#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/31/2233196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233196_Fobs loop_ _publ_author_name 'Wang, Xiao-Dan' 'Hou, Guang-Feng' 'Yu, Ying-Hui' 'Gao, Jin-Sheng' _publ_section_title ; Bis[1,1'-(1,3-phenylenedimethylene)di(1H-imidazol-3-ium)] \b-octamolybdate ; _journal_coeditor_code HY2492 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m50 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.817 _cell_angle_gamma 90.000 _cell_length_a 12.1630 _cell_length_b 12.7853 _cell_length_c 14.9374 _exptl_crystal_F_000 1600.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file hy2492Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wxd92111 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2522.30 2353.72 26.03 o 3 0 0 20233.59 20370.01 193.13 o 4 0 0 23096.20 23198.21 265.03 o 5 0 0 22286.80 21537.15 386.53 o 6 0 0 2.51 23.78 21.40 o 7 0 0 54683.50 56029.20 868.27 o 8 0 0 16998.15 16326.39 264.14 o 9 0 0 5176.17 5176.09 73.48 o 10 0 0 10055.24 10240.90 265.83 o 11 0 0 22038.41 22695.93 522.11 o 12 0 0 14848.99 15331.38 276.46 o 13 0 0 2421.78 2357.11 174.71 o 15 0 0 438.02 720.06 135.23 o 2 1 0 2550.32 2390.64 66.21 o 3 1 0 4171.60 4294.52 65.72 o 4 1 0 5270.68 5457.67 42.42 o 5 1 0 45292.30 47926.89 478.75 o 6 1 0 11018.45 11224.79 94.05 o 7 1 0 0.85 19.83 13.17 o 8 1 0 723.12 739.89 25.20 o 9 1 0 2829.84 3245.41 56.09 o 10 1 0 2449.17 2754.08 62.81 o 11 1 0 2332.94 2277.30 48.08 o 12 1 0 1931.68 1943.51 75.72 o 13 1 0 338.48 300.21 29.36 o 14 1 0 1083.18 291.68 180.63 o 15 1 0 186.17 64.63 67.74 o 0 2 0 21046.09 20519.14 209.61 o 1 2 0 396.84 375.80 14.58 o 2 2 0 36445.60 37036.03 342.61 o 3 2 0 25957.60 25552.43 214.43 o 4 2 0 1245.35 1240.70 26.49 o 5 2 0 12994.59 13365.15 100.02 o 6 2 0 18515.14 19468.53 151.17 o 7 2 0 86.21 133.67 17.27 o 8 2 0 1320.34 1617.63 92.36 o 9 2 0 3496.59 3450.81 64.55 o 10 2 0 4385.81 4656.19 72.38 o 11 2 0 2141.54 2221.49 41.42 o 12 2 0 37.97 30.17 27.34 o 13 2 0 607.98 670.38 44.65 o 14 2 0 1.69 -177.67 177.67 o 15 2 0 562.88 630.51 95.46 o 1 3 0 15154.18 15728.54 208.63 o 2 3 0 32206.01 31896.14 344.53 o 3 3 0 17490.15 17162.23 146.08 o 4 3 0 15573.65 15297.53 142.21 o 5 3 0 7455.92 7186.68 153.49 o 6 3 0 15778.01 15906.57 162.37 o 7 3 0 30597.19 30642.75 398.97 o 8 3 0 17623.96 17855.39 270.00 o 9 3 0 4038.04 3882.78 70.07 o 10 3 0 1500.54 1611.90 53.14 o 11 3 0 176.40 199.08 28.60 o 12 3 0 1146.15 1259.71 51.56 o 13 3 0 1854.16 1840.79 53.73 o 14 3 0 10005.08 9605.78 194.76 o 15 3 0 6276.60 6225.42 273.91 o 0 4 0 39834.21 39594.80 629.03 o 1 4 0 6846.99 7238.88 67.52 o 2 4 0 37.47 46.19 20.58 o 3 4 0 116.78 87.49 15.70 o 4 4 0 10584.25 10085.91 93.75 o 5 4 0 808.56 777.27 22.13 o 6 4 0 7241.95 7499.65 71.75 o 7 4 0 9616.82 10097.57 162.76 o 8 4 0 15.95 -18.70 22.65 o 9 4 0 16.85 42.62 27.82 o 10 4 0 3505.94 3873.95 90.33 o 11 4 0 17537.17 17574.87 247.43 o 12 4 0 258.64 264.64 33.46 o 13 4 0 1028.94 1182.45 56.87 o 14 4 0 0.16 36.14 25.68 o 15 4 0 3312.21 3125.05 186.56 o 1 5 0 38566.48 38417.59 387.46 o 2 5 0 33526.35 34409.52 375.55 o 3 5 0 14084.59 13473.90 176.54 o 4 5 0 10049.46 9429.41 78.80 o 5 5 0 8370.36 8135.06 103.48 o 6 5 0 37577.00 38761.73 387.30 o 7 5 0 6520.71 6808.45 66.77 o 8 5 0 2252.23 2335.65 66.32 o 9 5 0 2344.26 2434.77 80.97 o 10 5 0 997.49 1141.39 44.74 o 11 5 0 888.53 852.93 58.48 o 12 5 0 265.37 265.76 57.41 o 13 5 0 195.57 176.25 31.80 o 14 5 0 44.66 29.63 30.91 o 0 6 0 119.68 212.45 35.29 o 1 6 0 3710.00 4060.95 45.31 o 2 6 0 4826.70 5183.99 204.20 o 3 6 0 82.65 65.26 13.87 o 4 6 0 780.10 804.72 33.80 o 5 6 0 81.69 106.01 15.13 o 6 6 0 611.53 664.07 27.96 o 7 6 0 377.65 444.14 34.61 o 8 6 0 2250.78 2331.76 42.60 o 9 6 0 776.88 897.33 59.41 o 10 6 0 1.97 5.83 30.93 o 11 6 0 36.68 72.83 35.05 o 12 6 0 152.90 90.79 49.82 o 13 6 0 558.73 558.06 57.09 o 14 6 0 91.98 86.01 52.14 o 1 7 0 9096.78 9109.73 99.30 o 2 7 0 164.96 154.40 13.46 o 3 7 0 62728.71 63648.78 858.87 o 4 7 0 71704.41 67216.93 2352.40 o 5 7 0 18953.65 18527.02 239.46 o 6 7 0 3139.72 3007.13 100.57 o 7 7 0 12150.48 12114.50 118.99 o 8 7 0 13838.77 14114.19 128.93 o 9 7 0 7409.34 7682.73 116.00 o 10 7 0 0.15 8.41 21.90 o 11 7 0 845.29 854.05 48.92 o 12 7 0 1423.48 1408.37 62.31 o 13 7 0 1123.84 1243.99 60.06 o 14 7 0 1663.52 1576.24 77.03 o 0 8 0 1281.02 1478.94 51.58 o 1 8 0 11290.22 11523.48 136.16 o 2 8 0 6094.29 5387.70 358.01 o 3 8 0 782.81 787.19 37.88 o 4 8 0 3431.30 3416.27 70.38 o 5 8 0 16.89 -5.25 50.17 o 6 8 0 2607.22 2510.03 91.55 o 7 8 0 316.48 353.47 17.66 o 8 8 0 13861.10 14027.17 127.55 o 9 8 0 4391.69 4497.58 62.78 o 10 8 0 9.35 87.72 27.42 o 11 8 0 1025.81 1144.97 52.01 o 12 8 0 973.66 991.07 57.62 o 13 8 0 4707.22 4176.53 230.74 o 1 9 0 1520.98 1638.90 56.35 o 2 9 0 1.42 5.10 10.86 o 3 9 0 2964.54 3001.06 70.42 o 4 9 0 38.73 41.97 27.72 o 5 9 0 1288.80 1320.96 40.62 o 6 9 0 126.43 100.32 35.27 o 7 9 0 1629.93 1321.57 118.33 o 8 9 0 968.90 920.21 33.91 o 9 9 0 1648.90 1642.26 75.78 o 10 9 0 1638.54 1560.82 46.46 o 11 9 0 246.85 231.73 54.79 o 12 9 0 1033.01 1112.59 115.24 o 13 9 0 9.87 87.19 83.58 o 0 10 0 35.33 46.40 18.14 o 1 10 0 9197.63 9408.55 123.24 o 2 10 0 27860.56 28090.19 350.97 o 3 10 0 18257.93 18403.79 245.37 o 4 10 0 154.40 149.03 25.19 o 5 10 0 3434.37 3579.34 78.45 o 6 10 0 2283.67 2314.27 64.15 o 7 10 0 23.57 15.79 24.33 o 8 10 0 833.23 853.21 58.35 o 9 10 0 3736.78 3638.50 150.68 o 10 10 0 7158.67 6787.91 194.02 o 11 10 0 4807.43 4808.79 149.50 o 12 10 0 1738.12 1730.67 115.10 o 1 11 0 1165.51 1253.86 109.20 o 2 11 0 465.43 373.06 74.08 o 3 11 0 154.04 200.69 31.51 o 4 11 0 1109.47 1197.62 41.67 o 5 11 0 3.95 46.14 23.88 o 6 11 0 339.29 297.54 29.28 o 7 11 0 0.41 -16.05 22.81 o 8 11 0 338.70 388.37 41.46 o 9 11 0 8.48 24.24 19.76 o 10 11 0 8.68 122.00 54.29 o 11 11 0 47.24 121.40 57.40 o 0 12 0 4263.19 4311.74 66.81 o 1 12 0 355.05 335.47 38.58 o 2 12 0 9188.21 9357.44 125.03 o 3 12 0 7503.21 7206.86 251.92 o 4 12 0 952.83 1080.62 71.54 o 5 12 0 3782.32 3739.19 74.69 o 6 12 0 27.53 0.02 36.83 o 7 12 0 1389.16 1531.48 60.75 o 8 12 0 73.26 147.58 26.90 o 9 12 0 1128.75 1224.87 74.78 o 10 12 0 574.49 537.03 95.78 o 1 13 0 421.66 367.99 58.99 o 2 13 0 386.14 398.99 29.67 o 3 13 0 88.57 82.92 27.71 o 4 13 0 1745.96 1773.38 95.26 o 5 13 0 3810.88 3732.00 71.39 o 6 13 0 876.04 1003.94 39.57 o 7 13 0 390.41 372.19 30.78 o 8 13 0 239.79 172.10 36.18 o 9 13 0 930.39 1240.28 211.97 o 0 14 0 3026.11 3122.54 125.60 o 1 14 0 3182.05 3337.19 110.94 o 2 14 0 1333.60 1449.96 84.41 o 3 14 0 312.37 337.37 44.89 o 4 14 0 13.23 28.67 43.81 o 5 14 0 4.63 42.79 35.94 o 6 14 0 93.68 72.97 31.05 o 7 14 0 81.64 156.16 33.30 o 8 14 0 1506.06 1497.94 123.40 o 1 15 0 224.46 261.77 45.62 o 2 15 0 0.11 -39.18 43.58 o 3 15 0 786.09 786.80 66.04 o 4 15 0 2300.92 2300.26 105.86 o 5 15 0 1676.73 1426.01 75.37 o 6 15 0 79.01 85.21 41.49 o 0 16 0 232.42 280.99 87.03 o 1 16 0 19.30 29.26 50.04 o 2 16 0 1181.05 1197.00 82.15 o 3 16 0 118.25 148.86 48.64 o 4 16 0 245.65 242.38 49.13 o -14 1 1 147.57 181.13 96.24 o -13 1 1 2054.02 2062.01 53.13 o -12 1 1 11580.29 12023.39 105.46 o -11 1 1 14943.53 14940.66 138.68 o -10 1 1 124.34 99.44 18.90 o -9 1 1 7163.26 7209.46 76.70 o -8 1 1 6.95 21.78 10.57 o -7 1 1 15638.14 15572.54 154.70 o -6 1 1 206.60 191.38 12.68 o -5 1 1 30308.69 28824.72 318.02 o -4 1 1 105145.75 103555.08 1276.08 o -3 1 1 31405.26 32059.28 253.93 o -2 1 1 12472.37 12758.23 81.62 o 2 1 1 632.18 601.80 54.66 o 3 1 1 6183.45 6449.24 87.04 o 4 1 1 65.90 100.94 20.94 o 5 1 1 10251.12 10679.55 163.95 o 6 1 1 4178.04 4053.05 71.05 o 7 1 1 24517.73 25131.14 218.87 o 8 1 1 19941.03 20986.62 292.56 o 9 1 1 5280.20 5693.41 115.62 o 10 1 1 1321.60 1415.38 33.45 o 11 1 1 310.91 327.92 63.25 o 12 1 1 6.58 9.25 24.33 o 13 1 1 94.11 116.84 21.61 o 14 1 1 153.06 272.47 75.34 o 15 1 1 28.99 -27.47 78.49 o -15 2 1 2340.44 2290.48 179.65 o -14 2 1 6580.79 6361.63 264.04 o -13 2 1 755.78 842.83 70.34 o -12 2 1 1968.30 1962.61 43.38 o -11 2 1 1002.96 1028.82 45.33 o -10 2 1 3625.88 3693.93 50.54 o -9 2 1 1545.74 1588.99 40.94 o -8 2 1 3806.27 3903.61 64.14 o -7 2 1 3219.55 3286.30 32.60 o -6 2 1 22.01 41.20 11.75 o -5 2 1 0.43 18.25 11.40 o -4 2 1 25073.04 24586.39 189.93 o -3 2 1 15084.48 15315.29 112.14 o -2 2 1 995.84 1046.87 36.20 o -1 2 1 1964.40 1867.79 29.22 o 0 2 1 9398.46 9559.39 102.10 o 1 2 1 31044.58 30997.99 276.96 o 2 2 1 4022.54 3948.87 88.58 o 3 2 1 42722.29 39874.61 576.48 o 4 2 1 6091.39 5971.56 67.24 o 5 2 1 1834.22 1795.67 61.71 o 6 2 1 1979.22 2118.76 38.10 o 7 2 1 19663.62 19208.29 198.57 o 8 2 1 14862.36 14927.19 160.16 o 9 2 1 3232.29 3400.44 85.48 o 10 2 1 7386.31 7755.96 95.66 o 11 2 1 29.69 58.94 26.75 o 12 2 1 3040.08 2917.79 65.81 o 13 2 1 0.03 -11.21 19.23 o 14 2 1 4374.20 4347.30 171.93 o 15 2 1 1757.91 1700.15 498.71 o -15 3 1 6186.55 5817.76 263.05 o -14 3 1 1145.37 982.98 125.02 o -13 3 1 92.21 86.54 37.06 o -12 3 1 873.86 841.78 59.48 o -11 3 1 5808.88 5983.35 137.69 o -10 3 1 2965.03 2969.98 112.00 o -9 3 1 364.52 392.04 15.52 o -8 3 1 6636.31 7191.55 127.44 o -7 3 1 1654.03 1629.86 30.78 o -6 3 1 7121.66 7404.99 122.70 o -5 3 1 9945.50 9599.37 74.56 o -4 3 1 5850.30 5514.48 47.51 o -3 3 1 3644.41 3476.16 32.83 o -2 3 1 20883.34 20972.46 210.10 o -1 3 1 37400.54 37839.75 454.61 o 0 3 1 43591.79 43835.93 516.25 o 1 3 1 5014.62 4861.12 52.28 o 2 3 1 18005.47 18008.25 157.82 o 3 3 1 721.08 709.31 21.28 o 4 3 1 4846.47 4820.68 66.68 o 5 3 1 6433.51 6281.09 122.88 o 6 3 1 53462.84 50692.53 1881.98 o 7 3 1 17829.25 17867.05 192.74 o 8 3 1 1909.29 1983.82 47.89 o 9 3 1 0.63 7.48 20.77 o 10 3 1 8873.37 9365.77 127.57 o 11 3 1 12154.34 12553.00 188.56 o 12 3 1 331.17 524.52 54.18 o 13 3 1 3755.00 3807.69 107.81 o 14 3 1 714.38 856.34 240.35 o 15 3 1 196.07 224.56 176.68 o -15 4 1 160.54 264.04 90.81 o -14 4 1 647.60 528.25 61.12 o -13 4 1 753.68 698.55 69.81 o -12 4 1 487.69 567.00 91.16 o -11 4 1 9995.70 10426.35 147.88 o -10 4 1 8665.25 8804.66 124.66 o -9 4 1 4568.39 5133.48 202.03 o -8 4 1 4114.26 4029.59 192.54 o -7 4 1 18055.98 18172.74 155.56 o -6 4 1 29666.71 29785.83 286.90 o -5 4 1 32046.24 32498.25 312.53 o -4 4 1 2506.61 2554.95 31.92 o -3 4 1 9710.49 9655.45 124.45 o -2 4 1 6314.63 6341.40 77.53 o -1 4 1 4406.11 4696.89 59.87 o 0 4 1 2827.56 2774.79 31.53 o 1 4 1 48981.11 47792.20 658.56 o 2 4 1 91698.52 92459.79 1417.44 o 3 4 1 32401.61 31544.14 313.69 o 4 4 1 6438.53 6445.94 100.40 o 5 4 1 2200.04 2362.56 61.72 o 6 4 1 4798.78 5086.08 65.55 o 7 4 1 10625.98 11041.07 130.27 o 8 4 1 237.87 301.67 32.09 o 9 4 1 3790.76 3838.02 63.11 o 10 4 1 7449.43 7713.36 158.59 o 11 4 1 4023.21 3953.30 110.65 o 12 4 1 1267.37 1273.42 48.99 o 13 4 1 1623.73 1676.56 77.44 o 14 4 1 4209.69 4238.43 86.93 o 15 4 1 4490.58 4078.06 347.45 o -15 5 1 399.97 285.26 90.32 o -14 5 1 93.18 83.87 42.19 o -13 5 1 723.79 839.28 59.77 o -12 5 1 67.63 11.39 23.81 o -11 5 1 3067.50 3117.15 78.67 o -10 5 1 2718.93 2904.36 67.59 o -9 5 1 106.46 180.97 24.27 o -8 5 1 1382.29 1504.55 34.51 o -7 5 1 4708.24 4723.11 46.36 o -6 5 1 2691.15 2697.16 56.39 o -5 5 1 819.18 853.65 25.35 o -4 5 1 1185.89 1215.09 34.51 o -3 5 1 64.11 88.72 18.54 o -2 5 1 3221.46 3296.79 52.96 o -1 5 1 1373.91 1301.86 36.99 o 0 5 1 11804.43 11700.24 91.73 o 1 5 1 81.22 50.51 16.55 o 2 5 1 3873.10 4300.82 55.18 o 3 5 1 1994.56 1914.17 49.15 o 4 5 1 17767.31 17820.68 166.02 o 5 5 1 885.13 835.70 26.73 o 6 5 1 1122.54 1032.91 23.46 o 7 5 1 3895.96 4098.20 70.19 o 8 5 1 12.30 3.35 20.25 o 9 5 1 360.52 367.94 30.98 o 10 5 1 2614.58 2755.33 68.25 o 11 5 1 3298.30 3272.44 95.69 o 12 5 1 926.46 847.88 52.43 o 13 5 1 43.62 51.84 48.80 o 14 5 1 91.74 154.29 34.41 o -14 6 1 313.20 246.77 44.26 o -13 6 1 2577.03 2591.98 63.31 o -12 6 1 3516.18 3493.00 96.55 o -11 6 1 219.63 245.43 40.72 o -10 6 1 669.11 728.37 168.07 o -9 6 1 4577.19 4730.09 53.40 o -8 6 1 33050.54 33177.34 385.01 o -7 6 1 26530.46 26248.06 289.37 o -6 6 1 1426.02 1587.82 34.99 o -5 6 1 1392.22 1374.77 26.56 o -4 6 1 23222.70 23833.75 248.57 o -3 6 1 24445.71 24056.38 231.21 o -2 6 1 12744.54 13105.95 175.82 o -1 6 1 61094.61 59877.01 886.75 o 0 6 1 19977.07 19477.45 158.43 o 1 6 1 7213.10 8038.74 79.70 o 2 6 1 2091.03 2286.79 45.16 o 3 6 1 21542.07 20083.42 229.30 o 4 6 1 54995.23 54629.08 641.26 o 5 6 1 6947.25 6945.82 81.48 o 6 6 1 343.39 348.11 17.02 o 7 6 1 123.71 138.54 14.79 o 8 6 1 209.76 261.60 28.60 o 9 6 1 1196.33 1241.18 60.69 o 10 6 1 1538.96 1461.28 79.57 o 11 6 1 1176.77 1332.94 47.23 o 12 6 1 1212.51 1198.22 62.00 o 13 6 1 3561.20 3635.70 79.10 o 14 6 1 2350.24 2260.29 82.60 o -14 7 1 598.99 431.15 46.11 o -13 7 1 4774.16 4507.71 109.67 o -12 7 1 1858.40 1832.01 91.67 o -11 7 1 114.11 142.59 27.96 o -10 7 1 104.72 104.41 40.96 o -9 7 1 1840.20 1935.37 39.57 o -8 7 1 1121.84 1260.41 39.52 o -7 7 1 771.08 812.49 41.89 o -6 7 1 2713.86 2512.05 53.00 o -5 7 1 614.09 664.96 45.74 o -4 7 1 1850.00 1775.42 108.63 o -3 7 1 14016.87 13608.17 153.24 o -2 7 1 9541.94 9347.46 152.07 o -1 7 1 0.79 13.74 20.77 o 0 7 1 314.22 381.82 21.95 o 1 7 1 3441.42 3391.70 48.78 o 2 7 1 6004.64 5927.11 75.42 o 3 7 1 130.89 119.17 18.88 o 4 7 1 25330.79 25024.61 248.59 o 5 7 1 2610.24 2549.58 47.86 o 6 7 1 494.63 559.97 31.79 o 7 7 1 579.99 696.92 47.20 o 8 7 1 10391.45 10195.99 120.67 o 9 7 1 7395.99 7624.13 105.56 o 10 7 1 289.19 293.44 37.91 o 11 7 1 1150.91 1238.22 116.31 o 12 7 1 151.54 135.30 46.12 o 13 7 1 1465.36 1382.56 87.64 o 14 7 1 5.99 -1.56 78.04 o -13 8 1 465.06 762.57 265.82 o -12 8 1 97.58 38.98 30.12 o -11 8 1 279.82 266.15 32.49 o -10 8 1 322.74 297.37 16.04 o -9 8 1 2716.82 2620.14 98.12 o -8 8 1 6397.19 6389.95 81.34 o -7 8 1 6638.49 6700.31 120.72 o -6 8 1 2726.22 2847.85 166.04 o -5 8 1 1290.24 1261.58 45.04 o -4 8 1 5575.17 5742.40 85.47 o -3 8 1 1819.21 1903.84 60.69 o -2 8 1 155.80 125.28 28.14 o -1 8 1 4096.18 4525.16 80.01 o 0 8 1 8849.23 9362.05 95.76 o 1 8 1 692.27 723.86 22.73 o 2 8 1 834.48 787.67 18.80 o 3 8 1 0.71 3.50 8.96 o 4 8 1 18177.43 17906.82 170.95 o 5 8 1 20997.55 20995.46 241.52 o 6 8 1 3184.29 3298.53 50.04 o 7 8 1 536.87 567.62 33.00 o 8 8 1 4.56 22.63 14.24 o 9 8 1 1164.45 1393.99 55.44 o 10 8 1 803.40 947.23 52.05 o 11 8 1 610.86 513.76 42.02 o 12 8 1 3832.53 3794.27 118.48 o 13 8 1 1771.62 1827.60 70.71 o -13 9 1 286.48 104.49 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