#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/36/2233691.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233691_Fobs loop_ _publ_author_name 'Zhao, Min-Min' _publ_section_title ; Propane-1,3-diaminium bis(perchlorate)--18-crown-6 (1/2) ; _journal_coeditor_code XU5433 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o327 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.589 _cell_angle_gamma 90.000 _cell_length_a 22.9840 _cell_length_b 9.0055 _cell_length_c 21.6200 _exptl_crystal_F_000 1720.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file xu5433Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 39067.84 42814.87 432.84 o 6 0 0 85220.84 94968.41 1564.62 o 8 0 0 11766.34 11772.49 488.54 o 10 0 0 24.94 9.87 18.69 o 12 0 0 1035.30 1083.39 73.95 o 14 0 0 5600.18 5168.51 192.13 o 16 0 0 1570.56 1361.72 98.91 o 18 0 0 821.64 585.88 72.96 o 20 0 0 2159.15 2092.19 203.90 o 22 0 0 16.82 0.00 99.51 o 24 0 0 2.00 0.00 101.82 o 3 1 0 268.34 263.53 9.09 o 5 1 0 577.68 849.20 24.55 o 7 1 0 693.31 664.06 23.30 o 9 1 0 7019.55 6377.72 112.68 o 11 1 0 165.11 230.88 26.17 o 13 1 0 9.06 32.13 31.89 o 15 1 0 218.84 219.20 55.44 o 17 1 0 575.52 609.34 56.83 o 19 1 0 1284.07 1070.03 87.86 o 21 1 0 1.69 31.97 39.61 o 23 1 0 24.68 18.56 48.16 o 0 2 0 15357.96 17324.57 284.71 o 2 2 0 2609.82 2673.37 69.03 o 4 2 0 1605.05 1486.72 42.24 o 6 2 0 5.49 35.68 12.43 o 8 2 0 935.30 934.94 35.55 o 10 2 0 3309.74 3482.51 90.76 o 12 2 0 3.12 17.42 14.67 o 14 2 0 793.84 725.91 53.16 o 16 2 0 1.96 87.00 39.24 o 18 2 0 177.50 302.85 87.21 o 20 2 0 815.91 732.96 96.23 o 22 2 0 3.12 0.00 41.23 o 24 2 0 283.20 54.21 92.26 o 1 3 0 82.77 155.39 26.82 o 3 3 0 2082.03 1869.50 71.45 o 5 3 0 413.31 281.26 26.85 o 7 3 0 2305.20 2123.56 60.50 o 9 3 0 1059.55 1260.74 45.86 o 11 3 0 5634.52 5111.64 125.61 o 13 3 0 13.06 74.33 23.71 o 15 3 0 362.28 454.62 42.29 o 17 3 0 118.81 35.92 33.55 o 19 3 0 376.84 537.96 69.22 o 21 3 0 52.46 137.92 64.17 o 23 3 0 44.89 0.00 65.27 o 0 4 0 958.77 1157.67 94.48 o 2 4 0 8442.22 7282.43 189.27 o 4 4 0 958.72 917.33 48.33 o 6 4 0 516.48 469.51 32.93 o 8 4 0 568.24 433.77 36.06 o 10 4 0 296.40 397.46 36.36 o 12 4 0 211.48 357.04 39.83 o 14 4 0 1119.74 1013.03 65.24 o 16 4 0 8.32 0.00 33.45 o 18 4 0 235.27 311.25 70.53 o 20 4 0 67.21 159.65 89.22 o 22 4 0 99.41 232.78 82.08 o 1 5 0 6459.78 6360.64 208.15 o 3 5 0 845.56 786.96 48.96 o 5 5 0 4559.98 4497.83 139.13 o 7 5 0 1386.36 1617.30 74.17 o 9 5 0 3014.13 2726.05 99.91 o 11 5 0 422.06 499.65 48.25 o 13 5 0 1881.62 1892.05 91.54 o 15 5 0 412.20 428.25 71.71 o 17 5 0 542.22 546.04 68.53 o 19 5 0 459.61 503.01 95.48 o 21 5 0 61.22 0.00 52.90 o 0 6 0 2951.73 3055.77 210.10 o 2 6 0 1337.94 1416.44 93.80 o 4 6 0 362.35 443.69 53.97 o 6 6 0 1765.01 1584.12 132.14 o 8 6 0 89.77 94.12 33.10 o 10 6 0 1400.73 1309.21 82.70 o 12 6 0 132.14 198.83 42.95 o 14 6 0 24.62 78.35 37.77 o 16 6 0 644.08 527.67 108.93 o 18 6 0 131.62 188.09 88.78 o 20 6 0 55.13 126.75 72.46 o 1 7 0 0.86 9.23 29.55 o 3 7 0 9.30 111.82 45.02 o 5 7 0 61.80 128.46 41.01 o 7 7 0 25.99 69.40 31.04 o 9 7 0 66.18 83.96 36.85 o 11 7 0 162.09 192.72 45.49 o 13 7 0 29.30 75.01 36.65 o 15 7 0 62.58 111.95 65.14 o 17 7 0 77.61 0.00 49.79 o 0 8 0 2.05 40.73 50.50 o 2 8 0 154.09 376.64 68.26 o 4 8 0 20.12 115.98 60.26 o 6 8 0 7.63 0.00 29.57 o 8 8 0 0.02 6.36 26.03 o 10 8 0 47.66 151.71 56.08 o 12 8 0 13.92 15.86 37.48 o 14 8 0 38.55 33.09 47.39 o 16 8 0 40.95 66.02 59.14 o 1 9 0 118.88 194.81 89.32 o 3 9 0 43.98 167.19 75.09 o 5 9 0 66.95 42.76 48.41 o 7 9 0 13.96 21.08 36.42 o 9 9 0 81.70 62.50 50.51 o 11 9 0 45.68 68.13 66.46 o 13 9 0 144.15 100.00 76.22 o 0 10 0 1.86 0.00 80.38 o 2 10 0 0.11 0.00 56.40 o 4 10 0 2.34 77.97 54.46 o 6 10 0 17.74 23.74 50.16 o 8 10 0 25.04 0.00 66.90 o -25 1 1 71.32 26.19 58.73 o -23 1 1 157.62 130.67 61.47 o -21 1 1 142.30 154.21 57.18 o -19 1 1 140.31 135.49 40.51 o -17 1 1 454.31 627.69 50.44 o -15 1 1 326.65 470.71 40.41 o -13 1 1 0.06 50.05 20.40 o -11 1 1 1975.30 1802.19 56.59 o -9 1 1 1055.16 1016.65 44.34 o -7 1 1 9717.23 9473.98 137.97 o -5 1 1 124152.41 125353.84 1155.01 o -3 1 1 1037.16 793.76 16.75 o 3 1 1 10744.95 11365.67 148.29 o 5 1 1 23143.22 22330.74 214.78 o 7 1 1 976.54 1100.17 30.76 o 9 1 1 3318.17 2848.33 66.47 o 11 1 1 44.06 0.00 11.40 o 13 1 1 290.12 406.58 34.22 o 15 1 1 734.52 714.18 82.99 o 17 1 1 622.29 841.27 75.26 o 19 1 1 427.03 537.30 65.37 o 21 1 1 304.83 228.09 88.18 o 23 1 1 16.04 0.00 44.66 o -24 2 1 10.48 122.80 73.94 o -22 2 1 700.31 521.75 85.50 o -20 2 1 743.44 694.56 74.48 o -18 2 1 2483.37 2240.12 216.01 o -16 2 1 2440.03 2504.93 149.08 o -14 2 1 2395.85 2267.99 77.63 o -12 2 1 1860.46 1947.67 69.21 o -10 2 1 5775.70 4791.08 102.57 o -8 2 1 6835.32 4969.15 108.38 o -6 2 1 5.95 45.73 19.29 o -4 2 1 24800.66 22254.59 302.37 o -2 2 1 128.95 346.89 23.81 o 0 2 1 7054.22 9249.36 112.07 o 2 2 1 53031.62 54581.15 706.34 o 4 2 1 4064.12 3574.69 63.10 o 6 2 1 796.75 1259.53 48.25 o 8 2 1 2436.56 2961.21 88.24 o 10 2 1 185.03 128.99 28.05 o 12 2 1 157.71 294.00 36.61 o 14 2 1 82.71 74.27 21.77 o 16 2 1 40.34 86.83 39.28 o 18 2 1 1825.76 1710.90 117.36 o 20 2 1 220.52 191.46 77.79 o 22 2 1 188.26 250.31 78.94 o 24 2 1 153.17 88.59 84.63 o -23 3 1 58.33 67.48 58.64 o -21 3 1 276.36 310.77 90.81 o -19 3 1 363.29 326.80 58.17 o -17 3 1 363.93 431.93 48.59 o -15 3 1 1256.53 1155.56 74.06 o -13 3 1 408.86 374.92 39.77 o -11 3 1 11.62 100.74 22.53 o -9 3 1 885.15 1371.50 52.68 o -7 3 1 2397.54 1969.64 56.92 o -5 3 1 11.58 59.46 24.79 o -3 3 1 3535.19 3543.80 73.46 o -1 3 1 36569.09 37404.61 506.71 o 1 3 1 10788.32 10745.51 239.21 o 3 3 1 6975.76 5947.01 124.86 o 5 3 1 4762.77 4109.61 87.86 o 7 3 1 4651.53 4401.50 108.29 o 9 3 1 5337.43 4955.39 113.43 o 11 3 1 3156.24 3075.90 86.41 o 13 3 1 26.75 0.00 15.01 o 15 3 1 2529.71 2513.55 173.00 o 17 3 1 509.84 572.53 68.57 o 19 3 1 486.61 464.33 70.70 o 21 3 1 321.95 297.60 75.06 o 23 3 1 254.54 296.97 115.19 o -22 4 1 0.01 0.00 47.69 o -20 4 1 409.25 514.60 88.85 o -18 4 1 5.67 20.05 33.45 o -16 4 1 109.87 156.32 67.01 o -14 4 1 834.42 980.43 62.79 o -12 4 1 64.07 53.81 35.42 o -10 4 1 4543.93 5400.43 139.86 o -8 4 1 1991.34 1797.26 66.15 o -6 4 1 58.90 39.33 21.54 o -4 4 1 2468.35 2166.74 67.40 o -2 4 1 10143.65 8724.87 170.32 o 0 4 1 791.96 553.69 35.23 o 2 4 1 4938.12 4732.98 124.60 o 4 4 1 17486.17 16105.24 326.09 o 6 4 1 1410.32 1599.63 58.89 o 8 4 1 2255.24 2301.02 75.15 o 10 4 1 480.79 404.01 36.36 o 12 4 1 84.60 50.15 24.84 o 14 4 1 17.42 10.36 29.19 o 16 4 1 312.65 484.88 91.11 o 18 4 1 1.05 0.00 27.65 o 20 4 1 0.12 20.82 73.68 o 22 4 1 238.41 172.50 81.29 o -21 5 1 9.75 112.73 98.39 o -19 5 1 27.94 277.32 185.70 o -17 5 1 337.68 341.35 110.92 o -15 5 1 55.93 65.68 29.55 o -13 5 1 368.79 309.93 41.90 o -11 5 1 16.40 0.00 24.59 o -9 5 1 20.43 178.91 60.42 o -7 5 1 3724.93 4295.30 138.55 o -5 5 1 636.24 893.99 49.74 o -3 5 1 533.41 403.67 35.24 o -1 5 1 3543.45 2719.21 86.99 o 1 5 1 1110.71 1285.64 74.27 o 3 5 1 3927.80 3637.14 121.36 o 5 5 1 1367.47 1363.16 64.87 o 7 5 1 877.77 893.00 58.15 o 9 5 1 246.62 223.57 77.19 o 11 5 1 0.35 1.95 40.80 o 13 5 1 590.77 581.60 59.45 o 15 5 1 210.43 186.65 51.33 o 17 5 1 12.32 17.53 34.27 o 19 5 1 70.45 98.41 63.21 o 21 5 1 9.26 0.00 64.61 o -20 6 1 236.87 363.73 136.47 o -18 6 1 159.18 57.90 70.03 o -16 6 1 420.81 539.27 86.93 o -14 6 1 3.83 29.29 27.65 o -12 6 1 25.90 81.44 57.92 o -10 6 1 2378.88 2082.71 99.70 o -8 6 1 113.55 149.48 48.39 o -6 6 1 1978.63 1779.44 85.10 o -4 6 1 248.67 338.31 43.96 o -2 6 1 24.07 64.23 52.02 o 0 6 1 1568.70 1309.27 72.07 o 2 6 1 82.81 356.76 56.92 o 4 6 1 2504.90 2750.90 117.46 o 6 6 1 47.00 135.38 60.77 o 8 6 1 115.62 272.70 44.61 o 10 6 1 815.58 904.79 72.89 o 12 6 1 350.94 409.98 48.28 o 14 6 1 227.75 275.18 67.03 o 16 6 1 604.99 674.82 107.39 o 18 6 1 384.23 329.66 87.06 o 20 6 1 1.15 18.90 56.35 o -19 7 1 46.88 22.17 63.44 o -17 7 1 53.35 154.22 96.34 o -15 7 1 160.56 127.30 67.34 o -13 7 1 2474.56 2573.16 149.98 o -11 7 1 44.79 48.26 30.33 o -9 7 1 269.09 207.78 50.22 o -7 7 1 597.51 632.73 63.41 o -5 7 1 6.65 85.21 51.11 o -3 7 1 36.23 16.96 36.62 o -1 7 1 593.88 680.87 61.76 o 1 7 1 35.02 36.30 31.84 o 3 7 1 2320.44 2129.89 103.60 o 5 7 1 657.78 673.74 94.13 o 7 7 1 633.86 819.04 70.32 o 9 7 1 469.02 580.07 61.19 o 11 7 1 42.74 46.06 33.40 o 13 7 1 641.28 612.82 73.94 o 15 7 1 185.96 165.07 80.06 o 17 7 1 72.64 87.52 71.45 o -16 8 1 4.82 46.22 92.82 o -14 8 1 212.22 135.86 75.19 o -12 8 1 0.52 0.00 41.48 o -10 8 1 0.20 76.92 37.20 o -8 8 1 914.13 813.06 73.08 o -6 8 1 451.89 518.87 62.88 o -4 8 1 528.73 548.49 93.79 o -2 8 1 534.18 659.30 68.55 o 0 8 1 182.83 194.41 65.69 o 2 8 1 17.85 0.00 25.48 o 4 8 1 63.37 31.36 30.55 o 6 8 1 169.23 160.74 45.40 o 8 8 1 14.54 0.00 33.65 o 10 8 1 250.76 113.10 42.07 o 12 8 1 0.17 5.09 30.55 o 14 8 1 6.76 56.91 59.13 o 16 8 1 195.75 74.11 97.61 o -13 9 1 10.87 0.00 76.83 o -11 9 1 42.43 26.62 50.09 o -9 9 1 151.79 76.46 51.62 o -7 9 1 29.73 0.00 33.52 o -5 9 1 166.71 341.21 130.66 o -3 9 1 6.75 31.72 38.65 o -1 9 1 256.96 187.56 86.57 o 1 9 1 274.31 289.07 97.86 o 3 9 1 27.11 0.00 43.72 o 5 9 1 20.46 35.25 39.95 o 7 9 1 45.25 2.79 33.88 o 9 9 1 274.06 100.60 49.39 o 11 9 1 225.47 117.56 104.68 o 13 9 1 101.80 115.37 101.30 o -8 10 1 27.07 19.08 62.65 o -6 10 1 37.14 40.23 50.40 o -4 10 1 40.03 142.33 105.17 o -2 10 1 183.60 105.88 59.77 o 0 10 1 43.11 83.61 62.51 o 2 10 1 166.21 230.06 102.58 o 4 10 1 21.37 155.06 113.38 o 6 10 1 40.69 40.16 54.91 o 8 10 1 0.83 9.96 53.61 o -24 0 2 462.55 461.66 285.31 o -22 0 2 811.22 760.69 138.66 o -20 0 2 1553.47 2013.33 140.83 o -18 0 2 3200.81 2986.96 213.46 o -16 0 2 2009.19 2123.12 174.89 o -14 0 2 1323.77 1420.67 112.49 o -12 0 2 4564.90 4815.68 328.95 o -10 0 2 5467.45 5237.81 475.85 o -8 0 2 175.14 481.04 30.34 o -6 0 2 46413.34 45542.76 949.13 o -4 0 2 11455.83 9136.05 136.69 o 2 0 2 18630.41 22959.00 225.32 o 4 0 2 24153.82 27050.52 326.54 o 6 0 2 3081.63 2526.03 86.75 o 8 0 2 7929.26 7739.71 271.73 o 10 0 2 180.15 245.05 34.85 o 12 0 2 8.27 61.13 47.77 o 14 0 2 3021.61 3069.26 141.53 o 16 0 2 275.29 309.24 62.45 o 18 0 2 207.21 244.77 87.64 o 20 0 2 3021.94 2864.69 300.68 o 22 0 2 128.81 50.41 70.47 o 24 0 2 8.78 11.90 69.20 o -25 1 2 4.46 49.29 65.82 o -23 1 2 185.89 72.51 51.22 o -21 1 2 405.95 368.21 57.89 o -19 1 2 2.26 95.37 63.57 o -17 1 2 1038.85 965.17 61.65 o -15 1 2 199.06 399.24 37.76 o -13 1 2 276.76 416.82 38.38 o -11 1 2 3468.09 3607.80 265.49 o -9 1 2 1709.08 2269.09 119.13 o -7 1 2 26388.31 28683.04 539.25 o -5 1 2 56609.54 55954.20 1436.93 o -3 1 2 38365.82 46677.68 792.08 o 1 1 2 8415.16 9248.71 103.12 o 3 1 2 125542.88 126577.39 1777.01 o 5 1 2 2126.34 2090.94 78.11 o 7 1 2 713.07 738.41 45.74 o 9 1 2 3135.49 2826.42 65.10 o 11 1 2 7421.57 6467.21 393.72 o 13 1 2 1948.69 2038.64 83.85 o 15 1 2 30.33 81.38 40.39 o 17 1 2 1731.69 1554.51 96.27 o 19 1 2 120.17 273.55 91.81 o 21 1 2 101.11 9.28 43.94 o 23 1 2 4.30 55.22 64.42 o -24 2 2 12.39 48.53 70.10 o -22 2 2 16.76 0.00 44.46 o -20 2 2 61.01 117.43 44.35 o -18 2 2 4.48 13.94 23.71 o -16 2 2 128.72 241.88 51.63 o -14 2 2 387.14 455.53 36.11 o -12 2 2 142.04 164.68 48.95 o -10 2 2 1983.00 1749.81 50.59 o -8 2 2 6889.54 7596.83 139.65 o -6 2 2 2952.12 2910.18 58.67 o -4 2 2 9623.27 10969.50 143.12 o -2 2 2 2712.73 3053.77 54.20 o 0 2 2 25279.04 29235.89 323.59 o 2 2 2 6434.23 7115.37 104.29 o 4 2 2 347.44 218.32 28.50 o 6 2 2 30.05 3.33 8.77 o 8 2 2 1.00 25.04 18.14 o 10 2 2 5.92 3.28 9.76 o 12 2 2 14.18 26.74 32.05 o 14 2 2 190.65 248.45 42.87 o 16 2 2 103.97 262.56 60.90 o 18 2 2 1651.63 1708.10 134.26 o 20 2 2 180.06 210.64 56.34 o 22 2 2 60.08 58.04 60.50 o -23 3 2 135.97 307.24 102.50 o -21 3 2 253.66 363.33 80.07 o -19 3 2 2.75 0.00 24.85 o -17 3 2 144.14 200.37 42.83 o -15 3 2 262.61 288.18 40.57 o -13 3 2 284.80 193.12 40.67 o -11 3 2 323.03 581.36 35.55 o -9 3 2 384.61 350.87 25.19 o -7 3 2 1243.83 1205.24 47.40 o -5 3 2 2402.85 2941.50 65.77 o -3 3 2 5284.63 5337.77 104.27 o -1 3 2 1006.90 834.53 40.10 o 1 3 2 610.51 526.83 25.23 o 3 3 2 216.08 322.93 47.42 o 5 3 2 389.74 352.00 27.25 o 7 3 2 749.34 550.50 45.73 o 9 3 2 1053.23 815.45 39.75 o 11 3 2 523.96 445.86 31.73 o 13 3 2 1757.26 1541.35 89.90 o 15 3 2 158.36 90.30 40.23 o 17 3 2 585.57 830.98 80.59 o 19 3 2 10.80 3.00 34.33 o 21 3 2 0.20 0.00 42.86 o 23 3 2 2.11 32.88 82.86 o -24 4 2 21.58 0.00 57.38 o -22 4 2 18.72 65.53 65.66 o -20 4 2 430.09 450.29 92.61 o -18 4 2 1.17 0.00 32.69 o -16 4 2 783.39 712.95 51.66 o -14 4 2 37.18 47.18 33.81 o -12 4 2 1895.67 1584.47 67.54 o -10 4 2 1358.25 1337.65 53.45 o -8 4 2 924.37 919.86 48.65 o -6 4 2 879.86 974.54 40.92 o -4 4 2 1557.25 1695.57 54.96 o -2 4 2 7705.08 8109.80 154.92 o 0 4 2 4074.78 4107.46 92.09 o 2 4 2 20104.29 19109.33 327.04 o 4 4 2 852.23 670.86 44.86 o 6 4 2 88.76 66.33 20.31 o 8 4 2 910.39 1039.07 50.05 o 10 4 2 582.16 444.26 39.22 o 12 4 2 23.36 67.51 35.01 o 14 4 2 529.08 734.70 74.65 o 16 4 2 252.75 346.72 64.56 o 18 4 2 81.06 79.50 45.03 o 20 4 2 213.08 260.60 85.13 o 22 4 2 41.92 96.70 112.72 o -21 5 2 192.62 170.61 78.81 o -19 5 2 186.07 171.90 74.52 o -17 5 2 752.49 719.96 83.75 o -15 5 2 26.36 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109.07 63.16 o -8 2 23 255.84 365.75 80.85 o -6 2 23 35.13 0.00 48.23 o -4 2 23 4.55 8.26 47.95 o -2 2 23 287.72 448.67 175.71 o 0 2 23 2.16 0.00 77.30 o -17 3 23 202.37 130.48 72.85 o -15 3 23 379.40 330.46 117.86 o -13 3 23 57.83 38.83 73.62 o -11 3 23 0.52 56.73 64.34 o -9 3 23 392.57 460.80 102.15 o -7 3 23 24.03 142.97 89.28 o -5 3 23 164.95 292.16 119.54 o -3 3 23 103.89 229.53 101.36 o -14 4 23 21.06 40.22 61.88 o -12 4 23 1.56 154.70 90.49 o -10 4 23 8.20 88.24 75.60 o -8 4 23 192.28 119.10 79.44 o -6 4 23 7.21 44.94 73.02 o -4 4 23 23.31 0.00 97.62 o -18 0 24 446.56 336.32 242.99 o -16 0 24 508.68 301.92 136.93 o -14 0 24 120.95 237.09 176.97 o -12 0 24 755.19 746.01 157.29 o -10 0 24 344.73 203.94 92.73 o -8 0 24 53.19 0.00 66.79 o -6 0 24 193.53 258.16 197.99 o -4 0 24 333.85 175.33 87.36 o -2 0 24 29.31 0.00 86.62 o -17 1 24 54.61 16.40 62.59 o -15 1 24 11.21 1.94 51.61 o -13 1 24 81.79 48.74 84.65 o -11 1 24 5.37 10.87 39.10 o -9 1 24 151.86 140.87 75.91 o -7 1 24 11.08 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