#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/30/2233051.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233051_Fobs loop_ _publ_author_name 'Joo, Hea-Chung' 'Park, Ki-Min' 'Lee, Uk' _publ_section_title ; Anhydrous pentaguanidinium dihydrogen nonavanado(IV)platinate(IV) ; _journal_coeditor_code ZL2427 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1801 _journal_page_last m1802 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.143 _cell_angle_gamma 90.000 _cell_length_a 12.8861 _cell_length_b 18.5137 _cell_length_c 15.2299 _exptl_crystal_F_000 2704.00 _reflns_d_resolution_high 0.7493 _[local]_cod_data_source_file zl2427Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' GUPTV9 IN P2(1)/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 681.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3444.37 2428.23 61.88 o 4 0 0 12529.08 12942.42 195.01 o 6 0 0 12.04 144.81 45.27 o 8 0 0 40099.81 38454.84 530.42 o 10 0 0 37445.95 37513.53 545.87 o 12 0 0 40559.74 40922.56 859.93 o 14 0 0 2698.28 2617.76 253.12 o 16 0 0 8591.35 8038.90 421.22 o 1 1 0 378381.44 395905.59 3681.12 o 2 1 0 304.78 347.86 13.11 o 3 1 0 404.72 581.14 46.99 o 4 1 0 15627.49 15316.62 147.41 o 5 1 0 1863.15 2099.10 49.94 o 6 1 0 13111.22 12146.37 157.42 o 7 1 0 3960.25 3791.90 78.52 o 8 1 0 36313.71 35673.79 334.25 o 9 1 0 95190.23 94348.52 945.81 o 10 1 0 5863.65 5600.24 137.27 o 11 1 0 795.09 958.63 66.28 o 12 1 0 5588.17 5293.39 139.99 o 13 1 0 15816.26 15731.89 351.54 o 14 1 0 824.70 689.99 138.71 o 15 1 0 593.18 378.25 134.74 o 16 1 0 208.57 225.94 151.32 o 17 1 0 1520.59 1123.28 234.88 o 0 2 0 397725.03 428469.41 7961.61 o 1 2 0 7658.08 8441.30 166.00 o 3 2 0 15236.95 17794.03 150.90 o 4 2 0 89691.80 94662.49 728.68 o 5 2 0 35873.66 33681.25 291.76 o 6 2 0 98.01 70.92 28.21 o 7 2 0 16831.92 15264.40 172.10 o 8 2 0 30918.17 28970.49 285.59 o 9 2 0 60448.94 58825.11 544.32 o 10 2 0 8955.75 8512.04 162.87 o 11 2 0 112.86 138.21 59.21 o 12 2 0 11561.11 11399.62 209.14 o 13 2 0 7490.62 7472.58 250.89 o 14 2 0 146.56 137.73 117.34 o 15 2 0 105.42 51.76 132.83 o 16 2 0 2697.74 2274.85 245.55 o 17 2 0 3782.32 4508.82 310.85 o 1 3 0 3363.36 3754.35 48.73 o 2 3 0 1189.60 774.02 25.91 o 3 3 0 56525.15 57201.41 449.43 o 4 3 0 250198.89 253634.48 1799.83 o 5 3 0 40.86 115.85 31.38 o 6 3 0 18463.25 18278.61 187.59 o 7 3 0 1202.20 1129.81 47.25 o 8 3 0 58570.63 54941.15 476.21 o 9 3 0 5155.04 4873.62 111.61 o 10 3 0 1723.95 1655.21 81.55 o 11 3 0 352.03 292.36 60.58 o 12 3 0 662.68 857.04 119.64 o 13 3 0 6088.62 6189.14 201.71 o 14 3 0 1192.66 1577.61 227.55 o 15 3 0 851.86 878.57 150.57 o 16 3 0 5861.96 6049.94 328.99 o 17 3 0 153.33 282.82 198.63 o 0 4 0 7525.79 7447.67 172.81 o 1 4 0 2430.25 2331.52 46.66 o 2 4 0 28280.77 28416.29 250.82 o 3 4 0 121588.02 126014.35 1260.41 o 4 4 0 2718.40 2492.77 63.62 o 5 4 0 31618.21 26753.96 256.01 o 6 4 0 240.04 348.85 32.79 o 7 4 0 4227.66 4322.60 95.94 o 8 4 0 5734.11 5630.10 111.28 o 9 4 0 14708.31 14504.31 195.73 o 10 4 0 817.08 868.52 68.60 o 11 4 0 1530.65 1441.76 117.60 o 12 4 0 70.09 198.29 74.29 o 13 4 0 311.45 340.44 103.00 o 14 4 0 1660.67 1758.17 160.26 o 15 4 0 676.72 828.00 189.29 o 16 4 0 44.68 152.51 194.62 o 1 5 0 13885.75 13934.78 141.54 o 2 5 0 379.91 413.15 33.95 o 3 5 0 23224.87 22380.35 242.54 o 4 5 0 52110.40 46417.28 383.08 o 5 5 0 1571.20 2091.05 53.88 o 6 5 0 313.85 537.34 36.75 o 7 5 0 3974.68 4087.27 92.39 o 8 5 0 3508.07 3543.94 97.52 o 9 5 0 32379.19 31832.69 358.91 o 10 5 0 133.14 151.58 54.29 o 11 5 0 3343.02 3423.70 115.21 o 12 5 0 1764.68 1546.14 119.95 o 13 5 0 4836.98 4885.96 178.53 o 14 5 0 684.15 655.39 139.99 o 15 5 0 1744.09 1954.65 229.14 o 16 5 0 1465.51 1602.80 309.51 o 0 6 0 54533.14 56768.69 673.73 o 1 6 0 34.01 125.54 23.70 o 2 6 0 23510.70 23919.89 233.30 o 3 6 0 13281.27 13862.46 188.52 o 4 6 0 13807.83 12580.41 186.88 o 5 6 0 9394.83 8529.18 111.51 o 6 6 0 55.19 168.15 35.45 o 7 6 0 6258.23 6246.77 105.50 o 8 6 0 33242.03 31539.69 347.75 o 9 6 0 4193.96 4358.90 116.36 o 10 6 0 11405.94 11647.80 270.69 o 11 6 0 81.06 45.85 70.64 o 12 6 0 14629.69 13963.23 297.98 o 13 6 0 35.81 135.34 137.08 o 14 6 0 3263.84 3148.78 244.76 o 15 6 0 15.78 -201.93 201.93 o 16 6 0 64.41 144.97 200.99 o 1 7 0 33139.80 33995.16 307.03 o 2 7 0 25.95 37.00 23.27 o 3 7 0 15285.99 15654.40 178.98 o 4 7 0 82.13 166.74 33.56 o 5 7 0 2451.58 2571.31 64.53 o 6 7 0 13408.72 13513.86 159.87 o 7 7 0 6069.83 5800.41 116.89 o 8 7 0 945.66 933.53 58.91 o 9 7 0 44741.53 43616.56 484.89 o 10 7 0 1617.98 1538.84 112.55 o 11 7 0 5768.02 6087.39 245.06 o 12 7 0 184.22 94.38 81.63 o 13 7 0 9755.72 9826.88 292.77 o 14 7 0 6.84 -55.35 309.30 o 15 7 0 1106.67 921.20 214.75 o 16 7 0 2915.89 3401.65 288.03 o 0 8 0 73035.52 71448.47 850.63 o 1 8 0 5852.83 6030.42 93.30 o 2 8 0 12546.42 12712.00 141.04 o 3 8 0 11958.19 11607.01 151.00 o 4 8 0 727.01 961.22 49.20 o 5 8 0 30304.80 28985.44 273.28 o 6 8 0 316.21 360.13 42.06 o 7 8 0 8852.70 8569.35 136.60 o 8 8 0 18287.21 17957.66 222.19 o 9 8 0 3784.53 3927.33 113.57 o 10 8 0 17296.17 17246.95 294.48 o 11 8 0 1173.75 986.69 117.55 o 12 8 0 1420.79 1477.25 144.43 o 13 8 0 254.25 207.51 182.10 o 14 8 0 2007.97 1893.29 236.95 o 15 8 0 2884.98 2923.91 269.41 o 16 8 0 286.78 277.85 222.36 o 1 9 0 77611.09 83397.47 700.59 o 2 9 0 14050.38 13785.13 147.82 o 3 9 0 1616.17 1713.14 60.77 o 4 9 0 27120.97 26212.24 282.14 o 5 9 0 568.15 677.62 53.53 o 6 9 0 21411.48 21062.38 235.34 o 7 9 0 469.68 466.65 74.16 o 8 9 0 4358.44 4400.69 107.23 o 9 9 0 8799.80 8420.00 186.99 o 10 9 0 122.69 102.17 75.49 o 11 9 0 1060.13 991.58 100.92 o 12 9 0 1580.63 1847.71 147.70 o 13 9 0 373.59 262.65 168.75 o 14 9 0 3002.71 3496.82 267.52 o 15 9 0 301.47 349.09 293.82 o 0 10 0 244.91 331.19 50.27 o 1 10 0 1123.07 1216.46 52.67 o 2 10 0 758.73 817.93 40.86 o 3 10 0 22925.89 23064.46 245.40 o 4 10 0 8593.07 9010.37 138.88 o 5 10 0 26729.18 26278.25 295.53 o 6 10 0 3.10 -20.37 41.65 o 7 10 0 15862.90 16061.96 206.69 o 8 10 0 47.14 30.19 48.55 o 9 10 0 6283.39 6497.88 180.90 o 10 10 0 211.07 99.97 77.07 o 11 10 0 1059.32 1068.84 128.59 o 12 10 0 9743.86 10418.61 361.24 o 13 10 0 12461.29 13376.57 424.07 o 14 10 0 102.70 -31.35 177.90 o 15 10 0 2038.04 2248.55 261.01 o 1 11 0 8359.65 7863.87 119.96 o 2 11 0 5638.67 5790.11 95.46 o 3 11 0 5511.28 5828.99 146.10 o 4 11 0 26565.08 27063.93 301.41 o 5 11 0 1133.34 1159.56 69.79 o 6 11 0 12646.51 12494.93 189.98 o 7 11 0 132.07 152.12 49.17 o 8 11 0 1795.99 1833.20 101.97 o 9 11 0 3349.75 3361.02 138.42 o 10 11 0 3985.50 4328.35 185.83 o 11 11 0 6095.19 6627.99 235.40 o 12 11 0 13655.24 13841.65 666.08 o 13 11 0 1814.90 2082.89 228.38 o 14 11 0 4289.81 4148.21 284.81 o 15 11 0 385.15 516.89 211.43 o 0 12 0 123700.38 126321.75 1483.97 o 1 12 0 6556.46 6685.53 116.68 o 2 12 0 16622.49 16068.22 186.79 o 3 12 0 12612.91 12189.33 177.47 o 4 12 0 377.74 496.16 62.29 o 5 12 0 16952.25 16750.83 227.14 o 6 12 0 989.36 1024.28 79.95 o 7 12 0 389.98 312.89 78.95 o 8 12 0 7758.12 7746.06 198.35 o 9 12 0 378.48 332.13 140.59 o 10 12 0 3089.62 3396.58 173.56 o 11 12 0 905.10 747.87 166.29 o 12 12 0 11418.02 11335.02 377.08 o 13 12 0 5271.52 4866.15 338.29 o 14 12 0 1081.23 1285.43 220.36 o 15 12 0 133.20 -99.28 307.22 o 1 13 0 50620.71 51290.44 598.98 o 2 13 0 274.84 358.45 44.37 o 3 13 0 3605.02 3487.60 99.78 o 4 13 0 81.61 102.33 53.42 o 5 13 0 97.13 175.71 71.12 o 6 13 0 12.07 -41.46 71.49 o 7 13 0 12927.16 12756.85 245.10 o 8 13 0 39840.45 39222.86 515.79 o 9 13 0 8620.22 8431.79 247.60 o 10 13 0 6.95 -82.57 119.26 o 11 13 0 7941.67 7976.09 422.71 o 12 13 0 351.73 321.66 169.75 o 13 13 0 5453.06 5203.19 287.22 o 14 13 0 7.59 -120.21 188.12 o 0 14 0 17206.02 18389.69 629.19 o 1 14 0 4548.92 4610.76 283.07 o 2 14 0 14771.54 14808.56 316.50 o 3 14 0 1760.63 1440.01 100.13 o 4 14 0 4549.03 4415.03 150.55 o 5 14 0 3141.31 3152.47 140.40 o 6 14 0 282.37 144.95 99.98 o 7 14 0 18372.59 18051.35 305.31 o 8 14 0 26070.23 25797.69 390.64 o 9 14 0 16307.65 16586.58 348.80 o 10 14 0 2778.04 3129.01 294.29 o 11 14 0 74.31 7.65 152.21 o 12 14 0 4779.82 5223.31 328.60 o 13 14 0 286.12 364.35 232.41 o 14 14 0 2182.27 2601.22 451.12 o 1 15 0 9199.18 8709.05 261.66 o 2 15 0 4473.78 4332.58 256.34 o 3 15 0 72.02 175.17 115.79 o 4 15 0 31606.77 30942.06 516.79 o 5 15 0 8645.82 8791.73 298.66 o 6 15 0 3445.79 3520.18 170.80 o 7 15 0 11718.96 10922.01 307.06 o 8 15 0 23153.38 23089.69 516.45 o 9 15 0 315.45 673.37 174.22 o 10 15 0 47.83 54.59 167.56 o 11 15 0 2782.38 2754.93 261.91 o 12 15 0 236.63 602.75 217.90 o 13 15 0 459.00 699.01 233.89 o 0 16 0 909.93 1289.96 221.54 o 1 16 0 1457.16 1526.32 153.60 o 2 16 0 18.05 5.21 116.92 o 3 16 0 39069.52 38700.50 615.64 o 4 16 0 4130.07 3750.80 222.20 o 5 16 0 43668.41 42052.26 955.53 o 6 16 0 1522.22 1540.81 184.51 o 7 16 0 22871.27 21999.99 601.01 o 8 16 0 614.82 446.34 429.75 o 9 16 0 4479.43 4221.50 427.37 o 10 16 0 675.96 365.64 246.93 o 11 16 0 14.86 379.89 275.42 o 12 16 0 793.99 626.82 322.90 o 13 16 0 43.37 -9.50 294.41 o 1 17 0 363.95 212.21 130.91 o 2 17 0 6786.20 6190.03 293.12 o 3 17 0 19595.13 19129.31 462.51 o 4 17 0 42427.27 42694.70 775.02 o 5 17 0 10.10 -60.72 182.20 o 6 17 0 9734.27 9265.99 400.40 o 7 17 0 162.27 270.26 195.38 o 8 17 0 5819.56 5318.43 465.36 o 9 17 0 4142.59 4601.39 432.12 o 10 17 0 575.89 565.08 289.66 o 11 17 0 1024.33 1182.40 332.40 o 12 17 0 95.77 679.05 308.66 o 0 18 0 8340.09 7616.75 546.09 o 1 18 0 57.27 -24.60 185.25 o 2 18 0 3595.43 3826.77 249.90 o 3 18 0 22205.97 22395.20 579.96 o 4 18 0 20608.47 20507.94 524.63 o 5 18 0 6428.34 6612.03 377.47 o 6 18 0 118.57 -78.99 183.60 o 7 18 0 3207.77 3210.05 370.39 o 8 18 0 1553.88 1448.32 332.40 o 9 18 0 7448.30 6814.24 550.84 o 10 18 0 2372.92 2189.10 360.89 o 11 18 0 1072.75 978.21 313.41 o 1 19 0 26973.56 26525.71 852.37 o 2 19 0 238.55 383.44 199.26 o 3 19 0 18646.28 18568.13 580.17 o 4 19 0 4088.68 4571.52 328.86 o 5 19 0 3358.60 3289.69 292.64 o 6 19 0 12.56 63.96 215.48 o 7 19 0 282.81 389.39 261.17 o 8 19 0 771.87 455.87 299.16 o 9 19 0 4955.65 5475.13 512.85 o 10 19 0 552.53 479.61 322.90 o 0 20 0 33573.54 33458.63 1172.90 o 1 20 0 5412.72 6254.20 369.35 o 2 20 0 11942.19 11261.96 546.09 o 3 20 0 1264.62 1546.70 267.62 o 4 20 0 9175.19 8827.58 435.41 o 5 20 0 6279.05 6041.50 381.68 o 6 20 0 258.78 33.24 289.66 o 7 20 0 1036.47 1258.38 341.90 o 8 20 0 3039.09 3362.01 417.88 o 9 20 0 192.60 436.87 294.41 o 10 20 0 7248.58 7816.19 626.82 o 1 21 0 21314.76 22244.87 653.03 o 2 21 0 6854.43 6037.86 365.74 o 3 21 0 432.12 111.75 337.15 o 4 21 0 2877.86 2524.49 312.22 o 5 21 0 3176.85 2621.23 417.88 o 6 21 0 5051.86 4910.05 498.60 o 7 21 0 2492.97 2227.09 398.88 o 8 21 0 8311.79 9150.55 660.06 o 9 21 0 865.76 1054.19 341.90 o 0 22 0 18825.76 18581.27 887.99 o 1 22 0 7363.02 7129.85 484.36 o 2 22 0 2265.96 2301.80 553.21 o 3 22 0 1692.24 1870.95 281.22 o 4 22 0 473.10 469.07 241.75 o 5 22 0 11650.23 13267.59 759.78 o 6 22 0 100.94 137.71 322.90 o 7 22 0 12776.06 13148.87 769.27 o 1 23 0 316.38 182.02 240.52 o 2 23 0 3159.03 2892.13 372.77 o 3 23 0 1021.37 1105.76 281.75 o 4 23 0 4857.22 5389.66 546.09 o 5 23 0 2552.13 2815.92 455.87 o 6 23 0 10220.93 9744.13 688.55 o 0 24 0 2831.19 2654.47 465.36 o 1 24 0 56.75 308.21 266.17 o 2 24 0 1707.39 2029.94 339.52 o 3 24 0 1781.00 1813.96 398.88 o 4 24 0 377.12 479.61 375.14 o -17 0 1 10532.22 12777.10 1016.20 o -15 0 1 284.56 -42.32 462.99 o -13 0 1 1861.51 1753.91 219.60 o -11 0 1 368.34 375.76 82.89 o -9 0 1 384992.25 370717.50 4163.08 o -7 0 1 56414.09 53359.54 609.33 o -5 0 1 2146.45 2612.70 122.41 o -3 0 1 38285.86 35547.16 433.36 o -1 0 1 2313.59 3537.71 113.97 o 1 0 1 136324.98 161161.08 3995.68 o 3 0 1 62893.37 52068.48 609.67 o 5 0 1 34489.39 33858.44 443.45 o 7 0 1 11854.40 12560.62 226.43 o 9 0 1 30003.05 30584.18 476.80 o 11 0 1 4631.32 4413.74 155.65 o 13 0 1 5936.51 6341.16 260.19 o 15 0 1 5710.89 6182.38 641.06 o 17 0 1 4359.03 4957.54 688.55 o -17 1 1 4452.83 4842.63 259.94 o -16 1 1 7104.09 7805.18 293.84 o -15 1 1 2283.86 2121.64 176.99 o -14 1 1 173.51 125.11 116.72 o -13 1 1 3512.14 3282.32 179.41 o -12 1 1 14130.86 13677.35 212.51 o -11 1 1 141.86 94.62 49.53 o -10 1 1 35775.52 35024.91 543.60 o -9 1 1 3402.89 3371.66 118.56 o -8 1 1 286470.56 278149.72 2105.18 o -7 1 1 1201.30 1355.24 50.95 o -6 1 1 7285.67 7228.07 101.78 o -5 1 1 248.01 220.39 26.28 o -4 1 1 23564.16 23235.96 207.29 o -3 1 1 53479.84 48764.49 411.30 o -2 1 1 8184.97 9340.84 79.65 o -1 1 1 43069.77 48772.38 397.68 o 0 1 1 65536.64 85211.23 1681.68 o 1 1 1 39541.30 47151.17 637.20 o 2 1 1 10568.82 10543.29 101.00 o 3 1 1 19322.98 18017.59 169.33 o 4 1 1 90311.23 91805.84 746.58 o 5 1 1 8577.60 8691.19 112.55 o 6 1 1 1742.72 1967.59 62.69 o 7 1 1 1696.56 1854.69 56.40 o 8 1 1 38680.81 39831.54 362.83 o 9 1 1 2925.38 2979.89 84.44 o 10 1 1 124.85 125.88 69.93 o 11 1 1 1745.48 1648.53 85.56 o 12 1 1 316.34 400.20 61.69 o 13 1 1 1105.81 906.93 97.33 o 14 1 1 5565.94 5943.58 238.31 o 15 1 1 32.29 141.56 128.32 o 16 1 1 9019.10 9144.31 376.44 o 17 1 1 57.30 -133.45 610.19 o -17 2 1 5701.00 6457.13 548.66 o -16 2 1 14775.51 16203.20 570.94 o -15 2 1 1835.02 1805.98 171.07 o -14 2 1 2462.69 2709.78 204.45 o -13 2 1 4728.29 4454.00 202.34 o -12 2 1 34161.67 33973.97 484.21 o -11 2 1 1599.45 1744.12 99.39 o -10 2 1 1455.89 1512.26 82.66 o -9 2 1 52821.41 52031.39 492.95 o -8 2 1 7014.87 7139.68 119.42 o -7 2 1 6787.06 6010.71 98.83 o -6 2 1 5444.40 5914.01 96.43 o -5 2 1 8073.15 7098.97 94.72 o -4 2 1 116592.64 118670.63 861.33 o -3 2 1 35193.01 35929.82 293.04 o -2 2 1 1096.78 932.65 26.25 o -1 2 1 2713.36 3466.72 70.33 o 0 2 1 209539.72 226988.70 4522.64 o 1 2 1 24775.84 28371.05 258.44 o 2 2 1 252.53 249.72 19.66 o 3 2 1 2848.86 2542.46 45.17 o 4 2 1 5067.58 4630.30 67.39 o 5 2 1 18144.56 16841.00 165.20 o 6 2 1 10096.78 9734.62 119.71 o 7 2 1 1215.61 1192.44 48.50 o 8 2 1 7073.62 6546.92 111.12 o 9 2 1 2759.28 2715.02 89.85 o 10 2 1 3570.65 3718.70 110.49 o 11 2 1 150.83 151.81 75.34 o 12 2 1 11858.31 11211.28 203.51 o 13 2 1 1531.06 1359.88 103.23 o 14 2 1 18.40 -42.38 114.00 o 15 2 1 3344.89 3484.99 205.41 o 16 2 1 274.00 127.21 179.43 o 17 2 1 2981.93 3140.36 419.85 o -17 3 1 8574.67 8640.38 651.90 o -16 3 1 1450.73 1494.75 188.00 o -15 3 1 2496.47 2927.95 193.90 o -14 3 1 129.22 74.56 118.42 o -13 3 1 37589.73 38041.35 605.87 o -12 3 1 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