#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/36/2233692.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233692_Fobs loop_ _publ_author_name 'Choi, Hong Dae' 'Seo, Pil Ja' 'Lee, Uk' _publ_section_title ; 5-Bromo-3-cyclopentylsulfinyl-2,7-dimethyl-1-benzofuran ; _journal_coeditor_code XU5434 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o373 _journal_volume 68 _journal_year 2012 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.5624 _cell_length_b 8.3501 _cell_length_c 17.5346 _exptl_crystal_F_000 1392.00 _reflns_d_resolution_high 0.7474 _[local]_cod_data_source_file xu5434Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1145 IN PBCN' _shelx_refln_list_code 4 _shelx_f_calc_maximum 338.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2502.05 2585.45 66.15 o 4 0 0 3228.63 3221.99 82.52 o 6 0 0 20534.32 20542.38 471.07 o 8 0 0 24760.64 23696.67 546.51 o 10 0 0 23473.65 24102.41 563.24 o 12 0 0 53035.61 53948.62 1229.36 o 14 0 0 4619.52 4295.50 219.55 o 16 0 0 9983.25 10729.38 356.72 o 18 0 0 2605.60 2861.32 219.19 o 20 0 0 6279.57 5965.65 363.32 o 1 1 0 1888.36 2012.60 68.55 o 3 1 0 621.69 581.75 19.49 o 5 1 0 1741.86 1871.33 45.73 o 7 1 0 1168.97 1264.64 36.94 o 9 1 0 928.20 847.63 29.13 o 11 1 0 2242.81 2268.79 64.82 o 13 1 0 21.33 27.51 17.75 o 15 1 0 1120.16 1059.52 53.08 o 17 1 0 615.38 580.02 63.62 o 19 1 0 208.88 160.82 114.36 o 21 1 0 63.63 39.31 120.31 o 0 2 0 13881.87 14874.82 602.76 o 2 2 0 15394.02 16837.55 467.71 o 4 2 0 14441.09 15140.87 349.40 o 6 2 0 13044.63 13393.12 243.49 o 8 2 0 2869.53 2725.67 64.75 o 10 2 0 3800.27 3729.49 87.01 o 12 2 0 10537.86 10833.55 214.75 o 14 2 0 17.63 12.81 23.82 o 16 2 0 19.52 -33.62 33.62 o 18 2 0 4.87 -50.08 50.08 o 20 2 0 990.21 902.95 171.54 o 22 2 0 947.13 1137.62 200.13 o 1 3 0 2086.19 2157.46 186.43 o 3 3 0 1606.10 1796.48 70.78 o 5 3 0 87.63 43.38 10.66 o 7 3 0 4971.01 5215.12 143.12 o 9 3 0 3454.60 3497.39 151.13 o 11 3 0 7746.59 7921.31 145.81 o 13 3 0 991.02 988.00 49.23 o 15 3 0 486.83 675.63 55.53 o 17 3 0 1151.76 1206.71 175.11 o 19 3 0 389.45 409.78 145.33 o 21 3 0 1628.58 1549.78 227.52 o 23 3 0 2822.99 3217.50 322.82 o 0 4 0 17147.14 16566.36 708.78 o 2 4 0 18629.17 18987.05 566.42 o 4 4 0 11342.20 11093.86 280.15 o 6 4 0 28850.53 29888.34 589.15 o 8 4 0 11789.75 10416.71 264.90 o 10 4 0 19711.88 19364.06 754.64 o 12 4 0 3512.25 3036.55 141.90 o 14 4 0 9527.99 10400.58 551.54 o 16 4 0 3522.83 3598.69 296.61 o 18 4 0 3356.71 3548.66 320.44 o 20 4 0 1140.58 1296.05 226.33 o 22 4 0 2162.24 2270.47 287.09 o 24 4 0 83.18 77.43 173.92 o 1 5 0 2465.19 2530.73 133.51 o 3 5 0 2889.88 2867.85 104.71 o 5 5 0 101.66 29.44 26.78 o 7 5 0 717.48 803.16 35.65 o 9 5 0 153.87 81.27 73.86 o 11 5 0 7228.42 6710.17 306.14 o 13 5 0 542.29 445.52 141.76 o 15 5 0 339.57 204.89 126.27 o 17 5 0 2486.11 2459.88 278.75 o 19 5 0 15.23 302.57 170.35 o 21 5 0 3.16 -102.45 145.33 o 23 5 0 50.38 204.89 178.68 o 0 6 0 3549.73 3524.83 252.54 o 2 6 0 9374.42 9082.62 599.78 o 4 6 0 986.68 970.11 67.13 o 6 6 0 7228.01 7233.52 212.59 o 8 6 0 2458.54 2357.06 267.43 o 10 6 0 163.37 224.75 57.09 o 12 6 0 1218.69 1254.36 208.46 o 14 6 0 4650.81 3873.86 341.88 o 16 6 0 415.34 774.30 201.32 o 18 6 0 769.13 963.70 217.99 o 20 6 0 43.11 35.74 163.20 o 22 6 0 30.70 -45.27 185.83 o 1 7 0 6040.48 5865.41 434.20 o 3 7 0 573.36 648.73 64.52 o 5 7 0 1528.55 1522.12 138.20 o 7 7 0 23.60 25.11 64.27 o 9 7 0 1024.73 950.60 185.83 o 11 7 0 4.57 -114.36 114.36 o 13 7 0 753.49 572.98 184.64 o 15 7 0 739.27 729.03 208.46 o 17 7 0 192.05 466.96 197.74 o 19 7 0 53.62 277.56 195.36 o 0 8 0 1392.35 1120.94 181.07 o 2 8 0 1611.27 1524.88 98.85 o 4 8 0 2965.11 2599.72 161.56 o 6 8 0 306.02 301.77 56.80 o 8 8 0 1771.01 1450.91 238.24 o 10 8 0 977.59 911.29 212.04 o 12 8 0 60.20 113.17 170.35 o 14 8 0 2052.74 1571.23 277.56 o 16 8 0 2551.68 2961.38 362.13 o 18 8 0 58.69 42.88 184.64 o 1 9 0 423.04 394.60 75.88 o 3 9 0 33.43 -16.89 56.08 o 5 9 0 51.39 11.84 58.66 o 7 9 0 1090.32 676.62 200.13 o 9 9 0 141.16 184.64 176.30 o 11 9 0 56.15 65.52 163.20 o 13 9 0 432.52 810.03 251.35 o 15 9 0 670.96 488.40 233.48 o 0 10 0 155.40 115.22 82.74 o 2 10 0 1324.80 1748.47 123.59 o 4 10 0 1227.54 1179.31 243.01 o 6 10 0 345.25 310.91 202.51 o 8 10 0 832.56 724.26 243.01 o 10 10 0 804.54 1154.30 281.13 o 1 11 0 19.53 21.35 64.37 o 3 11 0 47.40 81.00 187.02 o 1 1 1 9912.00 10578.11 233.66 o 2 1 1 8387.86 8885.94 125.26 o 3 1 1 445.47 443.51 11.18 o 4 1 1 15832.76 16163.94 213.34 o 5 1 1 18623.81 18773.15 224.23 o 6 1 1 37.11 51.93 6.66 o 7 1 1 8284.99 8588.73 115.74 o 8 1 1 38.33 50.55 8.67 o 9 1 1 2439.42 2397.59 38.67 o 10 1 1 5244.05 5594.74 76.03 o 11 1 1 1947.33 1899.09 35.97 o 12 1 1 420.72 377.56 24.84 o 13 1 1 595.30 581.40 22.05 o 14 1 1 729.26 754.06 25.67 o 15 1 1 6.87 -4.19 16.93 o 16 1 1 696.51 705.24 36.36 o 17 1 1 289.60 277.07 29.89 o 18 1 1 1914.42 2010.96 111.54 o 19 1 1 41.89 32.03 54.02 o 20 1 1 233.19 214.68 95.30 o 21 1 1 856.67 528.37 119.72 o 22 1 1 208.34 297.81 139.37 o 0 2 1 10.37 24.05 30.97 o 1 2 1 21932.01 22695.98 448.92 o 2 2 1 20866.61 21269.22 375.77 o 3 2 1 111600.17 111851.79 1734.41 o 4 2 1 2933.46 3129.86 67.54 o 5 2 1 21728.89 20388.20 331.15 o 6 2 1 43.28 42.64 7.19 o 7 2 1 37460.68 37120.65 439.43 o 8 2 1 8669.25 9170.53 118.46 o 9 2 1 18129.80 18241.44 236.14 o 10 2 1 1437.67 1257.66 35.86 o 11 2 1 13700.78 13187.51 178.77 o 12 2 1 45.56 30.94 14.17 o 13 2 1 17900.20 17286.20 232.59 o 14 2 1 1901.37 1837.06 45.20 o 15 2 1 6682.24 6681.68 120.62 o 16 2 1 840.28 848.33 52.16 o 17 2 1 5568.12 5495.99 141.71 o 18 2 1 49.14 76.68 40.92 o 19 2 1 4100.69 4303.86 223.35 o 20 2 1 27.57 114.68 88.72 o 21 2 1 995.40 1141.40 244.20 o 22 2 1 51.67 63.81 96.86 o 23 2 1 2644.65 2643.33 287.09 o 24 2 1 88.05 96.49 159.62 o 1 3 1 3043.16 3112.27 100.57 o 2 3 1 19.76 -4.27 12.99 o 3 3 1 5559.98 5951.14 124.68 o 4 3 1 2513.61 2756.75 60.91 o 5 3 1 3367.58 3555.43 60.30 o 6 3 1 0.74 9.19 10.72 o 7 3 1 1491.13 1590.06 43.16 o 8 3 1 962.38 1150.36 32.30 o 9 3 1 703.11 712.53 30.09 o 10 3 1 72.61 70.25 11.70 o 11 3 1 524.76 543.12 18.80 o 12 3 1 54.13 18.53 12.83 o 13 3 1 145.98 175.82 20.97 o 14 3 1 1261.80 1200.57 43.76 o 15 3 1 16.62 -26.46 26.46 o 16 3 1 68.16 60.83 44.93 o 17 3 1 104.12 175.03 78.70 o 18 3 1 0.43 33.89 74.37 o 19 3 1 786.81 846.83 122.45 o 20 3 1 222.68 185.63 122.10 o 21 3 1 18.85 12.51 95.18 o 22 3 1 62.41 76.65 103.24 o 23 3 1 230.68 269.76 176.30 o 24 3 1 239.83 137.44 116.00 o 25 3 1 129.48 27.40 158.43 o 0 4 1 499.32 441.09 54.94 o 1 4 1 8128.49 7976.96 191.59 o 2 4 1 2787.22 3087.68 82.64 o 3 4 1 1617.87 1563.12 99.61 o 4 4 1 786.14 759.37 32.56 o 5 4 1 4469.83 4445.20 93.61 o 6 4 1 2239.02 2338.09 45.55 o 7 4 1 4249.05 4029.97 106.10 o 8 4 1 28.48 24.22 18.02 o 9 4 1 2128.72 2151.15 94.74 o 10 4 1 1632.95 1682.33 54.18 o 11 4 1 2763.30 2785.69 98.21 o 12 4 1 296.49 308.12 39.27 o 13 4 1 418.80 406.63 58.57 o 14 4 1 767.84 770.36 137.49 o 15 4 1 140.64 133.02 101.25 o 16 4 1 173.45 176.90 81.71 o 17 4 1 1782.65 1926.23 165.44 o 18 4 1 715.22 791.02 126.67 o 19 4 1 270.37 227.91 105.20 o 20 4 1 27.49 108.46 103.18 o 21 4 1 34.28 -58.74 95.00 o 22 4 1 1075.37 824.09 145.66 o 23 4 1 103.51 261.04 255.52 o 24 4 1 143.09 197.45 133.46 o 1 5 1 0.06 -15.83 27.74 o 2 5 1 40.67 53.53 25.28 o 3 5 1 91.12 118.89 27.29 o 4 5 1 941.48 1034.06 62.60 o 5 5 1 960.54 974.35 48.21 o 6 5 1 228.75 214.45 24.50 o 7 5 1 36.35 43.28 13.84 o 8 5 1 275.44 311.38 27.63 o 9 5 1 1698.85 1682.65 94.22 o 10 5 1 206.35 262.25 37.45 o 11 5 1 145.68 210.54 50.68 o 12 5 1 2073.90 2108.09 107.88 o 13 5 1 3.52 16.86 71.50 o 14 5 1 657.52 685.34 115.79 o 15 5 1 15.81 71.64 79.33 o 16 5 1 551.36 694.62 125.03 o 17 5 1 55.15 50.01 88.79 o 18 5 1 475.25 447.71 213.23 o 19 5 1 210.17 230.50 110.34 o 20 5 1 306.41 377.02 122.56 o 21 5 1 0.29 24.87 109.80 o 22 5 1 365.98 401.10 244.20 o 23 5 1 6.63 23.50 119.19 o 0 6 1 5398.47 4940.23 216.30 o 1 6 1 4932.60 4855.63 151.50 o 2 6 1 50.38 60.73 30.77 o 3 6 1 12245.22 11960.58 251.91 o 4 6 1 252.58 211.68 29.68 o 5 6 1 2655.11 2455.21 72.64 o 6 6 1 2862.41 2741.56 77.56 o 7 6 1 4090.06 4125.37 80.81 o 8 6 1 108.60 57.47 31.05 o 9 6 1 6889.11 6756.43 174.81 o 10 6 1 673.30 562.95 65.12 o 11 6 1 3691.88 3309.44 140.90 o 12 6 1 1142.27 947.56 129.24 o 13 6 1 2154.98 2379.57 420.50 o 14 6 1 93.10 33.71 87.17 o 15 6 1 2504.09 2268.67 191.91 o 16 6 1 6.83 -19.13 142.35 o 17 6 1 1571.54 1499.89 175.92 o 18 6 1 554.13 645.22 140.60 o 19 6 1 1107.01 1248.92 177.31 o 20 6 1 118.69 65.55 116.28 o 21 6 1 967.48 810.80 330.56 o 1 7 1 805.98 855.63 73.88 o 2 7 1 33.37 47.84 35.58 o 3 7 1 23.09 25.87 29.35 o 4 7 1 387.76 428.94 39.89 o 5 7 1 0.76 -24.21 25.67 o 6 7 1 287.91 288.29 38.80 o 7 7 1 74.38 54.26 30.26 o 8 7 1 101.99 108.68 49.68 o 9 7 1 363.92 334.23 87.20 o 10 7 1 290.11 275.71 139.37 o 11 7 1 413.27 267.75 161.41 o 12 7 1 525.78 721.91 198.93 o 13 7 1 175.80 98.37 154.86 o 14 7 1 363.45 166.79 113.63 o 15 7 1 1.42 -76.70 90.05 o 16 7 1 464.02 397.55 134.70 o 17 7 1 152.66 212.50 172.13 o 18 7 1 659.80 538.70 153.58 o 19 7 1 286.60 106.65 182.26 o 20 7 1 77.26 36.48 121.04 o 0 8 1 2153.13 2411.03 338.31 o 1 8 1 2586.60 2791.10 117.58 o 2 8 1 323.58 209.19 48.56 o 3 8 1 3023.51 3045.57 97.67 o 4 8 1 41.83 38.43 35.48 o 5 8 1 1385.72 1591.73 94.15 o 6 8 1 1037.29 1020.36 83.03 o 7 8 1 632.29 625.42 67.82 o 8 8 1 17.84 -10.03 71.64 o 9 8 1 2375.11 2708.11 496.15 o 10 8 1 9.44 17.16 99.60 o 11 8 1 1858.90 2139.13 200.21 o 12 8 1 660.88 706.18 142.68 o 13 8 1 373.06 511.73 138.91 o 14 8 1 83.84 46.23 105.55 o 15 8 1 554.72 862.71 166.37 o 16 8 1 60.72 -9.85 111.59 o 17 8 1 974.34 832.67 243.01 o 18 8 1 1.26 8.40 151.88 o 1 9 1 74.66 65.63 49.51 o 2 9 1 7.76 -24.52 40.46 o 3 9 1 22.65 20.89 41.17 o 4 9 1 72.42 86.00 41.93 o 5 9 1 40.38 41.36 54.03 o 6 9 1 9.92 38.57 53.82 o 7 9 1 6.78 44.82 107.33 o 8 9 1 0.60 -92.21 92.21 o 9 9 1 31.86 -77.30 102.75 o 10 9 1 20.75 149.34 118.76 o 11 9 1 406.82 410.63 146.10 o 12 9 1 11.10 159.19 127.44 o 13 9 1 436.73 417.28 150.25 o 14 9 1 669.31 516.64 224.55 o 15 9 1 148.86 324.82 149.83 o 0 10 1 10.72 16.50 54.31 o 1 10 1 610.12 596.49 76.75 o 2 10 1 15.18 -21.42 41.49 o 3 10 1 4.35 -8.02 62.32 o 4 10 1 2.87 -53.71 59.19 o 5 10 1 283.82 237.20 127.26 o 6 10 1 22.26 242.00 155.45 o 7 10 1 101.84 77.88 124.73 o 8 10 1 3.80 195.77 140.23 o 9 10 1 138.11 143.19 137.59 o 10 10 1 290.23 233.41 152.00 o 11 10 1 475.75 343.64 153.24 o 1 11 1 14.59 129.21 54.23 o 2 11 1 162.10 318.22 97.49 o 3 11 1 0.06 43.48 86.32 o 4 11 1 25.44 245.27 147.34 o 0 0 2 48572.56 46754.33 1045.30 o 1 0 2 533.07 553.04 12.74 o 2 0 2 7329.35 7833.75 129.27 o 3 0 2 20209.39 20955.10 335.76 o 4 0 2 114755.91 109686.49 3283.31 o 5 0 2 38336.53 38906.23 618.91 o 6 0 2 20394.08 20795.30 338.12 o 7 0 2 602.74 626.18 23.03 o 8 0 2 40177.26 39231.43 630.20 o 9 0 2 12065.12 11708.92 202.38 o 10 0 2 35791.93 34429.06 559.46 o 11 0 2 520.80 472.24 26.12 o 12 0 2 17324.23 17113.03 293.30 o 13 0 2 186.73 170.11 22.85 o 14 0 2 3403.81 3315.00 81.01 o 15 0 2 7176.44 6950.87 141.88 o 16 0 2 15760.14 15650.95 348.41 o 17 0 2 2459.68 2631.00 145.61 o 18 0 2 156.23 328.41 130.44 o 19 0 2 92.43 17.87 91.72 o 20 0 2 6501.27 6270.61 378.81 o 21 0 2 718.25 1094.74 173.92 o 22 0 2 849.96 690.91 165.58 o 1 1 2 9835.17 9995.59 184.10 o 2 1 2 12759.05 12837.42 171.83 o 3 1 2 30497.93 31264.68 386.53 o 4 1 2 253.15 260.43 10.55 o 5 1 2 1637.49 1766.35 28.10 o 6 1 2 950.39 1058.49 22.86 o 7 1 2 911.54 926.68 20.67 o 8 1 2 528.80 627.86 18.07 o 9 1 2 3264.78 3817.58 57.97 o 10 1 2 321.16 323.20 15.99 o 11 1 2 233.84 220.59 15.33 o 12 1 2 161.69 182.11 15.78 o 13 1 2 1622.01 1693.99 40.10 o 14 1 2 210.01 173.31 18.26 o 15 1 2 873.06 918.68 35.26 o 16 1 2 279.61 237.39 27.41 o 17 1 2 10.01 -2.83 27.31 o 18 1 2 467.19 474.25 69.21 o 19 1 2 24.85 47.25 56.82 o 20 1 2 20.75 2.41 60.09 o 21 1 2 136.15 228.72 132.23 o 22 1 2 163.92 -102.45 114.36 o 23 1 2 64.17 89.34 139.37 o 0 2 2 174.10 171.55 27.46 o 1 2 2 2722.88 2940.19 66.57 o 2 2 2 335.22 465.44 27.13 o 3 2 2 19217.18 19742.67 276.63 o 4 2 2 43069.81 43598.80 597.26 o 5 2 2 1529.03 1673.48 37.87 o 6 2 2 170.67 170.54 10.20 o 7 2 2 1.60 3.77 9.54 o 8 2 2 4539.35 4695.07 66.77 o 9 2 2 2649.45 2516.03 42.96 o 10 2 2 71.61 168.15 17.47 o 11 2 2 94.01 76.75 14.46 o 12 2 2 21.19 4.67 13.82 o 13 2 2 7.04 12.06 15.42 o 14 2 2 10.01 -15.87 15.95 o 15 2 2 124.87 145.06 29.78 o 16 2 2 4015.51 3915.41 110.88 o 17 2 2 0.96 -29.65 30.91 o 18 2 2 18.93 4.24 35.26 o 19 2 2 118.93 31.56 77.04 o 20 2 2 1271.46 983.36 124.59 o 21 2 2 89.31 -83.61 83.61 o 22 2 2 7.01 -54.76 88.79 o 23 2 2 8.82 46.46 138.18 o 24 2 2 56.62 -57.18 138.18 o 1 3 2 606.90 602.92 40.31 o 2 3 2 41.31 52.16 16.06 o 3 3 2 392.24 464.96 28.46 o 4 3 2 813.58 849.13 29.43 o 5 3 2 1717.93 1924.89 38.23 o 6 3 2 3048.29 3125.46 60.44 o 7 3 2 11349.16 11493.20 200.12 o 8 3 2 244.53 245.75 16.64 o 9 3 2 102.45 96.49 26.54 o 10 3 2 543.89 520.16 17.40 o 11 3 2 192.77 229.81 16.70 o 12 3 2 155.77 144.18 19.66 o 13 3 2 3666.51 3577.64 92.14 o 14 3 2 1793.19 1691.71 52.99 o 15 3 2 3162.53 3278.23 96.83 o 16 3 2 8.36 8.40 48.95 o 17 3 2 49.40 97.93 64.36 o 18 3 2 9.68 -11.08 79.97 o 19 3 2 1030.99 1181.30 135.42 o 20 3 2 230.58 339.55 103.56 o 21 3 2 1351.24 1191.97 146.50 o 22 3 2 76.75 87.44 98.52 o 23 3 2 18.65 76.07 173.92 o 24 3 2 58.04 -57.18 153.67 o 25 3 2 72.71 94.11 166.77 o 0 4 2 8657.55 8403.01 283.37 o 1 4 2 3382.54 3452.64 89.19 o 2 4 2 22594.74 22732.79 464.66 o 3 4 2 714.63 631.16 36.05 o 4 4 2 14717.10 14853.92 284.69 o 5 4 2 16772.93 17551.98 298.23 o 6 4 2 40583.32 39578.28 551.17 o 7 4 2 85.15 54.96 14.18 o 8 4 2 2545.42 2351.42 98.29 o 9 4 2 410.93 386.63 27.37 o 10 4 2 9311.71 9240.97 187.23 o 11 4 2 3960.65 3958.56 145.72 o 12 4 2 4900.21 4573.69 162.16 o 13 4 2 1346.73 1204.87 85.04 o 14 4 2 5414.31 5240.33 183.88 o 15 4 2 476.90 474.86 109.89 o 16 4 2 1605.44 1916.54 196.55 o 17 4 2 490.10 514.13 106.94 o 18 4 2 6153.49 5589.38 280.91 o 19 4 2 185.98 121.77 97.26 o 20 4 2 3611.29 3647.87 238.77 o 21 4 2 1131.12 833.16 143.85 o 22 4 2 667.17 490.66 131.73 o 23 4 2 8.93 13.01 110.74 o 24 4 2 151.51 54.06 122.76 o 1 5 2 2080.88 2172.98 145.41 o 2 5 2 1529.94 1497.45 61.54 o 3 5 2 1491.31 1476.27 60.06 o 4 5 2 158.98 105.89 27.61 o 5 5 2 412.60 501.52 34.01 o 6 5 2 4.60 -3.87 12.16 o 7 5 2 2647.81 2631.45 55.07 o 8 5 2 739.61 847.29 47.99 o 9 5 2 26.68 -31.12 31.12 o 10 5 2 326.86 293.56 51.70 o 11 5 2 58.72 77.08 60.45 o 12 5 2 25.27 129.79 49.24 o 13 5 2 201.31 194.37 57.81 o 14 5 2 218.38 186.54 83.73 o 15 5 2 1016.88 885.01 207.87 o 16 5 2 165.59 73.25 88.53 o 17 5 2 37.87 93.10 99.22 o 18 5 2 22.55 83.58 120.31 o 19 5 2 748.77 926.33 144.15 o 20 5 2 215.72 137.06 115.36 o 21 5 2 107.48 167.34 222.16 o 22 5 2 3.49 -128.65 128.65 o 23 5 2 15.68 217.82 135.60 o 0 6 2 1763.69 1794.12 126.98 o 1 6 2 2315.40 2240.80 82.82 o 2 6 2 4854.09 4594.59 154.39 o 3 6 2 710.28 695.84 48.99 o 4 6 2 2348.69 2290.28 70.42 o 5 6 2 690.26 647.37 39.88 o 6 6 2 3365.89 3521.53 90.48 o 7 6 2 221.08 270.79 22.35 o 8 6 2 1756.89 1677.17 64.25 o 9 6 2 2626.37 2424.31 133.41 o 10 6 2 3563.18 3612.42 169.18 o 11 6 2 378.96 329.02 62.55 o 12 6 2 809.53 935.94 135.81 o 13 6 2 4.26 -60.13 78.84 o 14 6 2 2460.65 2944.02 211.48 o 15 6 2 312.53 205.77 103.60 o 16 6 2 49.11 16.36 92.73 o 17 6 2 1.83 88.33 108.53 o 18 6 2 173.43 178.68 118.77 o 19 6 2 23.33 144.44 121.70 o 20 6 2 217.67 97.68 123.82 o 21 6 2 58.74 -21.26 306.14 o 1 7 2 39.11 31.92 36.45 o 2 7 2 1227.18 1215.39 75.56 o 3 7 2 57.49 30.58 35.49 o 4 7 2 348.73 367.42 49.01 o 5 7 2 2058.71 1979.47 71.26 o 6 7 2 208.58 178.65 33.21 o 7 7 2 29.94 33.12 43.44 o 8 7 2 112.77 123.38 78.50 o 9 7 2 14.94 -11.19 49.76 o 10 7 2 603.82 624.36 74.63 o 11 7 2 235.51 416.03 112.39 o 12 7 2 59.26 -24.92 86.31 o 13 7 2 7.38 -33.38 83.61 o 14 7 2 425.80 157.98 249.56 o 15 7 2 54.68 -0.31 96.67 o 16 7 2 182.89 177.03 114.86 o 17 7 2 1497.79 1384.94 302.57 o 18 7 2 185.36 285.91 134.02 o 19 7 2 65.71 40.27 188.21 o 20 7 2 0.88 -114.86 119.53 o 0 8 2 2602.32 2471.45 128.90 o 1 8 2 1590.81 1392.22 79.96 o 2 8 2 425.26 427.56 61.34 o 3 8 2 5.12 49.26 40.28 o 4 8 2 882.03 842.22 71.92 o 5 8 2 32.32 33.75 34.94 o 6 8 2 2025.59 1984.96 153.54 o 7 8 2 370.70 286.50 104.36 o 8 8 2 851.96 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365.96 83.73 o 13 7 10 2.82 26.68 65.51 o 14 7 10 1083.85 1100.24 98.23 o 15 7 10 0.21 -42.27 63.08 o 16 7 10 183.74 144.92 97.41 o 17 7 10 121.11 -39.31 121.60 o 0 8 10 31.43 17.44 90.53 o 1 8 10 310.13 413.23 64.63 o 2 8 10 430.73 304.60 99.07 o 3 8 10 1291.52 1391.53 86.91 o 4 8 10 168.81 118.18 59.05 o 5 8 10 162.17 177.50 62.41 o 6 8 10 1505.12 1303.11 94.50 o 7 8 10 236.79 356.02 69.86 o 8 8 10 45.09 66.58 61.80 o 9 8 10 523.52 510.83 81.44 o 10 8 10 4.33 -21.51 62.35 o 11 8 10 679.87 751.96 120.10 o 12 8 10 385.42 201.68 76.64 o 13 8 10 371.43 421.51 86.94 o 14 8 10 472.40 446.34 87.53 o 1 9 10 40.93 -22.16 58.86 o 2 9 10 36.12 -35.20 64.65 o 3 9 10 220.60 136.76 69.94 o 4 9 10 68.84 -3.51 61.08 o 5 9 10 22.07 -16.36 69.89 o 6 9 10 181.82 169.45 73.07 o 7 9 10 9.37 -20.12 90.61 o 8 9 10 48.37 162.84 88.72 o 9 9 10 59.28 16.85 74.15 o 10 9 10 277.89 301.23 85.99 o 0 10 10 656.03 787.73 324.01 o 1 10 10 206.74 134.74 84.42 o 2 10 10 128.65 65.17 78.06 o 3 10 10 459.89 646.48 140.19 o 1 1 11 730.26 676.71 24.48 o 2 1 11 13.06 24.45 13.55 o 3 1 11 1307.20 1436.07 35.47 o 4 1 11 2012.03 1983.63 54.89 o 5 1 11 1422.06 1435.37 37.46 o 6 1 11 645.97 630.19 25.14 o 7 1 11 3320.82 3146.23 56.94 o 8 1 11 1138.85 1243.00 34.42 o 9 1 11 25.83 8.95 18.62 o 10 1 11 481.80 441.65 31.25 o 11 1 11 4.16 -0.35 22.23 o 12 1 11 615.72 580.35 39.12 o 13 1 11 718.38 762.88 103.12 o 14 1 11 47.42 116.57 75.30 o 15 1 11 2053.21 2161.99 177.49 o 16 1 11 118.57 167.79 91.16 o 17 1 11 103.56 140.19 119.72 o 18 1 11 93.54 141.16 96.87 o 19 1 11 1584.03 1835.28 288.87 o 20 1 11 435.67 730.98 130.27 o 21 1 11 13.14 89.63 113.26 o 22 1 11 12.24 136.08 201.32 o 0 2 11 9847.54 9192.58 171.31 o 1 2 11 1867.18 1817.75 38.07 o 2 2 11 9591.51 8761.11 120.94 o 3 2 11 11999.47 11090.62 148.11 o 4 2 11 12707.21 12271.94 156.53 o 5 2 11 9644.65 9445.20 130.43 o 6 2 11 1885.48 1733.96 39.18 o 7 2 11 178.15 176.74 21.52 o 8 2 11 14211.51 14350.56 210.08 o 9 2 11 3111.97 3164.90 70.75 o 10 2 11 4097.52 4225.96 133.11 o 11 2 11 4461.37 4602.25 104.31 o 12 2 11 3096.73 3208.21 131.80 o 13 2 11 480.81 511.32 49.76 o 14 2 11 1916.93 2107.10 131.88 o 15 2 11 3878.69 3480.38 204.51 o 16 2 11 2015.20 1989.21 158.87 o 17 2 11 1192.88 1076.32 690.31 o 18 2 11 1445.32 1325.06 150.05 o 19 2 11 28.08 -20.30 93.22 o 20 2 11 648.77 808.39 329.37 o 21 2 11 946.42 911.62 146.41 o 22 2 11 1156.66 1675.34 185.41 o 1 3 11 6.35 5.11 20.99 o 2 3 11 398.81 454.64 46.06 o 3 3 11 1064.57 1057.75 65.16 o 4 3 11 676.35 784.04 44.87 o 5 3 11 1674.75 1590.65 48.45 o 6 3 11 54.92 51.61 21.17 o 7 3 11 1301.62 1243.57 46.46 o 8 3 11 667.14 677.71 60.55 o 9 3 11 176.17 151.06 24.31 o 10 3 11 135.81 113.07 24.28 o 11 3 11 2.02 -18.08 24.27 o 12 3 11 0.06 -17.04 29.85 o 13 3 11 24.34 24.36 49.13 o 14 3 11 20.50 26.59 49.29 o 15 3 11 25.76 34.03 50.34 o 16 3 11 33.30 2.90 56.85 o 17 3 11 272.84 414.16 114.14 o 18 3 11 200.89 215.55 104.70 o 19 3 11 6.20 3.89 100.06 o 20 3 11 133.19 28.57 104.93 o 21 3 11 38.07 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29.93 43.37 51.97 o 12 5 11 200.94 100.17 57.76 o 13 5 11 408.37 497.13 78.58 o 14 5 11 186.36 181.97 64.02 o 15 5 11 229.08 197.89 81.28 o 16 5 11 25.34 9.21 62.61 o 17 5 11 80.62 112.01 73.58 o 18 5 11 40.37 24.85 65.53 o 19 5 11 615.86 852.83 145.55 o 0 6 11 2266.09 2487.90 125.42 o 1 6 11 1743.00 1717.19 81.77 o 2 6 11 497.54 568.08 59.19 o 3 6 11 145.26 151.66 46.42 o 4 6 11 525.12 620.25 72.11 o 5 6 11 2412.00 2484.23 109.90 o 6 6 11 5728.60 5537.52 171.43 o 7 6 11 1214.75 1279.95 83.00 o 8 6 11 1122.01 1190.36 85.48 o 9 6 11 168.53 192.41 59.52 o 10 6 11 465.77 371.30 68.09 o 11 6 11 1978.51 2073.80 112.48 o 12 6 11 1142.72 1293.98 119.33 o 13 6 11 789.59 702.01 80.51 o 14 6 11 913.71 931.11 92.32 o 15 6 11 45.27 75.27 68.79 o 16 6 11 36.88 39.80 68.79 o 17 6 11 368.19 249.03 79.20 o 18 6 11 1544.75 1558.21 116.80 o 1 7 11 175.33 234.89 51.69 o 2 7 11 15.15 -2.87 43.11 o 3 7 11 412.59 420.75 62.36 o 4 7 11 0.19 -1.71 48.35 o 5 7 11 48.50 17.50 50.97 o 6 7 11 37.50 -22.67 49.09 o 7 7 11 33.22 102.43 57.41 o 8 7 11 13.08 76.97 60.74 o 9 7 11 129.68 168.92 65.02 o 10 7 11 43.58 96.57 62.67 o 11 7 11 3.62 -29.80 62.59 o 12 7 11 4.40 -58.50 58.50 o 13 7 11 692.95 732.06 92.21 o 14 7 11 300.31 388.81 82.08 o 15 7 11 487.73 585.84 88.96 o 16 7 11 4.46 46.04 75.10 o 0 8 11 954.68 1231.12 243.61 o 1 8 11 254.94 190.05 63.25 o 2 8 11 1403.11 1469.95 96.96 o 3 8 11 607.95 590.39 73.67 o 4 8 11 211.94 252.56 65.17 o 5 8 11 30.82 -13.70 56.38 o 6 8 11 1620.44 2021.28 113.27 o 7 8 11 187.00 166.85 66.29 o 8 8 11 332.62 264.61 69.65 o 9 8 11 209.04 147.61 70.11 o 10 8 11 51.20 110.42 71.98 o 11 8 11 23.82 -26.94 67.48 o 12 8 11 634.73 876.60 102.04 o 13 8 11 158.42 310.25 84.71 o 1 9 11 0.19 66.05 66.02 o 2 9 11 465.96 520.15 79.00 o 3 9 11 31.64 40.00 68.26 o 4 9 11 82.12 166.22 74.42 o 5 9 11 125.59 113.29 94.91 o 6 9 11 75.31 36.91 68.54 o 7 9 11 279.25 318.48 87.52 o 8 9 11 194.97 157.15 73.71 o 9 9 11 8.80 9.96 71.67 o 0 0 12 2531.69 2464.48 98.72 o 1 0 12 8241.01 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12 1 12 221.41 98.65 142.35 o 13 1 12 342.60 78.17 183.45 o 14 1 12 490.71 598.93 104.74 o 15 1 12 607.46 449.40 103.80 o 16 1 12 404.43 212.92 98.87 o 17 1 12 5.90 -48.59 91.72 o 18 1 12 95.37 174.24 103.44 o 19 1 12 611.55 701.34 132.24 o 20 1 12 30.29 295.57 110.88 o 21 1 12 137.44 125.58 116.47 o 22 1 12 21.42 150.17 118.53 o 0 2 12 456.85 401.33 35.39 o 1 2 12 968.49 924.12 31.43 o 2 2 12 700.35 725.73 29.52 o 3 2 12 4651.01 4332.20 74.48 o 4 2 12 314.70 317.85 22.02 o 5 2 12 183.94 200.39 20.42 o 6 2 12 4272.33 4026.27 81.93 o 7 2 12 220.85 183.86 24.76 o 8 2 12 139.74 113.71 22.61 o 9 2 12 2268.99 2246.65 65.22 o 10 2 12 11.89 3.47 24.21 o 11 2 12 99.66 51.03 26.12 o 12 2 12 14.20 -6.61 39.77 o 13 2 12 25.42 -23.85 41.56 o 14 2 12 350.57 317.56 97.22 o 15 2 12 643.93 839.93 165.58 o 16 2 12 3.24 -50.14 84.50 o 17 2 12 2.23 59.89 92.16 o 18 2 12 860.80 782.12 137.37 o 19 2 12 5.75 210.32 109.26 o 20 2 12 21.70 17.48 111.08 o 21 2 12 78.42 234.22 120.19 o 1 3 12 21.55 46.76 24.13 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