#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:34:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181255 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/33/2233348.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233348_Fobs loop_ _publ_author_name 'Chiririwa, Haleden' 'Muller, Alfred' _publ_section_title ; Chlorido{N-[(E)-2-(diphenylphosphanyl)benzylidene]-2-(thiophen-2-yl)ethanamine-\kP}gold(I) ; _journal_coeditor_code ZQ2145 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m49 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.630 _cell_angle_gamma 90.000 _cell_length_a 11.8660 _cell_length_b 10.6250 _cell_length_c 37.8110 _exptl_crystal_F_000 2448.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file zq2145Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hc185p21n in P2(1)/n New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 757.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 400.65 53.00 23.30 o 2 0 0 356944.38 412062.72 10605.26 o 3 0 0 9262.18 11831.63 336.79 o 4 0 0 124949.96 123040.98 3322.45 o 5 0 0 14069.95 14949.24 505.43 o 6 0 0 114250.59 113903.35 2920.54 o 7 0 0 2544.49 2923.33 129.14 o 8 0 0 23015.61 23411.59 476.63 o 9 0 0 78.07 -178.25 198.95 o 10 0 0 77.19 -110.72 265.78 o 11 0 0 55.25 -136.09 297.43 o 12 0 0 1231.95 865.95 430.42 o 13 0 0 1303.60 1376.34 523.04 o 14 0 0 4805.43 6028.34 857.44 o 15 0 0 3289.92 2773.76 740.83 o 2 1 0 3440.23 3284.94 51.36 o 3 1 0 335555.94 348862.56 4832.72 o 4 1 0 10234.82 10053.05 173.21 o 5 1 0 91177.88 88197.61 1360.58 o 6 1 0 30433.64 29946.71 379.78 o 7 1 0 37566.69 36997.36 647.85 o 8 1 0 11264.85 11124.71 214.12 o 9 1 0 5446.78 5640.50 196.11 o 10 1 0 7889.28 8098.46 268.32 o 11 1 0 2380.43 2205.24 257.69 o 12 1 0 15141.97 15526.15 450.81 o 13 1 0 176.98 232.55 355.76 o 14 1 0 3346.35 3402.89 439.57 o 15 1 0 2.79 180.03 543.93 o 0 2 0 22719.40 28758.27 850.92 o 1 2 0 31042.54 34698.96 490.96 o 2 2 0 7937.06 8216.51 118.00 o 3 2 0 81475.52 79019.53 1310.45 o 4 2 0 15112.06 15304.94 287.64 o 5 2 0 83644.55 79879.33 1368.20 o 6 2 0 11011.19 11222.88 219.27 o 7 2 0 105137.70 101844.09 1451.74 o 8 2 0 18068.13 18119.11 357.73 o 9 2 0 80370.25 79775.47 1316.65 o 10 2 0 9349.07 8310.29 290.42 o 11 2 0 32811.32 32806.25 597.01 o 12 2 0 10505.74 9646.71 408.14 o 13 2 0 14732.28 15244.96 512.03 o 14 2 0 5543.08 5399.44 434.75 o 1 3 0 30207.06 31535.11 571.34 o 2 3 0 5100.38 5324.68 110.68 o 3 3 0 20938.00 20880.13 411.06 o 4 3 0 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753.27 110.85 o 7 5 0 7013.25 7045.72 202.52 o 8 5 0 92.35 102.87 173.21 o 9 5 0 2865.72 2516.65 237.89 o 10 5 0 165.69 375.26 272.02 o 11 5 0 308.67 1116.05 378.79 o 12 5 0 48.67 62.87 382.16 o 13 5 0 855.37 594.48 424.45 o 14 5 0 790.31 632.64 612.95 o 0 6 0 23360.64 22552.74 600.26 o 1 6 0 4041.77 4406.79 112.10 o 2 6 0 8432.43 8005.65 150.35 o 3 6 0 9502.81 10119.58 249.84 o 4 6 0 1173.57 1411.98 133.78 o 5 6 0 16013.28 15725.12 274.16 o 6 6 0 1742.17 2223.52 163.34 o 7 6 0 11684.45 10907.66 290.34 o 8 6 0 85.31 568.99 198.67 o 9 6 0 21563.69 21232.80 542.98 o 10 6 0 3273.95 3264.21 310.96 o 11 6 0 8842.01 8997.14 462.86 o 12 6 0 2879.20 2551.96 426.24 o 13 6 0 3097.76 2352.98 589.07 o 1 7 0 12896.40 13172.22 356.78 o 2 7 0 4870.60 6279.23 237.59 o 3 7 0 9353.45 9272.77 228.69 o 4 7 0 2332.28 3266.44 175.42 o 5 7 0 2381.47 2571.27 183.11 o 6 7 0 14238.22 14019.89 330.03 o 7 7 0 261.76 510.54 193.91 o 8 7 0 11272.91 10494.05 449.83 o 9 7 0 1004.83 1242.97 372.46 o 10 7 0 5323.88 6597.11 551.45 o 11 7 0 2395.66 2785.44 489.90 o 12 7 0 4046.28 4952.86 637.54 o 13 7 0 2238.26 1469.94 629.81 o 0 8 0 3637.48 4166.73 274.63 o 1 8 0 1952.49 4407.68 188.95 o 2 8 0 6482.09 6930.77 229.70 o 3 8 0 1962.29 3640.69 229.98 o 4 8 0 357.32 629.10 195.70 o 5 8 0 4766.03 5419.24 301.12 o 6 8 0 451.63 688.89 223.10 o 7 8 0 1519.39 1630.74 298.54 o 8 8 0 124.78 59.74 370.27 o 9 8 0 1563.77 2247.73 376.84 o 10 8 0 29.06 -225.87 415.58 o 11 8 0 1187.13 1170.89 526.22 o 12 8 0 1161.37 2343.91 650.03 o 1 9 0 9008.64 9285.75 564.03 o 2 9 0 159.21 1283.75 255.29 o 3 9 0 5321.32 5149.16 338.75 o 4 9 0 11662.13 11301.30 385.25 o 5 9 0 2920.85 2858.89 297.80 o 6 9 0 13841.74 13531.31 465.98 o 7 9 0 21.52 326.19 371.46 o 8 9 0 8907.46 8812.08 598.04 o 9 9 0 1511.34 1380.74 501.60 o 10 9 0 2867.64 2443.06 503.77 o 11 9 0 2087.85 2194.25 684.96 o 0 10 0 4043.34 3410.89 552.48 o 1 10 0 1227.65 1023.71 295.34 o 2 10 0 3396.42 2901.13 310.58 o 3 10 0 491.90 1090.34 369.27 o 4 10 0 3879.58 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