#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/31/2233137.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233137_Fobs loop_ _publ_author_name 'Zipp, Caitlin F.' 'Fernandes, Manuel A.' 'Marques, Helder M.' 'Michael, Joseph P.' _publ_section_title ; (2-Aminophenyl)methanol ; _journal_coeditor_code FJ2480 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o174 _journal_volume 68 _journal_year 2012 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.6222 _cell_length_b 6.0675 _cell_length_c 4.7005 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file fj2480Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11c_czhmm_0s in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1086.37 1001.77 48.14 o 4 0 0 1798.61 1701.18 88.22 o 6 0 0 105.34 103.18 3.45 o 8 0 0 261.26 253.00 2.28 o 10 0 0 312.89 336.37 8.51 o 12 0 0 358.28 345.85 10.20 o 14 0 0 1839.26 1906.25 76.20 o 16 0 0 131.83 125.19 7.48 o 18 0 0 28.31 30.24 2.69 o 20 0 0 43.21 47.77 4.90 o 22 0 0 21.25 25.38 2.80 o 24 0 0 174.25 154.28 4.55 o 26 0 0 0.34 0.72 0.91 o 1 1 0 851.63 862.10 11.98 o 2 1 0 1563.72 1509.79 30.59 o 3 1 0 720.13 682.21 7.75 o 4 1 0 379.22 369.01 7.07 o 5 1 0 12.91 14.60 0.34 o 6 1 0 6.34 8.65 0.37 o 7 1 0 139.17 125.09 3.90 o 8 1 0 62.97 66.69 1.49 o 9 1 0 24.73 26.68 0.49 o 10 1 0 13.19 12.92 0.38 o 11 1 0 225.26 237.33 8.80 o 12 1 0 23.57 28.76 1.19 o 13 1 0 1.75 3.06 0.27 o 14 1 0 129.22 129.72 4.68 o 15 1 0 17.72 21.16 0.76 o 16 1 0 39.42 43.93 1.94 o 17 1 0 13.44 12.28 1.07 o 18 1 0 1.34 1.28 0.30 o 19 1 0 0.46 0.32 0.22 o 20 1 0 0.95 0.73 0.25 o 21 1 0 3.14 2.62 0.35 o 22 1 0 1.51 1.48 0.45 o 23 1 0 0.00 -0.27 0.41 o 24 1 0 6.99 6.26 0.66 o 25 1 0 7.64 6.11 0.85 o 26 1 0 15.48 13.87 1.17 o 27 1 0 10.14 10.92 1.09 o 0 2 0 698.03 704.22 8.96 o 1 2 0 549.21 540.58 7.43 o 2 2 0 1632.73 1633.71 14.34 o 3 2 0 1795.81 1763.42 18.36 o 4 2 0 619.49 629.03 10.23 o 5 2 0 68.07 64.59 1.22 o 6 2 0 2.83 3.45 0.20 o 7 2 0 316.83 319.45 8.75 o 8 2 0 133.15 136.72 2.53 o 9 2 0 220.88 220.16 7.76 o 10 2 0 55.79 56.93 2.30 o 11 2 0 0.13 0.24 0.15 o 12 2 0 38.67 43.35 1.67 o 13 2 0 208.75 209.72 9.86 o 14 2 0 153.05 158.84 7.17 o 15 2 0 13.54 14.41 0.96 o 16 2 0 257.29 235.91 7.88 o 17 2 0 55.71 55.91 2.69 o 18 2 0 95.22 97.00 7.12 o 19 2 0 0.01 0.81 0.47 o 20 2 0 22.01 20.49 0.93 o 21 2 0 189.11 185.50 8.21 o 22 2 0 70.17 70.62 6.73 o 23 2 0 7.32 8.66 0.74 o 24 2 0 0.65 0.42 0.45 o 25 2 0 16.54 15.78 1.31 o 26 2 0 0.03 -0.11 0.58 o 1 3 0 26.48 36.26 0.61 o 2 3 0 18.67 19.50 0.36 o 3 3 0 642.54 696.79 18.93 o 4 3 0 145.32 176.92 4.27 o 5 3 0 3.19 4.21 0.24 o 6 3 0 1.27 1.15 0.22 o 7 3 0 209.37 233.79 5.53 o 8 3 0 22.90 25.50 0.81 o 9 3 0 67.77 73.74 2.30 o 10 3 0 495.30 522.03 20.30 o 11 3 0 18.41 24.55 1.05 o 12 3 0 2.68 3.10 0.29 o 13 3 0 17.55 17.45 0.68 o 14 3 0 373.24 382.04 14.67 o 15 3 0 0.00 0.18 0.27 o 16 3 0 17.75 16.62 0.69 o 17 3 0 378.56 353.33 13.48 o 18 3 0 40.48 37.83 2.77 o 19 3 0 0.09 0.11 0.37 o 20 3 0 31.17 32.21 1.20 o 21 3 0 69.39 68.82 2.68 o 22 3 0 0.69 0.38 0.47 o 23 3 0 36.70 37.48 3.64 o 24 3 0 105.46 116.92 9.44 o 25 3 0 5.24 6.49 0.75 o 0 4 0 21.06 25.63 1.19 o 1 4 0 113.73 122.00 2.77 o 2 4 0 59.65 62.43 1.46 o 3 4 0 105.36 103.02 3.97 o 4 4 0 0.03 0.04 0.31 o 5 4 0 175.22 157.63 8.10 o 6 4 0 5.07 6.71 0.57 o 7 4 0 315.82 302.30 14.78 o 8 4 0 0.31 1.25 0.39 o 9 4 0 195.12 206.95 10.13 o 10 4 0 28.47 34.85 1.62 o 11 4 0 141.12 141.64 8.29 o 12 4 0 7.31 8.79 0.59 o 13 4 0 1.01 2.02 0.41 o 14 4 0 68.54 69.14 2.96 o 15 4 0 57.54 56.17 4.15 o 16 4 0 14.75 14.51 0.65 o 17 4 0 7.86 7.93 0.56 o 18 4 0 26.77 27.33 1.00 o 19 4 0 13.86 15.49 0.79 o 20 4 0 3.77 4.60 0.54 o 21 4 0 28.39 27.05 1.44 o 22 4 0 3.38 3.18 0.64 o 23 4 0 29.60 31.90 2.34 o 1 5 0 11.30 11.88 0.66 o 2 5 0 7.55 7.31 0.58 o 3 5 0 0.90 1.29 0.42 o 4 5 0 148.82 152.13 8.85 o 5 5 0 32.87 29.94 1.79 o 6 5 0 8.99 6.75 0.56 o 7 5 0 100.10 109.37 6.19 o 8 5 0 107.27 106.94 9.19 o 9 5 0 32.87 32.23 2.93 o 10 5 0 9.48 8.70 0.73 o 11 5 0 27.58 29.08 1.63 o 12 5 0 20.02 19.10 0.97 o 13 5 0 9.24 11.77 1.30 o 14 5 0 16.18 15.53 1.26 o 15 5 0 2.42 3.01 0.50 o 16 5 0 6.83 8.19 0.57 o 17 5 0 14.85 16.45 1.55 o 18 5 0 21.59 19.87 1.38 o 19 5 0 3.90 4.78 0.70 o 20 5 0 10.55 10.68 0.89 o 0 6 0 14.76 13.60 1.45 o 1 6 0 0.17 0.13 0.39 o 2 6 0 2.63 1.70 0.46 o 3 6 0 47.33 49.54 2.93 o 4 6 0 3.22 3.18 0.53 o 5 6 0 59.73 59.60 3.23 o 6 6 0 55.56 65.79 4.07 o 7 6 0 594.96 593.35 37.80 o 8 6 0 0.30 5.08 0.78 o 9 6 0 17.02 19.62 1.67 o 10 6 0 50.55 51.81 4.87 o 11 6 0 6.98 6.22 0.75 o 12 6 0 7.23 6.67 1.04 o 13 6 0 3.60 3.58 1.38 o 14 6 0 17.85 22.65 4.98 o 15 6 0 4.42 4.55 1.34 o 16 6 0 1.80 1.69 0.71 o 1 7 0 0.03 -0.35 0.62 o 2 7 0 1.37 1.33 0.74 o 3 7 0 0.14 -0.19 0.63 o 4 7 0 5.85 3.37 0.84 o 5 7 0 2.64 -0.20 0.66 o 6 7 0 3.63 3.66 0.89 o 7 7 0 2.85 2.41 0.82 o 8 7 0 0.01 0.41 0.71 o 9 7 0 7.55 4.22 1.95 o 2 0 1 3174.96 3202.73 136.71 o 4 0 1 8212.29 7088.11 376.31 o 6 0 1 378.65 368.41 9.87 o 8 0 1 445.86 435.27 12.09 o 10 0 1 799.33 836.00 33.63 o 12 0 1 211.85 230.69 6.90 o 14 0 1 168.37 160.94 4.35 o 16 0 1 173.66 165.33 4.42 o 18 0 1 237.96 243.03 6.92 o 20 0 1 124.93 115.18 9.22 o 22 0 1 67.29 69.60 3.83 o 24 0 1 2.56 3.91 0.59 o 26 0 1 11.69 11.94 1.73 o 0 1 1 3230.31 3086.35 81.44 o 1 1 1 474.65 478.88 7.58 o 2 1 1 446.78 409.26 9.58 o 3 1 1 1292.31 1248.90 23.16 o 4 1 1 434.21 411.45 7.14 o 5 1 1 530.80 519.78 9.58 o 6 1 1 717.41 727.92 13.38 o 7 1 1 585.95 611.20 11.80 o 8 1 1 98.64 110.48 2.69 o 9 1 1 41.00 43.28 0.86 o 10 1 1 213.61 229.15 5.36 o 11 1 1 30.89 37.21 1.14 o 12 1 1 5.42 5.56 0.23 o 13 1 1 77.59 84.22 2.49 o 14 1 1 52.91 58.47 1.70 o 15 1 1 44.76 48.03 1.57 o 16 1 1 17.42 20.18 0.76 o 17 1 1 3.39 3.87 0.24 o 18 1 1 28.71 29.44 0.94 o 19 1 1 76.50 74.24 1.95 o 20 1 1 44.20 46.56 1.24 o 21 1 1 26.69 25.64 0.96 o 22 1 1 13.31 12.31 0.56 o 23 1 1 11.86 10.82 0.54 o 24 1 1 7.28 6.10 0.46 o 25 1 1 2.93 2.38 0.44 o 26 1 1 0.91 1.16 0.47 o 27 1 1 1.15 1.37 0.48 o 1 2 1 503.23 476.46 7.81 o 2 2 1 83.06 82.95 1.39 o 3 2 1 603.34 596.14 7.81 o 4 2 1 1215.88 1228.34 15.30 o 5 2 1 205.75 219.15 3.38 o 6 2 1 812.76 812.67 14.40 o 7 2 1 511.77 536.88 10.50 o 8 2 1 244.71 240.92 6.42 o 9 2 1 44.57 51.02 1.46 o 10 2 1 173.27 174.05 5.63 o 11 2 1 95.76 104.35 3.84 o 12 2 1 23.79 22.21 0.71 o 13 2 1 70.01 69.76 2.92 o 14 2 1 29.95 31.09 1.36 o 15 2 1 34.87 32.83 1.42 o 16 2 1 23.24 24.98 1.20 o 17 2 1 349.58 358.55 15.18 o 18 2 1 245.18 252.73 12.65 o 19 2 1 2.28 3.60 0.32 o 20 2 1 123.96 122.25 5.29 o 21 2 1 69.07 68.99 2.63 o 22 2 1 22.75 22.73 1.01 o 23 2 1 3.40 3.81 0.47 o 24 2 1 8.41 8.13 0.67 o 25 2 1 10.91 11.83 0.78 o 26 2 1 1.53 1.45 0.50 o 0 3 1 161.78 160.18 3.31 o 1 3 1 187.16 191.88 2.94 o 2 3 1 14.05 13.80 0.51 o 3 3 1 133.06 142.35 2.82 o 4 3 1 23.36 20.68 0.35 o 5 3 1 57.01 66.74 1.13 o 6 3 1 93.60 94.88 1.87 o 7 3 1 43.49 42.10 1.26 o 8 3 1 49.93 50.05 1.53 o 9 3 1 26.84 32.49 1.07 o 10 3 1 82.05 86.24 2.78 o 11 3 1 5.14 5.41 0.26 o 12 3 1 69.23 70.94 2.87 o 13 3 1 140.59 142.58 6.05 o 14 3 1 23.12 24.39 1.23 o 15 3 1 46.45 48.08 1.70 o 16 3 1 38.98 40.62 1.78 o 17 3 1 2.08 2.04 0.28 o 18 3 1 21.50 23.17 0.73 o 19 3 1 29.88 30.17 1.44 o 20 3 1 39.79 40.82 2.15 o 21 3 1 49.12 46.85 2.42 o 22 3 1 13.68 12.84 0.78 o 23 3 1 12.43 11.73 0.77 o 24 3 1 4.44 4.58 0.65 o 25 3 1 10.84 9.50 0.76 o 1 4 1 256.92 251.43 4.62 o 2 4 1 217.28 224.67 4.11 o 3 4 1 369.81 380.86 7.61 o 4 4 1 28.42 28.84 0.56 o 5 4 1 1.86 2.03 0.19 o 6 4 1 3.96 2.98 0.19 o 7 4 1 5.70 6.26 0.26 o 8 4 1 26.14 25.74 0.86 o 9 4 1 9.33 9.93 0.35 o 10 4 1 146.04 152.59 4.68 o 11 4 1 239.56 242.74 9.32 o 12 4 1 31.73 32.05 1.22 o 13 4 1 148.06 151.02 6.51 o 14 4 1 158.24 160.73 8.75 o 15 4 1 44.36 45.94 2.66 o 16 4 1 14.53 13.70 0.50 o 17 4 1 23.40 22.99 1.40 o 18 4 1 14.07 13.99 0.73 o 19 4 1 2.75 2.97 0.36 o 20 4 1 6.70 7.72 0.47 o 21 4 1 0.38 0.89 0.46 o 22 4 1 4.89 4.08 0.59 o 23 4 1 0.96 1.93 0.54 o 0 5 1 189.01 189.23 7.46 o 1 5 1 68.74 67.87 1.08 o 2 5 1 16.22 16.83 0.59 o 3 5 1 57.18 57.07 1.34 o 4 5 1 67.42 65.17 2.58 o 5 5 1 38.69 40.60 1.63 o 6 5 1 46.21 43.96 1.94 o 7 5 1 91.60 87.51 2.68 o 8 5 1 16.85 13.73 0.91 o 9 5 1 1.95 1.85 0.27 o 10 5 1 38.12 36.19 1.39 o 11 5 1 17.47 19.40 1.06 o 12 5 1 1.78 2.15 0.32 o 13 5 1 20.34 20.72 1.15 o 14 5 1 11.80 10.08 0.69 o 15 5 1 3.82 3.29 0.39 o 16 5 1 2.89 1.83 0.39 o 17 5 1 3.35 2.75 0.38 o 18 5 1 1.43 1.55 0.36 o 19 5 1 11.62 10.78 0.81 o 20 5 1 10.87 10.73 0.80 o 1 6 1 14.46 14.12 0.60 o 2 6 1 0.12 0.87 0.31 o 3 6 1 112.75 110.32 3.41 o 4 6 1 10.87 11.96 0.58 o 5 6 1 60.37 60.32 2.26 o 6 6 1 18.10 17.89 1.20 o 7 6 1 20.70 22.68 1.27 o 8 6 1 26.37 27.20 1.44 o 9 6 1 73.87 74.50 5.81 o 10 6 1 34.48 37.77 3.24 o 11 6 1 138.33 134.57 8.74 o 12 6 1 1.68 3.15 0.51 o 13 6 1 28.18 29.52 1.72 o 14 6 1 18.09 17.50 1.24 o 15 6 1 20.07 21.15 0.90 o 0 7 1 45.41 44.78 2.06 o 1 7 1 3.34 3.65 0.62 o 2 7 1 1.02 0.63 0.52 o 3 7 1 12.83 10.71 0.83 o 4 7 1 23.09 22.60 1.37 o 5 7 1 0.45 0.85 0.52 o 6 7 1 10.98 11.33 0.85 o 7 7 1 18.71 16.66 0.99 o 8 7 1 7.66 8.85 0.79 o 0 0 2 1392.52 1299.15 76.28 o 2 0 2 491.25 518.02 27.48 o 4 0 2 627.32 680.17 39.96 o 6 0 2 66.29 65.62 1.96 o 8 0 2 104.65 103.15 3.61 o 10 0 2 167.74 171.04 3.76 o 12 0 2 436.06 452.42 18.58 o 14 0 2 219.01 224.27 12.04 o 16 0 2 48.54 48.33 4.13 o 18 0 2 81.65 81.36 5.39 o 20 0 2 0.18 0.02 0.56 o 22 0 2 1.53 0.81 0.62 o 24 0 2 6.26 7.21 1.48 o 26 0 2 29.52 36.89 6.50 o 1 1 2 23.07 27.59 0.56 o 2 1 2 143.97 143.76 1.94 o 3 1 2 171.07 155.18 6.89 o 4 1 2 994.53 984.98 15.13 o 5 1 2 245.20 251.74 4.41 o 6 1 2 45.42 39.76 1.07 o 7 1 2 278.53 273.74 5.54 o 8 1 2 71.55 73.31 1.69 o 9 1 2 302.00 308.61 7.17 o 10 1 2 151.99 151.43 4.22 o 11 1 2 101.09 107.37 2.65 o 12 1 2 25.25 24.86 0.67 o 13 1 2 60.78 60.46 1.87 o 14 1 2 146.60 153.33 6.14 o 15 1 2 46.47 45.68 1.99 o 16 1 2 23.17 25.21 1.53 o 17 1 2 174.21 176.76 9.17 o 18 1 2 88.33 80.71 3.35 o 19 1 2 1.66 1.64 0.37 o 20 1 2 35.03 30.91 2.12 o 21 1 2 59.86 58.51 2.89 o 22 1 2 0.66 0.89 0.56 o 23 1 2 24.35 25.98 2.87 o 24 1 2 19.23 22.20 1.65 o 25 1 2 8.56 9.33 0.93 o 0 2 2 577.02 572.74 13.60 o 1 2 2 39.02 40.38 1.40 o 2 2 2 104.51 101.39 3.33 o 3 2 2 518.56 490.53 20.00 o 4 2 2 100.81 96.12 2.15 o 5 2 2 226.83 239.97 5.51 o 6 2 2 358.76 353.30 7.99 o 7 2 2 573.54 570.19 13.69 o 8 2 2 253.47 251.39 5.54 o 9 2 2 115.30 107.26 2.86 o 10 2 2 196.44 202.20 4.78 o 11 2 2 1.57 1.25 0.19 o 12 2 2 21.84 23.21 0.77 o 13 2 2 58.14 55.25 2.20 o 14 2 2 165.29 156.67 5.97 o 15 2 2 0.13 0.56 0.24 o 16 2 2 91.39 82.65 4.23 o 17 2 2 37.42 37.77 1.94 o 18 2 2 16.22 15.52 0.73 o 19 2 2 27.27 28.04 2.00 o 20 2 2 73.19 69.87 3.66 o 21 2 2 51.77 50.30 2.74 o 22 2 2 26.87 25.79 1.62 o 23 2 2 0.09 0.48 0.38 o 24 2 2 20.40 19.17 2.61 o 25 2 2 8.62 9.64 2.13 o 1 3 2 106.58 106.35 2.37 o 2 3 2 78.13 74.08 1.86 o 3 3 2 10.71 10.62 0.31 o 4 3 2 3.06 2.52 0.19 o 5 3 2 11.27 11.80 0.36 o 6 3 2 20.53 19.51 0.47 o 7 3 2 14.61 14.93 0.37 o 8 3 2 1.50 1.70 0.19 o 9 3 2 1.66 1.38 0.18 o 10 3 2 4.80 4.98 0.24 o 11 3 2 0.12 0.30 0.16 o 12 3 2 19.16 18.62 0.91 o 13 3 2 10.70 11.15 0.49 o 14 3 2 11.47 10.46 0.74 o 15 3 2 7.89 6.33 0.42 o 16 3 2 0.64 0.61 0.29 o 17 3 2 25.06 23.52 1.20 o 18 3 2 12.84 11.99 0.56 o 19 3 2 4.88 5.00 0.57 o 20 3 2 0.60 0.42 0.37 o 21 3 2 3.62 3.28 0.46 o 22 3 2 0.43 0.77 0.45 o 23 3 2 1.38 2.05 0.52 o 0 4 2 533.44 522.14 9.41 o 1 4 2 171.17 158.19 3.06 o 2 4 2 32.00 30.59 0.75 o 3 4 2 98.13 93.18 1.65 o 4 4 2 214.13 201.91 3.60 o 5 4 2 36.09 36.05 0.90 o 6 4 2 67.52 68.17 1.37 o 7 4 2 276.06 281.07 7.65 o 8 4 2 32.26 31.74 1.10 o 9 4 2 63.23 66.45 1.97 o 10 4 2 112.38 103.13 4.21 o 11 4 2 21.15 19.49 0.94 o 12 4 2 51.73 47.08 2.03 o 13 4 2 48.95 44.55 2.61 o 14 4 2 11.47 9.60 0.52 o 15 4 2 38.84 34.91 2.50 o 16 4 2 4.95 4.50 0.48 o 17 4 2 34.86 32.24 2.89 o 18 4 2 4.25 4.07 0.47 o 19 4 2 3.69 3.84 0.56 o 20 4 2 2.40 2.69 0.55 o 21 4 2 33.38 39.89 3.10 o 1 5 2 12.57 11.05 0.62 o 2 5 2 67.17 63.09 2.46 o 3 5 2 109.06 107.73 1.75 o 4 5 2 0.98 1.07 0.24 o 5 5 2 13.44 13.07 0.42 o 6 5 2 37.29 35.98 1.00 o 7 5 2 21.57 23.82 0.65 o 8 5 2 12.30 13.05 0.42 o 9 5 2 23.58 22.39 0.72 o 10 5 2 21.47 21.92 0.75 o 11 5 2 75.17 67.35 2.84 o 12 5 2 9.92 8.96 0.64 o 13 5 2 2.74 3.44 0.50 o 14 5 2 15.10 13.93 0.76 o 15 5 2 0.40 -0.12 0.44 o 16 5 2 4.56 3.94 0.59 o 17 5 2 16.21 17.24 1.90 o 18 5 2 9.20 9.20 0.75 o 0 6 2 28.19 30.39 2.00 o 1 6 2 3.48 3.86 0.44 o 2 6 2 18.46 19.80 0.82 o 3 6 2 28.84 25.11 3.91 o 4 6 2 1.00 1.72 0.41 o 5 6 2 50.87 50.82 2.07 o 6 6 2 4.00 4.64 0.57 o 7 6 2 43.05 40.29 2.08 o 8 6 2 0.75 1.10 0.42 o 9 6 2 19.90 16.53 0.89 o 10 6 2 2.60 2.88 0.70 o 11 6 2 26.02 22.20 1.33 o 12 6 2 15.69 13.51 1.05 o 13 6 2 1.54 1.50 0.68 o 1 7 2 2.38 2.67 0.60 o 2 7 2 28.20 28.19 1.28 o 2 0 3 77.38 77.89 4.75 o 4 0 3 238.26 229.30 23.36 o 6 0 3 138.49 123.42 1.89 o 8 0 3 307.20 291.97 8.30 o 10 0 3 572.11 562.54 22.32 o 12 0 3 14.25 14.33 0.69 o 14 0 3 284.86 295.16 27.35 o 16 0 3 1.88 2.19 0.50 o 18 0 3 4.19 3.96 0.85 o 20 0 3 5.04 5.26 0.79 o 22 0 3 18.46 21.39 3.91 o 0 1 3 524.23 523.82 14.17 o 1 1 3 57.47 56.58 1.54 o 2 1 3 13.79 13.66 0.60 o 3 1 3 46.90 46.17 1.30 o 4 1 3 14.52 13.94 0.39 o 5 1 3 11.72 12.42 0.37 o 6 1 3 8.20 7.19 0.26 o 7 1 3 84.84 85.49 2.89 o 8 1 3 52.78 46.59 3.98 o 9 1 3 0.17 0.52 0.20 o 10 1 3 13.03 13.05 0.37 o 11 1 3 88.54 90.76 2.72 o 12 1 3 35.78 35.98 1.13 o 13 1 3 80.00 82.56 4.10 o 14 1 3 66.92 71.92 3.51 o 15 1 3 11.55 11.82 0.74 o 16 1 3 48.41 43.58 4.00 o 17 1 3 22.42 19.52 1.09 o 18 1 3 11.22 9.62 0.65 o 19 1 3 0.61 0.54 0.41 o 20 1 3 0.76 0.89 0.43 o 21 1 3 23.45 26.31 1.99 o 22 1 3 5.85 5.66 0.61 o 23 1 3 6.08 6.09 0.67 o 1 2 3 124.31 121.55 2.29 o 2 2 3 4.21 6.08 0.38 o 3 2 3 96.52 95.93 3.15 o 4 2 3 39.29 38.56 1.54 o 5 2 3 0.52 1.36 0.23 o 6 2 3 154.43 150.82 5.43 o 7 2 3 42.46 41.81 1.32 o 8 2 3 203.60 197.39 6.85 o 9 2 3 30.81 32.14 1.51 o 10 2 3 160.60 166.09 5.99 o 11 2 3 182.76 175.23 7.73 o 12 2 3 7.52 9.50 0.44 o 13 2 3 102.41 105.13 4.11 o 14 2 3 49.40 46.99 2.25 o 15 2 3 0.94 1.92 0.30 o 16 2 3 10.19 8.56 0.66 o 17 2 3 14.22 12.86 0.76 o 18 2 3 5.16 5.81 0.55 o 19 2 3 3.19 2.55 0.49 o 20 2 3 8.08 8.24 1.10 o 21 2 3 2.36 1.82 0.49 o 22 2 3 18.99 18.12 2.00 o 0 3 3 218.85 209.03 5.45 o 1 3 3 9.48 11.01 0.70 o 2 3 3 36.42 34.57 1.17 o 3 3 3 122.49 123.41 3.69 o 4 3 3 76.84 79.62 2.52 o 5 3 3 11.73 12.88 0.54 o 6 3 3 11.99 11.18 0.52 o 7 3 3 105.67 101.92 3.52 o 8 3 3 0.43 0.60 0.24 o 9 3 3 29.74 29.36 0.93 o 10 3 3 53.24 45.64 1.84 o 11 3 3 25.45 21.99 1.40 o 12 3 3 7.40 7.93 0.50 o 13 3 3 18.41 16.00 0.97 o 14 3 3 18.92 18.41 1.42 o 15 3 3 6.31 6.83 0.68 o 16 3 3 17.83 15.93 0.90 o 17 3 3 1.49 1.39 0.40 o 18 3 3 2.01 2.02 0.43 o 19 3 3 7.32 8.81 1.03 o 20 3 3 0.92 2.40 0.53 o 21 3 3 10.06 10.46 0.81 o 1 4 3 107.02 100.92 2.20 o 2 4 3 42.49 40.20 0.81 o 3 4 3 124.03 123.20 2.52 o 4 4 3 88.01 87.83 1.77 o 5 4 3 3.32 3.84 0.40 o 6 4 3 80.87 79.84 3.37 o 7 4 3 2.27 5.22 0.43 o 8 4 3 32.77 30.89 1.69 o 9 4 3 5.06 7.35 0.46 o 10 4 3 9.98 8.63 0.52 o 11 4 3 35.79 34.50 2.02 o 12 4 3 5.75 5.67 0.45 o 13 4 3 39.82 40.43 2.41 o 14 4 3 6.30 8.09 0.50 o 15 4 3 30.35 31.42 1.87 o 16 4 3 1.62 1.95 0.54 o 17 4 3 42.41 45.55 2.30 o 18 4 3 7.77 8.01 0.62 o 0 5 3 28.11 25.87 0.98 o 1 5 3 14.65 14.52 0.55 o 2 5 3 4.54 5.15 0.40 o 3 5 3 14.22 11.59 1.07 o 4 5 3 30.71 29.47 1.21 o 5 5 3 5.61 7.93 0.51 o 6 5 3 37.67 40.55 1.67 o 7 5 3 99.57 97.49 4.41 o 8 5 3 9.28 10.05 0.61 o 9 5 3 0.58 1.49 0.37 o 10 5 3 16.33 17.18 0.90 o 11 5 3 3.99 4.13 0.42 o 12 5 3 0.63 0.32 0.42 o 13 5 3 3.30 3.02 0.58 o 14 5 3 2.35 2.21 0.55 o 1 6 3 26.87 28.60 1.46 o 2 6 3 5.24 4.41 0.82 o 3 6 3 59.28 60.95 1.99 o 4 6 3 28.40 28.83 1.11 o 5 6 3 2.65 4.19 0.68 o 6 6 3 5.20 7.86 0.82 o 7 6 3 32.06 36.52 1.76 o 8 6 3 3.32 5.58 0.82 o 0 0 4 9.58 12.27 0.79 o 2 0 4 39.86 39.88 2.77 o 4 0 4 206.43 226.26 18.44 o 6 0 4 216.31 200.47 2.78 o 8 0 4 183.30 175.79 4.87 o 10 0 4 209.70 212.48 6.54 o 12 0 4 70.24 69.56 3.60 o 14 0 4 54.22 56.72 5.25 o 16 0 4 25.69 26.02 3.05 o 18 0 4 11.16 11.70 1.54 o 20 0 4 19.53 21.09 4.21 o 1 1 4 13.47 14.42 0.44 o 2 1 4 7.01 8.73 0.44 o 3 1 4 1.58 1.56 0.20 o 4 1 4 46.06 47.16 2.05 o 5 1 4 35.32 31.96 0.65 o 6 1 4 2.89 2.40 0.22 o 7 1 4 15.09 15.45 0.49 o 8 1 4 34.55 32.93 0.68 o 9 1 4 16.95 17.38 0.61 o 10 1 4 75.88 71.41 2.98 o 11 1 4 2.34 2.82 0.30 o 12 1 4 8.66 7.61 0.86 o 13 1 4 1.82 1.95 0.29 o 14 1 4 6.23 6.80 0.63 o 15 1 4 1.69 2.14 0.33 o 16 1 4 8.10 8.92 0.67 o 17 1 4 10.49 12.68 1.09 o 18 1 4 0.92 1.41 0.37 o 19 1 4 0.53 0.70 0.45 o 0 2 4 32.29 31.71 1.26 o 1 2 4 6.36 6.84 0.42 o 2 2 4 19.79 19.31 0.71 o 3 2 4 3.21 3.34 0.29 o 4 2 4 37.20 33.30 1.03 o 5 2 4 8.13 8.04 0.39 o 6 2 4 19.14 19.88 0.83 o 7 2 4 121.22 116.74 5.65 o 8 2 4 14.17 16.16 0.68 o 9 2 4 13.34 15.19 0.82 o 10 2 4 35.76 36.19 1.83 o 11 2 4 16.85 15.18 0.63 o 12 2 4 71.50 68.32 2.94 o 13 2 4 17.61 18.50 0.71 o 14 2 4 14.34 17.57 1.24 o 15 2 4 8.61 9.45 0.77 o 16 2 4 1.47 1.46 0.38 o 17 2 4 9.05 9.89 0.83 o 18 2 4 0.78 0.46 0.42 o 1 3 4 38.43 38.70 1.82 o 2 3 4 19.77 19.03 0.61 o 3 3 4 20.61 20.57 0.63 o 4 3 4 60.48 57.72 1.64 o 5 3 4 14.55 14.87 0.64 o 6 3 4 62.73 63.27 3.16 o 7 3 4 17.47 17.19 1.59 o 8 3 4 30.08 27.78 1.39 o 9 3 4 42.67 38.19 1.91 o 10 3 4 2.07 2.05 0.37 o 11 3 4 73.77 70.36 4.16 o 12 3 4 4.71 6.46 0.59 o 13 3 4 52.38 47.01 4.32 o 14 3 4 40.90 36.87 2.33 o 15 3 4 11.87 12.05 0.80 o 16 3 4 10.85 13.17 1.23 o 0 4 4 19.88 19.32 1.05 o 1 4 4 1.31 1.27 0.40 o 2 4 4 1.31 1.64 0.35 o 3 4 4 20.93 21.64 0.84 o 4 4 4 5.27 5.63 0.45 o 5 4 4 35.60 37.64 1.12 o 6 4 4 3.95 3.67 0.42 o 7 4 4 36.84 39.59 1.84 o 8 4 4 8.38 9.42 0.62 o 9 4 4 11.03 13.37 0.85 o 10 4 4 0.34 0.85 0.37 o 11 4 4 2.57 3.71 0.47 o 12 4 4 4.97 5.07 0.52 o 13 4 4 5.97 5.09 0.58 o 1 5 4 1.21 2.14 0.50 o 2 5 4 21.63 25.26 0.97 o 3 5 4 30.50 34.30 1.02 o 4 5 4 10.72 13.85 0.86 o 5 5 4 3.45 2.94 0.48 o 6 5 4 1.94 1.86 0.44 o 7 5 4 3.85 5.01 0.52 o 2 0 5 5.87 6.07 0.64 o 4 0 5 15.43 15.40 0.93 o 6 0 5 120.42 124.46 5.00 o 8 0 5 54.68 58.38 1.86 o 10 0 5 18.69 20.50 1.06 o 12 0 5 0.40 0.43 0.42 o 14 0 5 0.42 0.29 0.45 o 0 1 5 2.82 2.69 0.44 o 1 1 5 13.22 12.98 0.52 o 2 1 5 0.92 1.37 0.32 o 3 1 5 19.40 18.54 0.63 o 4 1 5 42.95 41.28 0.81 o 5 1 5 9.81 12.79 0.55 o 6 1 5 41.53 41.08 0.86 o 7 1 5 41.69 41.91 1.37 o 8 1 5 15.86 16.04 0.62 o 9 1 5 3.56 5.08 0.44 o 10 1 5 28.19 29.60 1.35 o 11 1 5 3.60 4.46 0.36 o 12 1 5 13.59 17.82 0.77 o 13 1 5 0.72 1.31 0.32 o 1 2 5 1.24 1.40 0.31 o 2 2 5 17.10 17.59 0.71 o 3 2 5 15.34 15.50 0.66 o 4 2 5 30.30 29.48 1.06 o 5 2 5 1.69 2.30 0.36 o 6 2 5 5.46 4.97 0.43 o 7 2 5 9.52 11.75 0.56 o 8 2 5 11.90 10.91 0.97 o 9 2 5 13.62 12.20 1.54 o 10 2 5 42.59 48.33 1.15 o 11 2 5 26.69 30.60 1.06 o 12 2 5 6.99 8.01 0.60 o 0 3 5 4.90 4.70 0.95 o 1 3 5 6.65 6.82 0.53 o 2 3 5 1.24 1.43 0.57 o 3 3 5 1.40 1.00 0.37 o 4 3 5 3.94 3.54 0.44 o 5 3 5 2.32 3.48 0.46 o 6 3 5 4.78 4.03 0.44 o 7 3 5 25.44 27.83 1.20 o 8 3 5 8.35 9.32 0.61 o