#------------------------------------------------------------------------------
#$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $
#$Revision: 66590 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/35/2233517.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2233517_Fobs
loop_
_publ_author_name
'Ludwig, Gerd'
'Block, Michael'
'Wagner, Christoph'
'Steinborn, Dirk'
_publ_section_title
;
 [3-Methoxy-1-(phenylsulfanyl)propyl]triphenyltin(IV) benzene 0.17-solvate
;
_journal_coeditor_code           IS5011
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m149
_journal_volume                  68
_journal_year                    2012
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   35.3384
_cell_length_b                   35.3384
_cell_length_c                   10.5660
_exptl_crystal_F_000             4986.00
_reflns_d_resolution_high        0.8127
_[local]_cod_data_source_file    is5011Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
'                              TEST STRUCTURE Z:\IPDS3208'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            841.66
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 3 0 111410.55 95743.62 1632.03 o
-2 4 0 225080.56 205334.95 2255.89 o
-1 5 0 3151.41 2498.69 341.10 o
-3 6 0 8065.31 8065.24 503.24 o
0 6 0 30383.46 35104.94 961.07 o
-5 7 0 2202.36 2076.25 384.69 o
-2 7 0 32971.25 29867.30 885.28 o
-7 8 0 89962.35 99682.91 1895.10 o
-4 8 0 46189.60 45580.20 671.86 o
-1 8 0 202709.84 209848.53 5977.22 o
-6 9 0 708387.00 808505.31 26896.76 o
-3 9 0 231661.97 257031.34 7131.75 o
0 9 0 1368.97 2132.79 434.77 o
-8 10 0 17964.99 18905.00 501.48 o
-5 10 0 30813.64 35666.77 561.46 o
-2 10 0 11920.95 12467.33 522.83 o
-10 11 0 196556.45 214133.53 3330.37 o
-7 11 0 3030.02 3545.64 334.81 o
-4 11 0 212512.72 223201.23 8052.18 o
-1 11 0 328080.19 347409.78 7959.92 o
-9 12 0 49734.73 51805.31 998.74 o
-6 12 0 5979.12 6091.13 368.26 o
-3 12 0 40417.50 38355.66 1235.03 o
0 12 0 48117.73 50708.76 1042.32 o
-11 13 0 6729.66 6477.02 329.28 o
-8 13 0 64343.65 64608.11 1208.78 o
-5 13 0 53797.51 52808.76 1102.54 o
-2 13 0 82350.55 89386.96 902.06 o
-13 14 0 15178.62 13742.16 334.31 o
-10 14 0 99154.02 98495.91 2386.98 o
-7 14 0 62063.98 62777.77 1242.58 o
-4 14 0 218.88 673.74 301.13 o
-1 14 0 79605.25 80097.35 1156.44 o
-12 15 0 25428.03 25822.63 442.39 o
-9 15 0 44619.54 47263.85 934.82 o
-6 15 0 12107.24 11384.31 341.35 o
-3 15 0 301162.28 285544.38 7548.09 o
0 15 0 201644.59 212727.80 2208.13 o
-14 16 0 57071.88 54696.01 794.74 o
-11 16 0 32179.36 32992.06 963.34 o
-8 16 0 175475.53 174052.22 3448.93 o
-5 16 0 33919.84 30802.30 756.14 o
-2 16 0 3714.63 3309.87 321.56 o
-16 17 0 3522.71 4101.99 352.30 o
-13 17 0 176835.48 180963.83 3326.94 o
-10 17 0 7939.51 8053.94 307.92 o
-7 17 0 72109.55 77630.02 825.75 o
-4 17 0 16735.29 15177.01 370.31 o
-1 17 0 796.28 972.04 306.60 o
-15 18 0 3488.62 3161.81 343.21 o
-12 18 0 34305.23 36612.49 575.00 o
-9 18 0 26242.06 26002.85 548.03 o
-6 18 0 3637.69 3270.71 339.07 o
-3 18 0 17644.42 16947.85 570.89 o
0 18 0 60450.18 60353.80 1978.64 o
-17 19 0 6361.66 5271.10 319.78 o
-14 19 0 34536.61 32704.82 1168.42 o
-11 19 0 752.15 705.19 280.21 o
-8 19 0 58770.47 65349.81 916.05 o
-5 19 0 1415.61 1215.84 382.64 o
-2 19 0 147630.22 148056.48 4288.60 o
-19 20 0 29424.35 30581.33 685.43 o
-16 20 0 3673.56 4229.37 364.78 o
-13 20 0 22006.08 21941.15 521.29 o
-10 20 0 38473.38 39122.23 1012.07 o
-7 20 0 134148.94 128314.78 3790.84 o
-4 20 0 43071.07 41075.06 575.31 o
-1 20 0 3244.52 3190.84 353.70 o
-18 21 0 24400.11 24361.53 669.40 o
-15 21 0 51146.30 48142.50 1569.96 o
-12 21 0 176882.08 191457.94 3839.81 o
-9 21 0 35840.64 38576.36 455.41 o
-6 21 0 1322.40 1754.83 345.02 o
-3 21 0 89.08 308.97 331.69 o
0 21 0 22070.68 20626.00 991.80 o
-20 22 0 7091.71 7042.47 392.75 o
-17 22 0 84015.23 83920.77 2217.75 o
-14 22 0 68.88 -19.54 346.17 o
-11 22 0 3985.83 3924.03 341.46 o
-8 22 0 6082.05 5877.43 289.10 o
-5 22 0 13274.09 13757.95 401.46 o
-2 22 0 65352.09 61719.65 2700.36 o
-22 23 0 8718.08 8494.95 372.04 o
-19 23 0 27762.64 27661.95 533.96 o
-16 23 0 1403.52 1131.02 314.67 o
-13 23 0 33117.97 35932.96 593.93 o
-10 23 0 2745.38 2779.37 311.02 o
-7 23 0 40994.81 41793.28 698.30 o
-4 23 0 8706.06 9230.21 475.00 o
-1 23 0 26612.44 27421.00 1392.02 o
-21 24 0 22964.24 23058.81 1046.18 o
-18 24 0 5234.01 4850.60 352.32 o
-15 24 0 12237.44 12202.84 381.08 o
-12 24 0 4436.20 4635.56 345.25 o
-9 24 0 251.86 155.78 309.96 o
-6 24 0 225783.36 225337.48 4640.77 o
-3 24 0 23290.32 23577.69 841.04 o
0 24 0 46345.64 47341.43 1134.09 o
-23 25 0 887.97 846.73 366.52 o
-20 25 0 15442.06 14493.80 432.58 o
-17 25 0 30838.48 30906.95 876.21 o
-14 25 0 59046.98 59772.41 561.12 o
-11 25 0 245870.64 239011.52 6592.56 o
-8 25 0 15271.07 16282.60 447.09 o
-5 25 0 31748.24 32456.73 1592.68 o
-2 25 0 414.34 230.02 413.69 o
-25 26 0 34932.17 35392.61 540.83 o
-22 26 0 246.47 575.78 388.28 o
-19 26 0 61969.16 62209.98 1642.26 o
-16 26 0 142121.73 145564.67 2179.58 o
-13 26 0 208.29 211.73 271.02 o
-10 26 0 183.94 83.27 359.89 o
-7 26 0 3303.75 3803.58 398.06 o
-4 26 0 39247.83 37923.72 1388.17 o
-1 26 0 30429.29 30211.47 894.49 o
-24 27 0 10905.21 10856.06 448.79 o
-21 27 0 8790.23 8905.07 395.40 o
-18 27 0 39326.05 40201.88 916.21 o
-15 27 0 20149.01 20437.68 436.69 o
-12 27 0 243.06 310.25 363.65 o
-9 27 0 29305.31 30442.42 1185.10 o
-6 27 0 52487.59 52514.64 2066.39 o
-3 27 0 1678.45 1710.91 368.41 o
0 27 0 9562.49 9968.42 446.42 o
-26 28 0 6233.26 5733.73 395.93 o
-23 28 0 48118.91 47835.78 1114.28 o
-20 28 0 30635.14 29928.88 580.58 o
-17 28 0 3613.76 3628.76 389.79 o
-14 28 0 17191.58 17857.11 439.20 o
-11 28 0 34481.24 36586.91 895.83 o
-8 28 0 12034.32 12954.14 510.29 o
-5 28 0 113757.50 115660.30 1467.15 o
-2 28 0 19778.95 19502.46 457.51 o
-28 29 0 121245.34 121037.80 5032.58 o
-25 29 0 18555.01 18899.15 517.55 o
-22 29 0 1983.95 1954.55 402.22 o
-19 29 0 31346.80 32370.77 748.77 o
-16 29 0 1291.61 884.13 350.06 o
-13 29 0 12187.44 12395.28 371.73 o
-10 29 0 175841.84 169370.97 4805.63 o
-7 29 0 30605.50 30702.85 1194.99 o
-4 29 0 88709.59 90615.67 701.58 o
-1 29 0 2305.40 2193.40 456.16 o
-27 30 0 72.70 -193.37 432.51 o
-24 30 0 8087.38 7693.52 432.57 o
-21 30 0 298.75 134.00 367.35 o
-18 30 0 7399.64 7458.64 392.00 o
-15 30 0 75028.76 71395.48 956.12 o
-12 30 0 5609.06 4707.94 388.82 o
-9 30 0 6711.54 6808.26 443.98 o
-6 30 0 14535.69 14969.99 463.08 o
-3 30 0 43831.68 42839.95 1960.94 o
0 30 0 1554.90 1546.15 433.21 o
-29 31 0 563.87 563.61 392.57 o
-26 31 0 168.22 633.38 461.15 o
-23 31 0 16643.24 17633.02 545.60 o
-20 31 0 34394.25 34821.41 601.99 o
-17 31 0 15287.70 15107.79 435.29 o
-14 31 0 28313.66 29128.99 474.63 o
-11 31 0 49656.18 49344.44 1005.57 o
-8 31 0 67326.48 66577.20 1932.62 o
-5 31 0 2863.68 2268.25 501.40 o
-2 31 0 8565.82 7837.09 652.15 o
-31 32 0 975.58 523.32 544.86 o
-28 32 0 1406.87 1658.76 464.09 o
-25 32 0 2247.80 2495.03 511.20 o
-22 32 0 9070.22 9033.71 464.70 o
-19 32 0 4192.68 4380.73 433.37 o
-16 32 0 22915.44 23341.49 590.83 o
-13 32 0 38715.59 42965.04 675.68 o
-10 32 0 15774.46 16388.48 542.31 o
-7 32 0 5043.23 4549.83 500.56 o
-4 32 0 1246.93 1332.83 468.87 o
-1 32 0 7452.44 8552.65 567.59 o
-30 33 0 1754.00 1628.87 614.34 o
-27 33 0 50759.21 53242.15 695.82 o
-24 33 0 13830.10 13376.93 663.29 o
-21 33 0 1936.89 2111.96 438.32 o
-18 33 0 20182.90 21409.55 561.94 o
-15 33 0 3628.93 4686.85 517.91 o
-12 33 0 21667.85 23458.65 829.38 o
-9 33 0 29416.55 29289.51 585.44 o
-6 33 0 16493.99 16550.10 529.23 o
-3 33 0 62306.98 62393.73 2583.85 o
0 33 0 334.88 655.85 607.90 o
-32 34 0 47534.31 48982.08 1260.63 o
-29 34 0 9085.68 9171.29 537.33 o
-26 34 0 1225.52 1228.48 466.70 o
-23 34 0 554.86 327.45 426.48 o
-20 34 0 4876.02 5050.95 409.23 o
-17 34 0 11498.65 12996.15 563.09 o
-14 34 0 28710.23 29117.75 575.48 o
-11 34 0 347.34 294.86 574.00 o
-8 34 0 11554.37 10918.82 449.82 o
-5 34 0 13335.05 12863.39 486.14 o
-2 34 0 5183.24 4940.67 513.23 o
-34 35 0 305.81 170.76 665.65 o
-31 35 0 5282.55 6562.41 837.84 o
-28 35 0 1699.64 1557.40 468.77 o
-25 35 0 4211.10 3919.96 668.94 o
-22 35 0 6722.67 6296.19 457.10 o
-19 35 0 3664.39 3483.09 448.31 o
-16 35 0 13560.07 12820.96 634.89 o
-13 35 0 377.78 479.18 422.01 o
-10 35 0 43013.49 45731.78 1061.92 o
-7 35 0 22454.91 21368.34 626.31 o
-4 35 0 2071.28 2195.62 588.93 o
-1 35 0 7561.00 7457.37 720.35 o
-33 36 0 856.90 825.51 846.41 o
-30 36 0 7435.79 6489.25 531.42 o
-27 36 0 7794.52 8305.38 577.14 o
-24 36 0 2115.04 1468.09 520.72 o
-21 36 0 37096.25 34852.59 2597.02 o
-18 36 0 6754.59 6721.56 556.88 o
-15 36 0 39663.88 39549.60 1148.34 o
-12 36 0 1831.43 1559.97 508.90 o
-9 36 0 1386.61 1024.74 547.64 o
-6 36 0 12111.81 11988.70 671.29 o
-3 36 0 803.61 1084.27 626.18 o
0 36 0 3322.15 3989.00 762.70 o
-35 37 0 704.94 -176.40 554.43 o
-32 37 0 1457.47 1374.54 602.97 o
-29 37 0 995.51 840.89 774.39 o
-26 37 0 21054.61 20720.33 3221.06 o
-23 37 0 2910.66 2819.25 522.51 o
-20 37 0 21385.92 19070.95 2706.91 o
-17 37 0 3625.48 3945.48 626.77 o
-14 37 0 10284.73 10448.94 651.39 o
-11 37 0 4152.07 4585.91 560.73 o
-8 37 0 676.79 980.01 539.15 o
-5 37 0 6404.48 7210.51 585.18 o
-2 37 0 12653.90 12089.82 560.38 o
-34 38 0 1530.37 2022.85 590.86 o
-31 38 0 38379.66 40321.15 1021.83 o
-28 38 0 5670.88 5815.53 650.71 o
-25 38 0 9512.85 7784.43 1338.79 o
-22 38 0 1200.72 801.90 551.93 o
-19 38 0 7707.33 7640.38 582.92 o
-16 38 0 28153.70 27884.95 990.45 o
-13 38 0 1064.99 1680.97 460.45 o
-10 38 0 11136.38 11428.32 774.39 o
-7 38 0 5010.79 5359.48 583.95 o
-4 38 0 2794.78 3018.79 568.16 o
-33 39 0 226.43 -261.17 607.92 o
-30 39 0 1369.54 1734.61 531.34 o
-27 39 0 1525.98 1266.40 568.69 o
-24 39 0 20132.39 17310.95 3431.21 o
-21 39 0 23099.86 18673.90 2893.33 o
-18 39 0 171.66 -162.01 521.43 o
-15 39 0 1517.53 1919.38 617.53 o
-12 39 0 44.42 -434.62 573.79 o
-9 39 0 27467.41 26544.21 840.71 o
-6 39 0 8556.49 10087.99 1019.82 o
-32 40 0 1243.05 2007.19 588.25 o
-29 40 0 12905.33 12962.28 716.27 o
-26 40 0 4115.37 3704.11 1069.54 o
-23 40 0 174.42 280.61 736.15 o
-20 40 0 2859.68 2485.59 596.97 o
-17 40 0 4631.17 3779.95 993.32 o
-14 40 0 48990.47 48754.23 1741.88 o
-11 40 0 4588.02 4702.74 630.89 o
-8 40 0 1172.56 2299.96 591.53 o
-31 41 0 4574.48 6105.25 687.56 o
-28 41 0 84.86 366.41 543.30 o
-25 41 0 6880.68 5666.14 1195.40 o
-22 41 0 157.77 -0.03 645.74 o
-19 41 0 46834.60 40139.02 9729.52 o
-16 41 0 122.81 228.17 1037.95 o
-13 41 0 284.65 -414.79 675.22 o
-10 41 0 55.78 -569.91 569.91 o
-30 42 0 18813.47 20966.01 4349.62 o
-27 42 0 1699.18 1187.75 546.05 o
-24 42 0 23306.57 19397.29 3414.95 o
-21 42 0 816.07 844.13 699.27 o
-18 42 0 4605.40 3833.74 1543.22 o
-15 42 0 297.49 1377.10 725.55 o
-12 42 0 2047.35 1990.00 1061.00 o
-26 43 0 238.14 913.59 884.01 o
-23 43 0 1908.54 1647.76 748.95 o
-20 43 0 3902.88 3780.87 1379.05 o
-17 43 0 7.65 763.59 1043.45 o
-1 1 1 316182.13 271663.97 3601.95 o
-3 2 1 163007.83 139165.83 2362.62 o
0 2 1 104929.23 86220.43 3345.25 o
-5 3 1 68305.63 70757.19 1374.59 o
-2 3 1 63669.00 55829.20 1062.76 o
1 3 1 13409.04 12215.66 588.29 o
-7 4 1 246480.33 279535.56 1878.34 o
-4 4 1 80851.11 70690.36 1493.73 o
-1 4 1 115415.36 103281.40 1446.69 o
2 4 1 260718.19 280682.16 10527.89 o
-9 5 1 344806.06 364275.03 11571.38 o
-6 5 1 51941.88 55938.88 1239.53 o
-3 5 1 202874.27 214976.36 2878.47 o
0 5 1 43801.79 43424.93 914.11 o
3 5 1 8299.26 8086.87 568.41 o
-11 6 1 60919.69 64198.61 927.35 o
-8 6 1 58102.90 67688.53 791.45 o
-5 6 1 197286.45 203003.16 2550.68 o
-2 6 1 514934.31 575519.19 7479.12 o
1 6 1 76024.49 82621.82 1135.43 o
4 6 1 145347.17 165518.67 1069.53 o
-13 7 1 32095.27 33272.65 650.91 o
-10 7 1 174969.11 169853.41 3926.65 o
-7 7 1 11970.68 12568.76 473.55 o
-4 7 1 474874.13 559054.56 3677.90 o
-1 7 1 228345.33 255343.05 3501.06 o
2 7 1 534.15 682.67 416.63 o
5 7 1 90902.33 90286.68 2610.07 o
-15 8 1 101814.09 100831.82 1100.92 o
-12 8 1 32379.30 33816.89 643.26 o
-9 8 1 2670.44 2849.84 352.09 o
-6 8 1 5175.04 6492.30 458.02 o
-3 8 1 152800.13 171066.55 3539.81 o
0 8 1 408664.06 447527.41 8939.70 o
3 8 1 53577.41 53125.86 1091.92 o
6 8 1 40983.89 42597.88 537.30 o
-17 9 1 2227.93 2192.97 302.85 o
-14 9 1 90.16 121.05 272.32 o
-11 9 1 197269.34 213628.63 6247.52 o
-8 9 1 6044.44 7041.96 403.96 o
-5 9 1 229315.47 254022.44 2987.98 o
-2 9 1 235203.97 248440.50 2709.97 o
1 9 1 29806.74 28315.55 756.79 o
4 9 1 10024.46 10006.18 392.46 o
7 9 1 211394.27 223010.41 4798.12 o
-19 10 1 40252.02 45089.39 1308.95 o
-16 10 1 162212.14 162096.61 2359.78 o
-13 10 1 16135.04 15531.55 429.53 o
-10 10 1 7506.96 7207.18 414.07 o
-7 10 1 2337.77 2091.58 340.00 o
-4 10 1 535953.69 595695.88 11092.02 o
-1 10 1 26478.13 26985.32 584.33 o
2 10 1 115475.75 119737.74 1526.10 o
5 10 1 23062.83 24314.88 749.75 o
8 10 1 64864.13 72800.63 917.75 o
-21 11 1 52219.80 54563.14 775.30 o
-18 11 1 19935.82 22802.09 456.96 o
-15 11 1 52948.50 53532.47 1243.83 o
-12 11 1 45929.26 50379.27 1505.32 o
-9 11 1 468998.56 486087.09 12134.73 o
-6 11 1 1985.59 2085.41 311.25 o
-3 11 1 53829.29 52998.62 1545.27 o
0 11 1 75395.06 79182.20 1581.66 o
3 11 1 60059.25 59046.08 1670.89 o
6 11 1 136140.59 136263.31 4002.38 o
9 11 1 95482.66 99822.84 1486.27 o
-23 12 1 27336.67 29398.97 1119.02 o
-20 12 1 98743.42 97426.15 2946.93 o
-17 12 1 76027.32 80404.87 1258.40 o
-14 12 1 288599.53 271177.97 6068.28 o
-11 12 1 259.37 119.99 259.12 o
-8 12 1 1113.63 2148.55 281.70 o
-5 12 1 93160.25 97885.65 2000.41 o
-2 12 1 5065.02 5640.95 321.56 o
1 12 1 116949.84 118281.02 826.21 o
4 12 1 28861.60 29582.84 461.87 o
7 12 1 6632.63 7061.74 527.02 o
10 12 1 4498.70 4575.48 343.78 o
-25 13 1 78697.20 74365.55 2470.30 o
-22 13 1 47920.84 49621.65 943.25 o
-19 13 1 113675.03 110630.60 3111.75 o
-16 13 1 1914.88 1435.55 302.13 o
-13 13 1 22871.49 25568.23 466.73 o
-10 13 1 44556.97 48352.00 565.17 o
-7 13 1 221552.47 241961.11 2553.12 o
-4 13 1 223628.55 221632.94 6000.24 o
-1 13 1 11808.51 12520.33 391.82 o
2 13 1 14538.78 15429.02 342.55 o
5 13 1 14419.00 14494.39 369.15 o
8 13 1 98951.60 101239.06 2479.76 o
11 13 1 7999.18 7002.00 366.37 o
-27 14 1 15550.86 15214.07 494.63 o
-24 14 1 23499.95 22334.63 466.21 o
-21 14 1 61147.25 64751.76 977.58 o
-18 14 1 24011.30 24488.45 615.82 o
-15 14 1 58151.89 58401.17 1914.56 o
-12 14 1 6276.08 5269.47 315.10 o
-9 14 1 247315.63 259152.92 3891.94 o
-6 14 1 26775.69 30140.35 718.59 o
-3 14 1 26039.73 25576.54 634.34 o
0 14 1 1982.09 1936.26 331.35 o
3 14 1 243758.30 267627.66 2647.66 o
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