#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/33/2233310.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233310_Fobs loop_ _publ_author_name 'Wang, Shen-Tang' 'Che, Guang-Bo' 'Liu, Chun-Bo' 'Wang, Xing' 'Liu, Ling' _publ_section_title ; Bis(1,10-phenanthroline-5,6-dione-\k^2^N,N')silver(I) 2-hydroxy-3,5-dinitrobenzoate ; _journal_coeditor_code VN2025 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m76 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.912 _cell_angle_gamma 90.000 _cell_length_a 11.7569 _cell_length_b 18.2974 _cell_length_c 13.2230 _exptl_crystal_F_000 1512.00 _reflns_d_resolution_high 0.8293 _[local]_cod_data_source_file vn2025Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelxl in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 311.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4366.62 3464.31 92.61 o 3 0 0 178.98 141.77 69.70 o 4 0 0 14187.04 12831.03 116.86 o 5 0 0 20880.09 19129.79 439.21 o 6 0 0 3220.44 3248.68 161.40 o 7 0 0 6610.64 6346.78 149.81 o 8 0 0 27.88 61.46 50.09 o 9 0 0 83.41 97.97 62.07 o 10 0 0 5425.13 5905.52 439.14 o 11 0 0 1173.69 1098.43 324.59 o 12 0 0 583.33 522.57 200.75 o 13 0 0 1.20 -5.35 29.53 o 2 1 0 353.82 122.25 18.02 o 3 1 0 4412.20 3841.96 86.34 o 4 1 0 1864.20 2036.38 114.13 o 5 1 0 11810.45 12046.10 149.24 o 6 1 0 304.54 448.72 44.41 o 7 1 0 652.03 651.39 72.49 o 8 1 0 7.84 79.76 25.56 o 9 1 0 1036.11 970.71 168.64 o 10 1 0 701.42 615.05 104.85 o 11 1 0 568.71 561.43 141.51 o 12 1 0 3.01 131.25 131.07 o 13 1 0 30.82 97.08 48.15 o 2 2 0 17161.15 16864.39 163.84 o 3 2 0 8719.95 7993.04 104.53 o 4 2 0 8551.18 7249.02 76.28 o 5 2 0 616.49 1132.73 98.25 o 6 2 0 163.26 162.10 39.96 o 7 2 0 2081.34 2337.73 100.80 o 8 2 0 308.12 235.75 28.72 o 9 2 0 1021.48 880.23 161.85 o 10 2 0 2026.41 2117.19 264.79 o 11 2 0 32.86 152.05 53.04 o 12 2 0 221.73 211.68 56.43 o 13 2 0 29.54 50.63 33.76 o 1 3 0 11953.55 10675.39 121.72 o 2 3 0 707.19 1100.63 46.64 o 3 3 0 5247.41 5458.15 102.43 o 4 3 0 10253.02 9181.84 103.65 o 5 3 0 3386.40 3232.90 86.42 o 6 3 0 9415.95 9143.14 122.66 o 7 3 0 12.21 80.95 30.79 o 8 3 0 5700.38 5843.48 134.42 o 9 3 0 2310.22 2518.36 204.56 o 10 3 0 1244.81 1295.22 190.06 o 11 3 0 1692.15 1538.62 325.15 o 12 3 0 5.22 95.94 42.14 o 13 3 0 398.30 186.36 59.53 o 0 4 0 11154.43 10959.33 189.15 o 1 4 0 6420.80 5887.88 116.20 o 2 4 0 171.21 158.75 34.24 o 3 4 0 68.51 33.73 15.59 o 4 4 0 8194.59 8167.33 106.79 o 5 4 0 5578.09 6058.84 196.61 o 6 4 0 90.69 71.51 21.33 o 7 4 0 105.70 123.93 26.20 o 8 4 0 256.75 254.57 35.68 o 9 4 0 8.18 83.60 33.44 o 10 4 0 5.95 95.16 37.18 o 11 4 0 18.17 68.50 53.64 o 12 4 0 15.11 59.71 39.53 o 13 4 0 1.82 57.28 80.51 o 1 5 0 19659.75 16973.23 79.61 o 2 5 0 6525.20 6924.94 55.85 o 3 5 0 9280.62 8196.23 100.83 o 4 5 0 10047.64 10726.61 182.38 o 5 5 0 1271.54 1674.09 72.82 o 6 5 0 11825.07 11300.73 207.02 o 7 5 0 293.50 359.71 43.09 o 8 5 0 5518.49 5618.57 124.76 o 9 5 0 1252.18 1351.88 113.12 o 10 5 0 1169.73 1376.30 117.52 o 11 5 0 947.57 868.74 150.55 o 12 5 0 105.71 146.28 46.99 o 13 5 0 533.03 571.86 113.84 o 0 6 0 727.14 1089.15 92.90 o 1 6 0 9309.00 8540.56 59.02 o 2 6 0 7362.40 7850.31 72.85 o 3 6 0 23487.37 22723.35 253.12 o 4 6 0 298.87 313.19 40.30 o 5 6 0 4545.53 4379.75 79.65 o 6 6 0 4.01 71.84 25.03 o 7 6 0 5676.69 5756.99 106.79 o 8 6 0 1668.08 1755.52 129.05 o 9 6 0 980.41 1098.20 114.06 o 10 6 0 254.94 346.56 64.96 o 11 6 0 16.80 152.39 80.66 o 12 6 0 212.56 408.98 67.78 o 13 6 0 1.91 60.51 35.61 o 1 7 0 1999.18 2358.86 55.60 o 2 7 0 293.28 650.46 48.08 o 3 7 0 542.36 598.60 63.09 o 4 7 0 6682.82 5789.19 112.66 o 5 7 0 164.14 108.28 23.22 o 6 7 0 127.12 172.38 25.19 o 7 7 0 840.88 883.77 86.05 o 8 7 0 503.41 556.87 82.07 o 9 7 0 3075.17 3488.42 216.45 o 10 7 0 620.47 646.67 214.80 o 11 7 0 130.15 281.67 81.20 o 12 7 0 0.32 82.27 34.95 o 13 7 0 11.92 74.40 34.35 o 0 8 0 66913.72 66894.49 370.01 o 1 8 0 14.90 48.86 16.18 o 2 8 0 16704.67 15148.14 180.82 o 3 8 0 725.82 835.16 67.86 o 4 8 0 129.37 166.67 23.79 o 5 8 0 7668.26 7785.83 160.53 o 6 8 0 580.37 581.93 64.99 o 7 8 0 3600.70 3991.34 220.82 o 8 8 0 483.10 285.32 77.84 o 9 8 0 1345.98 1418.68 149.27 o 10 8 0 1509.94 1286.71 192.84 o 11 8 0 182.40 223.36 55.69 o 12 8 0 777.63 600.56 136.59 o 1 9 0 90.63 112.92 18.94 o 2 9 0 456.77 756.22 55.53 o 3 9 0 981.97 1071.45 81.08 o 4 9 0 800.92 566.97 62.15 o 5 9 0 86.52 76.21 37.63 o 6 9 0 12.93 44.05 22.06 o 7 9 0 371.36 453.55 45.92 o 8 9 0 172.41 142.82 48.89 o 9 9 0 1188.61 1210.72 189.00 o 10 9 0 19.48 72.02 40.15 o 11 9 0 120.90 142.00 66.60 o 12 9 0 7.75 96.08 40.05 o 0 10 0 3504.60 3072.06 204.01 o 1 10 0 4802.89 5201.89 78.38 o 2 10 0 1678.29 1957.95 62.40 o 3 10 0 587.01 523.94 52.71 o 4 10 0 3228.43 3053.80 72.19 o 5 10 0 1806.79 1710.68 87.05 o 6 10 0 109.30 178.71 23.41 o 7 10 0 1574.62 1444.31 280.54 o 8 10 0 403.39 287.76 60.78 o 9 10 0 1303.85 1374.02 233.84 o 10 10 0 27.07 85.16 56.67 o 11 10 0 582.13 599.34 144.79 o 12 10 0 603.55 472.29 109.92 o 1 11 0 7079.24 6851.91 131.08 o 2 11 0 1493.46 1419.03 70.49 o 3 11 0 1373.91 1346.48 61.05 o 4 11 0 1344.07 1744.57 74.64 o 5 11 0 1083.12 1242.47 102.00 o 6 11 0 3388.08 3609.74 143.19 o 7 11 0 846.84 918.23 158.90 o 8 11 0 1245.54 1315.62 97.23 o 9 11 0 624.48 437.17 90.15 o 10 11 0 71.15 102.24 41.29 o 11 11 0 239.40 303.04 68.77 o 0 12 0 202.40 270.88 75.16 o 1 12 0 430.80 445.37 43.50 o 2 12 0 106.76 115.82 20.36 o 3 12 0 388.04 342.90 34.79 o 4 12 0 415.64 440.94 44.82 o 5 12 0 924.13 817.80 80.44 o 6 12 0 31.59 62.22 37.26 o 7 12 0 120.41 137.78 153.36 o 8 12 0 119.22 121.39 47.10 o 9 12 0 212.46 254.02 66.28 o 10 12 0 34.86 102.16 74.20 o 11 12 0 81.44 85.10 40.61 o 1 13 0 2276.98 2502.98 111.51 o 2 13 0 1096.98 1217.57 116.93 o 3 13 0 3004.13 3161.99 87.99 o 4 13 0 1914.80 1429.28 160.11 o 5 13 0 14.34 41.31 20.60 o 6 13 0 2891.31 2784.11 298.34 o 7 13 0 56.71 43.98 37.25 o 8 13 0 1264.20 1505.10 313.63 o 9 13 0 500.54 429.44 92.42 o 10 13 0 228.44 245.99 79.61 o 11 13 0 360.27 257.25 62.14 o 0 14 0 920.23 1219.40 183.32 o 1 14 0 2160.92 2317.36 110.13 o 2 14 0 786.96 679.85 67.40 o 3 14 0 625.98 704.20 89.11 o 4 14 0 607.00 517.15 59.00 o 5 14 0 623.87 668.22 109.70 o 6 14 0 430.82 327.17 65.10 o 7 14 0 701.29 665.83 119.93 o 8 14 0 123.08 148.10 55.64 o 9 14 0 45.35 91.61 45.09 o 10 14 0 65.25 94.59 43.73 o 1 15 0 1089.33 979.02 102.34 o 2 15 0 25.06 61.55 18.31 o 3 15 0 261.91 233.84 37.03 o 4 15 0 382.01 488.61 133.18 o 5 15 0 1329.21 1381.55 198.30 o 6 15 0 149.07 126.69 33.62 o 7 15 0 151.79 141.14 32.78 o 8 15 0 450.00 359.44 95.03 o 9 15 0 123.76 62.66 58.67 o 10 15 0 14.91 61.81 46.73 o 0 16 0 5437.24 5446.71 346.53 o 1 16 0 2.26 49.17 25.20 o 2 16 0 1584.79 1993.95 179.44 o 3 16 0 192.48 106.15 61.37 o 4 16 0 646.03 571.32 106.40 o 5 16 0 2925.18 2695.08 276.37 o 6 16 0 43.76 60.46 64.69 o 7 16 0 15.61 63.26 60.31 o 8 16 0 5.17 79.61 43.16 o 9 16 0 698.46 612.35 134.14 o 1 17 0 38.51 96.31 43.25 o 2 17 0 61.39 49.55 29.52 o 3 17 0 0.14 71.74 32.69 o 4 17 0 0.52 83.73 38.36 o 5 17 0 36.63 79.27 78.47 o 6 17 0 118.37 129.37 35.72 o 7 17 0 225.14 183.79 120.42 o 8 17 0 115.44 136.23 52.71 o 0 18 0 163.91 140.62 35.42 o 1 18 0 45.18 104.48 40.61 o 2 18 0 1036.26 1292.30 216.18 o 3 18 0 474.16 662.90 133.99 o 4 18 0 659.36 513.00 112.75 o 5 18 0 675.84 561.13 96.20 o 6 18 0 91.54 68.72 33.96 o 7 18 0 65.95 49.16 40.86 o 1 19 0 453.67 424.77 58.51 o 2 19 0 24.24 52.38 23.33 o 3 19 0 320.62 300.77 88.85 o 4 19 0 203.37 154.02 36.01 o 5 19 0 5.55 76.72 54.73 o 6 19 0 622.25 427.07 166.33 o 0 20 0 286.10 349.41 130.88 o 1 20 0 2.93 7.18 19.47 o 2 20 0 42.21 42.90 41.80 o 3 20 0 0.86 87.00 39.31 o 4 20 0 123.23 84.80 27.38 o 5 20 0 93.37 134.54 46.54 o 1 21 0 316.33 374.94 82.34 o 2 21 0 122.99 133.46 40.65 o 3 21 0 535.69 523.90 143.52 o 4 21 0 309.93 398.41 111.60 o 0 22 0 14.84 34.38 49.46 o -13 1 1 58.09 37.11 34.00 o -12 1 1 1115.24 841.52 214.52 o -11 1 1 107.04 160.48 60.21 o -10 1 1 1615.58 1419.71 246.08 o -9 1 1 3054.76 3708.80 147.21 o -8 1 1 1368.88 1494.38 87.59 o -7 1 1 4118.03 4260.21 127.01 o -6 1 1 4096.91 4036.67 77.22 o -5 1 1 6640.60 5893.41 163.94 o -4 1 1 10841.71 10950.22 135.89 o -3 1 1 59199.80 59815.70 175.53 o -2 1 1 11800.71 10515.56 118.15 o 2 1 1 2528.79 2121.92 65.09 o 3 1 1 2534.86 2425.44 65.93 o 4 1 1 1407.41 1295.79 49.20 o 5 1 1 7581.55 6760.75 156.34 o 6 1 1 505.25 614.19 63.87 o 7 1 1 9392.02 9640.89 149.39 o 8 1 1 1434.09 1537.10 85.18 o 10 1 1 225.36 219.82 53.62 o 11 1 1 1705.51 2076.68 442.45 o 12 1 1 349.58 330.07 97.31 o 13 1 1 142.32 107.41 52.74 o -13 2 1 177.54 199.65 59.00 o -12 2 1 10.53 80.18 60.37 o -11 2 1 2222.93 2383.48 304.70 o -10 2 1 131.41 253.20 59.06 o -9 2 1 1683.12 1796.41 100.97 o -8 2 1 3113.58 3094.19 121.29 o -7 2 1 825.64 790.20 69.85 o -6 2 1 3190.96 3352.09 87.46 o -5 2 1 4065.46 4034.99 99.69 o -4 2 1 41969.55 41043.73 263.93 o -3 2 1 36555.30 38081.07 309.39 o -2 2 1 1329.12 1209.58 68.57 o 2 2 1 143.45 148.76 18.61 o 3 2 1 7186.49 6765.34 94.96 o 4 2 1 2975.93 3185.81 187.70 o 5 2 1 7430.77 6974.06 121.57 o 6 2 1 2808.41 2675.98 77.75 o 7 2 1 8.19 63.99 31.72 o 8 2 1 3195.54 3539.52 127.15 o 9 2 1 872.49 922.98 140.78 o 10 2 1 522.21 576.29 108.24 o 11 2 1 595.69 409.37 112.82 o 12 2 1 22.72 28.93 44.18 o 13 2 1 122.14 150.39 57.96 o -13 3 1 35.37 84.52 44.80 o -12 3 1 350.22 327.23 88.06 o -11 3 1 137.83 248.94 123.67 o -10 3 1 84.68 155.17 51.04 o -9 3 1 306.88 352.02 61.58 o -8 3 1 480.65 681.76 55.05 o -7 3 1 3355.51 3324.25 131.40 o -6 3 1 1315.08 1457.69 73.26 o -5 3 1 8418.05 7139.58 186.62 o -4 3 1 3687.36 3702.75 105.78 o -3 3 1 14141.80 13730.09 292.13 o -2 3 1 6921.75 7208.77 48.42 o -1 3 1 812.29 681.31 25.90 o 0 3 1 412.58 329.47 29.98 o 1 3 1 1.89 31.79 12.89 o 2 3 1 145.62 111.10 19.48 o 3 3 1 1588.47 1236.29 44.91 o 4 3 1 150.90 186.99 34.22 o 5 3 1 3442.07 3764.67 77.84 o 6 3 1 78.22 142.94 27.54 o 7 3 1 2471.90 2399.12 75.34 o 8 3 1 2.96 27.46 26.32 o 9 3 1 1551.92 1979.06 261.24 o 10 3 1 94.94 112.10 48.25 o 11 3 1 81.70 110.45 39.43 o 12 3 1 28.42 56.69 40.27 o 13 3 1 66.29 37.01 47.84 o -13 4 1 267.43 210.45 121.46 o -12 4 1 45.24 148.95 108.17 o -11 4 1 1535.36 1191.77 236.32 o -10 4 1 257.00 338.92 60.85 o -9 4 1 2297.14 2110.04 267.53 o -8 4 1 2270.43 2506.67 139.99 o -7 4 1 207.27 381.53 39.74 o -6 4 1 15588.09 16122.21 278.41 o -5 4 1 188.67 273.85 66.99 o -4 4 1 8314.85 8732.79 124.28 o -3 4 1 3909.77 3083.02 95.65 o -2 4 1 13646.97 12196.09 150.14 o -1 4 1 68298.59 66796.39 124.45 o 0 4 1 1388.29 1362.49 34.34 o 1 4 1 12727.61 11746.08 60.14 o 2 4 1 544.48 556.71 28.71 o 3 4 1 9204.26 9621.99 98.90 o 4 4 1 16725.25 15712.37 202.11 o 5 4 1 7086.08 7503.72 184.89 o 6 4 1 13333.13 13221.15 231.82 o 7 4 1 60.34 107.36 26.92 o 8 4 1 4168.27 4160.12 99.15 o 9 4 1 968.46 888.13 187.47 o 10 4 1 894.40 1087.19 207.37 o 11 4 1 1131.47 1531.65 285.72 o 12 4 1 23.09 117.98 52.00 o 13 4 1 471.05 255.37 124.65 o -13 5 1 37.86 139.63 58.52 o -12 5 1 116.25 178.27 122.48 o -11 5 1 13.81 30.56 30.85 o -10 5 1 264.19 513.98 83.48 o -9 5 1 184.80 110.56 23.58 o -8 5 1 135.59 179.78 31.61 o -7 5 1 290.43 272.48 37.98 o -6 5 1 1327.05 1290.27 112.86 o -5 5 1 98.53 173.86 27.93 o -4 5 1 28.22 38.04 15.84 o -3 5 1 4891.24 4617.51 102.29 o -2 5 1 2427.83 2783.39 68.85 o -1 5 1 1461.56 1395.71 41.09 o 0 5 1 105.63 267.90 29.49 o 1 5 1 47.26 53.87 17.76 o 2 5 1 4186.10 3835.84 99.45 o 3 5 1 2.30 100.30 13.49 o 4 5 1 11568.00 11527.66 148.12 o 5 5 1 667.31 747.15 76.59 o 6 5 1 83.95 223.03 36.93 o 7 5 1 140.52 272.38 42.77 o 8 5 1 48.09 133.39 33.52 o 9 5 1 75.31 63.56 108.59 o 10 5 1 10.72 81.59 28.43 o 11 5 1 19.65 62.00 68.45 o 12 5 1 3.92 95.79 44.19 o 13 5 1 1.79 58.36 40.28 o -13 6 1 126.44 309.52 114.71 o -12 6 1 19.15 79.82 41.18 o -11 6 1 586.95 682.91 161.62 o -10 6 1 2106.02 2141.89 131.83 o -9 6 1 1567.63 1637.94 115.47 o -8 6 1 639.44 595.54 60.54 o -7 6 1 216.92 200.29 32.18 o -6 6 1 3655.58 3124.27 76.20 o -5 6 1 1516.79 1654.65 81.60 o -4 6 1 14509.35 14855.64 189.54 o -3 6 1 6584.48 6668.63 104.63 o -2 6 1 7533.18 6583.59 101.50 o -1 6 1 2946.21 2648.78 77.97 o 0 6 1 159.77 90.74 19.58 o 1 6 1 20136.86 19315.59 85.08 o 2 6 1 557.08 556.27 37.39 o 3 6 1 4582.91 3928.09 89.48 o 4 6 1 3278.56 2831.54 99.30 o 5 6 1 2414.89 2459.26 104.46 o 6 6 1 4764.71 5162.58 97.32 o 7 6 1 148.94 237.63 35.72 o 8 6 1 1548.20 1446.98 152.07 o 9 6 1 624.79 413.09 79.74 o 10 6 1 731.72 878.20 126.17 o 11 6 1 395.44 394.27 77.25 o 12 6 1 1.58 87.22 36.15 o -13 7 1 45.74 71.50 34.60 o -12 7 1 770.37 593.07 105.01 o -11 7 1 26.81 198.92 75.30 o -10 7 1 1186.12 1043.45 161.48 o -9 7 1 656.86 815.42 161.12 o -8 7 1 561.17 505.65 53.10 o -7 7 1 5170.94 5444.34 132.29 o -6 7 1 33.09 68.08 23.13 o -5 7 1 2879.81 3136.72 74.74 o -4 7 1 148.56 254.54 28.80 o -3 7 1 6548.59 6250.95 192.45 o -2 7 1 6245.74 6466.64 95.43 o -1 7 1 4114.43 3943.19 86.69 o 0 7 1 27958.79 28074.61 112.11 o 1 7 1 1983.03 2241.31 56.65 o 2 7 1 3925.85 4116.59 149.47 o 3 7 1 1602.93 1914.87 80.52 o 4 7 1 6531.03 6327.34 220.23 o 5 7 1 6630.97 6535.68 124.84 o 6 7 1 893.32 1014.00 97.09 o 7 7 1 2366.70 2029.14 99.82 o 8 7 1 49.54 47.83 42.77 o 9 7 1 2908.95 2487.11 324.24 o 10 7 1 392.21 773.83 92.75 o 11 7 1 127.31 191.88 62.43 o 12 7 1 170.61 67.14 68.98 o -12 8 1 68.94 226.28 54.53 o -11 8 1 6.15 118.79 63.87 o -10 8 1 465.72 592.02 110.21 o -9 8 1 105.65 96.48 45.65 o -8 8 1 1.70 41.32 65.85 o -7 8 1 1373.88 1402.89 118.83 o -6 8 1 294.55 229.19 37.87 o -5 8 1 54.31 121.36 32.54 o -4 8 1 105.18 121.50 39.23 o -3 8 1 1196.64 1063.80 49.94 o -2 8 1 1818.14 1948.79 64.08 o -1 8 1 550.11 859.67 63.03 o 0 8 1 75.65 120.86 22.91 o 1 8 1 4109.86 3965.69 88.04 o 2 8 1 17.95 28.83 12.12 o 3 8 1 2091.02 2119.90 88.89 o 4 8 1 0.05 36.37 18.40 o 5 8 1 285.09 291.53 47.44 o 6 8 1 6.90 83.77 21.75 o 7 8 1 744.35 628.44 71.02 o 8 8 1 176.81 248.20 71.81 o 9 8 1 178.40 199.24 48.57 o 10 8 1 19.40 138.51 76.62 o 11 8 1 13.20 89.87 47.01 o 12 8 1 28.69 125.76 49.24 o -12 9 1 715.97 542.69 129.55 o -11 9 1 150.29 88.72 51.46 o -10 9 1 1343.76 1344.31 316.89 o -9 9 1 669.96 609.46 108.52 o -8 9 1 79.04 70.71 19.66 o -7 9 1 3597.63 3316.22 226.71 o -6 9 1 70.66 138.54 23.67 o -5 9 1 4762.71 4593.41 92.59 o -4 9 1 38.59 17.34 24.70 o -3 9 1 2306.82 2190.00 86.25 o -2 9 1 14773.63 15196.67 291.38 o -1 9 1 2946.80 3468.61 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