#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/32/2233228.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233228_Fobs loop_ _publ_author_name 'Al-Adiwish, Wedad M.' 'Adan, D.' 'Mohamed Tahir, Mohamed Ibrahim' 'Yaacob, W.A.' 'Kassim, Mohammad B.' _publ_section_title ; 3-Amino-5-(piperidin-1-yl)thiophene-2,4-dicarbonitrile ; _journal_coeditor_code KP2376 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o138 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.131 _cell_angle_gamma 90.000 _cell_length_a 14.1637 _cell_length_b 11.2823 _cell_length_c 14.4413 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.8146 _[local]_cod_data_source_file kp2376Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1186_wedad58_c2c in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 370.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1299.95 1337.43 20.28 o 4 0 0 5764.24 6206.06 79.03 o 6 0 0 20248.29 19570.14 120.12 o 8 0 0 895.29 873.04 18.28 o 10 0 0 1544.93 1327.09 27.91 o 12 0 0 3959.31 3536.84 39.54 o 14 0 0 498.75 519.26 37.72 o 16 0 0 13.21 10.52 8.76 o 1 1 0 19307.59 16878.57 269.97 o 3 1 0 5703.93 5632.92 32.43 o 5 1 0 1681.80 1862.86 9.37 o 7 1 0 3861.86 4405.73 27.69 o 9 1 0 11.68 13.00 2.70 o 11 1 0 1224.67 1006.30 18.24 o 13 1 0 1810.68 1691.32 30.48 o 15 1 0 295.59 263.91 13.14 o 17 1 0 438.81 465.22 17.67 o 0 2 0 2499.74 2524.86 22.82 o 2 2 0 9268.68 9009.53 57.92 o 4 2 0 1107.16 1285.86 7.38 o 6 2 0 87.22 98.68 3.55 o 8 2 0 1057.81 1104.74 15.64 o 10 2 0 1.90 0.68 2.74 o 12 2 0 389.58 363.36 8.68 o 14 2 0 28.10 17.64 5.50 o 16 2 0 28.97 16.55 8.24 o 1 3 0 137359.33 127669.09 1055.96 o 3 3 0 1352.75 1529.57 9.29 o 5 3 0 9090.39 10052.34 69.55 o 7 3 0 2132.89 2040.81 16.18 o 9 3 0 1296.68 1122.50 17.49 o 11 3 0 2531.63 2317.21 27.58 o 13 3 0 62.00 57.54 6.11 o 15 3 0 74.95 67.93 8.06 o 0 4 0 32447.23 33306.96 291.96 o 2 4 0 5543.81 6210.49 36.40 o 4 4 0 1055.83 1023.20 10.51 o 6 4 0 6468.91 7407.88 46.18 o 8 4 0 905.70 956.46 14.64 o 10 4 0 879.11 786.13 16.99 o 12 4 0 2670.54 2336.21 33.54 o 14 4 0 158.69 141.74 9.93 o 16 4 0 883.64 933.40 20.92 o 1 5 0 2335.69 2697.61 22.75 o 3 5 0 1253.80 1431.42 15.33 o 5 5 0 4181.38 4655.48 28.81 o 7 5 0 538.57 523.97 10.38 o 9 5 0 62.82 48.49 6.16 o 11 5 0 8.27 12.48 3.68 o 13 5 0 108.69 80.36 7.65 o 15 5 0 73.08 79.66 7.75 o 0 6 0 8170.74 8999.57 186.94 o 2 6 0 11412.60 12096.68 69.22 o 4 6 0 2476.05 2726.29 26.21 o 6 6 0 63.84 81.23 5.70 o 8 6 0 1377.01 1291.83 18.87 o 10 6 0 1580.89 1424.70 21.27 o 12 6 0 7.80 7.89 4.54 o 14 6 0 0.16 4.78 4.21 o 1 7 0 2561.09 2859.86 29.19 o 3 7 0 5105.82 5070.87 44.77 o 5 7 0 345.72 365.65 13.31 o 7 7 0 1428.95 1464.60 21.77 o 9 7 0 1777.11 1771.69 24.79 o 11 7 0 946.25 850.41 21.87 o 13 7 0 331.00 330.11 11.95 o 0 8 0 803.22 873.43 25.33 o 2 8 0 3036.20 3064.04 47.68 o 4 8 0 3600.08 3653.22 47.14 o 6 8 0 217.34 218.20 10.23 o 8 8 0 128.36 123.51 11.37 o 10 8 0 463.55 463.16 21.56 o 12 8 0 8.95 7.15 5.85 o 14 8 0 100.51 85.90 11.40 o 1 9 0 327.82 307.10 14.16 o 3 9 0 75.93 74.66 7.17 o 5 9 0 500.86 461.98 12.10 o 7 9 0 5.40 0.74 2.78 o 9 9 0 477.34 416.71 19.89 o 11 9 0 176.42 177.43 14.88 o 0 10 0 595.82 512.02 19.36 o 2 10 0 1885.70 1877.61 29.61 o 4 10 0 981.55 902.69 25.63 o 6 10 0 30.12 20.16 13.14 o 8 10 0 1519.77 1560.73 101.08 o 10 10 0 648.08 671.89 26.95 o 1 11 0 804.08 783.16 24.12 o 3 11 0 13.90 10.12 6.77 o 5 11 0 238.57 189.53 16.08 o 7 11 0 447.35 437.33 31.58 o 9 11 0 539.99 628.42 28.79 o 0 12 0 51.15 49.08 14.90 o 2 12 0 423.38 423.47 19.88 o 4 12 0 558.44 528.78 24.45 o 6 12 0 261.70 212.19 21.04 o 8 12 0 83.90 108.68 13.15 o 1 13 0 268.00 260.42 22.80 o 3 13 0 803.22 770.02 34.24 o -17 1 1 251.92 253.76 13.94 o -15 1 1 2381.11 2358.09 37.59 o -13 1 1 241.65 202.91 12.31 o -11 1 1 1089.65 1048.82 18.38 o -9 1 1 813.63 721.39 13.33 o -7 1 1 49.35 23.25 2.40 o -5 1 1 1273.03 1552.98 8.89 o -3 1 1 274.04 227.75 2.33 o -1 1 1 8.85 19.64 1.06 o 1 1 1 3057.49 3083.36 17.97 o 3 1 1 479.88 646.95 6.01 o 5 1 1 8795.00 8910.18 63.30 o 7 1 1 2811.96 3261.35 27.14 o 9 1 1 4454.10 4625.47 31.73 o 11 1 1 5037.90 4812.65 39.68 o 13 1 1 1121.14 1042.27 21.96 o 15 1 1 0.52 6.53 6.03 o -16 2 1 1357.73 1470.39 30.19 o -14 2 1 3142.76 3182.37 86.40 o -12 2 1 186.88 185.06 6.37 o -10 2 1 1884.76 1877.66 23.27 o -8 2 1 1617.57 1354.44 15.87 o -6 2 1 21.00 43.07 2.24 o -4 2 1 1885.90 2084.28 10.84 o -2 2 1 6957.09 7130.46 52.69 o 0 2 1 11431.19 11169.22 30.45 o 2 2 1 1316.10 1424.15 13.29 o 4 2 1 25770.85 24591.80 188.49 o 6 2 1 1792.98 1950.13 15.64 o 8 2 1 3325.10 3553.65 28.43 o 10 2 1 8394.42 8159.47 43.59 o 12 2 1 2643.75 2459.45 23.86 o 14 2 1 360.97 352.32 17.21 o 16 2 1 18.66 32.12 5.89 o -15 3 1 34.30 33.34 6.73 o -13 3 1 904.24 797.74 21.66 o -11 3 1 875.46 838.38 17.91 o -9 3 1 564.57 541.16 12.11 o -7 3 1 142.79 178.09 5.27 o -5 3 1 1500.90 1542.74 13.03 o -3 3 1 22.28 17.74 1.11 o -1 3 1 27952.29 28622.69 89.57 o 1 3 1 33724.66 31083.46 320.71 o 3 3 1 3286.15 3675.93 12.73 o 5 3 1 8206.75 9173.00 58.98 o 7 3 1 2553.61 2806.66 22.51 o 9 3 1 2333.99 2319.65 27.13 o 11 3 1 7.36 6.19 2.19 o 13 3 1 1183.49 1079.23 20.94 o 15 3 1 179.90 168.79 11.62 o -16 4 1 481.12 491.46 13.92 o -14 4 1 101.69 106.36 9.07 o -12 4 1 173.67 170.46 8.77 o -10 4 1 161.74 171.78 9.78 o -8 4 1 316.89 292.37 8.39 o -6 4 1 1400.58 1600.97 14.25 o -4 4 1 260.52 272.96 6.44 o -2 4 1 11328.46 11904.62 73.69 o 0 4 1 27.73 41.08 1.57 o 2 4 1 3823.16 3985.80 23.07 o 4 4 1 5.79 11.71 2.85 o 6 4 1 196.94 156.90 4.53 o 8 4 1 514.04 523.38 11.80 o 10 4 1 2494.26 2495.01 31.66 o 12 4 1 1525.98 1419.97 29.51 o 14 4 1 16.04 22.03 4.67 o 16 4 1 4.16 1.65 5.24 o -15 5 1 1641.07 1748.14 40.37 o -13 5 1 265.91 243.48 9.95 o -11 5 1 20.28 34.32 3.13 o -9 5 1 1201.77 1153.14 20.12 o -7 5 1 778.68 673.60 11.70 o -5 5 1 8.26 10.83 2.69 o -3 5 1 707.08 767.21 10.86 o -1 5 1 2236.15 2417.61 34.14 o 1 5 1 577.23 484.90 9.80 o 3 5 1 10837.67 10976.60 115.20 o 5 5 1 6.76 6.20 2.14 o 7 5 1 507.48 511.82 10.37 o 9 5 1 4361.89 4170.18 40.95 o 11 5 1 4060.61 3850.06 43.88 o 13 5 1 274.19 315.69 12.16 o 15 5 1 186.18 169.85 13.02 o -14 6 1 309.50 285.65 19.48 o -12 6 1 127.82 104.50 8.44 o -10 6 1 1461.34 1394.77 20.75 o -8 6 1 346.74 310.78 9.50 o -6 6 1 228.79 189.26 8.12 o -4 6 1 1506.43 1405.00 22.52 o -2 6 1 3821.68 4348.68 41.72 o 0 6 1 6.72 29.87 3.40 o 2 6 1 20614.16 21296.86 125.21 o 4 6 1 7395.82 7676.93 48.06 o 6 6 1 7.70 10.94 2.84 o 8 6 1 2989.63 2901.07 34.59 o 10 6 1 1656.33 1635.28 28.28 o 12 6 1 281.74 236.40 12.15 o 14 6 1 402.11 448.74 18.06 o -13 7 1 258.14 253.83 10.07 o -11 7 1 167.52 155.09 11.27 o -9 7 1 888.05 832.90 13.94 o -7 7 1 2.22 7.32 4.84 o -5 7 1 459.79 439.23 14.58 o -3 7 1 873.54 962.31 26.29 o -1 7 1 5557.91 5770.12 49.65 o 1 7 1 3530.68 3545.23 32.72 o 3 7 1 3868.49 4027.16 59.15 o 5 7 1 439.13 475.58 11.80 o 7 7 1 84.09 106.82 6.70 o 9 7 1 66.22 79.87 12.83 o 11 7 1 857.78 817.85 24.33 o 13 7 1 107.37 135.61 15.44 o -14 8 1 84.61 85.09 8.35 o -12 8 1 306.00 268.28 14.95 o -10 8 1 19.81 11.32 7.58 o -8 8 1 256.20 260.92 13.79 o -6 8 1 562.75 524.46 17.09 o -4 8 1 366.59 339.56 15.00 o -2 8 1 1499.63 1577.34 24.42 o 0 8 1 254.78 245.33 9.69 o 2 8 1 1447.95 1308.94 24.62 o 4 8 1 93.58 95.12 7.58 o 6 8 1 6.62 8.43 3.13 o 8 8 1 1219.95 1148.86 33.45 o 10 8 1 1018.85 943.10 29.88 o 12 8 1 673.55 765.80 23.97 o -13 9 1 59.65 53.46 9.64 o -11 9 1 23.40 29.17 7.36 o -9 9 1 614.47 643.75 29.70 o -7 9 1 573.51 555.34 22.96 o -5 9 1 730.44 625.65 15.99 o -3 9 1 1592.33 1542.46 28.10 o -1 9 1 13.62 7.03 2.83 o 1 9 1 1094.67 1005.22 25.48 o 3 9 1 9760.34 9587.42 90.21 o 5 9 1 225.30 212.44 9.58 o 7 9 1 55.58 43.31 7.45 o 9 9 1 1785.11 1790.49 40.38 o 11 9 1 709.81 675.14 22.06 o -12 10 1 32.09 31.55 8.76 o -10 10 1 540.38 573.23 37.73 o -8 10 1 842.74 824.36 32.20 o -6 10 1 89.49 97.39 10.25 o -4 10 1 1018.02 973.82 23.50 o -2 10 1 499.65 448.88 16.35 o 0 10 1 127.10 110.65 7.73 o 2 10 1 4975.07 4889.14 58.04 o 4 10 1 1443.57 1390.70 31.40 o 6 10 1 184.96 182.14 16.42 o 8 10 1 75.19 87.38 9.94 o 10 10 1 17.56 17.94 4.60 o -9 11 1 135.74 123.16 8.60 o -7 11 1 155.70 145.36 13.32 o -5 11 1 304.72 282.95 20.14 o -3 11 1 851.30 785.18 27.84 o -1 11 1 59.45 49.20 7.81 o 1 11 1 491.61 453.84 23.48 o 3 11 1 652.97 610.79 25.88 o 5 11 1 138.01 120.96 20.16 o 7 11 1 120.83 139.11 14.90 o 9 11 1 185.65 169.84 10.28 o -8 12 1 173.74 177.09 16.66 o -6 12 1 957.31 982.52 29.37 o -4 12 1 216.91 224.17 16.70 o -2 12 1 20.29 11.31 6.54 o 0 12 1 133.16 134.53 14.35 o 2 12 1 1095.65 1080.33 29.38 o 4 12 1 469.30 471.91 33.33 o 6 12 1 153.83 147.27 17.53 o 8 12 1 343.40 372.79 22.81 o -3 13 1 339.14 331.51 23.68 o -1 13 1 0.67 14.90 8.76 o 1 13 1 286.86 307.12 16.98 o 3 13 1 1427.79 1414.08 43.09 o 5 13 1 502.15 505.46 26.33 o -16 0 2 1160.33 1304.65 53.59 o -14 0 2 44.16 58.78 10.83 o -12 0 2 3476.11 3358.40 42.19 o -10 0 2 102.93 82.70 7.53 o -8 0 2 803.37 644.90 15.74 o -6 0 2 5196.09 4831.53 26.42 o -4 0 2 9939.93 9988.31 119.45 o -2 0 2 2266.26 2338.60 22.10 o 0 0 2 22015.50 20990.33 46.08 o 2 0 2 9557.07 9952.40 48.29 o 4 0 2 4846.41 4616.66 37.33 o 6 0 2 6618.38 6899.49 36.54 o 8 0 2 499.30 413.64 12.13 o 10 0 2 1380.12 1417.52 29.53 o 12 0 2 135.24 130.48 8.14 o 14 0 2 4092.95 3939.79 71.83 o 16 0 2 6.33 9.54 5.47 o -17 1 2 81.70 102.98 9.59 o -15 1 2 255.82 270.95 15.93 o -13 1 2 129.00 119.01 11.62 o -11 1 2 230.43 226.13 8.78 o -9 1 2 245.60 263.43 8.08 o -7 1 2 406.58 352.51 6.64 o -5 1 2 7128.79 7401.06 38.91 o -3 1 2 2079.32 2227.31 10.45 o -1 1 2 24754.58 21493.26 183.06 o 1 1 2 5355.68 5240.99 19.80 o 3 1 2 332.43 289.05 4.08 o 5 1 2 2855.98 2855.50 15.14 o 7 1 2 797.18 771.74 10.32 o 9 1 2 267.18 262.47 8.16 o 11 1 2 1575.37 1500.35 25.08 o 13 1 2 816.57 786.33 24.11 o 15 1 2 76.11 58.34 6.83 o -16 2 2 105.25 106.04 11.45 o -14 2 2 10.33 4.11 8.12 o -12 2 2 608.37 550.10 10.88 o -10 2 2 2416.29 2382.24 25.68 o -8 2 2 95.78 120.75 4.52 o -6 2 2 338.85 356.03 5.45 o -4 2 2 7004.74 7430.06 36.44 o -2 2 2 8930.60 8927.83 41.39 o 0 2 2 1740.51 1973.65 21.26 o 2 2 2 807.16 651.93 7.34 o 4 2 2 5490.95 5616.32 40.20 o 6 2 2 1808.59 2216.30 17.25 o 8 2 2 155.35 165.44 6.30 o 10 2 2 768.17 683.21 14.59 o 12 2 2 175.18 139.19 9.45 o 14 2 2 1585.63 1493.58 37.18 o 16 2 2 18.24 23.64 5.01 o -15 3 2 602.13 632.14 19.14 o -13 3 2 251.78 284.38 14.85 o -11 3 2 2000.23 2013.41 29.43 o -9 3 2 99.02 75.02 4.91 o -7 3 2 1664.05 1593.13 14.74 o -5 3 2 4570.68 4495.63 44.06 o -3 3 2 3225.46 3564.46 17.70 o -1 3 2 10.78 16.75 1.00 o 1 3 2 17101.32 18044.84 63.79 o 3 3 2 24.66 17.49 1.30 o 5 3 2 6699.76 6931.11 26.92 o 7 3 2 1143.60 1131.62 14.74 o 9 3 2 216.69 243.16 8.63 o 11 3 2 104.03 130.17 5.46 o 13 3 2 79.14 61.76 5.53 o 15 3 2 1423.11 1551.50 52.74 o -16 4 2 465.72 561.88 15.35 o -14 4 2 563.62 558.95 18.96 o -12 4 2 699.53 643.83 17.76 o -10 4 2 0.95 3.55 3.55 o -8 4 2 175.96 136.72 5.90 o -6 4 2 4568.03 4518.29 29.55 o -4 4 2 2080.18 2127.50 16.24 o -2 4 2 2306.59 2638.53 20.29 o 0 4 2 1019.84 1159.58 10.12 o 2 4 2 2112.91 2214.42 14.08 o 4 4 2 455.84 388.76 6.73 o 6 4 2 1881.69 1773.81 16.49 o 8 4 2 2604.39 2551.50 26.11 o 10 4 2 260.31 227.84 9.88 o 12 4 2 2145.33 2057.50 31.28 o 14 4 2 1317.87 1343.06 25.17 o 16 4 2 88.80 78.01 11.39 o -15 5 2 2.99 6.51 3.83 o -13 5 2 2330.76 2264.99 31.71 o -11 5 2 86.15 85.26 5.40 o -9 5 2 1721.48 1734.74 20.39 o -7 5 2 1642.38 1608.95 18.00 o -5 5 2 361.84 374.77 10.18 o -3 5 2 6607.55 7314.27 40.16 o -1 5 2 25.59 37.70 2.98 o 1 5 2 3764.61 4160.37 23.59 o 3 5 2 6119.28 6372.15 32.32 o 5 5 2 2786.89 3154.36 22.57 o 7 5 2 1027.94 1030.99 16.88 o 9 5 2 648.60 601.83 18.03 o 11 5 2 60.83 31.80 4.49 o 13 5 2 2970.79 2851.33 43.19 o 15 5 2 1220.78 1449.12 45.71 o -14 6 2 439.45 485.60 18.72 o -12 6 2 3.43 -1.21 4.60 o -10 6 2 1242.29 1222.80 18.55 o -8 6 2 547.07 517.33 14.28 o -6 6 2 227.05 256.05 7.97 o -4 6 2 2660.95 2707.22 30.94 o -2 6 2 331.27 338.63 9.65 o 0 6 2 250.42 303.70 7.63 o 2 6 2 4053.31 4497.09 32.39 o 4 6 2 2387.28 2351.78 20.94 o 6 6 2 261.18 259.44 8.26 o 8 6 2 84.30 74.47 5.95 o 10 6 2 32.27 50.85 6.65 o 12 6 2 17.80 29.38 5.60 o 14 6 2 116.39 117.81 9.44 o -13 7 2 481.29 497.45 15.29 o -11 7 2 45.60 42.74 6.70 o -9 7 2 39.13 37.68 3.57 o -7 7 2 1530.44 1469.61 23.47 o -5 7 2 946.01 851.69 22.47 o -3 7 2 2286.40 2548.09 41.72 o -1 7 2 20.76 35.24 4.25 o 1 7 2 7.95 8.82 2.71 o 3 7 2 1377.23 1485.16 20.98 o 5 7 2 91.72 71.48 5.33 o 7 7 2 2156.25 2072.73 30.43 o 9 7 2 279.21 257.74 14.09 o 11 7 2 967.10 882.25 18.71 o 13 7 2 1556.32 1778.00 34.31 o -14 8 2 1047.08 1164.88 36.04 o -12 8 2 468.94 449.53 18.88 o -10 8 2 278.31 255.76 19.52 o -8 8 2 2199.41 2158.03 61.60 o -6 8 2 1026.79 973.69 21.03 o -4 8 2 53.49 66.06 7.31 o -2 8 2 61.37 75.25 7.37 o 0 8 2 926.71 947.81 16.35 o 2 8 2 55.40 53.95 5.83 o 4 8 2 348.98 353.98 15.34 o 6 8 2 2165.93 2124.73 48.39 o 8 8 2 839.76 807.40 34.69 o 10 8 2 161.04 128.00 10.24 o 12 8 2 1821.99 1729.53 47.00 o -13 9 2 6.44 10.25 3.99 o -11 9 2 16.78 13.58 7.44 o -9 9 2 185.00 197.23 25.42 o -7 9 2 0.65 8.73 3.70 o -5 9 2 293.15 292.56 10.43 o -3 9 2 92.37 84.90 5.66 o -1 9 2 76.40 73.46 8.36 o 1 9 2 431.53 423.37 15.09 o 3 9 2 328.69 289.72 13.12 o 5 9 2 17.79 10.78 4.50 o 7 9 2 124.20 117.31 11.62 o 9 9 2 421.47 479.95 25.96 o 11 9 2 440.22 427.62 17.32 o -12 10 2 8.21 6.13 6.13 o -10 10 2 3.06 3.51 7.01 o -8 10 2 20.92 15.95 7.58 o -6 10 2 674.61 642.82 30.40 o -4 10 2 397.67 401.77 17.34 o -2 10 2 762.91 767.28 24.20 o 0 10 2 69.18 74.33 6.74 o 2 10 2 488.33 531.14 19.48 o 4 10 2 3.13 6.54 4.76 o 6 10 2 333.02 340.56 22.29 o 8 10 2 185.08 172.33 15.80 o 10 10 2 7.53 5.26 6.20 o -9 11 2 399.04 401.72 25.44 o -7 11 2 705.13 766.60 28.81 o -5 11 2 184.34 174.27 16.08 o -3 11 2 100.00 85.06 10.40 o -1 11 2 288.18 279.31 17.02 o 1 11 2 45.58 41.24 8.36 o 3 11 2 394.42 437.85 25.40 o 5 11 2 580.80 583.41 39.48 o 7 11 2 1222.53 1236.99 36.31 o 9 11 2 32.79 28.39 5.21 o -6 12 2 10.54 13.14 5.58 o -4 12 2 0.51 -13.07 14.46 o -2 12 2 0.41 0.88 10.52 o 0 12 2 194.78 178.83 12.98 o 2 12 2 103.00 96.20 9.11 o 4 12 2 466.91 499.11 33.33 o 6 12 2 114.23 108.17 10.10 o 8 12 2 389.38 404.45 21.93 o -5 13 2 248.16 249.91 17.54 o -3 13 2 56.48 47.33 10.52 o -1 13 2 278.50 263.93 22.80 o 1 13 2 721.14 734.72 36.87 o 3 13 2 30.53 35.05 9.64 o 5 13 2 0.25 12.27 7.01 o -17 1 3 14.30 27.28 9.64 o -15 1 3 280.74 279.20 20.14 o -13 1 3 644.05 604.19 23.97 o -11 1 3 6337.90 6012.03 57.18 o -9 1 3 1539.58 1684.55 19.91 o -7 1 3 1032.45 1241.54 11.87 o -5 1 3 13218.50 13888.28 87.85 o -3 1 3 1352.69 1462.31 10.90 o -1 1 3 1842.70 2087.13 10.38 o 1 1 3 791.70 984.91 10.04 o 3 1 3 14653.39 14920.01 92.71 o 5 1 3 315.70 318.76 4.91 o 7 1 3 915.41 914.21 12.22 o 9 1 3 1455.10 1365.26 18.35 o 11 1 3 2649.92 2444.47 24.47 o 13 1 3 165.90 164.91 13.14 o 15 1 3 3491.34 3812.62 69.25 o -16 2 3 328.51 362.36 15.28 o -14 2 3 270.10 286.04 14.34 o -12 2 3 5400.97 5260.67 37.42 o -10 2 3 51.81 38.53 4.20 o -8 2 3 659.84 757.33 12.20 o -6 2 3 6277.13 6824.41 26.32 o -4 2 3 6383.01 6734.98 26.55 o -2 2 3 1286.94 1306.86 7.24 o 0 2 3 10894.20 11770.70 62.88 o 2 2 3 10450.20 10702.56 33.94 o 4 2 3 4011.29 4095.80 22.79 o 6 2 3 1766.91 1886.33 16.33 o 8 2 3 1266.48 1218.09 17.40 o 10 2 3 1656.81 1547.70 22.05 o 12 2 3 3150.57 2857.43 44.81 o 14 2 3 2627.07 2602.49 45.76 o 16 2 3 1996.29 2156.74 128.64 o -15 3 3 501.85 520.06 20.54 o -13 3 3 9.46 11.55 5.64 o -11 3 3 956.47 962.06 20.53 o -9 3 3 567.84 617.06 12.87 o -7 3 3 183.96 202.19 5.62 o -5 3 3 588.42 556.20 8.36 o -3 3 3 924.76 809.70 7.53 o -1 3 3 4640.28 4920.74 24.59 o 1 3 3 212.76 242.00 3.56 o 3 3 3 3785.83 3767.84 17.52 o 5 3 3 1254.69 1227.42 12.98 o 7 3 3 82.19 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