#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/32/2233232.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233232_Fobs loop_ _publ_author_name 'Cao, Qiang' 'Duan, Bao-Rong' 'Zhu, Bin' 'Cao, Zhen' _publ_section_title ; 1H-Imidazol-3-ium-4-carboxylate ; _journal_coeditor_code LD2040 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o134 _journal_page_last o135 _journal_volume 68 _journal_year 2012 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.4736 _cell_length_b 11.6763 _cell_length_c 3.6743 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8109 _[local]_cod_data_source_file ld2040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 73.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 244.78 262.37 3.69 o 4 0 0 137.93 160.63 2.80 o 6 0 0 1301.68 1346.51 37.58 o 8 0 0 2.00 2.57 0.91 o 10 0 0 23.30 23.50 2.14 o 12 0 0 15.71 12.58 2.09 o 1 1 0 101.53 99.49 1.58 o 2 1 0 2190.97 1941.80 19.77 o 3 1 0 24.17 21.29 0.52 o 4 1 0 29.64 26.12 0.63 o 5 1 0 12.31 11.43 0.55 o 6 1 0 85.35 88.25 1.43 o 7 1 0 64.91 60.90 1.23 o 8 1 0 12.34 15.66 0.95 o 9 1 0 1.76 1.35 0.62 o 10 1 0 86.98 90.57 3.94 o 11 1 0 145.32 141.36 3.84 o 12 1 0 31.28 31.87 2.68 o 0 2 0 150.71 101.17 1.55 o 1 2 0 250.89 242.15 2.62 o 2 2 0 1761.02 1717.49 20.46 o 3 2 0 266.05 234.36 2.49 o 4 2 0 662.45 676.70 6.78 o 5 2 0 15.16 15.71 0.66 o 6 2 0 9.66 9.85 0.54 o 7 2 0 496.83 521.30 5.49 o 8 2 0 16.53 17.62 0.96 o 9 2 0 0.06 -0.38 0.43 o 10 2 0 20.50 20.75 1.44 o 11 2 0 12.64 10.59 1.69 o 12 2 0 0.03 0.07 0.82 o 1 3 0 114.21 111.74 1.18 o 2 3 0 685.92 771.38 9.00 o 3 3 0 326.00 291.14 3.35 o 4 3 0 407.22 427.16 5.30 o 5 3 0 123.81 141.53 1.69 o 6 3 0 56.92 65.76 1.24 o 7 3 0 0.03 -0.04 0.24 o 8 3 0 196.68 202.50 3.45 o 9 3 0 186.68 197.91 3.56 o 10 3 0 19.18 19.71 1.26 o 11 3 0 10.54 8.71 2.06 o 12 3 0 18.72 19.48 5.01 o 0 4 0 78.31 84.89 1.65 o 1 4 0 585.86 544.00 4.57 o 2 4 0 169.03 150.43 1.60 o 3 4 0 818.46 829.06 6.88 o 4 4 0 78.64 85.12 1.19 o 5 4 0 8.27 10.44 0.48 o 6 4 0 130.29 144.87 1.85 o 7 4 0 0.57 0.41 0.28 o 8 4 0 3.88 4.53 0.64 o 9 4 0 404.01 430.01 7.71 o 10 4 0 2.87 1.81 0.67 o 11 4 0 109.08 107.90 3.39 o 12 4 0 0.02 -0.03 0.91 o 1 5 0 83.46 87.34 1.13 o 2 5 0 1808.35 1881.21 14.90 o 3 5 0 246.20 237.33 2.42 o 4 5 0 3.52 3.04 0.30 o 5 5 0 58.61 60.74 1.22 o 6 5 0 274.24 302.50 3.19 o 7 5 0 59.04 60.43 1.20 o 8 5 0 235.99 247.09 4.01 o 9 5 0 82.49 87.40 3.02 o 10 5 0 2.15 1.88 0.70 o 11 5 0 40.19 43.17 1.99 o 12 5 0 0.28 -0.55 0.80 o 0 6 0 247.51 290.08 4.45 o 1 6 0 8.11 7.48 0.51 o 2 6 0 486.39 500.80 4.49 o 3 6 0 0.26 0.26 0.20 o 4 6 0 192.77 223.63 2.45 o 5 6 0 47.05 56.44 1.08 o 6 6 0 6.98 10.73 0.58 o 7 6 0 0.45 0.50 0.31 o 8 6 0 123.23 124.59 2.60 o 9 6 0 38.62 38.70 1.52 o 10 6 0 93.73 101.23 4.06 o 11 6 0 4.72 7.55 1.02 o 1 7 0 143.83 142.20 1.74 o 2 7 0 1.69 1.11 0.25 o 3 7 0 29.55 30.43 0.81 o 4 7 0 138.20 151.12 1.94 o 5 7 0 376.38 393.30 3.96 o 6 7 0 59.64 55.28 1.21 o 7 7 0 50.68 52.40 1.21 o 8 7 0 1.91 2.14 0.63 o 9 7 0 47.76 49.58 1.88 o 10 7 0 27.86 25.73 1.44 o 11 7 0 21.13 24.54 1.53 o 0 8 0 914.88 923.53 12.41 o 1 8 0 0.05 0.16 0.21 o 2 8 0 33.34 34.69 0.93 o 3 8 0 112.73 110.59 1.59 o 4 8 0 38.32 40.34 1.23 o 5 8 0 108.78 107.60 1.67 o 6 8 0 125.31 123.87 1.92 o 7 8 0 168.90 169.18 2.36 o 8 8 0 43.03 42.45 1.57 o 9 8 0 2.65 2.60 1.18 o 10 8 0 0.35 1.24 0.96 o 1 9 0 122.87 113.95 2.65 o 2 9 0 11.26 12.06 0.98 o 3 9 0 5.60 7.12 1.31 o 4 9 0 0.01 -0.12 0.41 o 5 9 0 208.44 199.11 3.35 o 6 9 0 1.70 0.74 0.45 o 7 9 0 1.54 1.30 0.52 o 8 9 0 83.46 89.68 4.34 o 9 9 0 1.34 4.02 1.55 o 0 10 0 267.80 245.68 6.48 o 1 10 0 573.99 538.25 11.00 o 2 10 0 125.06 118.92 2.91 o 3 10 0 6.71 9.04 2.49 o 4 10 0 121.58 123.25 3.06 o 5 10 0 40.32 36.99 1.93 o 6 10 0 0.11 0.47 0.54 o 7 10 0 186.22 172.82 3.97 o 1 11 0 113.20 104.45 2.84 o 2 11 0 106.38 99.58 2.78 o 3 11 0 4.11 3.74 1.04 o 4 11 0 2.51 4.34 1.20 o 5 11 0 18.50 17.29 1.47 o 6 11 0 62.22 62.32 2.35 o 7 11 0 2.60 0.23 0.69 o 0 12 0 3.90 3.32 1.18 o 1 12 0 20.22 20.32 1.36 o 2 12 0 8.04 9.58 1.12 o 3 12 0 49.09 50.40 2.09 o 4 12 0 18.76 18.94 1.44 o 5 12 0 30.50 30.07 3.27 o 6 12 0 6.87 7.48 1.26 o 7 12 0 7.51 7.56 1.12 o 1 13 0 79.45 70.39 2.54 o 2 13 0 0.10 0.41 0.64 o 3 13 0 50.21 54.61 2.30 o 4 13 0 4.15 4.50 0.98 o 5 13 0 1.21 0.20 0.68 o 0 14 0 6.87 6.26 1.66 o 1 14 0 69.63 69.95 2.68 o 2 14 0 9.55 8.99 1.25 o 3 14 0 4.61 5.59 1.11 o 2 0 1 5470.30 5184.20 83.24 o 4 0 1 540.44 551.02 7.51 o 6 0 1 52.79 56.97 1.44 o 8 0 1 95.63 91.80 2.13 o 10 0 1 26.20 26.30 1.35 o 12 0 1 84.13 85.57 3.16 o 0 1 1 3959.75 3630.95 85.63 o 1 1 1 2211.08 2129.81 15.36 o 2 1 1 2071.75 1890.85 12.76 o 3 1 1 14.18 13.41 0.43 o 4 1 1 77.82 76.44 1.28 o 5 1 1 375.10 388.75 3.52 o 6 1 1 35.04 43.83 1.02 o 7 1 1 71.30 76.82 1.28 o 8 1 1 107.82 104.23 1.73 o 9 1 1 74.41 65.39 1.21 o 10 1 1 9.43 10.96 0.74 o 11 1 1 11.94 9.92 0.84 o 12 1 1 9.76 8.69 0.86 o 1 2 1 9.85 10.85 0.28 o 2 2 1 23.94 21.14 0.36 o 3 2 1 31.12 25.20 0.40 o 4 2 1 213.38 213.72 1.76 o 5 2 1 329.02 327.13 2.82 o 6 2 1 64.83 68.15 1.03 o 7 2 1 2.51 2.69 0.33 o 8 2 1 9.59 11.10 0.76 o 9 2 1 133.00 134.12 1.81 o 10 2 1 90.84 91.97 1.88 o 11 2 1 10.34 8.67 0.80 o 12 2 1 17.69 17.52 1.07 o 0 3 1 906.99 931.11 9.79 o 1 3 1 584.45 562.42 4.40 o 2 3 1 42.81 41.59 0.49 o 3 3 1 32.98 32.10 0.59 o 4 3 1 170.24 181.14 1.58 o 5 3 1 51.48 47.95 0.70 o 6 3 1 221.30 213.78 2.14 o 7 3 1 213.77 215.06 2.24 o 8 3 1 31.73 29.44 0.85 o 9 3 1 26.33 27.28 0.88 o 10 3 1 22.47 21.76 0.98 o 11 3 1 24.59 25.38 1.10 o 12 3 1 1.91 1.67 0.62 o 1 4 1 253.52 266.00 2.44 o 2 4 1 193.80 193.00 1.63 o 3 4 1 246.37 247.74 1.88 o 4 4 1 145.14 148.10 1.42 o 5 4 1 39.58 36.48 0.68 o 6 4 1 39.43 44.39 0.93 o 7 4 1 321.27 318.09 3.23 o 8 4 1 4.66 5.62 0.49 o 9 4 1 90.85 89.21 1.56 o 10 4 1 0.83 1.00 0.49 o 11 4 1 90.64 90.49 1.98 o 12 4 1 0.40 0.08 0.57 o 0 5 1 1415.70 1453.33 15.09 o 1 5 1 93.79 93.69 1.23 o 2 5 1 167.97 167.79 1.53 o 3 5 1 133.51 135.48 1.23 o 4 5 1 437.81 446.54 3.13 o 5 5 1 62.97 67.33 0.93 o 6 5 1 29.26 26.80 0.70 o 7 5 1 29.15 29.12 0.82 o 8 5 1 143.80 142.95 1.98 o 9 5 1 87.71 83.60 2.09 o 10 5 1 94.26 95.90 2.76 o 11 5 1 15.71 15.30 1.15 o 1 6 1 14.64 13.54 0.52 o 2 6 1 248.70 269.45 2.45 o 3 6 1 358.09 361.54 2.85 o 4 6 1 180.72 185.01 1.76 o 5 6 1 28.92 30.07 0.71 o 6 6 1 110.37 114.58 1.68 o 7 6 1 33.31 32.87 1.00 o 8 6 1 80.24 88.39 1.70 o 9 6 1 51.46 53.60 1.37 o 10 6 1 45.62 44.42 1.54 o 11 6 1 0.02 0.87 0.76 o 0 7 1 73.85 83.59 1.93 o 1 7 1 77.42 80.22 1.24 o 2 7 1 151.83 156.37 1.75 o 3 7 1 70.34 75.41 1.14 o 4 7 1 25.49 22.91 0.77 o 5 7 1 10.56 10.78 0.53 o 6 7 1 1.30 1.43 0.41 o 7 7 1 160.83 158.56 2.42 o 8 7 1 8.39 6.73 0.75 o 9 7 1 1.77 1.29 0.52 o 10 7 1 11.22 11.51 1.23 o 1 8 1 44.27 45.72 0.98 o 2 8 1 76.24 83.22 1.24 o 3 8 1 77.63 75.24 1.18 o 4 8 1 10.22 9.85 0.54 o 5 8 1 183.94 175.16 2.01 o 6 8 1 55.82 52.57 1.32 o 7 8 1 69.01 78.05 1.66 o 8 8 1 70.44 74.69 1.69 o 9 8 1 6.60 6.11 0.79 o 10 8 1 3.70 2.60 1.12 o 0 9 1 69.31 64.60 1.71 o 1 9 1 343.46 333.26 3.36 o 2 9 1 70.51 72.56 1.22 o 3 9 1 61.68 62.37 1.13 o 4 9 1 82.85 78.00 1.28 o 5 9 1 69.34 61.91 1.16 o 6 9 1 34.17 35.19 1.14 o 7 9 1 82.54 73.25 1.66 o 8 9 1 1.56 1.89 0.52 o 9 9 1 64.53 69.73 2.34 o 1 10 1 185.93 188.10 2.55 o 2 10 1 107.00 106.25 1.57 o 3 10 1 180.82 175.30 2.39 o 4 10 1 11.92 11.34 0.72 o 5 10 1 75.59 71.11 1.31 o 6 10 1 23.01 25.30 1.12 o 7 10 1 14.88 16.16 0.96 o 8 10 1 4.62 4.21 0.65 o 0 11 1 230.58 226.66 4.14 o 1 11 1 44.55 46.58 1.24 o 2 11 1 17.47 16.60 0.91 o 3 11 1 15.68 14.42 0.85 o 4 11 1 76.66 79.06 1.67 o 5 11 1 5.74 5.23 0.66 o 6 11 1 67.89 65.80 2.13 o 7 11 1 16.32 16.60 1.29 o 1 12 1 36.89 32.01 1.22 o 2 12 1 14.69 15.76 1.02 o 3 12 1 18.89 20.61 1.06 o 4 12 1 11.94 12.73 1.17 o 5 12 1 5.49 5.50 0.72 o 6 12 1 4.24 5.53 1.39 o 0 13 1 64.64 63.40 2.47 o 1 13 1 50.89 47.18 1.54 o 2 13 1 50.76 58.85 1.71 o 3 13 1 10.19 8.95 1.22 o 4 13 1 0.24 1.17 0.55 o 1 14 1 3.88 2.45 0.63 o 0 0 2 1.44 0.32 0.59 o 2 0 2 881.47 859.74 9.89 o 4 0 2 368.07 357.54 4.88 o 6 0 2 26.90 27.34 1.16 o 8 0 2 20.46 21.42 1.17 o 10 0 2 25.78 23.82 1.35 o 1 1 2 208.84 214.85 2.87 o 2 1 2 237.72 232.04 2.35 o 3 1 2 760.48 754.74 5.70 o 4 1 2 469.23 486.35 4.40 o 5 1 2 32.06 33.10 0.85 o 6 1 2 10.50 9.76 0.60 o 7 1 2 42.81 43.61 1.06 o 8 1 2 17.77 17.06 0.77 o 9 1 2 39.20 36.39 1.08 o 10 1 2 42.57 42.67 1.12 o 11 1 2 1.61 0.84 0.50 o 0 2 2 310.09 322.97 5.95 o 1 2 2 97.80 93.32 1.28 o 2 2 2 362.27 367.12 3.32 o 3 2 2 8.91 9.58 0.51 o 4 2 2 24.17 24.10 0.78 o 5 2 2 11.13 13.15 0.61 o 6 2 2 7.53 7.61 0.54 o 7 2 2 92.09 87.90 1.39 o 8 2 2 110.59 107.26 1.63 o 9 2 2 31.44 28.50 0.90 o 10 2 2 5.68 5.46 0.56 o 11 2 2 9.94 8.90 0.80 o 1 3 2 52.21 47.22 1.01 o 2 3 2 15.78 15.63 0.74 o 3 3 2 44.88 41.52 0.75 o 4 3 2 3.16 3.23 0.33 o 5 3 2 133.01 132.88 1.64 o 6 3 2 90.02 93.57 1.38 o 7 3 2 21.82 20.40 0.72 o 8 3 2 13.89 14.53 0.70 o 9 3 2 17.79 16.06 0.79 o 10 3 2 2.89 1.20 0.51 o 11 3 2 17.09 15.55 1.24 o 0 4 2 353.63 333.46 4.54 o 1 4 2 197.73 193.98 2.51 o 2 4 2 43.26 45.88 1.11 o 3 4 2 59.72 60.39 1.03 o 4 4 2 52.75 54.11 1.17 o 5 4 2 284.25 273.65 3.24 o 6 4 2 0.08 0.63 0.33 o 7 4 2 68.96 63.67 1.44 o 8 4 2 17.36 16.32 0.81 o 9 4 2 15.21 12.27 0.87 o 10 4 2 2.29 2.15 0.59 o 11 4 2 33.78 37.40 1.54 o 1 5 2 38.59 42.92 0.95 o 2 5 2 75.60 84.24 1.44 o 3 5 2 25.26 27.94 1.01 o 4 5 2 22.81 20.02 0.98 o 5 5 2 26.41 26.78 1.13 o 6 5 2 190.23 185.00 3.02 o 7 5 2 106.42 102.26 2.20 o 8 5 2 67.04 71.94 1.88 o 9 5 2 3.70 1.86 0.80 o 10 5 2 26.59 25.24 2.23 o 0 6 2 233.29 247.00 3.84 o 1 6 2 185.12 186.68 2.25 o 2 6 2 47.55 43.57 1.06 o 3 6 2 56.43 57.31 1.15 o 4 6 2 77.35 75.74 1.81 o 5 6 2 60.93 59.52 1.63 o 6 6 2 53.37 53.60 1.57 o 7 6 2 21.56 22.54 1.12 o 8 6 2 2.61 1.41 0.58 o 9 6 2 16.15 15.48 1.15 o 10 6 2 17.37 18.32 1.82 o 1 7 2 41.05 42.89 1.03 o 2 7 2 60.46 62.36 1.24 o 3 7 2 26.42 26.82 0.80 o 4 7 2 38.15 35.55 1.36 o 5 7 2 82.28 80.89 1.94 o 6 7 2 3.45 3.25 0.63 o 7 7 2 17.55 18.09 1.13 o 8 7 2 34.35 36.84 1.58 o 9 7 2 1.28 1.31 0.61 o 0 8 2 58.74 57.74 1.76 o 1 8 2 20.30 18.97 0.79 o 2 8 2 55.72 55.23 1.22 o 3 8 2 25.80 25.14 0.82 o 4 8 2 13.54 15.17 0.96 o 5 8 2 4.44 4.22 0.65 o 6 8 2 12.18 11.75 1.00 o 7 8 2 19.22 19.19 1.20 o 8 8 2 9.01 11.05 1.01 o 9 8 2 51.95 53.76 1.81 o 1 9 2 2.20 1.96 0.42 o 2 9 2 65.90 65.80 1.38 o 3 9 2 394.70 403.76 3.88 o 4 9 2 36.07 37.44 1.29 o 5 9 2 18.32 15.41 1.03 o 6 9 2 41.50 41.55 1.40 o 7 9 2 19.60 20.54 1.73 o 8 9 2 4.87 7.73 0.91 o 0 10 2 9.50 9.84 1.02 o 1 10 2 50.53 49.08 1.25 o 2 10 2 23.96 25.68 0.90 o 3 10 2 6.20 6.97 0.61 o 4 10 2 26.43 26.99 1.18 o 5 10 2 73.55 73.34 1.82 o 6 10 2 14.15 13.49 1.44 o 7 10 2 6.48 7.55 0.93 o 1 11 2 44.46 44.32 1.33 o 2 11 2 60.91 60.63 1.34 o 3 11 2 18.93 17.87 0.88 o 4 11 2 51.24 51.51 2.82 o 5 11 2 1.43 0.67 0.54 o 6 11 2 7.92 7.95 0.86 o 0 12 2 51.01 53.64 1.99 o 1 12 2 52.93 53.79 1.42 o 2 12 2 7.22 7.90 0.79 o 3 12 2 22.72 22.42 1.10 o 4 12 2 0.58 -0.79 0.53 o 2 0 3 88.69 94.94 2.26 o 4 0 3 264.87 266.07 4.34 o 6 0 3 98.93 103.19 2.53 o 8 0 3 21.55 21.21 1.35 o 0 1 3 11.99 10.96 1.19 o 1 1 3 22.89 23.83 1.58 o 2 1 3 87.11 96.16 2.09 o 3 1 3 21.47 20.28 0.81 o 4 1 3 91.84 90.39 1.59 o 5 1 3 43.64 45.01 1.15 o 6 1 3 27.28 26.37 0.93 o 7 1 3 21.66 19.60 0.88 o 8 1 3 8.38 6.61 0.68 o 9 1 3 5.06 4.00 0.69 o 1 2 3 8.02 6.92 0.68 o 2 2 3 56.01 56.49 1.48 o 3 2 3 66.71 64.63 1.94 o 4 2 3 103.88 107.59 2.18 o 5 2 3 44.44 43.49 1.24 o 6 2 3 10.33 10.74 0.79 o 7 2 3 29.00 28.51 1.11 o 8 2 3 13.12 11.87 0.89 o 9 2 3 0.65 -0.11 0.56 o 0 3 3 159.80 165.17 3.86 o 1 3 3 12.03 10.63 0.83 o 2 3 3 27.08 29.66 1.12 o 3 3 3 6.19 6.99 0.78 o 4 3 3 6.03 5.96 0.76 o 5 3 3 30.55 30.78 1.27 o 6 3 3 40.85 42.96 1.50 o 7 3 3 31.26 31.46 1.36 o 8 3 3 1.83 1.45 0.64 o 9 3 3 3.26 2.39 0.72 o 1 4 3 11.00 10.80 0.85 o 2 4 3 72.83 72.35 1.73 o 3 4 3 79.10 83.60 2.03 o 4 4 3 2.10 0.54 0.54 o 5 4 3 138.72 139.08 3.10 o 6 4 3 1.90 2.28 0.87 o 7 4 3 21.25 19.58 1.20 o 8 4 3 3.16 2.61 0.80 o 0 5 3 4.43 4.17 0.88 o 1 5 3 0.66 0.09 0.43 o 2 5 3 25.51 23.36 1.07 o 3 5 3 1.39 0.28 0.76 o 4 5 3 21.05 21.90 1.20 o 5 5 3 34.81 34.33 1.41 o 6 5 3 26.99 28.46 1.49 o 7 5 3 9.78 7.97 1.08 o 8 5 3 5.45 3.90 0.85 o 1 6 3 52.27 55.22 1.59 o 2 6 3 20.65 22.91 1.10 o 3 6 3 30.88 32.13 1.46 o 4 6 3 49.65 51.17 1.70 o 5 6 3 8.87 8.38 0.94 o 6 6 3 18.88 18.42 1.48 o 7 6 3 37.47 36.35 1.68 o 8 6 3 6.54 5.71 0.90 o 0 7 3 50.25 54.96 2.30 o 1 7 3 70.68 71.23 1.85 o 2 7 3 6.91 7.48 1.01 o 3 7 3 8.77 10.56 1.02 o 4 7 3 27.98 25.94 1.58 o 5 7 3 10.94 10.80 1.06 o 6 7 3 3.88 4.66 0.81 o 7 7 3 3.57 3.06 0.79 o 1 8 3 16.42 15.90 0.98 o 2 8 3 23.71 26.63 1.53 o 3 8 3 41.08 43.10 1.64 o 4 8 3 22.91 22.60 1.47 o 5 8 3 9.29 8.69 1.01 o 6 8 3 49.44 53.03 2.06 o 0 9 3 27.65 28.66 1.53 o 1 9 3 27.82 28.84 1.17 o 2 9 3 6.47 5.86 0.99 o 3 9 3 0.21 0.44 0.65 o 4 9 3 25.24 29.80 1.54 o 5 9 3 41.25 43.42 1.74 o 1 10 3 25.72 23.36 1.57 o 2 10 3 1.02 0.90 0.60 o 3 10 3 67.04 69.69 2.14 o 1 1 4 7.37 8.06 1.02 o 2 1 4 3.63 3.79 1.14 o 3 1 4 2.91 2.81 1.00 o 4 1 4 7.19 5.83 1.23 o 5 1 4 37.25 38.99 3.29 o 6 1 4 14.90 13.96 1.62 o 0 2 4 16.55 13.56 1.69 o 1 2 4 5.81 5.87 0.93 o 2 2 4 4.46 4.15 0.81 o 3 2 4 9.34 10.68 1.18 o 4 2 4 18.32 18.88 1.34 o 5 2 4 29.26 32.25 1.54 o 1 3 4 1.46 0.53 0.69 o 2 3 4 32.90 33.05 1.49 o 3 3 4 60.54 62.57 1.97 o 4 3 4 24.58 26.91 1.41 o 5 3 4 7.95 5.80 1.11 o 0 4 4 22.80 24.70 2.01 o 1 4 4 5.65 3.52 0.88 o 2 4 4 6.49 5.24 0.86 o 3 4 4 9.55 9.19 1.05 o 4 4 4 1.37 2.03 0.74 o 1 5 4 6.66 5.21 1.95 o 2 5 4 3.54 2.24 0.75 o 3 5 4 18.88 19.05 1.38 o 4 5 4 35.28 34.21 1.59 o 0 6 4 5.94 7.50 2.36 o 1 6 4 14.35 17.56 1.95 o 2 6 4 12.63 11.03 1.59 o