#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/30/2233054.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233054_Fobs loop_ _publ_author_name 'Yang, Wei' 'Qiu, Qi-Ming' 'Zhou, Li-Li' 'Jin, Qiong-Hua' 'Zhang, Cun-Lin' _publ_section_title ; An orthorhombic polymorph of pyrazino[2,3-f][1,10]phenanthroline-2,3-dicarbonitrile ; _journal_coeditor_code ZQ2127 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3250 _journal_page_last o3251 _journal_volume 67 _journal_year 2011 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1055 _cell_length_b 16.3331 _cell_length_c 5.2694 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file zq2127Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 110503h in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 171.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4134.96 3722.40 54.34 o 4 0 0 13104.14 11847.12 116.40 o 6 0 0 2526.82 2535.13 38.92 o 8 0 0 742.55 699.66 14.06 o 10 0 0 8.78 12.89 7.83 o 12 0 0 154.31 151.98 7.99 o 14 0 0 7.05 15.76 8.38 o 16 0 0 57.76 57.23 13.79 o 2 1 0 2188.15 2065.07 46.60 o 4 1 0 365.12 343.96 6.46 o 6 1 0 23.84 22.75 2.05 o 8 1 0 23.52 23.99 2.57 o 10 1 0 77.09 72.93 5.13 o 12 1 0 53.25 53.17 4.99 o 14 1 0 13.20 21.17 6.14 o 16 1 0 9.92 16.83 7.60 o 2 2 0 3680.85 3414.79 98.12 o 4 2 0 276.81 266.58 5.19 o 6 2 0 133.73 124.98 3.53 o 8 2 0 1.15 0.47 1.54 o 10 2 0 0.34 -0.86 1.96 o 12 2 0 0.67 -0.30 2.92 o 14 2 0 5.14 2.34 3.60 o 16 2 0 36.60 41.74 9.08 o 2 3 0 2448.25 2288.53 25.92 o 4 3 0 1242.02 1233.17 12.02 o 6 3 0 28.05 26.82 2.32 o 8 3 0 1392.17 1494.34 16.43 o 10 3 0 1112.55 1233.84 15.71 o 12 3 0 38.16 45.73 5.46 o 14 3 0 6.61 5.57 4.23 o 16 3 0 3.26 1.73 7.03 o 0 4 0 7719.69 7724.07 147.15 o 2 4 0 1104.51 1083.56 12.24 o 4 4 0 31.30 30.59 3.25 o 6 4 0 1465.41 1461.05 15.14 o 8 4 0 1945.09 2029.54 25.37 o 10 4 0 10.20 6.88 2.67 o 12 4 0 373.32 395.16 11.12 o 14 4 0 90.40 103.33 9.02 o 16 4 0 0.14 -6.74 7.71 o 2 5 0 4703.78 4740.42 41.63 o 4 5 0 14.61 13.11 1.97 o 6 5 0 155.49 145.53 4.71 o 8 5 0 1449.06 1525.22 19.43 o 10 5 0 1549.97 1659.16 35.06 o 12 5 0 0.85 0.40 3.05 o 14 5 0 32.59 36.83 7.10 o 16 5 0 3.99 13.67 9.13 o 0 6 0 5983.66 6218.44 65.47 o 2 6 0 683.56 688.22 10.10 o 4 6 0 33.23 41.85 3.28 o 6 6 0 260.85 265.73 6.64 o 8 6 0 148.59 152.89 5.53 o 10 6 0 14.10 16.75 4.29 o 12 6 0 214.23 225.74 11.95 o 14 6 0 5.16 6.85 5.06 o 2 7 0 1604.59 1710.63 19.75 o 4 7 0 812.31 800.29 12.19 o 6 7 0 108.04 95.49 4.31 o 8 7 0 26.82 25.51 3.45 o 10 7 0 125.34 118.58 7.97 o 12 7 0 11.40 12.68 5.11 o 14 7 0 20.97 17.23 6.03 o 0 8 0 6659.46 7676.43 104.90 o 2 8 0 1138.89 1145.09 18.48 o 4 8 0 133.13 135.68 4.98 o 6 8 0 139.30 139.39 5.35 o 8 8 0 0.11 -1.29 2.78 o 10 8 0 1.75 -3.09 3.22 o 12 8 0 1.74 0.41 4.04 o 14 8 0 33.40 29.30 7.30 o 2 9 0 1053.51 1147.73 17.30 o 4 9 0 375.64 390.90 8.90 o 6 9 0 158.25 161.24 6.00 o 8 9 0 582.86 553.22 19.06 o 10 9 0 0.44 0.66 3.73 o 12 9 0 60.12 77.60 8.88 o 14 9 0 13.18 4.35 5.62 o 0 10 0 17.31 15.68 3.49 o 2 10 0 8.55 11.34 2.50 o 4 10 0 17.00 14.98 2.56 o 6 10 0 5.15 4.40 2.58 o 8 10 0 1.22 -1.24 3.59 o 10 10 0 1.61 3.11 4.27 o 12 10 0 41.60 53.16 8.00 o 14 10 0 0.41 -3.08 5.32 o 2 11 0 202.14 226.17 7.59 o 4 11 0 29.21 25.93 3.15 o 6 11 0 271.73 262.28 10.30 o 8 11 0 1194.22 1168.83 24.28 o 10 11 0 4249.55 4395.26 60.67 o 12 11 0 16.32 18.82 6.47 o 0 12 0 186.30 167.13 11.25 o 2 12 0 5.00 6.06 2.46 o 4 12 0 53.87 56.20 4.35 o 6 12 0 0.46 -4.31 3.86 o 8 12 0 849.93 852.29 20.80 o 10 12 0 0.52 8.52 5.33 o 12 12 0 184.26 182.62 11.37 o 2 13 0 65.23 59.56 5.61 o 4 13 0 211.36 200.67 6.50 o 6 13 0 47.86 41.12 6.43 o 8 13 0 368.94 378.32 14.08 o 10 13 0 1579.84 1564.93 32.07 o 12 13 0 2.19 4.96 6.07 o 0 14 0 125.20 94.91 8.58 o 2 14 0 164.37 141.34 7.09 o 4 14 0 2.14 2.14 3.57 o 6 14 0 89.54 109.72 9.63 o 8 14 0 16.93 16.80 5.64 o 10 14 0 1.99 3.19 5.69 o 2 15 0 111.71 116.68 7.55 o 4 15 0 9.74 9.06 4.99 o 6 15 0 68.64 77.58 19.68 o 8 15 0 24.18 18.41 6.45 o 10 15 0 125.31 135.50 12.87 o 0 16 0 1040.15 903.93 59.53 o 2 16 0 71.36 59.17 6.43 o 4 16 0 75.93 76.36 8.93 o 6 16 0 5.76 6.68 5.22 o 8 16 0 7.86 10.87 5.89 o 2 17 0 7.63 -3.56 4.84 o 4 17 0 73.14 64.67 13.28 o 6 17 0 4.21 -2.24 4.82 o 8 17 0 25.71 40.08 8.16 o 0 18 0 31.70 24.59 11.92 o 2 18 0 9.96 6.96 9.55 o 4 18 0 18.84 22.71 6.97 o 6 18 0 5.60 1.74 6.03 o 2 19 0 60.42 45.87 13.73 o 1 0 1 2701.53 2544.02 34.27 o 2 0 1 6555.46 6238.05 170.46 o 3 0 1 70.14 78.93 2.51 o 4 0 1 29336.18 26784.64 500.73 o 5 0 1 872.02 867.74 19.02 o 6 0 1 59.49 59.12 2.64 o 7 0 1 11.12 9.94 1.86 o 8 0 1 855.46 877.95 11.57 o 9 0 1 0.83 -2.28 1.62 o 10 0 1 219.21 214.47 5.91 o 11 0 1 81.31 94.16 7.06 o 12 0 1 230.90 232.98 8.62 o 13 0 1 8.92 11.28 4.18 o 14 0 1 93.74 92.62 7.77 o 15 0 1 263.84 299.89 22.80 o 16 0 1 919.03 1012.13 41.89 o 0 1 1 30.86 25.25 2.28 o 1 1 1 325.38 287.47 3.93 o 2 1 1 95.50 98.88 2.89 o 3 1 1 26018.84 23449.42 338.33 o 4 1 1 401.74 466.98 12.26 o 5 1 1 501.53 549.43 6.79 o 6 1 1 293.98 296.18 4.57 o 7 1 1 343.39 364.77 4.60 o 8 1 1 92.40 83.88 2.48 o 9 1 1 151.78 148.84 3.33 o 10 1 1 15.97 14.06 1.86 o 11 1 1 7.50 7.12 2.01 o 12 1 1 0.29 -1.37 2.23 o 13 1 1 1.60 -2.24 2.47 o 14 1 1 117.18 127.34 7.62 o 15 1 1 251.21 263.79 9.53 o 16 1 1 8.10 10.29 6.78 o 1 2 1 246.54 221.89 3.50 o 2 2 1 1144.55 1120.94 17.39 o 3 2 1 588.51 607.02 12.25 o 4 2 1 652.14 737.93 17.96 o 5 2 1 13.03 11.27 1.29 o 6 2 1 57.31 54.52 1.78 o 7 2 1 76.60 70.73 2.77 o 8 2 1 3.13 1.08 1.06 o 9 2 1 80.67 82.83 2.66 o 10 2 1 3.99 2.56 1.66 o 11 2 1 43.52 47.18 3.22 o 12 2 1 0.65 -2.73 1.87 o 13 2 1 8.75 3.57 2.65 o 14 2 1 69.63 77.45 5.78 o 15 2 1 14.86 13.64 4.57 o 16 2 1 67.05 70.39 7.26 o 0 3 1 1839.23 1789.79 17.19 o 1 3 1 1554.06 1459.98 12.69 o 2 3 1 1092.90 1042.22 17.84 o 3 3 1 765.15 731.93 12.74 o 4 3 1 494.83 544.20 8.28 o 5 3 1 1026.39 1068.46 13.66 o 6 3 1 1706.21 1842.66 23.98 o 7 3 1 153.14 154.51 3.42 o 8 3 1 351.56 367.81 5.32 o 9 3 1 112.62 114.54 3.41 o 10 3 1 13.65 11.84 2.10 o 11 3 1 115.10 112.67 3.94 o 12 3 1 252.20 255.89 5.81 o 13 3 1 25.07 30.81 4.12 o 14 3 1 117.84 126.79 8.01 o 15 3 1 72.07 80.83 7.16 o 16 3 1 1.94 6.63 4.60 o 1 4 1 966.02 997.86 8.29 o 2 4 1 999.48 998.24 9.82 o 3 4 1 261.49 257.91 9.66 o 4 4 1 2665.01 2769.42 22.85 o 5 4 1 2277.31 2517.11 22.75 o 6 4 1 24.98 32.02 2.26 o 7 4 1 883.76 1006.05 18.45 o 8 4 1 145.70 162.09 4.10 o 9 4 1 75.78 75.76 3.36 o 10 4 1 85.37 80.35 3.60 o 11 4 1 30.79 26.87 2.84 o 12 4 1 57.67 61.53 4.30 o 13 4 1 315.87 318.82 8.17 o 14 4 1 1.97 1.26 3.66 o 15 4 1 13.39 10.11 4.67 o 16 4 1 58.23 62.99 7.30 o 0 5 1 440.24 429.80 5.90 o 1 5 1 43.61 36.89 1.49 o 2 5 1 386.58 396.56 5.98 o 3 5 1 1597.33 1656.42 14.82 o 4 5 1 83.66 87.66 2.97 o 5 5 1 246.02 259.26 7.81 o 6 5 1 195.12 235.38 7.43 o 7 5 1 0.43 0.26 1.37 o 8 5 1 150.36 160.61 4.18 o 9 5 1 135.06 131.80 4.28 o 10 5 1 19.09 16.33 2.75 o 11 5 1 88.53 94.48 4.53 o 12 5 1 222.94 197.57 6.13 o 13 5 1 10.75 7.75 3.34 o 14 5 1 36.63 29.34 4.65 o 15 5 1 6.57 6.22 4.67 o 16 5 1 2.25 -2.32 5.13 o 1 6 1 0.07 -0.63 0.69 o 2 6 1 287.38 281.50 5.08 o 3 6 1 0.02 0.51 0.83 o 4 6 1 187.65 191.18 4.74 o 5 6 1 400.69 428.56 6.98 o 6 6 1 16.45 17.76 2.20 o 7 6 1 371.83 367.71 8.29 o 8 6 1 131.61 125.74 4.29 o 9 6 1 0.05 -1.30 1.86 o 10 6 1 112.31 109.65 4.93 o 11 6 1 84.32 78.59 4.92 o 12 6 1 2.88 0.59 2.93 o 13 6 1 90.55 103.40 12.38 o 14 6 1 18.38 16.11 4.20 o 15 6 1 2.93 -2.13 4.38 o 0 7 1 276.81 261.38 5.39 o 1 7 1 0.33 -0.36 0.79 o 2 7 1 27.59 38.02 1.75 o 3 7 1 1799.12 1956.00 21.29 o 4 7 1 135.66 135.82 3.77 o 5 7 1 858.56 854.23 9.13 o 6 7 1 328.83 304.23 6.25 o 7 7 1 143.66 137.37 5.10 o 8 7 1 92.10 90.03 4.11 o 9 7 1 183.12 179.86 5.43 o 10 7 1 2.49 -0.64 2.21 o 11 7 1 103.98 101.43 6.75 o 12 7 1 1.38 -1.41 2.74 o 13 7 1 5.40 3.92 3.39 o 14 7 1 45.57 43.18 5.94 o 15 7 1 256.72 264.58 9.46 o 1 8 1 1140.41 1207.80 9.64 o 2 8 1 1283.30 1407.91 12.21 o 3 8 1 0.10 0.26 1.10 o 4 8 1 906.62 992.26 9.18 o 5 8 1 645.68 664.39 9.58 o 6 8 1 2.53 0.19 1.65 o 7 8 1 130.76 112.42 4.23 o 8 8 1 9.63 7.80 2.38 o 9 8 1 7.02 3.94 2.33 o 10 8 1 32.14 30.08 5.07 o 11 8 1 9.40 4.60 3.01 o 12 8 1 14.43 12.99 3.70 o 13 8 1 0.88 0.52 3.33 o 14 8 1 40.27 48.37 6.03 o 15 8 1 70.02 78.78 7.14 o 0 9 1 122.03 125.85 4.07 o 1 9 1 57.08 52.14 2.14 o 2 9 1 233.80 235.04 5.13 o 3 9 1 91.03 107.97 2.94 o 4 9 1 51.00 49.17 2.50 o 5 9 1 3.59 4.53 1.85 o 6 9 1 51.80 52.60 3.74 o 7 9 1 36.34 39.80 3.51 o 8 9 1 134.23 116.96 4.63 o 9 9 1 47.59 52.18 5.20 o 10 9 1 11.43 9.25 3.25 o 11 9 1 11.87 6.78 4.74 o 12 9 1 71.02 69.63 6.07 o 13 9 1 13.94 12.55 4.14 o 14 9 1 25.04 28.15 5.70 o 1 10 1 10.84 9.29 1.52 o 2 10 1 0.32 -0.95 1.13 o 3 10 1 12.35 12.73 1.70 o 4 10 1 3.23 0.33 1.70 o 5 10 1 434.10 408.06 7.89 o 6 10 1 5.82 10.64 2.75 o 7 10 1 253.43 233.56 6.37 o 8 10 1 19.96 16.06 3.08 o 9 10 1 7.07 3.99 2.88 o 10 10 1 0.34 -3.91 2.61 o 11 10 1 92.63 85.88 6.52 o 12 10 1 0.50 -1.85 3.65 o 13 10 1 208.40 194.26 9.77 o 14 10 1 0.16 -2.01 4.12 o 0 11 1 47.04 45.28 3.79 o 1 11 1 5.27 0.84 1.33 o 2 11 1 280.41 296.82 4.97 o 3 11 1 3.25 2.59 1.65 o 4 11 1 74.94 70.18 4.31 o 5 11 1 165.33 157.73 5.26 o 6 11 1 2116.26 2141.96 25.64 o 7 11 1 0.02 5.95 2.79 o 8 11 1 275.91 269.50 8.10 o 9 11 1 10.84 7.90 3.38 o 10 11 1 69.01 73.18 6.80 o 11 11 1 53.91 59.90 5.86 o 12 11 1 382.59 387.42 11.12 o 13 11 1 0.04 6.17 4.18 o 1 12 1 35.94 31.70 3.81 o 2 12 1 10.87 14.12 2.29 o 3 12 1 111.75 106.85 4.18 o 4 12 1 429.28 425.20 7.86 o 5 12 1 399.45 385.57 8.29 o 6 12 1 64.63 76.07 5.09 o 7 12 1 1805.55 1838.28 20.78 o 8 12 1 17.96 20.30 4.38 o 9 12 1 141.54 139.11 6.37 o 10 12 1 10.65 8.45 3.73 o 11 12 1 0.98 -1.59 3.60 o 12 12 1 32.17 38.40 5.68 o 0 13 1 178.06 167.82 5.85 o 1 13 1 3.65 2.28 1.93 o 2 13 1 57.02 54.09 4.51 o 3 13 1 8.70 4.36 2.48 o 4 13 1 16.20 10.81 2.70 o 5 13 1 158.11 147.60 5.01 o 6 13 1 696.47 643.83 11.39 o 7 13 1 0.27 2.32 2.91 o 8 13 1 7.16 -2.76 2.89 o 9 13 1 10.71 4.78 3.41 o 10 13 1 13.08 6.01 3.75 o 11 13 1 60.97 73.70 6.87 o 12 13 1 61.34 64.63 6.90 o 1 14 1 18.45 15.00 2.95 o 2 14 1 141.61 124.49 4.61 o 3 14 1 36.78 32.29 3.86 o 4 14 1 73.61 75.96 5.67 o 5 14 1 31.87 29.45 3.57 o 6 14 1 5.78 3.32 2.77 o 7 14 1 14.14 13.93 4.20 o 8 14 1 41.22 37.12 4.94 o 9 14 1 14.64 9.87 4.32 o 10 14 1 78.96 99.59 7.68 o 11 14 1 81.91 104.26 9.95 o 0 15 1 1.43 1.75 3.65 o 1 15 1 8.87 4.06 3.00 o 2 15 1 46.06 51.23 4.90 o 3 15 1 90.84 89.50 10.26 o 4 15 1 1.61 1.05 2.53 o 5 15 1 11.18 8.72 2.93 o 6 15 1 99.00 100.14 10.31 o 7 15 1 0.22 -3.48 3.03 o 8 15 1 0.04 -4.82 3.21 o 9 15 1 7.95 3.47 3.83 o 10 15 1 0.29 -1.25 3.72 o 1 16 1 83.58 88.14 6.19 o 2 16 1 87.66 78.89 5.84 o 3 16 1 0.00 -2.60 3.00 o 4 16 1 118.08 102.25 5.58 o 5 16 1 25.41 20.59 4.25 o 6 16 1 0.09 -0.06 3.50 o 7 16 1 46.39 51.23 5.94 o 8 16 1 1.96 1.78 3.69 o 9 16 1 1.60 2.21 4.31 o 0 17 1 61.48 61.20 9.39 o 1 17 1 1.02 -0.36 3.27 o 2 17 1 0.93 1.14 3.44 o 3 17 1 179.11 161.94 6.75 o 4 17 1 6.74 7.05 4.66 o 5 17 1 36.35 31.28 8.32 o 6 17 1 24.08 28.63 4.97 o 7 17 1 18.96 11.09 5.69 o 1 18 1 16.38 17.88 5.11 o 2 18 1 0.00 -2.92 4.20 o 3 18 1 6.35 8.63 4.63 o 4 18 1 10.06 14.29 5.66 o 5 18 1 88.23 122.41 10.01 o 0 19 1 0.43 -5.07 5.73 o 1 19 1 18.02 17.76 8.59 o 2 19 1 0.03 -7.52 5.42 o 0 0 2 385.76 377.26 13.34 o 1 0 2 162.94 167.60 6.19 o 2 0 2 744.94 679.47 10.34 o 3 0 2 169.35 166.57 9.32 o 4 0 2 95.08 97.20 3.39 o 5 0 2 410.91 395.81 8.01 o 6 0 2 5943.92 6270.53 170.29 o 7 0 2 598.50 604.18 17.84 o 8 0 2 2943.00 3048.51 86.35 o 9 0 2 226.58 205.87 7.42 o 10 0 2 221.43 221.71 8.04 o 11 0 2 693.80 725.62 15.51 o 12 0 2 1505.13 1597.74 43.63 o 13 0 2 36.15 49.68 8.80 o 14 0 2 218.69 226.48 12.76 o 15 0 2 5.93 2.67 6.39 o 1 1 2 1363.20 1334.45 14.47 o 2 1 2 4.37 5.03 1.18 o 3 1 2 217.40 218.57 6.33 o 4 1 2 6.90 4.94 1.71 o 5 1 2 204.79 221.42 5.04 o 6 1 2 41.65 48.67 2.81 o 7 1 2 5033.55 5351.96 79.32 o 8 1 2 86.33 92.43 3.49 o 9 1 2 34.10 39.94 3.95 o 10 1 2 94.91 94.56 4.23 o 11 1 2 26.43 33.75 4.01 o 12 1 2 124.33 140.61 6.26 o 13 1 2 965.95 1045.00 16.28 o 14 1 2 10.05 9.91 4.46 o 15 1 2 15.12 10.31 4.81 o 0 2 2 63.12 41.17 4.08 o 1 2 2 53.43 57.86 2.81 o 2 2 2 17.26 14.66 1.47 o 3 2 2 45.48 42.08 2.13 o 4 2 2 399.36 432.05 9.45 o 5 2 2 17.12 12.41 1.67 o 6 2 2 620.24 662.30 9.30 o 7 2 2 26.64 31.07 2.73 o 8 2 2 85.11 97.26 4.10 o 9 2 2 9.68 8.93 2.04 o 10 2 2 36.88 34.79 4.62 o 11 2 2 62.84 61.70 5.69 o 12 2 2 86.85 90.93 6.02 o 13 2 2 2.16 -2.36 3.12 o 14 2 2 5.00 2.95 3.71 o 15 2 2 0.67 -2.12 4.10 o 1 3 2 1949.69 1959.89 20.49 o 2 3 2 1558.94 1656.66 13.44 o 3 3 2 0.69 -1.72 1.14 o 4 3 2 1102.80 1242.63 23.54 o 5 3 2 739.46 811.73 16.87 o 6 3 2 179.26 165.65 3.88 o 7 3 2 378.55 368.40 11.84 o 8 3 2 62.02 63.39 4.48 o 9 3 2 125.99 106.86 4.68 o 10 3 2 113.04 99.62 6.48 o 11 3 2 164.59 157.49 6.50 o 12 3 2 2.78 -0.80 2.99 o 13 3 2 40.99 53.17 5.64 o 14 3 2 107.99 129.22 8.33 o 15 3 2 22.63 21.32 6.11 o 0 4 2 191.03 213.17 19.50 o 1 4 2 90.39 103.05 2.86 o 2 4 2 304.90 331.50 5.47 o 3 4 2 1123.12 1322.57 23.81 o 4 4 2 1.25 1.04 1.61 o 5 4 2 316.27 331.22 5.05 o 6 4 2 101.73 104.79 3.96 o 7 4 2 18.80 18.30 3.13 o 8 4 2 8.66 6.51 2.18 o 9 4 2 39.83 38.50 4.36 o 10 4 2 1.31 -2.78 2.18 o 11 4 2 9.29 5.45 2.67 o 12 4 2 0.07 -3.84 2.74 o 13 4 2 4.73 -0.13 3.40 o 14 4 2 8.72 5.33 4.15 o 15 4 2 110.36 152.51 12.56 o 1 5 2 1260.35 1377.73 22.19 o 2 5 2 1376.19 1567.47 17.70 o 3 5 2 125.41 133.15 4.02 o 4 5 2 115.51 139.78 5.19 o 5 5 2 4.12 3.35 1.76 o 6 5 2 386.04 377.46 8.77 o 7 5 2 592.67 593.02 12.70 o 8 5 2 20.42 19.78 2.74 o 9 5 2 0.10 -2.85 1.90 o 10 5 2 139.46 126.10 5.17 o 11 5 2 39.94 37.58 5.35 o 12 5 2 15.89 11.61 3.32 o 13 5 2 84.32 103.35 9.25 o 14 5 2 5.70 4.24 5.82 o 15 5 2 18.22 18.71 5.60 o 0 6 2 638.80 653.27 14.84 o 1 6 2 258.93 252.02 4.61 o 2 6 2 1.55 3.83 1.26 o 3 6 2 635.18 720.75 25.91 o 4 6 2 135.89 134.48 4.34 o 5 6 2 61.04 75.44 5.02 o 6 6 2 58.74 64.95 4.13 o 7 6 2 29.26 31.04 3.26 o 8 6 2 98.91 90.17 4.48 o 9 6 2 0.50 -0.71 2.06 o 10 6 2 19.14 14.16 2.97 o 11 6 2 25.93 22.70 3.68 o 12 6 2 79.63 77.94 5.66 o 13 6 2 24.65 30.09 5.22 o 14 6 2 3.03 7.05 5.01 o 15 6 2 70.13 78.77 8.35 o 1 7 2 216.67 196.74 3.40 o 2 7 2 26.23 19.01 3.54 o 3 7 2 9.14 10.49 1.67 o 4 7 2 34.66 34.49 3.07 o 5 7 2 1067.45 1131.91 27.83 o 6 7 2 2.96 3.37 2.10 o 7 7 2 389.52 403.04 10.30 o 8 7 2 11.14 8.76 2.58 o 9 7 2 0.03 -2.53 2.26 o 10 7 2 16.36 6.80 2.84 o 11 7 2 58.63 54.71 5.75 o 12 7 2 22.81 20.49 4.80 o 13 7 2 83.88 85.68 7.31 o 14 7 2 9.40 8.78 4.74 o 0 8 2 25.64 31.03 2.75 o 1 8 2 81.21 76.00 3.07 o 2 8 2 33.47 30.10 3.32 o 3 8 2 457.45 407.95 12.14 o 4 8 2 7.63 6.01 2.02 o 5 8 2 416.22 391.50 8.57 o 6 8 2 587.25 598.85 17.85 o 7 8 2 15.36 12.53 2.64 o 8 8 2 360.91 340.39 7.98 o 9 8 2 248.48 236.32 6.91 o 10 8 2 31.66 31.04 3.92 o 11 8 2 287.20 257.36 7.66 o 12 8 2 219.52 186.60 7.60 o 13 8 2 3.46 -0.21 3.76 o 14 8 2 40.79 44.84 7.23 o 1 9 2 2.53 1.04 1.35 o 2 9 2 41.34 48.85 3.63 o 3 9 2 13.00 9.15 2.22 o 4 9 2 5.26 1.89 2.03 o 5 9 2 1.52 -0.56 1.93 o 6 9 2 8.48 4.53 2.33 o 7 9 2 43.89 53.29 5.13 o 8 9 2 44.74 43.32 4.17 o 9 9 2 2.81 -0.14 2.55 o 10 9 2 24.82 20.45 3.79 o 11 9 2 15.99 10.34 3.52 o 12 9 2 9.91 3.92 3.64 o 13 9 2 32.26 23.64 5.19 o 0 10 2 1.04 -0.38 2.40 o 1 10 2 121.91 123.54 4.09 o 2 10 2 36.70 32.34 3.01 o 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