Crystallography Open Database

Information card for entry 2233290

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Structure parameters

Chemical name	Bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)bis{[2-(2<i>H</i>- benzotriazol-2-yl)-4,6-di-<i>tert</i>-pentylphenolato- κ^2^<i>N</i>,<i>O</i>]zinc}
Formula	C50 H74 N6 O4 Si2 Zn2
Calculated formula	C50 H74 N6 O4 Si2 Zn2
Title of publication	Bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)bis{[2-(2<i>H</i>-benzotriazol-2-yl)-4,6-di-<i>tert</i>-pentylphenolato-κ^2^<i>N</i>,<i>O</i>]zinc}
Authors of publication	Lee, Hwi Hyun; Go, Min Jeong; Park, Ka Hyun; Kim, Youngjo; Lee, Junseong
Journal of publication	Acta Crystallographica Section E
Year of publication	2012
Journal volume	68
Journal issue	1
Pages of publication	m87
a	10.764 ± 0.0004 Å
b	10.728 ± 0.0004 Å
c	23.2314 ± 0.0009 Å
α	90°
β	90.597 ± 0.002°
γ	90°
Cell volume	2682.53 ± 0.18 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0685
Residual factor for significantly intense reflections	0.0394
Weighted residual factors for significantly intense reflections	0.0896
Weighted residual factors for all reflections included in the refinement	0.1083
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181254 (current)	2016-04-03	hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/32.	2233290.cif 2233290.hkl
176798	2016-02-21	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23.	2233290.cif 2233290.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2233290.cif 2233290.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2233290.cif 2233290.hkl
34292	2012-02-14	hkl/ Adding Fobs data for the recently deposited IUCr structures.	2233290.cif 2233290.hkl
32353	2012-02-08	../uploads/cif-deposit/cod/cif Adding structures of 2233290 via cif-deposit CGI script.	2233290.cif