#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/32/2233298.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233298_Fobs loop_ _publ_author_name 'Gelbrich, Thomas' 'Rossi, Denise' 'Griesser, Ulrich J.' _publ_section_title ; Tetragonal polymorph of 5,5-dichlorobarbituric acid ; _journal_coeditor_code SU2351 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o235 _journal_page_last o236 _journal_volume 68 _journal_year 2012 _space_group_IT_number 114 _symmetry_space_group_name_Hall 'P -4 2n' _symmetry_space_group_name_H-M 'P -4 21 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.8883 _cell_length_b 13.8883 _cell_length_c 6.9126 _exptl_crystal_F_000 784.00 _reflns_d_resolution_high 0.8109 _[local]_cod_data_source_file su2351Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11thg013_1 in P -4 21 c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 168.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' '-y, x, -z' 'y, -x, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 1201.46 1185.67 25.10 o 1 2 0 2971.23 3022.07 36.40 o 2 2 0 488.52 487.40 9.22 o 1 3 0 1444.82 1554.00 15.89 o 2 3 0 3541.95 3579.86 28.47 o 3 3 0 28491.33 27912.50 505.12 o 0 4 0 1085.02 1013.63 14.02 o 1 4 0 6610.40 6474.80 46.24 o 2 4 0 14917.92 15062.91 87.51 o 3 4 0 11451.89 11428.44 107.99 o 4 4 0 9850.85 9603.79 107.80 o 1 5 0 17861.51 18289.54 112.90 o 2 5 0 1241.15 1346.03 12.93 o 3 5 0 2193.57 2263.24 18.20 o 4 5 0 460.42 442.68 7.04 o 5 5 0 5441.59 5163.05 55.24 o 0 6 0 25142.27 25872.91 217.18 o 1 6 0 2.77 11.02 2.58 o 2 6 0 1295.12 1289.17 14.60 o 3 6 0 1101.91 1177.90 12.36 o 4 6 0 1002.85 999.96 13.65 o 5 6 0 1182.35 1282.27 13.58 o 6 6 0 15030.17 14805.72 142.44 o 1 7 0 2050.01 2033.29 21.17 o 2 7 0 1306.07 1342.22 13.97 o 3 7 0 1019.94 1069.49 13.59 o 4 7 0 1239.76 1333.37 14.92 o 5 7 0 76.27 69.24 3.52 o 6 7 0 2407.57 2316.75 20.52 o 7 7 0 393.71 407.20 11.02 o 0 8 0 1469.15 1468.83 32.16 o 1 8 0 191.00 181.64 5.47 o 2 8 0 274.85 261.19 5.77 o 3 8 0 1791.79 1712.43 18.52 o 4 8 0 2.33 3.54 2.84 o 5 8 0 2.20 7.96 3.07 o 6 8 0 735.62 763.95 10.45 o 7 8 0 601.77 589.19 9.97 o 8 8 0 668.07 700.18 15.96 o 1 9 0 146.38 149.80 4.98 o 2 9 0 962.26 959.67 12.69 o 3 9 0 1415.13 1420.58 15.33 o 4 9 0 0.61 3.60 3.14 o 5 9 0 1172.69 1187.62 15.23 o 6 9 0 1020.71 998.42 13.39 o 7 9 0 665.53 680.29 12.24 o 8 9 0 3063.53 3069.72 30.43 o 9 9 0 5667.91 5526.35 68.44 o 0 10 0 656.87 668.05 15.02 o 1 10 0 260.68 265.33 7.17 o 2 10 0 1415.80 1381.00 15.95 o 3 10 0 1891.21 1922.48 19.30 o 4 10 0 4986.84 5006.56 40.87 o 5 10 0 144.99 152.82 6.21 o 6 10 0 69.03 74.46 6.02 o 7 10 0 13.47 18.22 3.84 o 8 10 0 616.38 608.63 13.57 o 9 10 0 1564.24 1496.23 22.70 o 10 10 0 342.39 391.90 20.81 o 1 11 0 2187.92 2187.83 25.30 o 2 11 0 532.29 513.56 9.48 o 3 11 0 6.88 11.56 3.15 o 4 11 0 1527.10 1504.54 17.72 o 5 11 0 5656.01 5634.10 49.53 o 6 11 0 74.93 73.41 5.04 o 7 11 0 972.23 952.11 18.66 o 8 11 0 56.22 53.68 6.82 o 9 11 0 272.15 288.86 14.54 o 10 11 0 117.12 136.80 10.77 o 11 11 0 1268.43 1295.35 63.39 o 0 12 0 2183.29 2231.79 36.06 o 1 12 0 205.04 193.76 6.43 o 2 12 0 1059.37 1041.76 17.18 o 3 12 0 87.79 88.42 5.81 o 4 12 0 132.14 123.34 6.28 o 5 12 0 405.02 378.96 8.28 o 6 12 0 37.13 37.61 4.98 o 7 12 0 157.77 129.96 9.55 o 8 12 0 584.39 589.65 23.15 o 9 12 0 560.96 512.62 20.74 o 10 12 0 958.67 934.84 34.11 o 11 12 0 963.67 1075.36 41.79 o 12 12 0 880.67 854.82 53.73 o 1 13 0 1.05 4.29 4.79 o 2 13 0 10.34 20.36 4.64 o 3 13 0 7.71 8.95 4.32 o 4 13 0 99.50 121.88 7.23 o 5 13 0 10.27 20.85 4.40 o 6 13 0 1264.48 1250.36 29.91 o 7 13 0 1663.97 1654.66 35.35 o 8 13 0 845.66 902.39 38.09 o 9 13 0 1376.37 1325.77 40.95 o 10 13 0 10.70 32.67 12.42 o 11 13 0 137.69 145.71 18.51 o 0 14 0 411.00 387.21 19.32 o 1 14 0 1.15 -2.58 5.16 o 2 14 0 205.60 158.63 11.79 o 3 14 0 240.70 250.75 14.80 o 4 14 0 12.10 11.74 6.29 o 5 14 0 0.12 -3.63 7.27 o 6 14 0 224.59 224.50 12.81 o 7 14 0 1382.80 1308.66 30.11 o 8 14 0 3.43 2.83 10.27 o 9 14 0 33.14 12.79 9.90 o 1 15 0 64.45 63.05 10.25 o 2 15 0 171.85 183.70 13.97 o 3 15 0 1594.22 1583.10 38.70 o 4 15 0 66.79 74.63 10.55 o 5 15 0 182.07 190.96 14.94 o 6 15 0 149.15 149.25 13.56 o 7 15 0 1044.78 1083.14 38.39 o 8 15 0 16.59 41.73 11.33 o 0 16 0 296.46 308.26 25.99 o 1 16 0 541.52 534.55 23.07 o 2 16 0 262.27 269.99 16.72 o 3 16 0 18.47 37.01 11.18 o 4 16 0 0.48 -3.15 9.57 o 5 16 0 738.20 711.71 31.30 o 6 16 0 259.68 279.69 21.04 o 1 17 0 513.40 504.56 26.19 o 2 17 0 330.50 319.20 21.05 o 0 1 1 946.97 917.34 14.34 o -1 2 1 9806.16 9747.62 70.53 o 0 2 1 1478.57 1471.39 17.12 o 1 2 1 9715.77 9666.67 96.80 o -2 3 1 1196.33 1180.44 14.96 o -1 3 1 420.75 391.72 7.73 o 0 3 1 4.32 6.58 4.69 o 1 3 1 418.66 383.08 7.98 o 2 3 1 1243.85 1212.33 13.52 o -3 4 1 11215.57 11276.17 92.83 o -2 4 1 2030.25 2072.41 20.33 o -1 4 1 4300.57 4484.12 53.29 o 0 4 1 99.28 120.38 6.40 o 1 4 1 4329.81 4427.43 47.40 o 2 4 1 2003.69 2071.80 19.34 o 3 4 1 11387.36 11238.93 72.66 o -4 5 1 132.90 157.53 5.47 o -3 5 1 1708.82 1907.53 26.12 o -2 5 1 2069.00 2081.66 18.29 o -1 5 1 52.92 59.82 5.02 o 0 5 1 4875.34 4828.99 43.05 o 1 5 1 53.36 69.19 3.72 o 2 5 1 2125.49 2071.98 22.99 o 3 5 1 1695.51 1916.37 17.88 o 4 5 1 136.49 144.15 4.27 o -5 6 1 2476.03 2418.06 31.12 o -4 6 1 566.34 549.01 10.75 o -3 6 1 2486.51 2438.84 22.01 o -2 6 1 170.16 170.98 4.36 o -1 6 1 5249.67 5440.01 44.32 o 0 6 1 2103.77 2271.52 24.39 o 1 6 1 5202.85 5208.06 49.37 o 2 6 1 174.53 177.60 5.58 o 3 6 1 2356.39 2302.14 24.99 o 4 6 1 575.94 576.87 8.71 o 5 6 1 2420.55 2380.50 21.05 o -6 7 1 2176.51 2135.49 25.16 o -5 7 1 83.26 80.57 5.41 o -4 7 1 1817.77 1867.07 23.87 o -3 7 1 121.28 138.84 4.70 o -2 7 1 2165.26 2215.57 22.27 o -1 7 1 541.26 593.54 10.29 o 0 7 1 662.89 644.39 11.88 o 1 7 1 530.44 563.02 9.17 o 2 7 1 2232.25 2200.22 25.31 o 3 7 1 123.41 148.82 6.39 o 4 7 1 1844.55 1817.82 19.21 o 5 7 1 91.03 99.56 4.33 o 6 7 1 2146.46 2169.65 20.72 o -7 8 1 2950.32 2905.08 33.73 o -6 8 1 116.87 125.18 7.40 o -5 8 1 3708.57 3638.52 40.42 o -4 8 1 1332.47 1341.96 18.02 o -3 8 1 152.55 161.95 7.14 o -2 8 1 446.65 426.76 9.75 o -1 8 1 4937.16 4878.72 37.90 o 0 8 1 4972.82 5206.61 57.04 o 1 8 1 4914.12 4805.10 38.77 o 2 8 1 433.40 396.80 8.53 o 3 8 1 154.31 163.04 5.66 o 4 8 1 1339.72 1335.50 14.38 o 5 8 1 3780.87 3661.45 29.34 o 6 8 1 105.94 109.25 4.83 o 7 8 1 2958.79 2916.11 25.79 o -8 9 1 397.07 401.13 13.33 o -7 9 1 917.42 943.87 16.60 o -6 9 1 1892.25 1911.47 28.29 o -5 9 1 253.98 259.09 7.37 o -4 9 1 3667.77 3645.86 34.81 o -3 9 1 377.74 378.68 7.92 o -2 9 1 3641.93 3744.52 42.63 o -1 9 1 70.42 66.20 3.08 o 0 9 1 1980.25 2030.42 27.31 o 1 9 1 71.76 69.26 4.51 o 2 9 1 3634.01 3699.76 31.44 o 3 9 1 371.47 396.42 8.65 o 4 9 1 3686.24 3578.99 30.28 o 5 9 1 263.17 250.99 6.90 o 6 9 1 1931.87 1922.38 22.04 o 7 9 1 932.27 897.53 13.52 o 8 9 1 387.89 374.65 9.17 o -9 10 1 1164.43 1230.18 21.89 o -8 10 1 523.38 528.02 11.27 o -7 10 1 631.74 624.95 12.68 o -6 10 1 611.26 613.60 11.37 o -5 10 1 341.51 342.05 7.99 o -4 10 1 331.49 333.43 7.88 o -3 10 1 7448.91 7259.58 59.38 o -2 10 1 886.28 885.90 13.06 o -1 10 1 1027.94 997.38 14.35 o 0 10 1 13.03 11.28 2.55 o 1 10 1 1029.39 1025.69 16.23 o 2 10 1 893.05 895.96 13.34 o 3 10 1 7476.19 7243.16 60.68 o 4 10 1 326.01 331.73 8.88 o 5 10 1 331.92 317.68 9.16 o 6 10 1 605.46 589.03 11.39 o 7 10 1 616.65 606.36 11.49 o 8 10 1 551.20 549.60 13.66 o 9 10 1 1173.96 1172.24 22.37 o -10 11 1 90.81 93.94 14.80 o -9 11 1 9.99 -5.56 11.12 o -8 11 1 406.97 437.03 12.09 o -7 11 1 1106.44 1134.06 23.96 o -6 11 1 978.19 1009.94 16.68 o -5 11 1 65.59 69.31 4.46 o -4 11 1 26.93 36.55 4.25 o -3 11 1 106.89 98.72 5.27 o -2 11 1 1113.00 1147.40 16.64 o -1 11 1 45.28 33.58 3.90 o 0 11 1 830.93 767.73 17.29 o 1 11 1 41.60 37.48 3.99 o 2 11 1 1139.74 1166.79 18.32 o 3 11 1 111.35 100.16 5.39 o 4 11 1 25.36 30.04 4.22 o 5 11 1 62.87 53.56 5.39 o 6 11 1 944.94 947.25 14.64 o 7 11 1 1100.33 1111.33 16.38 o 8 11 1 388.67 418.01 13.59 o 9 11 1 9.11 2.89 5.60 o 10 11 1 88.06 85.43 7.96 o -11 12 1 51.32 58.08 13.27 o -10 12 1 367.95 347.48 25.76 o -9 12 1 732.48 726.86 37.09 o -8 12 1 73.77 83.06 13.60 o -7 12 1 341.00 347.95 24.46 o -6 12 1 369.10 380.73 12.34 o -5 12 1 1104.24 1124.28 18.11 o -4 12 1 241.27 243.17 8.23 o -3 12 1 3040.77 3017.60 30.51 o -2 12 1 848.69 876.98 14.82 o -1 12 1 624.12 596.34 17.49 o 0 12 1 377.99 390.65 8.83 o 1 12 1 602.70 572.15 13.20 o 2 12 1 866.06 875.06 17.20 o 3 12 1 3104.58 3045.03 35.92 o 4 12 1 239.35 240.98 8.54 o 5 12 1 1105.79 1117.50 26.20 o 6 12 1 364.10 363.75 12.58 o 7 12 1 340.02 341.42 13.39 o 8 12 1 74.41 59.83 9.33 o 9 12 1 727.40 705.12 19.65 o 10 12 1 382.84 372.94 17.83 o 11 12 1 50.86 32.12 10.83 o -10 13 1 443.42 436.02 31.66 o -9 13 1 1.47 1.05 11.44 o -8 13 1 858.51 832.08 35.20 o -7 13 1 334.92 347.41 16.61 o -6 13 1 176.45 168.45 10.04 o -5 13 1 504.52 497.14 15.13 o -4 13 1 725.26 717.38 16.32 o -3 13 1 1111.84 1126.75 17.38 o -2 13 1 527.33 543.17 16.91 o -1 13 1 9.98 10.54 5.39 o 0 13 1 173.43 186.92 11.23 o 1 13 1 10.62 15.16 4.65 o 2 13 1 524.87 525.42 14.76 o 3 13 1 1121.69 1131.95 20.83 o 4 13 1 740.45 741.67 16.27 o 5 13 1 481.21 514.64 16.75 o 6 13 1 176.37 185.40 11.70 o 7 13 1 332.94 330.58 13.60 o 8 13 1 886.56 898.68 22.37 o 9 13 1 1.08 6.73 6.90 o 10 13 1 461.52 450.22 21.34 o -9 14 1 193.78 190.33 17.29 o -8 14 1 2.21 22.11 10.36 o -7 14 1 1301.89 1308.57 38.99 o -6 14 1 864.94 881.84 25.30 o -5 14 1 691.93 701.57 20.12 o -4 14 1 94.87 110.61 9.41 o -3 14 1 1.37 10.28 6.84 o -2 14 1 126.49 130.45 12.40 o -1 14 1 2844.69 2881.76 45.30 o 0 14 1 2131.19 2186.08 38.35 o 1 14 1 2745.21 2744.70 45.00 o 2 14 1 121.35 121.23 11.31 o 3 14 1 1.43 8.78 7.86 o 4 14 1 92.98 93.78 9.70 o 5 14 1 676.61 699.94 27.80 o 6 14 1 861.90 931.93 27.43 o 7 14 1 1307.90 1276.46 30.82 o 8 14 1 1.84 11.70 7.99 o 9 14 1 184.70 184.85 14.93 o -8 15 1 456.76 466.11 24.60 o -7 15 1 319.39 295.28 19.27 o -6 15 1 35.30 22.50 13.85 o -5 15 1 60.97 60.81 9.14 o -4 15 1 868.42 898.57 25.01 o -3 15 1 427.30 460.35 19.67 o -2 15 1 625.63 658.81 23.42 o -1 15 1 951.88 997.19 29.07 o 0 15 1 19.08 31.31 8.82 o 1 15 1 939.56 966.00 28.95 o 2 15 1 643.58 612.45 23.11 o 3 15 1 429.08 439.84 23.35 o 4 15 1 893.28 898.40 33.03 o 5 15 1 61.06 61.06 10.01 o 6 15 1 32.08 24.04 9.49 o 7 15 1 326.30 352.84 20.28 o 8 15 1 442.70 390.01 24.52 o -5 16 1 702.93 687.29 34.06 o -4 16 1 847.09 885.05 37.34 o -3 16 1 2019.36 2135.96 51.73 o -2 16 1 502.82 507.21 24.60 o -1 16 1 481.93 490.78 24.37 o 0 16 1 336.61 349.98 21.42 o 1 16 1 469.84 486.33 24.92 o 2 16 1 498.04 501.58 25.39 o 3 16 1 2030.17 2005.41 51.96 o 4 16 1 860.59 828.66 30.29 o 5 16 1 719.71 713.73 28.61 o 0 17 1 270.40 264.81 19.95 o 0 0 2 9458.83 8813.94 155.83 o -1 1 2 2556.56 2590.85 34.91 o 0 1 2 3349.98 3493.70 40.83 o 1 1 2 2497.38 2567.75 67.66 o -2 2 2 28101.16 28563.93 466.93 o -1 2 2 304.11 305.16 7.45 o 0 2 2 5993.26 5939.94 47.22 o 1 2 2 306.85 287.83 14.07 o 2 2 2 27968.24 28071.14 396.59 o -3 3 2 119.54 83.71 6.64 o -2 3 2 601.11 607.71 9.10 o -1 3 2 8305.07 8250.81 69.20 o 0 3 2 0.53 -1.13 3.66 o 1 3 2 8323.01 8222.54 66.99 o 2 3 2 592.61 604.44 14.67 o 3 3 2 110.39 96.78 8.28 o -4 4 2 6067.61 6034.65 69.42 o -3 4 2 271.06 321.31 7.39 o -2 4 2 13163.04 13293.10 98.29 o -1 4 2 882.49 879.17 12.74 o 0 4 2 2737.22 2579.43 27.44 o 1 4 2 896.60 892.22 12.34 o 2 4 2 13284.89 13359.73 96.59 o 3 4 2 258.08 324.63 8.62 o 4 4 2 5945.97 5846.15 73.75 o -5 5 2 3798.18 3923.71 55.52 o -4 5 2 1130.48 1224.20 15.28 o -3 5 2 524.51 526.96 9.15 o -2 5 2 268.53 272.78 6.66 o -1 5 2 243.01 243.50 6.53 o 0 5 2 0.30 1.64 4.40 o 1 5 2 263.27 258.48 7.81 o 2 5 2 268.58 281.55 6.64 o 3 5 2 490.76 504.28 9.85 o 4 5 2 1102.72 1175.65 15.76 o 5 5 2 3654.45 3825.73 50.29 o -6 6 2 4350.59 4333.93 82.82 o -5 6 2 942.56 951.36 12.25 o -4 6 2 762.24 815.99 12.01 o -3 6 2 98.13 95.58 3.28 o -2 6 2 2210.70 2321.31 22.62 o -1 6 2 3476.92 3755.05 36.14 o 0 6 2 6138.11 6087.38 61.44 o 1 6 2 3521.52 3794.86 35.41 o 2 6 2 2260.93 2331.28 25.58 o 3 6 2 93.22 95.83 3.82 o 4 6 2 742.91 782.27 13.15 o 5 6 2 959.77 952.67 13.71 o 6 6 2 4373.08 4285.85 55.35 o -7 7 2 2903.46 2898.26 42.10 o -6 7 2 143.69 130.98 6.57 o -5 7 2 393.20 415.55 10.02 o -4 7 2 1415.37 1381.25 18.07 o -3 7 2 9366.62 9649.13 69.79 o -2 7 2 394.81 391.91 14.35 o -1 7 2 2441.36 2513.14 31.56 o 0 7 2 413.61 442.59 8.31 o 1 7 2 2422.68 2426.37 25.03 o 2 7 2 403.50 434.10 10.01 o 3 7 2 9429.01 9743.63 92.01 o 4 7 2 1422.68 1392.06 17.12 o 5 7 2 389.21 387.08 8.01 o 6 7 2 140.54 130.39 5.82 o 7 7 2 2865.05 2874.64 61.61 o -8 8 2 513.59 517.36 19.53 o -7 8 2 229.43 226.59 9.55 o -6 8 2 173.77 173.55 8.86 o -5 8 2 360.31 335.53 10.00 o -4 8 2 2807.73 2773.68 26.10 o -3 8 2 348.77 378.89 8.50 o -2 8 2 2704.92 2605.69 30.89 o -1 8 2 252.92 273.41 8.30 o 0 8 2 515.96 515.28 10.62 o 1 8 2 268.24 284.64 7.74 o 2 8 2 2749.48 2668.58 31.25 o 3 8 2 332.84 352.44 7.49 o 4 8 2 2757.84 2709.61 28.25 o 5 8 2 360.57 336.69 8.86 o 6 8 2 171.84 180.34 6.60 o 7 8 2 225.46 224.18 8.11 o 8 8 2 501.46 541.48 15.95 o -9 9 2 1415.05 1357.25 41.58 o -8 9 2 433.05 386.97 14.60 o -7 9 2 2175.32 2090.88 31.37 o -6 9 2 275.75 270.50 10.12 o -5 9 2 348.45 328.08 8.66 o -4 9 2 512.13 517.70 9.93 o -3 9 2 800.35 803.52 12.54 o -2 9 2 2459.16 2519.34 26.46 o -1 9 2 1096.77 1033.67 16.05 o 0 9 2 147.40 150.44 6.25 o 1 9 2 1086.99 1042.72 14.90 o 2 9 2 2430.51 2494.97 30.39 o 3 9 2 790.64 799.52 14.53 o 4 9 2 520.67 526.23 10.92 o 5 9 2 335.22 327.11 8.51 o 6 9 2 268.02 263.33 8.38 o 7 9 2 2165.00 2062.48 28.69 o 8 9 2 413.97 391.69 10.59 o 9 9 2 1396.37 1414.24 30.01 o -10 10 2 393.36 358.79 53.90 o -9 10 2 292.28 301.25 16.82 o -8 10 2 368.49 350.22 15.26 o -7 10 2 950.81 917.74 24.12 o -6 10 2 752.30 782.70 20.93 o -5 10 2 248.59 248.93 7.57 o -4 10 2 590.76 609.18 13.34 o -3 10 2 60.11 61.11 6.40 o -2 10 2 405.34 389.02 11.07 o -1 10 2 30.95 25.55 4.51 o 0 10 2 0.64 3.50 4.78 o 1 10 2 32.28 30.26 5.62 o 2 10 2 383.49 365.89 11.88 o 3 10 2 66.42 66.59 4.60 o 4 10 2 587.62 587.41 12.47 o 5 10 2 248.81 253.45 8.12 o 6 10 2 737.92 712.65 16.35 o 7 10 2 946.76 944.86 16.73 o 8 10 2 380.20 369.76 11.84 o 9 10 2 286.80 286.48 11.97 o 10 10 2 394.90 397.61 21.18 o -11 11 2 1094.07 1064.77 60.85 o -10 11 2 379.92 364.33 37.39 o -9 11 2 406.12 404.35 29.04 o -8 11 2 387.18 380.63 19.85 o -7 11 2 237.61 239.93 12.69 o -6 11 2 273.68 263.33 10.81 o -5 11 2 1996.55 1916.10 35.01 o -4 11 2 234.79 243.10 10.20 o -3 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