#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/35/2233527.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233527_Fobs loop_ _publ_author_name 'Kumar, Sarvendra' 'Thapa, Suresh' _publ_section_title ; Butylbis(dimethylglyoximato-\k^2^N,N')(pyridine-\kN)cobalt(III) ; _journal_coeditor_code IS5041 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m156 _journal_page_last m157 _journal_volume 68 _journal_year 2012 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yac' _symmetry_space_group_name_H-M 'P 1 n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.768 _cell_angle_gamma 90.000 _cell_length_a 8.3653 _cell_length_b 10.4083 _cell_length_c 11.4872 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file is5041Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -3 0 -13 12.23 11.15 9.98 o -1 0 -13 151.45 118.17 26.39 o -3 1 -13 5.85 6.54 6.09 o -2 1 -13 99.66 112.67 32.23 o -1 1 -13 101.29 129.72 26.89 o -2 2 -13 67.11 69.95 18.37 o 0 2 -13 60.75 74.52 17.47 o 1 2 -13 163.26 186.19 27.94 o 0 3 -13 100.75 140.02 23.70 o 1 3 -13 39.07 43.71 14.13 o 2 3 -13 102.75 128.49 24.96 o -1 4 -13 245.60 277.21 32.62 o 0 4 -13 23.97 24.72 10.94 o 1 4 -13 126.22 127.73 24.25 o -4 0 -12 364.53 359.07 37.33 o -2 0 -12 375.36 350.49 35.11 o -4 1 -12 117.05 134.83 19.18 o -3 1 -12 72.58 112.26 23.41 o -2 1 -12 30.05 38.57 10.20 o -1 1 -12 479.26 535.49 59.23 o 0 1 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