#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/31/2233113.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233113_Fobs loop_ _publ_author_name 'Necefo\(glu, Hacali' '\"Ozbek, F\"ureya Elif' '\"Ozt\"urk, Vijdan' 'Ad\?ig\"uzel, Vedat' 'H\"okelek, Tuncer' _publ_section_title ; Aquabis(4-fluorobenzoato-\kO)bis(nicotinamide-\kN^1^)copper(II) nicotinamide hemisolvate trihydrate ; _journal_coeditor_code CV5200 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m52 _journal_page_last m53 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.247 _cell_angle_gamma 90.000 _cell_length_a 18.4108 _cell_length_b 14.8908 _cell_length_c 22.8569 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7461 _[local]_cod_data_source_file cv5200Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' w_3y in P 1 21/c 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 943.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 30.26 -5.97 5.97 o 2 0 0 128136.67 137865.42 2305.04 o 3 0 0 1980.46 1992.69 61.32 o 4 0 0 66183.58 63114.13 642.85 o 5 0 0 678.14 536.40 45.93 o 6 0 0 339288.84 374533.81 3716.12 o 7 0 0 1001.56 861.64 37.01 o 8 0 0 16997.53 17930.41 258.27 o 9 0 0 4222.29 4268.26 112.87 o 10 0 0 151.42 156.02 47.83 o 11 0 0 331.69 209.02 45.57 o 12 0 0 55674.02 54204.64 763.50 o 13 0 0 479.45 886.67 82.40 o 14 0 0 40367.71 39924.04 536.76 o 15 0 0 16088.08 16386.95 381.05 o 16 0 0 20863.81 20309.15 364.90 o 17 0 0 10659.67 10527.52 282.24 o 18 0 0 2160.33 2564.37 137.39 o 19 0 0 594.51 811.10 93.70 o 20 0 0 10433.43 10528.57 370.80 o 21 0 0 761.25 924.33 164.06 o 22 0 0 271.30 315.13 155.69 o 23 0 0 2733.86 3204.54 298.90 o 2 1 0 386.93 228.61 9.27 o 3 1 0 13650.77 13455.30 108.27 o 4 1 0 91.66 130.66 19.81 o 5 1 0 92246.02 86775.86 598.04 o 6 1 0 2142.19 2085.91 40.90 o 7 1 0 39218.24 37449.92 273.90 o 8 1 0 601.58 443.65 21.97 o 9 1 0 5824.62 5658.97 66.42 o 10 1 0 337.17 247.33 24.43 o 11 1 0 20899.07 21262.12 190.36 o 12 1 0 7443.41 6730.36 98.01 o 13 1 0 62.99 167.78 34.05 o 14 1 0 543.06 522.05 49.50 o 15 1 0 3437.55 3535.17 102.06 o 16 1 0 288.84 518.32 58.36 o 17 1 0 7790.09 7914.30 173.41 o 18 1 0 58.99 78.03 60.69 o 19 1 0 67.19 45.96 61.46 o 20 1 0 247.57 229.09 73.67 o 21 1 0 38.84 -38.22 76.07 o 22 1 0 23.90 -58.54 97.86 o 23 1 0 3097.44 3072.36 206.79 o 0 2 0 1970.54 2290.05 90.92 o 1 2 0 4294.21 4660.86 54.54 o 2 2 0 1393.74 1131.34 29.22 o 3 2 0 13381.76 13744.70 106.43 o 4 2 0 2347.60 2345.46 47.66 o 5 2 0 12.03 39.32 12.51 o 6 2 0 3635.01 3525.63 50.93 o 7 2 0 27991.88 28674.29 230.44 o 8 2 0 2600.44 3950.40 193.85 o 9 2 0 7461.19 6918.45 86.13 o 10 2 0 4848.48 4495.55 66.86 o 11 2 0 171.76 111.88 25.12 o 12 2 0 1797.70 1514.80 51.38 o 13 2 0 2668.13 2872.81 81.49 o 14 2 0 1140.85 1426.04 72.11 o 15 2 0 1301.00 1706.43 93.06 o 16 2 0 2952.04 2949.10 124.99 o 17 2 0 1006.44 1081.89 73.69 o 18 2 0 1.36 -46.72 46.72 o 19 2 0 161.58 138.26 64.44 o 20 2 0 80.13 26.42 71.12 o 21 2 0 210.83 264.43 79.72 o 22 2 0 1511.03 1546.73 128.30 o 23 2 0 637.55 780.48 122.08 o 1 3 0 8417.25 6878.36 70.29 o 2 3 0 10909.69 10793.93 108.15 o 3 3 0 1118.30 1263.64 32.45 o 4 3 0 3663.59 2392.87 37.49 o 5 3 0 10.99 -11.26 13.39 o 6 3 0 2315.66 2170.11 37.22 o 7 3 0 1587.39 1774.27 35.50 o 8 3 0 1554.64 1636.43 38.09 o 9 3 0 7605.11 6668.69 76.45 o 10 3 0 14600.68 14347.51 147.81 o 11 3 0 2089.58 2414.23 58.12 o 12 3 0 411.83 604.02 37.84 o 13 3 0 530.15 638.93 43.88 o 14 3 0 7618.78 7824.04 150.38 o 15 3 0 817.12 980.37 64.90 o 16 3 0 4109.72 4060.91 114.99 o 17 3 0 645.84 720.07 67.11 o 18 3 0 2781.99 2850.89 111.57 o 19 3 0 130.37 55.37 57.27 o 20 3 0 499.97 153.77 207.92 o 21 3 0 99.20 -63.63 133.47 o 22 3 0 1273.28 1440.04 217.40 o 23 3 0 14.75 -60.92 118.23 o 0 4 0 468462.81 515427.66 6445.38 o 1 4 0 36354.62 37493.77 592.84 o 2 4 0 231109.67 237379.36 2039.25 o 3 4 0 1548.50 2994.80 127.47 o 4 4 0 29236.30 29487.62 264.16 o 5 4 0 234.90 294.92 34.84 o 6 4 0 9615.57 8400.41 86.24 o 7 4 0 19306.45 17999.79 158.63 o 8 4 0 8667.96 9893.43 107.25 o 9 4 0 286.62 377.78 25.20 o 10 4 0 1745.88 1824.56 44.77 o 11 4 0 48.81 107.01 24.47 o 12 4 0 3880.80 3700.18 89.68 o 13 4 0 1395.62 1533.72 62.07 o 14 4 0 24534.16 25078.31 298.06 o 15 4 0 1.69 77.29 45.29 o 16 4 0 0.99 53.12 47.72 o 17 4 0 5070.08 5295.56 136.16 o 18 4 0 13.58 133.63 65.19 o 19 4 0 1499.24 1666.06 111.74 o 20 4 0 1553.01 1867.11 122.07 o 21 4 0 104.66 -6.71 128.23 o 22 4 0 282.38 141.23 140.43 o 23 4 0 770.84 691.34 155.13 o 1 5 0 4148.80 4200.13 63.86 o 2 5 0 1818.95 1635.09 46.18 o 3 5 0 101.65 77.42 19.85 o 4 5 0 1346.33 1078.54 36.46 o 5 5 0 3167.25 3449.76 58.56 o 6 5 0 5800.84 5967.22 74.10 o 7 5 0 424.74 329.15 26.62 o 8 5 0 142.77 236.54 22.81 o 9 5 0 602.25 564.56 30.37 o 10 5 0 1648.60 1508.29 43.44 o 11 5 0 277.96 407.36 32.17 o 12 5 0 808.02 1047.97 48.53 o 13 5 0 577.59 747.84 49.25 o 14 5 0 512.23 624.75 57.31 o 15 5 0 264.07 274.75 53.77 o 16 5 0 16.55 8.28 51.51 o 17 5 0 249.08 398.47 65.55 o 18 5 0 45.84 158.16 65.52 o 19 5 0 100.15 20.35 80.46 o 20 5 0 106.06 35.95 98.77 o 21 5 0 16.80 -69.24 89.00 o 22 5 0 3.53 65.25 99.83 o 23 5 0 15.71 -137.51 268.54 o 0 6 0 153.83 86.43 27.49 o 1 6 0 78258.49 82033.15 757.65 o 2 6 0 316.60 191.95 42.88 o 3 6 0 13705.31 14965.14 169.54 o 4 6 0 195.91 119.61 27.63 o 5 6 0 53202.52 50056.48 443.60 o 6 6 0 187.38 442.75 29.62 o 7 6 0 34065.79 34498.91 280.77 o 8 6 0 683.86 578.06 29.60 o 9 6 0 14642.77 13483.94 140.31 o 10 6 0 842.17 937.68 41.44 o 11 6 0 429.95 565.50 35.45 o 12 6 0 13.04 -0.31 30.28 o 13 6 0 3673.59 3564.71 89.08 o 14 6 0 1168.43 724.41 62.44 o 15 6 0 6652.22 6917.85 151.10 o 16 6 0 1418.69 1519.44 87.81 o 17 6 0 5246.88 5347.70 160.33 o 18 6 0 2189.60 2099.98 132.23 o 19 6 0 23.83 55.34 80.18 o 20 6 0 67.61 78.54 102.08 o 21 6 0 456.83 555.95 115.30 o 22 6 0 1368.76 1304.97 130.46 o 1 7 0 0.12 56.14 22.37 o 2 7 0 81668.94 82167.45 758.33 o 3 7 0 83.94 158.15 28.36 o 4 7 0 23819.56 23896.28 237.47 o 5 7 0 1269.34 1279.14 47.90 o 6 7 0 9.67 444.19 38.70 o 7 7 0 1096.36 1138.96 43.37 o 8 7 0 32701.30 31603.35 274.42 o 9 7 0 1068.86 1165.84 43.97 o 10 7 0 22299.54 22151.38 224.92 o 11 7 0 312.34 386.97 38.29 o 12 7 0 452.32 625.37 54.37 o 13 7 0 426.07 431.08 46.19 o 14 7 0 5308.23 5032.07 124.59 o 15 7 0 1261.28 1327.62 90.35 o 16 7 0 14360.80 14555.18 274.10 o 17 7 0 298.56 411.59 76.78 o 18 7 0 2292.64 2173.15 138.79 o 19 7 0 12.15 -70.65 70.65 o 20 7 0 2514.66 2701.04 153.62 o 21 7 0 12.62 -8.32 89.50 o 22 7 0 3403.49 3234.71 304.58 o 0 8 0 138.40 685.86 48.53 o 1 8 0 70616.88 69901.35 581.74 o 2 8 0 1801.27 2307.14 59.37 o 3 8 0 4681.91 4653.91 87.62 o 4 8 0 2595.47 3188.74 73.14 o 5 8 0 970.66 1333.92 48.87 o 6 8 0 1887.94 2261.94 65.86 o 7 8 0 23354.46 21954.82 230.08 o 8 8 0 2624.80 3077.39 72.65 o 9 8 0 858.29 981.84 46.00 o 10 8 0 665.82 570.18 44.40 o 11 8 0 440.43 581.73 42.73 o 12 8 0 222.54 316.45 52.33 o 13 8 0 17294.52 16995.83 223.89 o 14 8 0 1360.28 1501.73 80.72 o 15 8 0 2868.62 2768.38 113.73 o 16 8 0 38.39 -20.02 57.54 o 17 8 0 769.10 740.25 80.22 o 18 8 0 6.40 53.32 74.64 o 19 8 0 1048.44 1148.40 121.27 o 20 8 0 117.71 231.36 89.64 o 21 8 0 844.87 829.82 116.93 o 1 9 0 633.36 470.90 30.57 o 2 9 0 37.02 61.69 23.60 o 3 9 0 2206.88 2010.11 70.89 o 4 9 0 234.48 397.30 38.76 o 5 9 0 8822.29 8708.58 127.77 o 6 9 0 627.30 793.90 46.38 o 7 9 0 1405.01 1266.37 56.82 o 8 9 0 761.22 986.74 53.17 o 9 9 0 11678.02 11215.41 148.41 o 10 9 0 34.16 147.54 36.20 o 11 9 0 277.00 331.65 51.30 o 12 9 0 1941.20 2287.88 91.68 o 13 9 0 1927.84 2235.00 97.90 o 14 9 0 4.13 73.48 50.21 o 15 9 0 5532.56 6032.18 178.47 o 16 9 0 193.65 232.09 64.38 o 17 9 0 296.59 363.67 94.95 o 18 9 0 127.79 166.37 78.64 o 19 9 0 831.61 809.69 123.96 o 20 9 0 34.98 118.52 120.16 o 21 9 0 336.65 301.24 133.06 o 0 10 0 30767.60 31883.98 639.13 o 1 10 0 2605.92 3109.92 108.15 o 2 10 0 18053.44 17091.82 191.89 o 3 10 0 5.56 214.30 42.42 o 4 10 0 1120.64 1319.47 59.97 o 5 10 0 462.98 412.71 54.11 o 6 10 0 7565.90 7388.16 140.97 o 7 10 0 755.71 1275.12 87.30 o 8 10 0 17820.54 16513.94 289.59 o 9 10 0 1715.30 1700.69 123.49 o 10 10 0 182.88 320.97 41.69 o 11 10 0 79.35 144.97 54.80 o 12 10 0 7852.48 8190.61 165.16 o 13 10 0 84.08 173.83 62.46 o 14 10 0 1015.07 894.66 86.56 o 15 10 0 1.98 63.18 63.64 o 16 10 0 2153.64 2258.92 119.30 o 17 10 0 447.61 492.99 97.49 o 18 10 0 24.72 74.63 90.41 o 19 10 0 158.39 59.35 99.92 o 20 10 0 1221.47 1789.45 180.73 o 1 11 0 85.62 258.15 36.64 o 2 11 0 1424.00 1459.63 56.99 o 3 11 0 2903.22 2857.30 89.18 o 4 11 0 1583.86 1491.76 75.25 o 5 11 0 122.42 111.09 49.24 o 6 11 0 83.24 222.04 54.73 o 7 11 0 125.49 49.43 61.74 o 8 11 0 2829.83 3165.60 126.42 o 9 11 0 1927.68 2106.32 107.84 o 10 11 0 884.37 1096.88 87.05 o 11 11 0 627.35 810.14 92.73 o 12 11 0 2043.86 2270.49 115.55 o 13 11 0 57.61 -0.72 48.81 o 14 11 0 324.13 391.62 81.06 o 15 11 0 1237.35 1176.32 108.93 o 16 11 0 1104.97 985.39 133.78 o 17 11 0 2234.23 2417.43 161.72 o 18 11 0 81.83 -30.83 123.82 o 19 11 0 168.12 82.00 104.35 o 0 12 0 7731.64 9717.16 289.41 o 1 12 0 4193.02 4212.50 103.24 o 2 12 0 57.25 639.67 47.15 o 3 12 0 771.08 771.55 52.84 o 4 12 0 441.25 641.72 76.56 o 5 12 0 4819.84 4907.27 140.34 o 6 12 0 2247.85 3062.63 161.91 o 7 12 0 171.09 340.51 72.67 o 8 12 0 47.09 161.71 127.52 o 9 12 0 197.52 317.42 85.20 o 10 12 0 53.09 39.20 81.81 o 11 12 0 117.08 137.74 64.79 o 12 12 0 1607.72 1886.00 118.14 o 13 12 0 137.39 154.36 85.80 o 14 12 0 2.34 272.95 106.64 o 15 12 0 1360.40 1336.95 129.02 o 16 12 0 392.76 408.69 246.13 o 17 12 0 558.34 290.99 277.42 o 18 12 0 429.20 417.59 118.86 o 19 12 0 353.95 248.22 158.80 o 1 13 0 9811.11 9949.99 246.68 o 2 13 0 689.36 645.12 70.61 o 3 13 0 1243.61 1225.80 121.79 o 4 13 0 0.61 -8.02 37.76 o 5 13 0 6243.45 6771.05 208.06 o 6 13 0 9.40 360.22 72.79 o 7 13 0 1210.90 1430.64 107.62 o 8 13 0 104.39 93.66 78.22 o 9 13 0 2409.65 2743.43 224.81 o 10 13 0 1126.54 1045.05 123.74 o 11 13 0 4121.14 3943.11 223.48 o 12 13 0 1276.34 1379.48 127.76 o 13 13 0 903.23 907.93 123.51 o 14 13 0 1463.70 1136.85 134.17 o 15 13 0 367.56 244.44 131.89 o 16 13 0 686.29 583.69 228.30 o 17 13 0 3363.95 3669.23 283.02 o 0 14 0 21198.72 20374.01 572.06 o 1 14 0 56.47 174.32 72.11 o 2 14 0 6214.18 6792.06 194.43 o 3 14 0 492.17 508.60 71.78 o 4 14 0 652.93 617.33 72.54 o 5 14 0 115.19 334.10 91.62 o 6 14 0 13109.62 11765.41 316.95 o 7 14 0 493.65 331.52 91.27 o 8 14 0 10574.48 9699.96 300.52 o 9 14 0 19.10 124.42 126.80 o 10 14 0 103.67 167.43 132.96 o 11 14 0 1.88 75.88 150.90 o 12 14 0 12729.64 12169.06 321.62 o 13 14 0 1323.21 1128.62 205.20 o 14 14 0 3348.28 3358.00 201.66 o 15 14 0 275.28 10.21 280.31 o 16 14 0 320.01 373.84 150.43 o 1 15 0 1346.68 1646.40 136.95 o 2 15 0 1108.35 1288.54 110.55 o 3 15 0 2964.47 3449.81 155.95 o 4 15 0 4338.51 4109.05 167.04 o 5 15 0 3385.29 3325.85 148.18 o 6 15 0 179.44 184.59 110.29 o 7 15 0 812.31 772.91 157.50 o 8 15 0 386.59 69.37 128.83 o 9 15 0 654.90 617.49 154.85 o 10 15 0 1062.04 1019.65 181.29 o 11 15 0 4535.09 4782.23 313.88 o 12 15 0 611.08 364.75 172.47 o 13 15 0 177.53 106.89 144.55 o 14 15 0 145.71 184.95 111.24 o 15 15 0 2355.92 2145.11 182.84 o 0 16 0 288.59 1764.49 528.12 o 1 16 0 8813.96 8632.30 248.51 o 2 16 0 386.60 634.70 198.13 o 3 16 0 412.35 241.13 99.29 o 4 16 0 0.95 10.14 128.98 o 5 16 0 4561.86 4220.85 235.33 o 6 16 0 0.11 302.87 170.07 o 7 16 0 7628.03 8504.15 338.04 o 8 16 0 52.05 191.16 269.31 o 9 16 0 1158.04 923.73 174.91 o 10 16 0 134.37 22.98 144.07 o 11 16 0 10.36 21.89 157.30 o 12 16 0 111.51 11.82 293.94 o 13 16 0 1527.86 1646.20 233.86 o 14 16 0 121.94 214.83 126.59 o 1 17 0 35.68 348.63 119.76 o 2 17 0 1547.12 1760.97 205.88 o 3 17 0 1491.30 1516.18 163.39 o 4 17 0 2592.01 2735.09 224.81 o 5 17 0 46.20 46.03 94.64 o 6 17 0 1349.19 1362.04 188.12 o 7 17 0 14.48 227.54 178.35 o 8 17 0 3102.40 3319.82 814.56 o 9 17 0 726.93 867.82 239.37 o 10 17 0 1751.87 1647.31 296.93 o 11 17 0 1.31 -103.57 153.40 o 12 17 0 24.03 -182.55 247.68 o 0 18 0 361.60 116.37 161.12 o 1 18 0 1413.16 1878.05 192.97 o 2 18 0 249.05 251.32 134.27 o 3 18 0 53.40 148.19 111.84 o 4 18 0 102.01 114.38 111.84 o 5 18 0 34.21 129.79 109.26 o 6 18 0 9.35 -16.41 105.72 o 7 18 0 171.33 394.83 232.73 o 8 18 0 130.69 268.54 232.73 o 9 18 0 274.33 268.54 241.68 o 10 18 0 9.16 -26.85 232.73 o 1 19 0 222.29 353.27 142.31 o 2 19 0 275.80 204.60 131.12 o 3 19 0 789.99 906.32 214.83 o 4 19 0 277.72 151.52 126.88 o 5 19 0 194.98 274.21 126.88 o 6 19 0 4.49 -51.64 113.86 o 7 19 0 21.52 136.45 134.27 o -23 1 1 1993.17 2186.81 179.83 o -22 1 1 1313.77 1297.36 106.61 o -21 1 1 1205.49 1405.64 103.24 o -20 1 1 62.79 17.09 63.84 o -19 1 1 255.36 277.07 66.89 o -18 1 1 25.77 57.21 55.75 o -17 1 1 3061.11 3433.45 103.00 o -16 1 1 11658.19 11867.96 180.63 o -15 1 1 10119.75 10646.70 193.05 o -14 1 1 3162.81 3243.24 89.49 o -13 1 1 93.72 87.43 27.22 o -12 1 1 2636.38 2662.16 53.94 o -11 1 1 8872.86 9498.53 106.73 o -10 1 1 4062.77 4240.68 58.29 o -9 1 1 10049.63 9577.43 92.08 o -8 1 1 3007.97 2688.90 41.33 o -7 1 1 11272.21 11297.17 99.94 o -6 1 1 3643.38 4339.72 50.08 o -5 1 1 13970.04 13112.75 107.81 o -4 1 1 8897.16 9422.38 85.51 o -3 1 1 35648.91 33355.34 235.68 o -2 1 1 1115.62 641.10 14.79 o -1 1 1 2511.44 1523.76 505.87 o 0 1 1 273.30 30.13 5.81 o 1 1 1 9500.61 8703.07 332.76 o 2 1 1 2846.97 3325.62 34.67 o 3 1 1 23971.98 21741.65 165.60 o 4 1 1 121.03 77.58 25.59 o 5 1 1 15425.42 14777.54 122.16 o 6 1 1 89.21 84.94 13.54 o 7 1 1 14234.63 14113.08 117.57 o 8 1 1 11389.70 11273.54 106.56 o 9 1 1 11099.57 10251.18 99.84 o 10 1 1 53.74 99.55 18.32 o 11 1 1 693.42 804.83 36.90 o 12 1 1 81.74 47.46 25.21 o 13 1 1 552.74 528.23 55.84 o 14 1 1 1335.02 1434.34 68.75 o 15 1 1 9822.82 9874.06 195.26 o 16 1 1 301.43 450.09 62.19 o 17 1 1 2268.76 2564.96 109.64 o 18 1 1 428.59 598.69 75.05 o 19 1 1 196.53 238.45 66.14 o 20 1 1 2384.01 2365.59 118.19 o 21 1 1 747.42 891.85 112.05 o 22 1 1 41.46 -63.45 102.75 o 23 1 1 473.00 678.59 137.05 o -23 2 1 2133.64 2391.53 242.89 o -22 2 1 3224.16 2869.93 158.19 o -21 2 1 196.98 125.85 87.73 o -20 2 1 991.62 868.39 100.23 o -19 2 1 22.14 28.58 59.42 o -18 2 1 3987.24 3778.90 168.88 o -17 2 1 2113.72 2385.77 110.98 o -16 2 1 23797.19 23488.48 293.04 o -15 2 1 850.49 1181.10 70.40 o -14 2 1 49243.97 47634.10 512.02 o -13 2 1 108.24 230.80 31.80 o -12 2 1 41357.59 42451.73 368.88 o -11 2 1 8605.97 8538.29 106.04 o 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