7 1 4.52 0.00 47.06 o 9 7 1 24.77 24.56 49.08 o 10 7 1 28.81 19.68 67.49 o 11 7 1 97.36 55.79 68.54 o 12 7 1 1337.22 1258.43 117.88 o 13 7 1 33.73 14.33 99.05 o 14 7 1 500.45 526.17 107.60 o -14 8 1 8.05 0.00 89.81 o -13 8 1 14.80 0.00 100.30 o -12 8 1 3.96 15.12 85.87 o -11 8 1 34.49 9.55 75.01 o -10 8 1 467.24 380.13 67.56 o -9 8 1 2706.41 2911.72 77.05 o -8 8 1 157.85 128.39 37.92 o -7 8 1 21.97 36.71 34.50 o -6 8 1 273.79 253.80 28.44 o -5 8 1 318.36 330.32 28.30 o -4 8 1 7.10 8.75 24.79 o -3 8 1 6037.29 6028.53 72.17 o -2 8 1 12.45 10.02 23.07 o -1 8 1 2134.75 2057.63 42.73 o 0 8 1 175.09 150.58 21.28 o 1 8 1 1376.67 1334.23 30.24 o 2 8 1 849.77 892.17 29.89 o 3 8 1 696.66 643.94 26.50 o 4 8 1 3016.02 2999.30 65.82 o 5 8 1 3111.20 2990.76 65.44 o 6 8 1 217.88 198.18 54.17 o 7 8 1 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