#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/30/2233047.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233047_Fobs loop_ _publ_author_name 'Tomyn, Stefania' 'Gumienna-Kontecka, El\.zbieta' 'Usenko, Natalia I.' 'Iskenderov, Turganbay S.' 'Prisyazhnaya, Elena V.' _publ_section_title ; cis-Bis(2,2'-bipyridine-\k^2^N,N')bis(dimethyl sulfoxide-\kO)zinc bis(tetraphenylborate) dimethyl sulfoxide monosolvate ; _journal_coeditor_code ZL2419 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1774 _journal_page_last m1775 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.225 _cell_angle_gamma 90.000 _cell_length_a 13.8836 _cell_length_b 18.0029 _cell_length_c 26.1594 _exptl_crystal_F_000 2632.00 _reflns_d_resolution_high 0.7450 _[local]_cod_data_source_file zl2419Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 352.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 38582.78 40722.76 187.81 o 4 0 0 124136.32 126039.37 564.62 o 5 0 0 6227.29 6701.90 106.05 o 6 0 0 4728.13 5008.61 61.71 o 7 0 0 7883.11 8322.82 83.90 o 8 0 0 15.88 45.73 39.51 o 9 0 0 2238.04 2117.84 67.01 o 10 0 0 600.97 524.77 59.98 o 14 0 0 3471.05 3271.57 187.81 o 15 0 0 941.00 1010.14 187.81 o 16 0 0 766.43 514.85 203.81 o 17 0 0 3.12 17.61 131.07 o 18 0 0 96.37 87.71 129.06 o 2 1 0 20076.85 19738.41 104.87 o 3 1 0 30353.80 29806.90 98.36 o 4 1 0 13391.26 12637.13 51.25 o 5 1 0 7977.61 8597.34 136.57 o 6 1 0 22737.13 22069.37 171.63 o 7 1 0 2401.90 2725.75 41.00 o 8 1 0 1629.32 1539.81 64.56 o 9 1 0 4084.71 4179.87 50.54 o 10 1 0 10083.80 10395.16 122.92 o 11 1 0 127.77 -4.74 118.49 o 12 1 0 105.59 103.68 123.23 o 13 1 0 3.01 176.55 137.45 o 14 1 0 686.12 638.67 172.41 o 15 1 0 386.80 445.89 125.14 o 16 1 0 81.69 104.83 101.40 o 17 1 0 1232.07 1237.50 123.57 o 18 1 0 13.08 -8.59 96.54 o 2 2 0 103.38 120.33 18.56 o 3 2 0 54260.96 51822.71 546.27 o 4 2 0 59344.70 59020.90 455.11 o 5 2 0 43.45 100.43 19.00 o 6 2 0 327.50 367.32 25.39 o 7 2 0 398.28 589.06 30.82 o 8 2 0 3167.61 3367.70 61.01 o 9 2 0 15547.32 15661.75 121.87 o 10 2 0 264.53 251.23 47.49 o 11 2 0 14584.34 14942.37 125.10 o 12 2 0 3779.07 3827.89 175.96 o 13 2 0 188.12 164.70 117.31 o 14 2 0 1473.90 1276.16 192.55 o 15 2 0 3941.34 4269.86 215.66 o 16 2 0 941.69 1151.15 142.26 o 17 2 0 189.93 193.67 92.44 o 18 2 0 122.18 158.18 160.54 o 1 3 0 733.94 613.33 21.91 o 2 3 0 32592.65 30869.83 154.95 o 3 3 0 32482.71 31512.51 281.77 o 4 3 0 1394.34 1193.84 29.80 o 5 3 0 15229.98 14921.71 179.24 o 6 3 0 7645.19 6950.47 80.43 o 7 3 0 1961.47 1891.54 45.14 o 8 3 0 2665.93 2584.06 49.83 o 9 3 0 4335.62 4279.38 61.56 o 10 3 0 11717.92 12435.78 96.17 o 11 3 0 283.30 310.10 63.06 o 12 3 0 712.54 613.59 111.38 o 13 3 0 522.80 649.34 158.78 o 14 3 0 16.93 81.76 152.85 o 15 3 0 2887.85 3072.54 224.25 o 16 3 0 275.74 129.49 104.31 o 17 3 0 936.87 991.78 223.36 o 18 3 0 265.60 457.38 227.50 o 0 4 0 84637.38 83337.11 2708.13 o 1 4 0 47448.44 49146.13 293.50 o 2 4 0 7090.50 6439.02 46.35 o 3 4 0 1325.05 1469.64 36.99 o 4 4 0 1822.08 1706.17 56.81 o 5 4 0 634.97 652.15 32.75 o 6 4 0 5342.45 5887.84 112.11 o 7 4 0 280.76 387.38 43.43 o 8 4 0 2295.54 2348.98 52.56 o 9 4 0 3447.62 3532.77 63.90 o 10 4 0 94.06 119.34 46.68 o 11 4 0 1514.45 1493.30 81.17 o 12 4 0 937.88 895.23 99.28 o 13 4 0 235.32 271.94 114.94 o 14 4 0 127.11 94.96 88.32 o 15 4 0 1375.63 1389.91 189.59 o 16 4 0 798.54 806.34 223.36 o 17 4 0 12.33 55.69 160.56 o 18 4 0 8.29 109.61 205.58 o 1 5 0 3790.11 4163.94 44.47 o 2 5 0 475.32 419.13 21.91 o 3 5 0 104.76 148.93 28.39 o 4 5 0 3394.34 3238.31 56.85 o 5 5 0 481.05 626.37 38.61 o 6 5 0 8669.62 8711.88 72.68 o 7 5 0 132.56 183.89 44.70 o 8 5 0 878.49 1513.77 171.72 o 9 5 0 2995.51 3113.04 111.75 o 10 5 0 6647.31 6711.93 80.72 o 11 5 0 2862.32 2902.43 93.14 o 12 5 0 170.78 165.30 83.34 o 13 5 0 302.44 332.31 99.33 o 14 5 0 294.16 258.91 129.75 o 15 5 0 967.88 806.93 194.92 o 16 5 0 95.24 104.27 193.73 o 17 5 0 244.12 195.51 201.44 o 18 5 0 564.75 616.75 198.47 o 0 6 0 53351.66 53086.49 1722.88 o 1 6 0 13059.73 13246.13 96.06 o 2 6 0 2787.90 2766.72 65.69 o 3 6 0 194.16 255.93 43.99 o 4 6 0 15849.22 15866.88 186.08 o 5 6 0 273.75 345.82 28.74 o 6 6 0 510.68 443.73 42.92 o 7 6 0 3277.35 3390.33 61.91 o 8 6 0 2376.98 2583.26 65.39 o 9 6 0 326.30 334.38 53.56 o 10 6 0 431.03 439.59 61.21 o 11 6 0 1128.99 1090.87 81.03 o 12 6 0 387.46 368.79 106.10 o 13 6 0 1297.41 1101.21 119.98 o 14 6 0 232.77 260.68 158.19 o 15 6 0 113.59 17.77 134.49 o 16 6 0 0.63 85.91 182.48 o 17 6 0 307.92 189.59 160.56 o 1 7 0 1963.92 1934.46 35.30 o 2 7 0 3353.95 3376.19 72.17 o 3 7 0 5307.75 5144.97 46.66 o 4 7 0 16086.92 17696.43 161.38 o 5 7 0 29.22 196.70 46.52 o 6 7 0 2435.67 2285.41 80.38 o 7 7 0 2935.67 2898.80 77.56 o 8 7 0 52.44 88.47 39.17 o 9 7 0 32.44 54.13 48.73 o 10 7 0 2386.05 2376.81 85.69 o 11 7 0 1962.29 1874.83 85.61 o 12 7 0 383.63 395.14 105.91 o 13 7 0 1.83 108.30 92.72 o 14 7 0 380.88 242.21 108.02 o 15 7 0 193.59 3.55 207.95 o 16 7 0 9.78 37.33 199.66 o 17 7 0 377.27 506.55 231.65 o 0 8 0 4985.55 5038.90 125.60 o 1 8 0 2764.73 2906.45 44.66 o 2 8 0 3854.12 3810.10 58.92 o 3 8 0 7704.75 7665.90 154.61 o 4 8 0 5110.65 5303.72 101.68 o 5 8 0 1691.04 1652.90 87.50 o 6 8 0 4466.51 4884.43 78.25 o 7 8 0 685.91 687.80 56.98 o 8 8 0 277.11 286.11 54.54 o 9 8 0 272.69 418.74 62.39 o 10 8 0 53.74 120.02 59.60 o 11 8 0 1.06 104.15 75.28 o 12 8 0 11.36 83.54 100.39 o 13 8 0 1098.40 998.78 126.86 o 14 8 0 45.22 127.50 110.93 o 15 8 0 70.25 45.03 199.07 o 16 8 0 320.10 597.79 268.98 o 17 8 0 794.45 755.39 260.09 o 1 9 0 145.59 187.98 31.75 o 2 9 0 295.20 289.36 39.78 o 3 9 0 2836.58 2651.50 46.32 o 4 9 0 124.40 89.30 30.40 o 5 9 0 116.98 181.28 56.19 o 6 9 0 286.52 314.64 69.71 o 7 9 0 5533.75 5508.20 90.13 o 8 9 0 690.74 646.16 63.47 o 9 9 0 266.37 403.37 60.52 o 10 9 0 3.29 62.44 58.66 o 11 9 0 58.94 44.25 72.05 o 12 9 0 120.76 160.15 105.73 o 13 9 0 27.30 54.14 106.77 o 14 9 0 27.84 111.88 124.41 o 15 9 0 3.17 8.59 118.98 o 16 9 0 0.91 49.17 210.92 o 0 10 0 1671.50 1661.40 117.60 o 1 10 0 5.64 77.73 35.59 o 2 10 0 2407.86 2377.37 48.88 o 3 10 0 5927.63 6057.61 177.44 o 4 10 0 805.97 805.23 57.86 o 5 10 0 27.91 35.52 51.42 o 6 10 0 86.55 72.42 73.06 o 7 10 0 1317.97 1200.62 94.10 o 8 10 0 403.24 371.84 73.42 o 9 10 0 9008.12 9415.43 106.15 o 10 10 0 91.97 131.74 68.27 o 11 10 0 82.10 66.75 70.71 o 12 10 0 99.18 127.65 118.65 o 13 10 0 1558.17 1538.57 151.81 o 14 10 0 1895.86 2066.94 185.28 o 15 10 0 120.38 65.40 131.12 o 16 10 0 38.52 66.36 183.07 o 1 11 0 857.84 807.90 47.66 o 2 11 0 1649.11 1685.74 50.44 o 3 11 0 6523.15 6979.55 109.97 o 4 11 0 3413.69 3276.54 77.16 o 5 11 0 7.16 80.81 56.27 o 6 11 0 68.24 -6.08 68.46 o 7 11 0 2819.56 2589.21 101.19 o 8 11 0 202.56 158.70 71.60 o 9 11 0 294.44 315.21 85.50 o 10 11 0 874.20 845.06 95.98 o 11 11 0 0.20 87.93 100.93 o 12 11 0 413.55 427.16 115.40 o 13 11 0 1475.20 1418.80 164.74 o 14 11 0 1253.19 1290.16 152.45 o 15 11 0 321.98 194.74 123.79 o 16 11 0 51.96 71.69 181.29 o 0 12 0 14391.41 14692.43 355.77 o 1 12 0 29.60 46.14 40.23 o 2 12 0 7852.78 7710.32 79.29 o 3 12 0 5217.22 5579.39 216.26 o 4 12 0 837.41 860.17 62.96 o 5 12 0 5712.42 6264.37 124.91 o 6 12 0 1144.92 1022.71 82.20 o 7 12 0 1035.54 994.40 86.05 o 8 12 0 712.90 640.28 87.77 o 9 12 0 783.34 845.67 106.04 o 10 12 0 17.79 39.88 80.01 o 11 12 0 1315.12 1576.05 144.12 o 12 12 0 22.06 -75.98 109.42 o 13 12 0 2830.05 2961.44 164.91 o 14 12 0 112.88 128.36 134.94 o 15 12 0 33.35 60.78 139.63 o 1 13 0 8307.30 8509.16 187.96 o 2 13 0 1040.87 971.17 57.01 o 3 13 0 2841.94 2679.57 73.35 o 4 13 0 1214.00 1198.07 76.66 o 5 13 0 12.48 155.34 64.84 o 6 13 0 497.96 396.54 73.32 o 7 13 0 970.41 775.84 112.26 o 8 13 0 512.49 489.48 97.07 o 9 13 0 41.15 166.54 80.79 o 10 13 0 94.72 59.03 82.52 o 11 13 0 200.80 146.62 119.13 o 12 13 0 470.27 516.03 136.50 o 13 13 0 314.99 294.36 154.79 o 14 13 0 9.23 36.22 134.66 o 15 13 0 15.74 -10.66 190.77 o 0 14 0 8061.92 8738.66 375.32 o 1 14 0 7.23 129.61 51.36 o 2 14 0 1113.95 1103.16 77.48 o 3 14 0 256.10 277.35 73.94 o 4 14 0 3245.76 3353.93 96.07 o 5 14 0 720.04 766.49 81.64 o 6 14 0 1354.62 1354.13 86.52 o 7 14 0 3772.19 3936.02 153.60 o 8 14 0 1485.68 1635.85 132.41 o 9 14 0 4169.65 4501.76 192.91 o 10 14 0 262.75 194.50 138.72 o 11 14 0 4924.98 5780.72 185.18 o 12 14 0 377.16 308.34 116.63 o 13 14 0 1825.35 1888.13 190.53 o 14 14 0 1406.88 1380.17 191.74 o 1 15 0 444.78 352.96 66.29 o 2 15 0 541.43 531.89 67.21 o 3 15 0 28.76 36.91 61.90 o 4 15 0 172.34 139.27 78.79 o 5 15 0 695.82 597.93 83.40 o 6 15 0 59.68 102.71 73.61 o 7 15 0 9.51 -12.15 87.47 o 8 15 0 3259.43 3196.81 141.72 o 9 15 0 275.47 225.71 96.65 o 10 15 0 1057.03 1442.94 176.78 o 11 15 0 1.03 105.69 141.95 o 12 15 0 3551.78 3886.48 214.83 o 13 15 0 1950.01 1648.94 254.76 o 14 15 0 40.71 130.93 167.07 o 0 16 0 6636.04 6310.37 126.05 o 1 16 0 882.39 928.83 85.49 o 2 16 0 1673.90 1649.92 88.67 o 3 16 0 5.56 35.94 73.03 o 4 16 0 170.96 186.43 77.90 o 5 16 0 928.66 830.32 134.13 o 6 16 0 9.23 -21.60 81.26 o 7 16 0 41.93 86.10 100.27 o 8 16 0 106.06 106.51 110.31 o 9 16 0 1905.88 2091.97 159.43 o 10 16 0 846.48 764.84 200.84 o 11 16 0 1444.12 1204.35 165.25 o 12 16 0 14.68 63.19 147.03 o 13 16 0 418.28 494.11 215.66 o 1 17 0 1403.84 1416.63 98.21 o 2 17 0 2298.58 2263.81 155.14 o 3 17 0 607.87 565.18 94.01 o 4 17 0 2060.07 2109.46 110.68 o 5 17 0 5.01 18.41 82.62 o 6 17 0 1079.15 1166.27 111.08 o 7 17 0 256.54 240.46 132.90 o 8 17 0 323.93 390.74 119.49 o 9 17 0 231.77 227.07 132.18 o 10 17 0 402.49 356.89 140.94 o 11 17 0 482.37 352.62 152.51 o 12 17 0 454.87 466.86 211.51 o 0 18 0 1117.40 1349.62 195.51 o 1 18 0 20.79 97.50 86.79 o 2 18 0 1220.84 1314.55 110.26 o 3 18 0 20.21 55.35 76.52 o 4 18 0 854.63 773.97 107.49 o 5 18 0 3.81 28.07 82.49 o 6 18 0 444.28 358.03 91.92 o 7 18 0 574.36 364.02 119.95 o 8 18 0 0.61 95.39 134.06 o 9 18 0 9.63 181.87 141.80 o 10 18 0 13.36 118.31 184.85 o 11 18 0 160.43 242.32 235.21 o 1 19 0 46.35 117.16 115.12 o 2 19 0 5.16 -15.53 77.85 o 3 19 0 165.55 269.10 93.94 o 4 19 0 1697.06 1720.69 124.81 o 5 19 0 454.56 505.21 116.24 o 6 19 0 863.29 829.18 121.13 o 7 19 0 59.02 57.06 140.68 o 8 19 0 366.77 402.22 161.02 o 9 19 0 113.62 66.07 136.51 o 0 20 0 68.47 115.53 141.60 o 1 20 0 129.55 192.84 113.63 o 2 20 0 903.63 828.80 97.66 o 3 20 0 31.41 -14.45 98.46 o 4 20 0 88.64 87.23 87.14 o 5 20 0 0.64 69.70 108.85 o 6 20 0 122.00 133.68 103.27 o 7 20 0 50.59 58.84 126.86 o 8 20 0 2.57 52.77 152.50 o 1 21 0 3.31 125.96 137.60 o 2 21 0 0.43 -1.73 124.00 o 3 21 0 35.21 130.82 102.24 o 4 21 0 191.67 425.78 106.75 o 5 21 0 16.83 103.07 110.54 o 6 21 0 80.90 127.57 113.34 o 7 21 0 617.36 437.40 134.83 o 0 22 0 653.23 720.43 240.54 o 1 22 0 19.99 28.17 151.99 o 2 22 0 499.88 411.24 123.57 o 3 22 0 988.11 1118.17 176.38 o 4 22 0 175.59 255.72 106.26 o 5 22 0 54.87 38.17 107.70 o 6 22 0 149.53 100.60 150.66 o 1 23 0 32.71 205.63 150.19 o 2 23 0 33.78 150.00 155.98 o 3 23 0 53.00 95.98 174.78 o 4 23 0 24.69 126.79 184.26 o 5 23 0 67.49 23.11 173.59 o -18 1 1 1335.69 1711.44 196.86 o -17 1 1 260.31 159.52 101.79 o -16 1 1 726.34 586.55 118.80 o -15 1 1 4.89 90.45 96.08 o -14 1 1 60.37 114.94 138.04 o -13 1 1 530.00 443.16 113.75 o -12 1 1 0.66 7.11 97.76 o -11 1 1 649.01 599.94 67.62 o -10 1 1 27.70 97.36 43.50 o -9 1 1 318.00 296.73 41.26 o -8 1 1 2881.33 2885.11 45.42 o -7 1 1 326.58 344.06 31.59 o -6 1 1 2885.96 2888.93 35.92 o -5 1 1 2452.08 2483.26 30.92 o -4 1 1 1877.05 1907.67 36.53 o -3 1 1 9481.69 9056.79 86.75 o -2 1 1 10111.88 10341.32 140.41 o 2 1 1 5.55 53.91 19.55 o 3 1 1 149.29 242.99 18.40 o 4 1 1 1655.16 1597.77 41.13 o 5 1 1 196.78 233.23 21.77 o 6 1 1 798.64 1034.83 55.93 o 7 1 1 1022.05 1145.03 33.42 o 8 1 1 1453.60 1540.70 40.58 o 9 1 1 0.42 67.35 35.05 o 10 1 1 530.45 634.86 53.60 o 12 1 1 2.57 -52.73 101.31 o 13 1 1 399.05 487.59 169.44 o 14 1 1 1015.04 1064.06 184.85 o 15 1 1 84.62 33.53 103.08 o 16 1 1 462.80 550.84 88.97 o 17 1 1 823.43 700.94 99.08 o 18 1 1 3.31 27.65 97.20 o -18 2 1 337.61 223.29 129.57 o -17 2 1 757.15 756.30 148.87 o -16 2 1 1212.51 981.03 124.44 o -15 2 1 1733.44 1808.19 230.47 o -14 2 1 391.05 190.18 116.71 o -13 2 1 86.83 93.02 142.19 o -12 2 1 3273.74 3227.13 140.41 o -11 2 1 297.76 267.51 51.99 o -10 2 1 1596.49 1665.46 58.35 o -9 2 1 3941.76 3999.36 59.27 o -8 2 1 148.57 143.74 29.15 o -7 2 1 1818.88 1843.61 36.76 o -6 2 1 7051.09 7584.99 47.42 o -5 2 1 416.11 451.11 22.11 o -4 2 1 2168.53 2152.51 32.29 o -3 2 1 24768.46 24611.46 195.98 o -2 2 1 3139.21 3154.45 34.36 o 2 2 1 10900.13 10124.66 188.36 o 3 2 1 1779.76 1670.67 25.23 o 4 2 1 88.73 116.96 21.63 o 5 2 1 1395.81 1483.58 32.35 o 6 2 1 804.56 853.44 27.84 o 7 2 1 2571.18 2419.85 39.20 o 8 2 1 401.06 376.52 28.45 o 9 2 1 19.76 53.56 35.39 o 10 2 1 228.08 181.56 43.35 o 11 2 1 461.42 438.63 73.90 o 12 2 1 792.97 668.89 148.71 o 13 2 1 0.82 96.57 133.90 o 14 2 1 24.80 19.87 87.94 o 15 2 1 8.87 -0.31 100.89 o 16 2 1 709.97 734.54 105.67 o 17 2 1 95.21 35.86 86.08 o 18 2 1 217.48 36.13 113.01 o -18 3 1 1692.48 1643.48 255.35 o -17 3 1 706.85 456.19 201.44 o -16 3 1 681.35 710.95 222.77 o -15 3 1 2.90 -34.96 167.07 o -14 3 1 985.39 1087.16 184.26 o -13 3 1 1086.11 1033.84 154.63 o -12 3 1 120.79 113.16 103.68 o -11 3 1 1375.69 1310.82 57.64 o -10 3 1 190.83 239.74 51.34 o -9 3 1 716.23 654.80 47.12 o -8 3 1 838.18 833.73 67.85 o -7 3 1 4678.53 4221.90 66.30 o -6 3 1 5053.82 5257.94 54.35 o -5 3 1 5632.79 5232.63 77.98 o -4 3 1 125.72 196.46 33.27 o -3 3 1 16987.30 17526.15 117.32 o -2 3 1 9624.83 9623.37 76.20 o -1 3 1 6161.07 5997.42 48.23 o 0 3 1 142.53 133.28 13.93 o 1 3 1 24.36 64.40 17.58 o 2 3 1 13102.56 13399.25 129.55 o 3 3 1 560.17 508.81 25.83 o 4 3 1 53.31 57.53 20.06 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