#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:33:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181253 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/31/2233151.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233151_Fobs loop_ _publ_author_name 'Brzezinski, Krzysztof' 'Lazny, Ryszard' 'Sienkiewicz, Michal' 'Wojtulewski, S\/lawomir' 'Dauter, Zbigniew' _publ_section_title ; (2R)-8-Benzyl-2-[(S)-hydroxy(phenyl)methyl]-8-azabicyclo[3.2.1]octan-3-one ; _journal_coeditor_code GK2429 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o149 _journal_page_last o150 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.9354 _cell_length_b 13.3091 _cell_length_c 22.1511 _exptl_crystal_F_000 688.00 _reflns_d_resolution_high 0.8035 _cod_data_source_file gk2429Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ms_N-Bn_aldol2 in P212121 19' _shelx_refln_list_code 4 _shelx_f_calc_maximum 119.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 534.49 473.56 2.53 o 4 0 0 3740.95 3609.03 17.97 o 1 1 0 4634.04 4258.81 5.06 o 2 1 0 2306.52 2205.80 5.06 o 3 1 0 51.71 53.11 0.93 o 4 1 0 142.23 156.12 2.26 o 5 1 0 564.13 575.64 9.45 o 0 2 0 1947.01 1877.59 4.53 o 1 2 0 664.62 584.56 2.00 o 2 2 0 1203.32 1230.87 3.46 o 3 2 0 1553.80 1529.81 5.32 o 4 2 0 0.99 0.93 0.40 o 5 2 0 0.10 0.40 0.93 o 1 3 0 878.77 793.25 2.53 o 2 3 0 958.61 989.44 3.59 o 3 3 0 1043.25 1089.39 4.79 o 4 3 0 8.98 14.37 0.80 o 5 3 0 185.30 192.86 4.53 o 6 3 0 46.98 50.71 4.79 o 0 4 0 3407.39 3503.49 9.45 o 1 4 0 7065.39 6900.24 11.31 o 2 4 0 195.82 188.46 1.73 o 3 4 0 874.90 978.12 4.92 o 4 4 0 640.88 635.13 4.53 o 5 4 0 9.89 7.45 1.20 o 6 4 0 76.09 71.61 3.86 o 1 5 0 491.45 493.79 2.66 o 2 5 0 17.36 14.37 0.53 o 3 5 0 143.55 171.16 2.26 o 4 5 0 31.61 24.49 1.06 o 5 5 0 25.98 23.82 1.86 o 6 5 0 25.83 23.29 1.86 o 0 6 0 10967.36 11642.85 20.23 o 1 6 0 0.09 1.46 0.27 o 2 6 0 332.50 317.30 2.80 o 3 6 0 351.59 333.27 3.46 o 4 6 0 15.45 10.38 0.80 o 5 6 0 14.53 11.45 1.46 o 6 6 0 130.71 121.52 3.86 o 1 7 0 3673.62 3965.60 13.44 o 2 7 0 2.92 4.26 0.53 o 3 7 0 114.76 107.94 1.60 o 4 7 0 365.80 364.95 5.32 o 5 7 0 1622.59 1561.48 11.58 o 6 7 0 19.61 26.49 1.86 o 0 8 0 908.16 967.74 5.99 o 1 8 0 2.26 1.33 0.40 o 2 8 0 404.98 411.40 3.99 o 3 8 0 809.26 791.39 4.26 o 4 8 0 750.63 732.16 7.05 o 5 8 0 34.07 30.61 1.86 o 6 8 0 12.26 23.03 2.53 o 1 9 0 2.98 5.99 0.67 o 2 9 0 60.80 70.14 1.20 o 3 9 0 11.01 8.39 0.67 o 4 9 0 19.04 19.17 1.33 o 5 9 0 63.51 72.01 2.66 o 6 9 0 14.78 14.11 1.06 o 0 10 0 237.76 266.86 3.86 o 1 10 0 281.18 280.43 2.53 o 2 10 0 21.87 29.01 0.93 o 3 10 0 1539.01 1566.67 8.12 o 4 10 0 9.86 10.25 1.20 o 5 10 0 46.08 42.59 1.60 o 1 11 0 37.84 43.12 1.20 o 2 11 0 45.41 36.60 1.46 o 3 11 0 25.93 23.42 1.06 o 4 11 0 0.18 0.00 0.80 o 5 11 0 0.42 0.13 0.80 o 0 12 0 21.73 26.62 1.73 o 1 12 0 142.35 156.12 2.40 o 2 12 0 3.00 2.80 0.67 o 3 12 0 13.07 12.38 1.06 o 4 12 0 18.32 18.23 1.46 o 5 12 0 246.87 256.88 3.86 o 1 13 0 8.49 2.13 0.67 o 2 13 0 30.02 32.08 1.33 o 3 13 0 0.07 0.27 0.67 o 4 13 0 1.18 0.27 0.67 o 0 14 0 418.81 323.42 5.46 o 1 14 0 8.07 8.65 0.80 o 2 14 0 28.84 25.82 1.06 o 3 14 0 0.60 -0.13 0.67 o 1 15 0 31.67 38.33 1.20 o 2 15 0 23.24 17.97 0.93 o 3 15 0 12.80 16.64 0.93 o 0 16 0 176.05 178.62 2.80 o 1 16 0 0.09 -0.13 0.40 o 1 0 1 782.72 722.05 2.00 o 2 0 1 1007.89 913.17 2.66 o 3 0 1 36.46 37.40 0.80 o 4 0 1 942.81 864.46 5.46 o 5 0 1 401.56 416.99 7.99 o -5 1 1 343.60 370.01 6.12 o -4 1 1 180.47 175.69 2.40 o -3 1 1 141.96 142.68 1.60 o -2 1 1 176.71 178.62 1.33 o -1 1 1 1874.75 1702.83 3.73 o 0 1 1 213.57 196.45 1.06 o 1 1 1 1865.53 1732.78 3.33 o 2 1 1 177.07 177.95 1.20 o 3 1 1 140.74 141.75 1.46 o 4 1 1 179.94 177.02 2.40 o 5 1 1 343.81 356.30 9.45 o -5 2 1 487.74 518.54 6.52 o -4 2 1 37.69 38.60 1.33 o -3 2 1 233.27 230.52 2.00 o -2 2 1 232.01 229.72 1.60 o -1 2 1 3044.19 2875.28 4.66 o 0 2 1 479.92 419.12 1.73 o 1 2 1 3038.64 2840.27 4.79 o 2 2 1 229.37 226.66 1.46 o 3 2 1 233.31 232.52 1.86 o 4 2 1 38.62 39.66 1.20 o 5 2 1 488.15 517.34 7.32 o -6 3 1 534.47 503.90 9.58 o -5 3 1 94.92 90.77 2.80 o -4 3 1 49.62 47.25 1.33 o -3 3 1 29.03 25.69 0.93 o -2 3 1 75.95 76.66 0.93 o -1 3 1 3809.55 3527.18 6.52 o 0 3 1 4351.44 4260.01 6.65 o 1 3 1 3800.06 3594.93 6.39 o 2 3 1 76.58 76.40 0.93 o 3 3 1 29.04 24.36 0.80 o 4 3 1 49.34 45.39 1.20 o 5 3 1 94.99 91.57 3.19 o 6 3 1 535.72 514.82 14.91 o -7 4 1 137.50 128.70 4.53 o -6 4 1 44.08 48.71 3.19 o -5 4 1 398.05 395.83 5.86 o -4 4 1 54.25 50.58 1.20 o -3 4 1 130.81 127.64 2.13 o -2 4 1 375.17 374.13 2.53 o -1 4 1 4549.84 4481.35 8.65 o 0 4 1 287.37 285.09 1.60 o 1 4 1 4545.18 4487.60 7.32 o 2 4 1 375.61 376.40 2.40 o 3 4 1 131.35 128.30 1.86 o 4 4 1 53.79 50.04 1.33 o 5 4 1 397.64 399.55 6.65 o 6 4 1 43.29 48.58 4.66 o -6 5 1 19.94 21.03 1.73 o -5 5 1 34.97 33.54 1.86 o -4 5 1 138.30 143.61 2.26 o -3 5 1 65.93 80.52 1.73 o -2 5 1 8.78 19.03 0.67 o -1 5 1 1463.73 1482.03 3.99 o 0 5 1 11.14 10.91 0.40 o 1 5 1 1468.95 1513.30 4.53 o 2 5 1 8.85 18.77 0.67 o 3 5 1 65.72 80.39 1.46 o 4 5 1 138.84 143.08 2.13 o 5 5 1 35.44 33.67 2.13 o 6 5 1 19.73 21.03 1.86 o -6 6 1 31.89 36.34 2.13 o -5 6 1 160.02 145.61 3.33 o -4 6 1 241.33 226.40 3.19 o -3 6 1 281.65 288.55 3.33 o -2 6 1 154.91 139.48 2.00 o -1 6 1 1026.83 1075.95 4.53 o 0 6 1 7.05 7.32 0.53 o 1 6 1 1031.41 1090.19 3.99 o 2 6 1 154.52 139.62 2.00 o 3 6 1 280.35 289.48 3.19 o 4 6 1 240.55 230.26 2.80 o 5 6 1 161.81 147.60 4.13 o 6 6 1 31.73 33.54 2.26 o -6 7 1 13.89 17.57 1.60 o -5 7 1 334.03 335.00 5.46 o -4 7 1 185.21 195.92 3.86 o -3 7 1 222.12 209.23 2.26 o -2 7 1 521.29 550.22 4.13 o -1 7 1 199.80 220.54 2.26 o 0 7 1 8.79 11.31 0.53 o 1 7 1 198.64 219.61 2.40 o 2 7 1 522.74 545.29 4.53 o 3 7 1 221.50 208.83 2.13 o 4 7 1 185.61 202.71 3.33 o 5 7 1 331.78 330.88 5.46 o 6 7 1 13.73 15.84 1.60 o -6 8 1 113.16 130.17 2.80 o -5 8 1 74.16 86.11 3.06 o -4 8 1 748.22 742.54 7.05 o -3 8 1 19.69 19.70 0.80 o -2 8 1 210.90 223.07 2.80 o -1 8 1 610.59 653.37 4.53 o 0 8 1 2859.60 2942.76 9.98 o 1 8 1 608.56 642.06 4.66 o 2 8 1 210.86 222.94 3.06 o 3 8 1 19.48 20.90 0.80 o 4 8 1 749.52 747.20 6.12 o 5 8 1 73.91 84.25 2.93 o 6 8 1 113.36 130.03 2.66 o -6 9 1 60.79 63.75 3.59 o -5 9 1 191.14 191.66 3.73 o -4 9 1 92.47 90.64 2.53 o -3 9 1 450.78 444.27 3.59 o -2 9 1 130.58 124.05 1.73 o -1 9 1 41.77 42.32 1.33 o 0 9 1 9.69 12.24 0.53 o 1 9 1 41.54 42.32 1.33 o 2 9 1 133.96 128.44 1.73 o 3 9 1 452.53 445.47 3.46 o 4 9 1 91.87 89.04 2.13 o 5 9 1 190.85 182.21 3.59 o 6 9 1 61.36 67.61 2.66 o -5 10 1 89.45 89.31 2.13 o -4 10 1 97.46 100.89 2.53 o -3 10 1 34.55 37.27 1.33 o -2 10 1 380.59 375.73 3.06 o -1 10 1 185.50 198.18 2.13 o 0 10 1 15.02 12.64 0.67 o 1 10 1 188.00 200.18 2.13 o 2 10 1 378.37 379.99 3.06 o 3 10 1 35.07 40.06 1.46 o 4 10 1 99.78 96.49 2.40 o 5 10 1 88.54 90.37 2.53 o -5 11 1 33.30 34.07 1.86 o -4 11 1 71.37 71.07 2.26 o -3 11 1 113.52 116.73 2.26 o -2 11 1 0.93 0.40 0.67 o -1 11 1 43.38 57.10 1.20 o 0 11 1 190.22 188.60 2.53 o 1 11 1 43.77 56.57 1.33 o 2 11 1 0.78 0.67 0.67 o 3 11 1 110.53 109.80 2.53 o 4 11 1 70.98 68.68 2.26 o 5 11 1 33.24 35.80 1.86 o -5 12 1 73.86 73.07 3.59 o -4 12 1 6.40 5.99 0.80 o -3 12 1 153.13 151.73 3.99 o -2 12 1 11.57 10.65 0.93 o -1 12 1 131.65 131.37 2.26 o 0 12 1 302.85 343.92 3.99 o 1 12 1 131.20 128.44 2.40 o 2 12 1 11.17 10.91 0.93 o 3 12 1 151.81 144.81 2.93 o 4 12 1 6.42 7.72 1.06 o 5 12 1 74.01 76.80 2.66 o -4 13 1 4.74 6.12 0.80 o -3 13 1 116.13 113.26 3.19 o -2 13 1 69.00 75.20 2.00 o -1 13 1 31.75 31.14 1.20 o 0 13 1 11.34 14.91 0.93 o 1 13 1 31.48 30.21 1.20 o 2 13 1 68.90 73.34 2.00 o 3 13 1 117.94 114.20 2.26 o 4 13 1 4.57 6.39 0.80 o -3 14 1 50.86 54.84 1.86 o -2 14 1 98.43 94.10 2.13 o -1 14 1 7.18 8.52 0.80 o 0 14 1 502.25 514.95 4.92 o 1 14 1 7.16 8.39 0.80 o 2 14 1 99.07 96.23 2.00 o 3 14 1 50.92 48.85 1.46 o -3 15 1 124.14 121.38 2.66 o -2 15 1 81.81 79.19 1.73 o -1 15 1 58.09 68.28 1.60 o 0 15 1 16.35 15.97 0.80 o 1 15 1 59.08 67.48 1.60 o 2 15 1 82.24 77.99 1.46 o 3 15 1 123.98 124.71 2.40 o -1 16 1 2.92 2.00 0.40 o 0 16 1 202.28 218.41 2.53 o 1 16 1 2.90 2.26 0.40 o 0 0 2 2952.62 2816.18 11.18 o 2 0 2 3.24 2.93 0.13 o 3 0 2 185.58 174.49 1.60 o 4 0 2 923.40 916.37 5.32 o 5 0 2 4695.97 5066.17 23.42 o -5 1 2 632.86 669.21 6.65 o -4 1 2 54.42 58.16 1.46 o -3 1 2 414.70 420.98 2.66 o -2 1 2 1454.67 1415.08 4.13 o -1 1 2 8835.92 8104.49 9.58 o 0 1 2 5891.83 5602.68 6.92 o 1 1 2 8846.97 8089.98 12.24 o 2 1 2 1447.38 1404.56 3.33 o 3 1 2 414.28 422.05 2.53 o 4 1 2 54.55 58.83 1.46 o 5 1 2 632.50 662.02 7.72 o -7 2 2 67.26 56.57 2.53 o -5 2 2 154.22 159.85 3.73 o -4 2 2 6.24 7.19 0.67 o -3 2 2 341.34 350.44 2.53 o -2 2 2 282.49 264.73 1.86 o -1 2 2 159.80 176.09 1.06 o 0 2 2 1818.64 1709.62 4.53 o 1 2 2 158.53 176.88 1.20 o 2 2 2 282.25 265.39 1.60 o 3 2 2 341.66 349.64 2.26 o 4 2 2 6.42 6.52 0.53 o 5 2 2 153.20 157.72 4.26 o -7 3 2 144.71 119.52 3.86 o -5 3 2 271.52 269.39 4.79 o -4 3 2 35.93 41.79 1.06 o -3 3 2 2153.59 2338.10 9.72 o -2 3 2 957.96 976.93 3.86 o -1 3 2 650.54 644.19 2.66 o 0 3 2 6989.34 6566.70 7.45 o 1 3 2 643.95 636.33 2.93 o 2 3 2 952.04 981.45 3.59 o 3 3 2 2157.40 2331.31 7.99 o 4 3 2 36.53 41.79 1.20 o 5 3 2 270.85 276.57 4.39 o 6 3 2 95.74 95.16 6.65 o -6 4 2 169.38 167.57 5.32 o -5 4 2 90.13 80.66 2.80 o -4 4 2 166.28 149.07 2.13 o -3 4 2 525.34 584.03 4.26 o -2 4 2 574.80 611.84 3.33 o -1 4 2 550.06 555.41 2.80 o 0 4 2 0.05 1.20 0.13 o 1 4 2 550.31 553.28 2.53 o 2 4 2 572.61 594.81 3.33 o 3 4 2 527.96 586.16 3.99 o 4 4 2 164.39 148.67 2.00 o 5 4 2 91.50 85.31 2.53 o 6 4 2 170.23 179.15 8.78 o -6 5 2 37.47 35.67 2.13 o -5 5 2 35.89 34.21 1.86 o -4 5 2 9.93 9.58 0.67 o -3 5 2 140.56 146.81 2.53 o -2 5 2 97.65 101.02 1.60 o -1 5 2 1059.95 1039.48 4.39 o 0 5 2 1.26 1.86 0.27 o 1 5 2 1059.89 1035.09 4.13 o 2 5 2 99.19 103.28 1.46 o 3 5 2 138.42 143.88 2.00 o 4 5 2 9.94 9.58 0.67 o 5 5 2 35.86 35.54 1.86 o 6 5 2 37.68 38.20 2.93 o -6 6 2 5.21 7.45 1.20 o -5 6 2 528.75 508.83 6.12 o -4 6 2 235.48 208.43 2.53 o -3 6 2 261.55 263.53 3.06 o -2 6 2 562.52 572.18 4.13 o -1 6 2 691.22 735.22 3.59 o 0 6 2 1426.36 1582.65 4.92 o 1 6 2 695.76 747.73 3.73 o 2 6 2 562.58 571.91 3.99 o 3 6 2 261.46 261.67 2.93 o 4 6 2 232.66 209.76 2.53 o 5 6 2 531.25 529.06 6.65 o 6 6 2 5.42 4.13 1.06 o -6 7 2 271.19 258.61 4.79 o -5 7 2 127.61 129.50 3.33 o -4 7 2 105.71 96.10 2.66 o -3 7 2 194.61 190.33 2.13 o -2 7 2 83.21 74.40 1.46 o -1 7 2 878.02 925.02 4.53 o 0 7 2 4872.67 5292.17 13.44 o 1 7 2 881.30 924.88 4.53 o 2 7 2 81.71 76.26 1.73 o 3 7 2 195.84 187.80 2.13 o 4 7 2 106.65 97.96 2.40 o 5 7 2 127.21 129.64 3.59 o 6 7 2 272.93 265.66 5.32 o -6 8 2 3.68 7.99 1.46 o -5 8 2 128.49 122.45 3.46 o -4 8 2 100.08 91.70 2.53 o -3 8 2 30.07 31.68 1.06 o -2 8 2 96.93 96.36 1.86 o -1 8 2 218.71 215.62 2.53 o 0 8 2 662.34 723.91 4.26 o 1 8 2 220.74 214.55 2.53 o 2 8 2 97.60 93.30 1.86 o 3 8 2 30.06 30.75 0.93 o 4 8 2 99.02 91.70 2.26 o 5 8 2 128.56 121.52 3.06 o 6 8 2 3.95 3.86 0.93 o -6 9 2 58.59 49.91 3.06 o -5 9 2 15.27 17.57 2.53 o -4 9 2 67.05 67.88 2.26 o -3 9 2 459.42 444.14 3.86 o -2 9 2 203.49 203.10 2.13 o -1 9 2 88.45 102.75 2.00 o 0 9 2 93.74 99.29 1.73 o 1 9 2 90.68 104.88 2.13 o 2 9 2 203.61 206.70 2.26 o 3 9 2 458.20 448.00 3.59 o 4 9 2 67.07 68.01 1.86 o 5 9 2 15.28 14.24 1.20 o 6 9 2 59.17 51.91 2.26 o -5 10 2 39.66 42.32 1.60 o -4 10 2 4.28 8.12 1.33 o -3 10 2 459.47 468.63 5.19 o -2 10 2 1152.40 1124.40 5.46 o -1 10 2 157.04 159.05 1.73 o 0 10 2 184.18 202.17 2.13 o 1 10 2 156.16 158.25 2.00 o 2 10 2 1152.53 1143.16 5.59 o 3 10 2 458.68 472.09 5.06 o 4 10 2 4.11 5.86 0.80 o 5 10 2 39.10 40.73 2.00 o -5 11 2 2.10 1.46 0.53 o -4 11 2 9.00 8.78 1.06 o -3 11 2 609.11 608.25 5.72 o -2 11 2 179.61 183.14 2.66 o -1 11 2 2.69 3.06 0.53 o 0 11 2 36.75 27.95 1.06 o 1 11 2 3.03 3.73 0.53 o 2 11 2 181.30 189.40 3.06 o 3 11 2 608.24 613.04 5.59 o 4 11 2 9.22 9.98 1.06 o 5 11 2 2.13 1.06 0.93 o -5 12 2 41.16 37.93 2.66 o -4 12 2 32.15 34.07 1.46 o -3 12 2 10.51 8.52 1.06 o -2 12 2 104.79 97.03 2.40 o -1 12 2 330.36 337.13 3.46 o 0 12 2 168.39 158.65 2.80 o 1 12 2 331.16 334.20 4.26 o 2 12 2 105.55 98.36 2.13 o 3 12 2 10.35 7.85 0.93 o 4 12 2 33.20 35.54 1.60 o 5 12 2 40.59 35.80 1.86 o -4 13 2 8.48 9.98 0.93 o -3 13 2 9.45 10.12 1.20 o -2 13 2 42.22 42.46 2.00 o -1 13 2 122.17 111.80 2.00 o 0 13 2 18.72 7.32 0.80 o 1 13 2 121.17 107.67 2.26 o 2 13 2 42.20 40.86 1.60 o 3 13 2 9.08 8.12 0.80 o 4 13 2 8.60 11.58 1.06 o -3 14 2 15.24 13.98 1.06 o -2 14 2 0.20 -0.27 0.53 o -1 14 2 73.71 57.10 1.60 o 0 14 2 24.23 28.75 1.20 o 1 14 2 73.65 56.57 1.60 o 2 14 2 0.22 -0.13 0.53 o 3 14 2 15.50 13.31 0.80 o -3 15 2 6.64 6.52 0.93 o -2 15 2 59.26 63.62 2.00 o -1 15 2 123.64 125.11 2.53 o 0 15 2 6.75 6.12 0.67 o 1 15 2 122.90 120.59 2.00 o 2 15 2 60.79 60.56 1.33 o 3 15 2 6.93 6.39 0.93 o -1 16 2 92.94 97.96 2.13 o 0 16 2 63.30 56.03 1.33 o 1 16 2 94.19 95.16 1.73 o 1 0 3 7795.44 7243.49 7.59 o 2 0 3 15.86 17.57 0.40 o 3 0 3 1481.95 1611.79 5.32 o 4 0 3 18.57 19.17 1.06 o 5 0 3 356.39 392.77 6.79 o -5 1 3 296.32 307.45 4.53 o -4 1 3 994.56 991.70 6.12 o -3 1 3 324.78 338.46 2.40 o -2 1 3 457.91 453.06 2.13 o -1 1 3 1956.77 1824.22 2.93 o 0 1 3 1408.14 1366.36 2.66 o 1 1 3 1948.50 1802.12 3.59 o 2 1 3 456.45 451.46 1.73 o 3 1 3 323.13 341.26 2.26 o 4 1 3 997.08 1005.28 5.99 o 5 1 3 297.31 311.44 5.46 o -5 2 3 232.58 239.84 4.53 o -4 2 3 127.18 114.20 2.00 o -3 2 3 845.20 898.80 4.53 o -2 2 3 3628.09 3601.85 7.59 o -1 2 3 946.26 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146.42 146.94 2.00 o 4 3 22 17.68 16.10 1.06 o -3 4 22 262.10 257.81 2.93 o -2 4 22 11.91 9.85 0.67 o -1 4 22 14.90 11.05 0.80 o 0 4 22 73.63 68.81 1.73 o 1 4 22 15.21 10.78 0.80 o 2 4 22 12.11 10.12 0.67 o 3 4 22 261.87 262.33 2.93 o -3 5 22 11.71 11.71 0.67 o -2 5 22 78.46 78.26 1.46 o -1 5 22 50.23 50.58 1.33 o 0 5 22 3.53 3.86 0.67 o 1 5 22 49.71 50.58 1.46 o 2 5 22 77.55 80.12 1.86 o 3 5 22 11.80 12.24 0.93 o -3 6 22 73.79 80.12 1.86 o -2 6 22 113.52 113.13 1.86 o -1 6 22 48.84 44.85 1.33 o 0 6 22 707.49 727.24 5.86 o 1 6 22 49.26 45.12 1.46 o 2 6 22 113.05 112.20 2.00 o 3 6 22 73.91 87.04 2.53 o -2 7 22 8.61 8.92 0.67 o -1 7 22 195.67 193.79 2.53 o 0 7 22 9.10 11.45 0.80 o 1 7 22 194.70 196.58 2.26 o 2 7 22 8.50 8.52 0.67 o -2 8 22 11.66 10.65 0.53 o -1 8 22 45.42 46.18 1.46 o 0 8 22 8.79 7.32 0.53 o 1 8 22 45.00 44.45 0.93 o 2 8 22 11.74 12.64 0.93 o -1 9 22 40.95 40.73 1.20 o 0 9 22 374.28 345.12 3.46 o 1 9 22 39.90 36.73 1.33 o 1 0 23 53.41 50.04 1.33 o 2 0 23 159.76 156.52 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