#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:34:08 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181254 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/32/2233249.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233249_Fobs loop_ _publ_author_name 'Okawara, Toru' 'Feng, Jiang' 'Abe, Masaaki' 'Hisaeda, Yoshio' _publ_section_title ; Aquabis(1,1,1,5,5,5-hexafluoroacetylacetonato)[4'-(4-pyridyl)-2,2':6',2''-terpyridine]ytterbium(III) chloride methanol monosolvate monohydrate ; _journal_coeditor_code MW2026 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m29 _journal_page_last m30 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.870 _cell_angle_beta 104.717 _cell_angle_gamma 93.559 _cell_length_a 9.7559 _cell_length_b 12.4035 _cell_length_c 16.5543 _exptl_crystal_F_000 978.00 _reflns_d_resolution_high 0.7400 _cod_data_source_file mw2026Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Jiang8_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 319.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 52954.53 49629.77 1003.15 o 2 0 0 8274.73 9428.44 209.58 o 3 0 0 1952.69 1830.68 62.96 o 4 0 0 1857.97 2012.10 73.72 o 5 0 0 192.01 195.49 29.82 o 6 0 0 1146.24 1140.66 66.27 o 7 0 0 1399.66 1351.06 74.55 o 9 0 0 1079.21 945.16 62.13 o 10 0 0 584.54 468.03 53.02 o 11 0 0 421.76 309.81 49.70 o 12 0 0 376.56 371.94 57.16 o -12 1 0 1.87 -15.74 33.13 o -11 1 0 29.94 -0.83 27.34 o -10 1 0 73.06 86.15 29.82 o -9 1 0 720.56 810.14 57.16 o -8 1 0 1229.98 1259.94 64.61 o -6 1 0 4776.00 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113.49 41.42 o -11 4 0 306.70 285.79 47.22 o -10 4 0 75.31 94.76 22.50 o -9 4 0 2.36 9.85 15.52 o -8 4 0 1.78 -11.82 12.73 o -7 4 0 375.53 391.21 26.42 o -6 4 0 1742.95 1857.69 47.86 o -5 4 0 5630.66 5215.29 93.19 o -4 4 0 9734.94 9887.18 155.01 o -3 4 0 36819.70 39990.01 612.99 o -2 4 0 16421.88 17554.69 371.94 o -1 4 0 4322.76 3841.75 68.78 o 0 4 0 8599.35 9353.06 203.78 o 1 4 0 6491.68 6632.01 112.17 o 2 4 0 341.67 376.59 10.33 o 3 4 0 3108.17 3068.67 69.52 o 4 4 0 892.83 874.28 35.50 o 5 4 0 5284.16 5584.00 173.13 o 6 4 0 3264.11 3277.01 126.74 o 7 4 0 1583.53 1505.14 86.98 o 8 4 0 478.32 463.06 62.96 o 10 4 0 337.51 371.11 55.50 o 11 4 0 63.48 28.16 34.79 o -12 5 0 140.33 199.64 48.05 o -11 5 0 260.77 233.60 46.39 o -10 5 0 148.40 133.37 33.96 o -9 5 0 445.20 508.62 52.19 o -8 5 0 2148.77 2308.63 84.91 o -7 5 0 1653.41 1605.45 53.84 o -6 5 0 875.90 829.50 31.05 o -5 5 0 1823.93 1800.83 61.30 o -4 5 0 6.88 25.68 13.67 o -3 5 0 3254.63 3365.36 58.08 o -2 5 0 463.75 467.20 29.82 o -1 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99.40 o -1 8 0 226.16 211.42 18.22 o 0 8 0 2181.39 2117.91 71.65 o 1 8 0 1662.80 1597.76 49.13 o 2 8 0 2062.00 2027.32 40.72 o 3 8 0 3899.57 3820.97 92.25 o 4 8 0 6178.21 6185.22 144.96 o 5 8 0 2953.05 2856.26 83.76 o 6 8 0 1678.13 1580.09 63.53 o 8 8 0 36.96 25.68 33.13 o 9 8 0 90.19 60.47 36.45 o 10 8 0 4.20 -8.28 29.82 o -11 9 0 279.96 265.90 52.19 o -10 9 0 462.91 585.65 67.10 o -9 9 0 145.86 125.91 38.93 o -8 9 0 194.74 194.67 36.45 o -7 9 0 0.07 5.80 19.88 o -6 9 0 632.34 705.77 58.81 o -5 9 0 76.89 57.99 23.19 o -4 9 0 47.44 64.61 21.54 o -3 9 0 3478.58 3466.70 116.80 o -2 9 0 6669.96 6453.78 182.24 o -1 9 0 3302.27 3288.60 115.14 o 0 9 0 4177.68 3988.57 132.54 o 1 9 0 2356.60 2236.94 60.97 o 2 9 0 1733.99 1632.27 54.83 o 3 9 0 953.29 919.66 46.54 o 4 9 0 136.19 129.89 24.26 o 5 9 0 68.10 55.56 29.41 o 6 9 0 1134.80 1204.46 123.01 o 7 9 0 668.62 760.44 76.21 o 8 9 0 528.82 495.36 61.30 o 9 9 0 439.87 485.42 62.96 o -10 10 0 196.75 236.91 50.53 o -9 10 0 533.70 512.76 62.13 o -8 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