#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:34:08 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181254 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/32/2233255.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233255_Fobs loop_ _publ_author_name 'Phasha, Zanele H.' 'Makhoba, Sizwe' 'Muller, Alfred' _publ_section_title ; Dicyclohexyl[4-(dimethylamino)phenyl]phosphine selenide ; _journal_coeditor_code NC2259 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o243 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.050 _cell_angle_gamma 90.000 _cell_length_a 12.3860 _cell_length_b 6.8331 _cell_length_c 24.1126 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.7499 _cod_data_source_file nc2259Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_11fm_hp2_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 288.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6087.30 5897.57 56.93 o 2 0 0 15082.61 16031.88 168.47 o 3 0 0 12114.41 11829.67 125.70 o 4 0 0 46.62 36.91 5.33 o 5 0 0 6218.58 6085.61 67.57 o 6 0 0 14006.43 14106.80 151.67 o 7 0 0 254.54 159.56 8.61 o 8 0 0 1176.02 1111.76 24.49 o 9 0 0 172.57 140.75 17.12 o 10 0 0 3596.33 3649.59 54.79 o 11 0 0 2641.85 2657.98 45.53 o 12 0 0 1044.71 1107.78 31.22 o 13 0 0 2230.27 2361.86 46.25 o 14 0 0 186.64 231.42 27.24 o 15 0 0 1135.12 1266.74 46.47 o 16 0 0 544.35 558.46 34.60 o 1 1 0 1971.13 1779.81 13.58 o 2 1 0 15522.28 15962.97 104.25 o 3 1 0 4643.35 4674.36 36.57 o 4 1 0 10959.42 11177.48 85.04 o 5 1 0 263.05 256.83 6.21 o 6 1 0 7829.79 7757.92 64.20 o 7 1 0 845.95 739.46 13.61 o 8 1 0 1373.19 1356.85 17.75 o 9 1 0 6007.14 6108.02 53.82 o 10 1 0 15.09 8.20 8.29 o 11 1 0 2139.93 2150.09 28.40 o 12 1 0 336.32 312.08 13.89 o 13 1 0 803.04 841.89 22.49 o 14 1 0 638.87 653.83 19.60 o 15 1 0 8.85 -10.76 15.91 o 16 1 0 161.28 165.73 19.68 o 0 2 0 16016.52 18066.58 241.30 o 1 2 0 1716.53 1714.93 19.59 o 2 2 0 10582.27 11421.87 86.02 o 3 2 0 3844.76 4028.48 32.14 o 4 2 0 540.48 522.35 7.97 o 5 2 0 5403.13 5362.13 45.52 o 6 2 0 27.35 28.71 4.98 o 7 2 0 2283.53 2151.54 22.74 o 8 2 0 2295.35 2297.71 23.59 o 9 2 0 2346.57 2271.27 24.35 o 10 2 0 4145.58 4067.05 44.13 o 11 2 0 75.63 59.80 9.94 o 12 2 0 2642.04 2663.63 37.10 o 13 2 0 1211.80 1257.81 30.63 o 14 2 0 259.66 245.97 18.95 o 15 2 0 3262.02 3342.89 55.89 o 1 3 0 12074.58 12490.85 114.48 o 2 3 0 10866.21 11872.18 101.67 o 3 3 0 2043.29 2116.69 19.94 o 4 3 0 10703.83 10686.37 86.57 o 5 3 0 285.76 214.64 6.81 o 6 3 0 5792.47 5852.02 53.67 o 7 3 0 2615.58 2560.47 26.10 o 8 3 0 744.13 738.33 14.35 o 9 3 0 1715.76 1655.91 25.55 o 10 3 0 383.31 377.33 14.35 o 11 3 0 615.48 599.17 17.77 o 12 3 0 1889.51 1868.84 37.22 o 13 3 0 25.92 6.89 14.05 o 14 3 0 1556.50 1594.00 34.92 o 15 3 0 151.89 135.93 19.96 o 0 4 0 11927.45 12700.05 179.79 o 1 4 0 669.88 649.24 12.44 o 2 4 0 4363.31 4299.50 39.88 o 3 4 0 6204.88 6106.43 56.36 o 4 4 0 306.89 294.77 7.25 o 5 4 0 8270.72 8343.82 89.16 o 6 4 0 1504.67 1479.99 23.74 o 7 4 0 2535.71 2473.33 30.61 o 8 4 0 5474.99 5505.39 57.41 o 9 4 0 96.58 104.56 10.99 o 10 4 0 4972.13 4846.04 53.79 o 11 4 0 1454.43 1445.48 33.05 o 12 4 0 1586.84 1581.15 36.45 o 13 4 0 578.06 593.30 22.53 o 14 4 0 12.41 4.16 22.74 o 1 5 0 3017.45 2969.01 32.84 o 2 5 0 38.64 34.48 6.20 o 3 5 0 2645.07 2735.93 37.24 o 4 5 0 560.43 598.15 12.48 o 5 5 0 9.68 2.88 7.42 o 6 5 0 3587.91 3549.20 47.69 o 7 5 0 80.02 80.69 10.84 o 8 5 0 1388.25 1451.94 27.16 o 9 5 0 1681.07 1593.57 29.44 o 10 5 0 165.74 174.73 15.23 o 11 5 0 954.17 889.42 32.87 o 12 5 0 208.48 214.65 18.09 o 13 5 0 757.10 723.14 25.26 o 0 6 0 4916.91 4876.56 78.78 o 1 6 0 907.92 892.80 24.21 o 2 6 0 803.21 805.33 23.65 o 3 6 0 3332.78 3399.41 41.08 o 4 6 0 2888.48 2776.05 32.53 o 5 6 0 3668.59 3654.61 42.17 o 6 6 0 486.71 444.65 16.70 o 7 6 0 1047.03 1057.73 24.17 o 8 6 0 2222.48 2201.64 34.96 o 9 6 0 269.44 261.05 15.91 o 10 6 0 2829.19 2785.40 42.46 o 11 6 0 360.49 369.75 19.99 o 12 6 0 600.00 605.37 23.67 o 1 7 0 5308.59 5247.53 77.95 o 2 7 0 2399.31 2472.28 41.26 o 3 7 0 654.64 666.82 21.04 o 4 7 0 4752.83 4831.86 55.81 o 5 7 0 639.46 639.20 23.42 o 6 7 0 2700.51 2661.69 41.87 o 7 7 0 1473.52 1502.45 32.49 o 8 7 0 99.54 65.31 14.12 o 9 7 0 1499.27 1519.32 32.30 o 10 7 0 282.03 271.53 18.64 o 0 8 0 368.64 394.94 32.89 o 1 8 0 9.05 -1.62 17.52 o 2 8 0 1636.70 1626.65 65.48 o 3 8 0 1279.54 1267.93 33.09 o 4 8 0 109.96 113.21 22.67 o 5 8 0 2133.76 2145.29 37.44 o 6 8 0 68.68 60.88 14.15 o 7 8 0 1668.09 1620.04 53.08 o 1 9 0 1323.68 1384.17 53.98 o 2 9 0 163.38 196.09 46.02 o -16 1 1 38.10 38.14 17.62 o -15 1 1 376.51 368.37 19.60 o -14 1 1 80.77 83.06 15.88 o -13 1 1 292.00 300.44 14.16 o -12 1 1 87.48 78.47 11.78 o -11 1 1 275.70 298.59 12.70 o -10 1 1 265.54 252.46 11.30 o -9 1 1 339.19 314.07 10.03 o -8 1 1 56.00 49.99 6.98 o -7 1 1 1009.99 1047.83 17.60 o -6 1 1 2532.42 2617.97 24.88 o -5 1 1 596.83 708.69 10.53 o -4 1 1 20.81 17.69 4.08 o -3 1 1 1984.77 1919.85 16.67 o -2 1 1 174.34 196.48 3.57 o -1 1 1 12183.81 12548.00 89.26 o 0 1 1 2169.70 2375.61 29.92 o 1 1 1 2.58 1.62 1.69 o 2 1 1 25.81 26.82 2.23 o 3 1 1 3.91 -6.33 3.17 o 4 1 1 0.38 -4.86 3.86 o 5 1 1 994.63 990.84 12.51 o 6 1 1 20.99 13.18 6.65 o 7 1 1 29.70 28.05 5.96 o 8 1 1 2612.38 2633.45 26.90 o 9 1 1 12.54 -3.44 7.28 o 10 1 1 578.22 592.54 13.54 o 11 1 1 290.82 266.80 11.27 o 12 1 1 21.81 22.53 11.14 o 13 1 1 204.44 200.46 19.94 o 14 1 1 896.58 898.87 22.07 o 15 1 1 0.00 5.28 15.84 o 16 1 1 136.76 132.15 21.43 o -16 2 1 198.59 223.64 26.37 o -15 2 1 199.49 240.66 20.54 o -14 2 1 244.88 242.24 18.87 o -13 2 1 82.31 73.20 18.05 o -12 2 1 4.66 -2.14 11.17 o -11 2 1 356.71 319.69 14.18 o -10 2 1 64.77 29.58 8.28 o -9 2 1 512.92 514.55 11.75 o -8 2 1 1.51 -11.89 6.29 o -7 2 1 101.11 105.31 6.34 o -6 2 1 16.93 20.92 4.97 o -5 2 1 223.40 219.34 6.44 o -4 2 1 222.76 240.43 5.16 o -3 2 1 3712.25 3930.16 33.34 o -2 2 1 1902.27 2194.66 19.48 o -1 2 1 4.80 3.81 3.55 o 0 2 1 22.18 9.52 3.22 o 1 2 1 143.92 199.90 6.75 o 2 2 1 110.10 131.79 3.60 o 3 2 1 1175.49 1206.07 12.81 o 4 2 1 60.77 57.37 3.74 o 5 2 1 229.63 255.85 6.25 o 6 2 1 34.91 27.64 5.04 o 7 2 1 52.08 37.30 5.93 o 8 2 1 0.35 -9.54 6.37 o 9 2 1 1790.41 1757.51 21.04 o 10 2 1 309.36 280.89 10.32 o 11 2 1 3.47 -9.48 9.38 o 12 2 1 371.09 381.88 15.65 o 13 2 1 59.04 46.45 12.65 o 14 2 1 61.46 38.69 16.74 o 15 2 1 311.03 320.76 21.39 o -15 3 1 90.59 84.74 19.23 o -14 3 1 7.08 0.57 16.81 o -13 3 1 8.64 -7.39 13.96 o -12 3 1 594.00 585.39 18.62 o -11 3 1 3.66 -11.99 11.43 o -10 3 1 662.53 624.40 18.23 o -9 3 1 105.44 92.23 9.25 o -8 3 1 174.13 171.08 8.48 o -7 3 1 1864.80 1903.23 22.98 o -6 3 1 501.90 485.73 10.39 o -5 3 1 359.41 409.54 9.11 o -4 3 1 24.29 42.62 4.51 o -3 3 1 276.48 283.73 6.03 o -2 3 1 1.15 -7.02 3.51 o -1 3 1 1490.03 1630.50 18.85 o 0 3 1 2162.30 2228.46 28.27 o 1 3 1 390.36 408.87 9.11 o 2 3 1 29.21 11.05 4.06 o 3 3 1 20.65 28.81 3.96 o 4 3 1 142.58 184.21 6.00 o 5 3 1 1438.87 1450.80 19.27 o 6 3 1 46.77 45.86 6.47 o 7 3 1 218.77 238.19 9.10 o 8 3 1 116.69 101.02 7.52 o 9 3 1 303.74 266.88 12.37 o 10 3 1 0.62 -13.02 10.28 o 11 3 1 776.95 739.76 19.79 o 12 3 1 57.86 50.04 13.36 o 13 3 1 17.28 2.00 14.08 o 14 3 1 220.89 230.18 17.62 o 15 3 1 247.16 233.56 20.86 o -14 4 1 8.58 -28.56 19.05 o -13 4 1 1019.00 945.93 27.41 o -12 4 1 19.57 13.14 13.28 o -11 4 1 656.96 602.12 25.17 o -10 4 1 217.18 219.66 13.39 o -9 4 1 738.69 688.23 17.45 o -8 4 1 676.06 617.94 16.38 o -7 4 1 641.66 650.94 17.56 o -6 4 1 58.27 71.90 6.85 o -5 4 1 61.63 31.78 6.44 o -4 4 1 1434.59 1435.73 22.11 o -3 4 1 21.01 19.32 6.52 o -2 4 1 922.20 924.15 13.18 o -1 4 1 114.36 186.39 8.09 o 0 4 1 43.11 38.06 7.60 o 1 4 1 2341.53 2620.48 28.57 o 2 4 1 4.12 12.28 4.69 o 3 4 1 96.34 95.95 4.89 o 4 4 1 153.29 157.50 6.22 o 5 4 1 48.56 46.79 5.60 o 6 4 1 797.88 772.97 16.13 o 7 4 1 123.36 103.44 9.12 o 8 4 1 114.18 124.27 10.37 o 9 4 1 82.45 86.55 10.90 o 10 4 1 643.30 626.24 24.34 o 11 4 1 3.95 8.54 12.21 o 12 4 1 611.05 598.70 21.38 o 13 4 1 171.86 159.01 18.12 o 14 4 1 22.11 2.65 17.38 o -13 5 1 40.70 43.92 17.79 o -12 5 1 36.42 54.70 16.38 o -11 5 1 1.06 -12.89 14.23 o -10 5 1 43.86 21.82 13.58 o -9 5 1 33.91 25.91 12.51 o -8 5 1 1001.45 937.11 23.26 o -7 5 1 214.50 201.21 16.31 o -6 5 1 276.23 289.84 10.84 o -5 5 1 233.46 203.30 9.41 o -4 5 1 1087.10 1002.05 15.70 o -3 5 1 2.29 7.56 4.76 o -2 5 1 233.96 238.69 8.38 o -1 5 1 132.00 139.26 7.15 o 0 5 1 23.39 25.78 7.85 o 1 5 1 202.44 225.82 8.85 o 2 5 1 455.24 459.85 10.24 o 3 5 1 1367.37 1402.15 16.57 o 4 5 1 94.79 97.98 8.91 o 5 5 1 370.02 338.60 10.65 o 6 5 1 119.01 109.77 9.10 o 7 5 1 190.82 181.72 15.98 o 8 5 1 9.25 29.52 11.27 o 9 5 1 56.58 43.10 12.76 o 10 5 1 208.32 192.75 15.47 o 11 5 1 252.29 270.13 17.55 o 12 5 1 17.54 13.18 15.93 o 13 5 1 13.20 11.54 17.26 o -12 6 1 60.65 88.62 17.78 o -11 6 1 78.85 79.15 17.58 o -10 6 1 81.22 113.04 15.60 o -9 6 1 176.47 207.46 15.53 o -8 6 1 498.38 495.72 17.56 o -7 6 1 911.45 832.02 27.68 o -6 6 1 285.91 261.63 12.80 o -5 6 1 2676.53 2593.77 40.00 o -4 6 1 0.40 8.09 7.64 o -3 6 1 847.13 888.00 19.13 o -2 6 1 610.83 657.44 19.06 o -1 6 1 1354.83 1371.29 28.20 o 0 6 1 65.49 65.57 9.54 o 1 6 1 433.77 465.69 17.53 o 2 6 1 622.57 612.81 14.03 o 3 6 1 96.72 115.84 9.03 o 4 6 1 379.90 362.87 11.56 o 5 6 1 65.06 47.33 8.97 o 6 6 1 54.42 45.08 10.62 o 7 6 1 0.20 4.69 11.11 o 8 6 1 232.30 204.77 14.98 o 9 6 1 367.25 370.06 17.50 o 10 6 1 58.56 40.39 15.37 o 11 6 1 5.30 -22.51 15.34 o 12 6 1 290.62 309.61 20.39 o -10 7 1 53.73 48.83 16.02 o -9 7 1 46.85 36.37 14.73 o -8 7 1 73.74 49.77 13.76 o -7 7 1 71.17 43.77 13.94 o -6 7 1 310.17 319.38 16.13 o -5 7 1 6.53 -2.70 12.01 o -4 7 1 137.48 158.68 11.21 o -3 7 1 11.70 23.49 11.13 o -2 7 1 35.87 47.87 13.56 o -1 7 1 489.00 522.68 22.57 o 0 7 1 1094.73 1017.09 32.13 o 1 7 1 6.11 8.02 15.17 o 2 7 1 531.97 574.01 28.96 o 3 7 1 34.75 37.83 11.66 o 4 7 1 0.47 -10.16 9.40 o 5 7 1 104.42 102.70 12.50 o 6 7 1 28.17 31.13 12.68 o 7 7 1 260.21 243.03 14.91 o 8 7 1 114.96 117.95 14.70 o 9 7 1 75.64 71.47 18.03 o 10 7 1 36.43 61.89 19.50 o -7 8 1 0.88 8.70 16.90 o -6 8 1 0.41 -10.33 13.57 o -5 8 1 202.01 220.92 18.73 o -4 8 1 263.07 268.56 21.56 o -3 8 1 153.19 171.36 15.77 o -2 8 1 75.73 50.46 20.74 o -1 8 1 448.58 467.58 30.50 o 0 8 1 99.69 101.45 18.91 o 1 8 1 273.75 304.85 22.11 o 2 8 1 24.37 50.42 18.32 o 3 8 1 450.02 477.26 20.11 o 4 8 1 386.00 394.82 22.77 o 5 8 1 131.65 124.26 13.80 o 6 8 1 466.28 500.62 19.45 o 7 8 1 532.11 577.94 21.58 o -2 9 1 245.25 231.71 39.79 o -1 9 1 1.11 -14.75 22.92 o 0 9 1 1.30 -22.42 20.03 o 1 9 1 67.82 37.06 21.21 o 2 9 1 54.95 58.18 24.07 o -16 0 2 398.19 436.25 33.18 o -15 0 2 243.46 257.09 23.93 o -14 0 2 796.45 702.54 31.59 o -13 0 2 517.70 422.32 22.59 o -12 0 2 2357.54 2642.78 47.23 o -11 0 2 760.09 804.31 32.71 o -10 0 2 5.25 -10.70 12.46 o -9 0 2 4758.17 4736.64 65.37 o -8 0 2 2097.11 2134.39 35.21 o -7 0 2 5010.97 5401.82 70.22 o -6 0 2 27226.05 28241.79 333.89 o -5 0 2 1045.63 1100.70 19.93 o -4 0 2 2763.95 2502.53 42.66 o -3 0 2 58696.30 58701.63 684.81 o -2 0 2 363.99 292.15 14.02 o -1 0 2 47760.00 47108.25 636.26 o 0 0 2 263.58 180.06 3.35 o 1 0 2 7716.86 8112.61 95.76 o 2 0 2 29193.36 30859.75 360.30 o 3 0 2 2873.90 2912.23 37.47 o 4 0 2 5323.58 5226.26 58.25 o 5 0 2 2634.44 2479.22 33.87 o 6 0 2 12353.31 12999.78 140.34 o 7 0 2 20976.99 20987.98 224.12 o 8 0 2 4303.85 4528.99 54.64 o 9 0 2 10589.80 10659.13 118.73 o 10 0 2 2099.04 2086.38 32.41 o 11 0 2 1728.90 1728.53 37.31 o 12 0 2 2582.78 2715.93 48.01 o 13 0 2 1374.08 1454.44 36.80 o 14 0 2 250.76 260.86 22.13 o 15 0 2 658.69 622.13 33.56 o 16 0 2 4.85 -30.07 26.16 o -16 1 2 0.54 -37.65 18.83 o -15 1 2 687.46 678.63 22.63 o -14 1 2 286.31 282.85 18.44 o -13 1 2 134.34 129.93 12.67 o -12 1 2 2836.15 2836.99 33.05 o -11 1 2 62.40 53.04 10.39 o -10 1 2 4360.27 4490.03 46.74 o -9 1 2 1795.45 1790.33 23.50 o -8 1 2 1210.92 1235.21 17.03 o -7 1 2 6941.83 6826.13 57.79 o -6 1 2 2331.36 2433.00 22.52 o -5 1 2 1398.35 1221.89 13.51 o -4 1 2 9249.26 9171.39 70.36 o -3 1 2 6733.70 6868.08 52.84 o -2 1 2 73.16 75.90 3.17 o -1 1 2 1644.81 1799.86 13.30 o 0 1 2 4032.86 4153.69 31.69 o 1 1 2 3114.79 2853.52 22.29 o 2 1 2 4885.77 5202.86 44.61 o 3 1 2 16682.74 17335.13 154.28 o 4 1 2 530.53 521.81 11.63 o 5 1 2 9587.55 9863.40 79.87 o 6 1 2 3857.40 3959.34 35.22 o 7 1 2 1702.08 1804.60 19.92 o 8 1 2 4376.05 4370.86 39.84 o 9 1 2 189.58 180.67 8.93 o 10 1 2 224.40 190.57 9.85 o 11 1 2 1573.39 1599.99 22.41 o 12 1 2 201.91 178.91 11.43 o 13 1 2 1018.11 1022.77 24.94 o 14 1 2 14.31 -23.72 13.30 o 15 1 2 990.89 1048.31 27.83 o 16 1 2 328.25 317.14 22.61 o -16 2 2 2413.98 2568.98 55.08 o -15 2 2 465.11 427.73 22.81 o -14 2 2 1385.84 1429.93 33.85 o -13 2 2 3122.51 3074.56 49.60 o -12 2 2 5.62 -4.24 12.17 o -11 2 2 3795.96 3680.72 44.05 o -10 2 2 2049.08 2020.05 25.30 o -9 2 2 1520.45 1453.34 20.46 o -8 2 2 5950.67 5899.15 52.18 o -7 2 2 150.15 129.82 7.15 o -6 2 2 8054.00 8064.31 67.11 o -5 2 2 1466.59 1353.15 13.44 o -4 2 2 2008.06 2041.29 17.44 o -3 2 2 7603.63 7887.92 57.74 o -2 2 2 1927.96 2099.67 16.93 o -1 2 2 8534.78 8992.21 82.63 o 0 2 2 9616.96 10399.97 94.87 o 1 2 2 1604.83 1656.09 17.71 o 2 2 2 6588.67 7214.66 55.32 o 3 2 2 818.13 910.58 11.43 o 4 2 2 3339.15 3400.60 29.83 o 5 2 2 571.12 602.53 9.77 o 6 2 2 2204.47 2141.84 20.67 o 7 2 2 3483.29 3482.05 31.10 o 8 2 2 891.75 918.24 14.75 o 9 2 2 5279.73 5265.56 45.56 o 10 2 2 360.26 362.80 13.67 o 11 2 2 2693.51 2657.08 31.40 o 12 2 2 1578.49 1579.52 29.88 o 13 2 2 188.38 147.09 13.49 o 14 2 2 1672.06 1742.14 42.14 o 15 2 2 14.12 7.32 18.02 o -15 3 2 59.48 64.85 19.13 o -14 3 2 130.68 143.45 18.43 o -13 3 2 462.74 471.73 20.55 o -12 3 2 659.20 625.90 19.08 o -11 3 2 86.16 56.00 14.67 o -10 3 2 701.07 696.49 18.69 o -9 3 2 124.31 127.20 9.70 o -8 3 2 4940.96 4855.08 44.49 o -7 3 2 7011.75 6936.75 59.61 o -6 3 2 181.95 190.11 6.13 o -5 3 2 11751.60 12042.47 104.03 o -4 3 2 2812.70 2891.86 26.52 o -3 3 2 3550.49 3834.11 31.34 o -2 3 2 9963.89 10105.51 76.69 o -1 3 2 87.64 106.40 5.23 o 0 3 2 5040.78 5301.69 59.99 o 1 3 2 6236.00 6243.96 70.87 o 2 3 2 7819.03 8450.11 72.98 o 3 3 2 10630.92 10795.60 82.93 o 4 3 2 842.95 869.25 11.76 o 5 3 2 8958.31 9036.22 84.96 o 6 3 2 2903.23 2693.90 30.70 o 7 3 2 152.84 156.68 7.18 o 8 3 2 5571.93 5516.31 52.92 o 9 3 2 1960.64 1931.75 27.89 o 10 3 2 61.93 37.57 9.67 o 11 3 2 1873.62 1885.74 30.19 o 12 3 2 145.15 122.07 14.14 o 13 3 2 2022.30 1983.20 50.52 o 14 3 2 398.09 370.91 21.13 o 15 3 2 425.70 396.53 22.84 o -14 4 2 666.33 589.21 26.54 o -13 4 2 828.03 766.91 24.54 o -12 4 2 155.57 173.69 15.10 o -11 4 2 1464.67 1408.14 26.90 o -10 4 2 236.26 210.80 17.78 o -9 4 2 2881.74 2778.43 35.45 o -8 4 2 1900.64 1883.71 26.99 o -7 4 2 875.40 883.01 16.12 o -6 4 2 5470.73 5460.05 51.12 o -5 4 2 129.49 143.05 6.97 o -4 4 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