#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/33/2233339.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233339_Fobs loop_ _publ_author_name 'Sunitha, K.' 'Devarajegowda, H. C.' 'Al-eryani, Waleed Fadl Ali' 'Prasad, Y. Rajendra' 'Kumar, A. Uma Mahesh' _publ_section_title ; (2E)-1-(5-Bromothiophen-2-yl)-3-(2,3,4-trimethoxyphenyl)prop-2-en-1-one ; _journal_coeditor_code ZJ2039 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o61 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.813 _cell_angle_gamma 90.000 _cell_length_a 8.1140 _cell_length_b 12.7750 _cell_length_c 15.4040 _exptl_crystal_F_000 776.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file zj2039Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' VSBCHALCONE_r in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 300.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 79.17 54.46 2.94 o 2 0 0 128.33 178.49 7.34 o 3 0 0 130.13 110.13 7.97 o 4 0 0 3924.68 4097.55 53.29 o 5 0 0 2.54 1.03 6.04 o 6 0 0 1564.84 1516.24 44.73 o 7 0 0 347.14 357.85 32.58 o 8 0 0 1017.71 1095.24 71.76 o 9 0 0 236.75 180.46 29.82 o 1 1 0 469.07 507.66 5.64 o 2 1 0 1181.12 1216.31 14.63 o 3 1 0 51.22 44.59 3.37 o 4 1 0 1146.94 1074.24 16.88 o 5 1 0 244.06 221.42 10.79 o 6 1 0 154.46 175.67 10.50 o 7 1 0 257.06 242.58 21.39 o 8 1 0 78.53 65.38 13.74 o 9 1 0 11.59 18.23 11.72 o 0 2 0 2201.40 2160.28 42.34 o 1 2 0 708.98 776.61 7.58 o 2 2 0 90313.37 75260.39 333.30 o 3 2 0 37.35 65.79 4.10 o 4 2 0 601.70 531.57 13.82 o 5 2 0 895.74 884.18 20.07 o 6 2 0 2005.66 1957.35 27.72 o 7 2 0 236.05 238.20 18.60 o 8 2 0 414.30 505.50 28.22 o 9 2 0 1.93 8.51 11.54 o 1 3 0 3809.90 4094.57 33.06 o 2 3 0 61.17 52.62 3.20 o 3 3 0 448.94 420.98 11.53 o 4 3 0 564.18 609.01 14.40 o 5 3 0 155.63 162.62 9.74 o 6 3 0 647.12 640.56 19.79 o 7 3 0 214.01 217.71 16.10 o 8 3 0 0.10 0.00 12.46 o 9 3 0 26.46 17.70 12.86 o 0 4 0 14944.49 14145.11 114.91 o 1 4 0 10.90 23.83 2.39 o 2 4 0 5040.86 4757.80 36.00 o 3 4 0 7660.97 8288.41 65.32 o 4 4 0 17155.49 16577.27 80.64 o 5 4 0 1474.55 1488.62 22.58 o 6 4 0 317.31 311.30 14.67 o 7 4 0 111.98 102.14 12.38 o 8 4 0 270.17 272.04 21.21 o 9 4 0 48.68 43.83 13.74 o 1 5 0 865.23 993.35 19.65 o 2 5 0 338.11 379.47 10.60 o 3 5 0 933.65 1050.26 20.74 o 4 5 0 27.86 37.01 5.03 o 5 5 0 155.78 146.74 9.11 o 6 5 0 54.42 47.28 6.10 o 7 5 0 87.91 85.41 11.72 o 8 5 0 9.69 8.84 14.30 o 9 5 0 0.71 5.10 16.81 o 0 6 0 3268.75 3274.44 88.85 o 1 6 0 5432.23 5938.35 52.76 o 2 6 0 8543.62 8450.94 69.30 o 3 6 0 18.14 21.87 3.93 o 4 6 0 2356.86 2271.33 37.15 o 5 6 0 65.66 70.36 7.69 o 6 6 0 1945.94 1852.76 38.30 o 7 6 0 73.11 34.55 9.29 o 8 6 0 118.05 128.45 17.26 o 1 7 0 247.25 291.50 10.91 o 2 7 0 669.23 802.79 16.35 o 3 7 0 1592.42 1544.14 26.27 o 4 7 0 12.89 10.17 4.68 o 5 7 0 635.81 647.23 22.19 o 6 7 0 374.99 388.49 18.99 o 7 7 0 11.75 14.83 10.88 o 8 7 0 87.11 79.60 19.61 o 0 8 0 11641.70 11904.28 117.30 o 1 8 0 737.88 766.73 16.78 o 2 8 0 1864.95 1925.11 26.16 o 3 8 0 233.65 226.94 10.78 o 4 8 0 1332.80 1319.22 30.50 o 5 8 0 49.35 54.87 9.06 o 6 8 0 577.64 550.00 27.40 o 7 8 0 151.13 178.54 30.34 o 8 8 0 560.78 536.05 41.89 o 1 9 0 201.92 192.87 15.01 o 2 9 0 15.70 11.52 4.11 o 3 9 0 1745.70 1727.09 36.74 o 4 9 0 53.67 35.78 6.35 o 5 9 0 124.60 107.46 11.90 o 6 9 0 2.44 12.42 10.61 o 7 9 0 36.07 34.04 19.31 o 0 10 0 3903.55 4057.62 124.94 o 1 10 0 877.44 888.92 37.74 o 2 10 0 2667.73 2884.82 90.54 o 3 10 0 254.49 262.57 13.78 o 4 10 0 365.50 332.59 24.33 o 5 10 0 303.86 314.33 24.20 o 6 10 0 679.03 667.82 39.98 o 7 10 0 4.59 0.00 19.95 o 1 11 0 1297.24 1280.79 64.29 o 2 11 0 563.93 540.80 28.89 o 3 11 0 7.34 8.92 8.90 o 4 11 0 1.06 3.11 9.52 o 5 11 0 302.11 259.10 31.30 o 6 11 0 278.30 254.51 36.55 o 0 12 0 441.54 500.77 97.40 o 1 12 0 3.59 8.60 17.20 o 2 12 0 1625.45 1667.42 82.57 o 3 12 0 15.96 25.03 13.01 o 4 12 0 1020.62 1014.73 45.12 o 5 12 0 65.19 44.30 14.48 o 1 13 0 649.14 650.42 41.55 o 2 13 0 63.99 62.45 16.57 o 3 13 0 66.59 98.13 21.63 o 4 13 0 25.37 26.14 16.48 o 0 14 0 306.96 318.01 43.72 o 1 14 0 144.83 121.71 20.13 o 2 14 0 213.32 254.07 29.79 o 3 14 0 0.27 22.35 15.45 o 1 15 0 5.74 0.00 15.44 o -9 1 1 11.84 8.46 11.34 o -8 1 1 342.86 320.26 25.67 o -7 1 1 1397.57 1436.32 32.56 o -6 1 1 408.66 370.36 16.03 o -5 1 1 5037.35 4952.02 52.73 o -4 1 1 166.76 185.10 7.79 o -3 1 1 1925.28 1780.72 22.40 o -2 1 1 2890.21 3039.60 29.94 o -1 1 1 713.12 692.59 7.90 o 1 1 1 16110.16 15685.26 63.90 o 2 1 1 8121.57 8957.54 60.08 o 3 1 1 6182.02 6229.08 47.88 o 4 1 1 517.84 586.86 11.73 o 5 1 1 2839.77 2866.85 27.98 o 6 1 1 536.80 573.85 15.60 o 7 1 1 1140.09 1136.68 38.71 o 8 1 1 54.78 53.89 12.31 o 9 1 1 419.45 428.57 28.77 o -9 2 1 5.60 0.29 14.24 o -8 2 1 0.93 0.00 10.08 o -7 2 1 217.59 218.14 12.07 o -6 2 1 384.67 371.28 13.12 o -5 2 1 1034.23 1051.81 23.69 o -4 2 1 120.02 144.08 8.46 o -3 2 1 116.96 129.62 5.79 o -2 2 1 10914.94 11124.59 56.21 o -1 2 1 8789.65 9177.98 54.52 o 0 2 1 329.59 372.12 6.88 o 1 2 1 2876.01 3040.40 22.07 o 2 2 1 28443.30 27673.69 140.59 o 3 2 1 318.16 299.64 8.17 o 4 2 1 1105.36 1201.56 16.45 o 5 2 1 165.51 185.91 9.18 o 6 2 1 55.36 56.56 5.17 o 7 2 1 155.24 159.02 15.68 o 8 2 1 182.25 188.47 23.64 o 9 2 1 9.09 29.31 13.67 o -9 3 1 162.56 216.15 21.87 o -8 3 1 48.35 45.50 10.17 o -7 3 1 345.50 356.00 15.70 o -6 3 1 148.09 123.07 8.59 o -5 3 1 2738.88 2630.06 35.11 o -4 3 1 2935.37 2932.61 30.27 o -3 3 1 6065.39 5859.19 39.99 o -2 3 1 539.62 611.26 12.55 o -1 3 1 3655.55 3838.90 32.62 o 0 3 1 146.92 183.11 6.91 o 1 3 1 564.00 493.23 9.29 o 2 3 1 96.51 157.23 6.89 o 3 3 1 14826.20 15217.14 83.31 o 4 3 1 73.90 85.57 5.41 o 5 3 1 3281.22 3250.59 34.90 o 6 3 1 26.75 28.80 5.38 o 7 3 1 938.04 965.09 35.86 o 8 3 1 24.81 16.54 10.68 o 9 3 1 62.32 80.17 18.56 o -9 4 1 18.41 41.41 13.78 o -8 4 1 4.53 15.69 9.58 o -7 4 1 11.59 5.44 6.01 o -6 4 1 35.56 38.64 7.41 o -5 4 1 0.01 2.82 3.62 o -4 4 1 448.63 479.69 14.93 o -3 4 1 606.06 612.02 14.70 o -2 4 1 43.86 59.77 3.73 o -1 4 1 211.47 218.42 6.91 o 0 4 1 1176.69 1294.69 25.13 o 1 4 1 1094.16 1110.66 18.22 o 2 4 1 54.63 50.15 4.02 o 3 4 1 2678.81 2994.03 36.04 o 4 4 1 2059.28 2069.61 29.21 o 5 4 1 22.21 27.96 4.57 o 6 4 1 16.07 21.72 4.91 o 7 4 1 123.59 129.39 14.15 o 8 4 1 108.91 114.22 15.16 o 9 4 1 28.69 20.57 10.84 o -9 5 1 77.97 127.26 30.75 o -8 5 1 41.24 45.34 12.46 o -7 5 1 404.49 435.61 23.00 o -6 5 1 403.82 374.93 15.80 o -5 5 1 931.13 936.16 24.62 o -4 5 1 2378.50 2467.18 33.92 o -3 5 1 6839.95 6826.79 50.82 o -2 5 1 1186.87 1328.19 17.45 o -1 5 1 3839.88 3627.16 38.64 o 0 5 1 1.43 3.86 2.86 o 1 5 1 2532.55 2588.83 28.68 o 2 5 1 12.31 5.61 4.00 o 3 5 1 3878.63 3776.06 39.38 o 4 5 1 621.54 548.21 16.75 o 5 5 1 6662.27 6763.08 72.20 o 6 5 1 741.65 641.58 19.12 o 7 5 1 130.08 150.48 15.45 o 8 5 1 139.30 123.22 14.91 o -8 6 1 0.90 11.51 13.92 o -7 6 1 65.76 50.88 9.53 o -6 6 1 113.47 97.68 9.57 o -5 6 1 302.62 311.88 15.61 o -4 6 1 775.70 868.24 20.96 o -3 6 1 721.26 795.29 17.25 o -2 6 1 456.01 479.98 11.32 o -1 6 1 4790.30 4944.75 66.20 o 0 6 1 536.91 609.38 14.64 o 1 6 1 54.27 91.07 6.28 o 2 6 1 236.17 273.28 10.12 o 3 6 1 1164.53 1174.69 32.54 o 4 6 1 227.83 223.54 12.68 o 5 6 1 37.27 35.99 5.94 o 6 6 1 1318.00 1207.15 27.68 o 7 6 1 187.80 166.38 15.97 o 8 6 1 171.64 146.74 15.91 o -8 7 1 37.22 27.63 17.91 o -7 7 1 141.24 129.88 18.15 o -6 7 1 18.66 27.80 7.74 o -5 7 1 1353.22 1330.14 34.12 o -4 7 1 1134.89 1161.66 24.97 o -3 7 1 1869.85 1849.81 27.05 o -2 7 1 1129.76 1183.93 19.63 o -1 7 1 4316.37 4171.40 53.10 o 0 7 1 2.65 5.06 3.15 o 1 7 1 3870.73 3848.72 39.50 o 2 7 1 951.68 973.54 21.37 o 3 7 1 2605.50 2651.48 49.02 o 4 7 1 510.34 487.81 19.10 o 5 7 1 1144.85 1108.26 29.78 o 6 7 1 3.80 3.54 6.04 o 7 7 1 738.60 729.66 39.42 o 8 7 1 36.94 11.56 20.52 o -8 8 1 57.53 123.45 23.29 o -7 8 1 40.22 31.96 17.67 o -6 8 1 36.01 33.93 8.01 o -5 8 1 252.57 260.38 16.14 o -4 8 1 109.77 131.52 8.79 o -3 8 1 3.90 4.72 3.49 o -2 8 1 3007.65 3128.74 32.63 o -1 8 1 169.87 152.99 9.49 o 0 8 1 73.74 92.22 7.54 o 1 8 1 416.47 453.75 14.30 o 2 8 1 4.38 8.59 5.89 o 3 8 1 1246.73 1195.57 30.29 o 4 8 1 772.31 755.54 24.50 o 5 8 1 7.79 20.37 7.66 o 6 8 1 25.98 21.66 6.57 o 7 8 1 148.87 174.62 28.67 o 8 8 1 51.40 30.45 20.16 o -7 9 1 708.38 803.58 45.66 o -6 9 1 226.80 192.70 18.87 o -5 9 1 342.01 376.43 24.71 o -4 9 1 189.40 198.45 10.95 o -3 9 1 940.87 942.03 20.45 o -2 9 1 445.82 451.38 14.59 o -1 9 1 1982.06 1946.78 33.44 o 0 9 1 2349.76 2282.61 39.96 o 1 9 1 4247.90 4221.56 67.16 o 2 9 1 859.65 913.85 28.81 o 3 9 1 1478.35 1502.11 55.66 o 4 9 1 81.06 66.31 8.98 o 5 9 1 215.09 216.65 15.63 o 6 9 1 1.94 20.10 9.86 o 7 9 1 301.12 294.61 35.06 o -7 10 1 54.09 40.91 15.19 o -6 10 1 158.10 191.96 22.72 o -5 10 1 173.80 151.28 17.91 o -4 10 1 205.27 176.21 19.03 o -3 10 1 53.71 48.29 8.49 o -2 10 1 46.24 55.06 8.11 o -1 10 1 128.65 151.79 9.90 o 0 10 1 612.02 621.49 25.76 o 1 10 1 196.16 193.04 16.48 o 2 10 1 1128.22 1167.95 33.94 o 3 10 1 81.04 80.03 10.48 o 4 10 1 208.66 199.20 16.73 o 5 10 1 19.52 0.00 11.82 o 6 10 1 43.31 10.67 14.80 o 7 10 1 44.52 64.13 27.76 o -6 11 1 131.90 109.28 19.06 o -5 11 1 911.17 940.26 42.78 o -4 11 1 4.19 5.48 8.48 o -3 11 1 241.65 256.50 19.35 o -2 11 1 25.74 25.80 8.79 o -1 11 1 897.35 893.29 43.40 o 0 11 1 19.76 21.05 12.12 o 1 11 1 2345.51 2340.32 61.79 o 2 11 1 1.16 4.86 8.13 o 3 11 1 824.78 839.63 31.04 o 4 11 1 49.37 17.06 10.32 o 5 11 1 49.38 46.52 13.27 o 6 11 1 0.50 0.00 14.15 o -5 12 1 89.80 79.63 15.12 o -4 12 1 27.69 27.08 12.79 o -3 12 1 129.59 126.78 22.81 o -2 12 1 18.58 26.90 24.23 o -1 12 1 183.88 172.89 21.73 o 0 12 1 1649.85 1564.94 59.58 o 1 12 1 124.18 148.23 20.68 o 2 12 1 228.73 263.63 27.23 o 3 12 1 181.13 191.96 19.67 o 4 12 1 24.64 10.36 10.82 o 5 12 1 12.38 7.08 11.88 o -4 13 1 296.98 251.93 35.10 o -3 13 1 780.29 856.74 49.60 o -2 13 1 213.81 211.06 25.94 o -1 13 1 1222.91 1227.48 58.53 o 0 13 1 33.08 25.00 12.24 o 1 13 1 89.90 37.42 16.61 o 2 13 1 129.08 172.88 24.71 o 3 13 1 156.22 145.17 32.28 o 4 13 1 0.88 0.00 17.35 o -3 14 1 33.37 35.11 16.64 o -2 14 1 335.49 342.62 33.06 o -1 14 1 57.07 48.49 17.93 o 0 14 1 154.65 163.30 24.30 o 1 14 1 37.01 26.70 14.71 o 2 14 1 214.94 225.57 28.43 o 3 14 1 1.37 0.62 14.24 o -1 15 1 440.82 446.87 37.56 o 0 15 1 42.36 45.36 16.68 o 1 15 1 76.08 72.68 25.46 o -9 0 2 202.57 178.81 25.40 o -8 0 2 16.07 43.34 23.29 o -7 0 2 1722.86 1613.97 54.37 o -6 0 2 1521.41 1548.84 44.27 o -5 0 2 16.72 28.20 7.61 o -4 0 2 11621.78 11783.35 90.89 o -3 0 2 170.31 214.65 8.42 o -2 0 2 5268.74 5443.91 37.77 o -1 0 2 5705.79 5950.54 59.88 o 0 0 2 220.57 256.67 7.28 o 1 0 2 26958.09 24915.71 120.35 o 2 0 2 23684.32 23106.71 88.13 o 3 0 2 109.10 179.71 8.21 o 4 0 2 4663.92 4458.02 42.91 o 5 0 2 35.01 41.02 4.25 o 6 0 2 580.89 515.56 29.82 o 7 0 2 79.08 55.67 13.71 o 8 0 2 464.25 486.58 40.13 o 9 0 2 98.76 92.69 21.93 o -9 1 2 164.70 169.81 21.33 o -8 1 2 35.51 17.92 10.90 o -7 1 2 86.63 93.21 9.76 o -6 1 2 579.64 559.17 20.44 o -5 1 2 427.66 456.01 11.04 o -4 1 2 100.18 96.84 5.88 o -3 1 2 891.23 878.99 11.56 o -2 1 2 811.28 806.11 11.15 o -1 1 2 439.12 492.03 6.86 o 0 1 2 10821.03 10493.65 80.11 o 1 1 2 8.70 19.15 1.57 o 2 1 2 7848.99 8307.39 71.32 o 3 1 2 570.16 574.18 11.14 o 4 1 2 35.76 33.96 3.41 o 5 1 2 60.89 51.47 4.11 o 6 1 2 140.89 141.17 10.06 o 7 1 2 154.25 134.94 14.15 o 8 1 2 199.15 173.25 16.30 o 9 1 2 84.36 71.88 13.02 o -9 2 2 97.07 85.33 14.18 o -8 2 2 538.53 537.56 28.59 o -7 2 2 398.97 390.12 17.47 o -6 2 2 1109.27 1106.74 22.48 o -5 2 2 2020.14 2019.26 31.43 o -4 2 2 3081.82 3083.37 30.67 o -3 2 2 301.33 287.53 8.98 o -2 2 2 11956.42 12122.27 112.34 o -1 2 2 6166.97 6494.71 39.62 o 0 2 2 24339.74 21791.10 150.31 o 1 2 2 6769.45 6795.66 61.19 o 2 2 2 2689.39 2613.29 47.32 o 3 2 2 1774.57 1803.70 21.16 o 4 2 2 4175.50 4060.58 37.26 o 5 2 2 558.80 647.34 11.29 o 6 2 2 1021.68 994.37 25.47 o 7 2 2 94.80 87.72 12.86 o 8 2 2 558.73 562.72 30.20 o 9 2 2 2.48 9.37 12.69 o -9 3 2 8.71 20.46 13.75 o -8 3 2 78.46 74.64 12.43 o -7 3 2 0.62 7.39 6.95 o -6 3 2 265.99 279.74 12.86 o -5 3 2 533.71 567.83 14.08 o -4 3 2 12.30 14.76 3.81 o -3 3 2 530.14 541.23 14.93 o -2 3 2 4.05 8.46 2.06 o -1 3 2 437.24 457.08 9.16 o 0 3 2 440.35 478.79 10.12 o 1 3 2 155.72 168.94 6.26 o 2 3 2 26.75 23.18 3.94 o 3 3 2 1470.01 1550.25 29.40 o 4 3 2 3444.79 3628.73 43.14 o 5 3 2 622.84 700.23 16.17 o 6 3 2 20.05 18.29 6.19 o 7 3 2 0.64 4.70 8.65 o 8 3 2 92.08 119.13 18.15 o 9 3 2 86.49 60.96 14.70 o -9 4 2 141.55 132.18 18.71 o -8 4 2 890.76 929.27 40.26 o -7 4 2 180.85 143.98 13.50 o -6 4 2 443.42 400.94 12.47 o -5 4 2 77.55 83.54 7.05 o -4 4 2 1009.45 972.65 20.90 o -3 4 2 5719.27 6152.62 52.14 o -2 4 2 24496.09 23964.19 107.01 o -1 4 2 148.94 140.13 6.32 o 0 4 2 23871.13 21956.33 86.20 o 1 4 2 421.71 441.65 11.25 o 2 4 2 4271.73 4373.96 38.32 o 3 4 2 918.87 867.02 24.11 o 4 4 2 62.16 55.56 6.54 o 5 4 2 951.21 939.66 22.66 o 6 4 2 2713.18 2700.41 40.22 o 7 4 2 79.35 63.98 12.09 o 8 4 2 432.69 431.59 26.99 o -9 5 2 51.30 58.82 18.18 o -8 5 2 57.16 67.49 13.57 o -7 5 2 14.58 18.97 8.44 o -6 5 2 8.35 8.18 4.41 o -5 5 2 160.61 153.66 9.98 o -4 5 2 173.30 183.21 10.31 o -3 5 2 1073.77 1180.16 23.45 o -2 5 2 312.79 311.38 8.67 o -1 5 2 76.84 59.60 4.10 o 0 5 2 262.97 278.21 10.23 o 1 5 2 377.26 389.32 14.59 o 2 5 2 30.46 34.97 3.65 o 3 5 2 414.27 475.88 18.27 o 4 5 2 37.08 40.98 6.50 o 5 5 2 786.34 771.12 22.35 o 6 5 2 24.80 19.31 4.91 o 7 5 2 27.74 33.30 9.09 o 8 5 2 26.43 12.67 8.96 o -8 6 2 148.12 163.53 22.94 o -7 6 2 76.06 68.91 10.62 o -6 6 2 546.43 501.02 19.80 o -5 6 2 313.22 304.16 14.15 o -4 6 2 3228.79 3198.86 43.45 o -3 6 2 1056.72 1048.36 20.74 o -2 6 2 9437.05 9349.04 69.20 o -1 6 2 3155.96 3339.07 45.89 o 0 6 2 13469.27 13126.11 125.56 o 1 6 2 231.14 231.98 12.42 o 2 6 2 2023.51 1870.27 38.79 o 3 6 2 1245.56 1280.70 29.59 o 4 6 2 1773.58 1715.97 35.47 o 5 6 2 477.08 502.51 18.80 o 6 6 2 850.07 858.69 26.91 o 7 6 2 1.55 1.84 8.12 o 8 6 2 25.71 35.17 10.91 o -8 7 2 21.54 45.13 16.88 o -7 7 2 40.16 58.70 15.04 o -6 7 2 119.68 127.90 13.04 o -5 7 2 48.17 53.34 7.20 o -4 7 2 97.96 110.72 8.89 o -3 7 2 559.73 562.98 15.73 o -2 7 2 1186.91 1194.70 27.96 o -1 7 2 2060.73 2095.00 30.62 o 0 7 2 167.68 161.62 8.63 o 1 7 2 99.64 136.04 10.52 o 2 7 2 233.04 184.09 13.76 o 3 7 2 47.08 48.21 8.49 o 4 7 2 1012.50 1012.13 30.05 o 5 7 2 497.79 461.48 19.38 o 6 7 2 52.30 57.80 7.72 o 7 7 2 373.85 373.24 22.52 o 8 7 2 125.04 87.41 19.54 o -8 8 2 45.90 55.60 17.46 o -7 8 2 489.75 527.09 35.59 o -6 8 2 996.17 976.25 35.73 o -5 8 2 469.51 440.34 22.90 o -4 8 2 2374.66 2356.43 39.07 o -3 8 2 262.57 250.42 10.10 o -2 8 2 1897.61 1810.01 39.93 o -1 8 2 17.60 21.73 4.47 o 0 8 2 3604.48 3438.61 51.28 o 1 8 2 5068.02 5087.41 64.02 o 2 8 2 4118.64 4081.54 63.05 o 3 8 2 19.17 17.65 6.42 o 4 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