#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/37/2233700.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233700_Fobs loop_ _publ_author_name 'Roteta, Leslie' 'Tanski, Joseph M.' _publ_section_title ; [(4R,5R)-(2,2-Dimethyl-1,3-dioxolane-4,5-diyl)bis(diphenylmethanolato)-\k^2^O:O']bis(N-methylmethanaminato)titanium(IV) ; _journal_coeditor_code YK2040 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m217 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.562 _cell_angle_gamma 90.000 _cell_length_a 9.4932 _cell_length_b 21.4059 _cell_length_c 15.7431 _exptl_crystal_F_000 1272.00 _reflns_d_resolution_high 0.7397 _[local]_cod_data_source_file yk2040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LR1049Ti in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -28 0 8.50 -3.82 59.20 o 2 -28 0 123.67 147.23 57.76 o 3 -28 0 139.84 209.97 57.77 o 1 -27 0 2.94 -47.26 47.26 o 2 -27 0 148.34 86.41 50.63 o 3 -27 0 96.88 144.34 52.61 o 4 -27 0 85.96 233.93 59.40 o 0 -26 0 262.08 299.80 86.88 o 1 -26 0 166.88 277.09 67.31 o 2 -26 0 5.68 -36.76 37.81 o 3 -26 0 73.03 67.95 45.89 o 4 -26 0 418.50 500.18 69.50 o 5 -26 0 30.82 147.99 73.52 o 1 -25 0 166.67 194.12 75.90 o 2 -25 0 119.21 108.63 42.47 o 3 -25 0 73.95 64.50 47.26 o 4 -25 0 7.26 28.58 40.44 o 5 -25 0 108.33 158.24 56.81 o 6 -25 0 254.72 186.18 77.34 o 0 -24 0 894.54 1323.84 222.46 o 1 -24 0 46.50 1.71 37.25 o 2 -24 0 228.15 207.09 49.90 o 3 -24 0 236.23 247.57 51.62 o 4 -24 0 46.45 12.81 39.14 o 5 -24 0 409.75 467.93 105.02 o 6 -24 0 25.69 36.28 63.01 o 1 -23 0 96.36 135.32 36.37 o 2 -23 0 515.36 654.52 72.09 o 3 -23 0 30.55 77.80 39.09 o 4 -23 0 7.41 8.93 37.46 o 5 -23 0 80.27 66.71 36.58 o 6 -23 0 165.74 175.79 43.07 o 7 -23 0 35.70 25.59 80.20 o 0 -22 0 324.81 299.30 49.62 o 1 -22 0 308.36 462.65 47.69 o 2 -22 0 293.37 256.27 48.94 o 3 -22 0 47.60 33.26 36.97 o 4 -22 0 30.12 -28.58 28.58 o 5 -22 0 155.79 124.68 53.24 o 6 -22 0 0.36 -58.62 58.62 o 7 -22 0 18.33 14.25 46.83 o 1 -21 0 240.07 233.52 31.40 o 2 -21 0 203.07 352.49 51.64 o 3 -21 0 195.49 220.08 46.24 o 4 -21 0 46.93 17.75 31.00 o 5 -21 0 405.68 523.83 57.92 o 6 -21 0 26.23 41.02 34.60 o 7 -21 0 491.59 547.67 59.35 o 8 -21 0 116.13 62.43 142.26 o 0 -20 0 739.69 972.98 71.41 o 1 -20 0 290.91 283.21 32.03 o 2 -20 0 140.56 236.97 44.56 o 3 -20 0 548.14 605.45 54.43 o 4 -20 0 1147.05 1365.91 72.71 o 5 -20 0 61.33 87.12 34.96 o 6 -20 0 134.59 110.12 36.73 o 7 -20 0 124.36 115.62 39.47 o 8 -20 0 90.57 134.39 87.84 o 9 -20 0 113.13 128.89 78.29 o 1 -19 0 19.11 23.54 20.89 o 2 -19 0 19.96 53.64 33.74 o 3 -19 0 163.12 163.13 34.09 o 4 -19 0 523.81 507.99 50.09 o 5 -19 0 188.00 204.61 42.24 o 6 -19 0 761.97 978.90 65.95 o 7 -19 0 28.86 16.97 32.13 o 8 -19 0 379.96 496.42 70.95 o 9 -19 0 95.88 55.97 53.52 o 0 -18 0 2357.40 2663.68 159.45 o 1 -18 0 127.59 133.42 25.02 o 2 -18 0 7.52 -2.06 19.48 o 3 -18 0 103.17 71.70 40.49 o 4 -18 0 293.77 308.66 40.66 o 5 -18 0 456.17 464.65 48.61 o 6 -18 0 364.65 411.40 47.83 o 7 -18 0 20.77 40.41 33.91 o 8 -18 0 2.68 -25.94 51.80 o 9 -18 0 44.98 75.66 52.87 o 10 -18 0 48.41 44.87 74.47 o 1 -17 0 956.76 1146.51 69.96 o 2 -17 0 1958.52 1892.13 62.68 o 3 -17 0 230.32 262.46 36.07 o 4 -17 0 279.25 348.05 41.26 o 5 -17 0 899.51 1129.56 84.18 o 6 -17 0 1.67 -24.35 27.66 o 7 -17 0 820.77 892.56 64.12 o 8 -17 0 132.34 87.82 37.92 o 9 -17 0 172.54 145.78 73.99 o 10 -17 0 74.08 115.24 57.64 o 0 -16 0 2296.49 2546.05 80.25 o 1 -16 0 1687.55 2060.71 55.44 o 2 -16 0 731.43 888.04 37.82 o 3 -16 0 1686.39 1631.42 70.72 o 4 -16 0 592.32 680.28 51.25 o 5 -16 0 88.28 139.58 33.02 o 6 -16 0 168.00 184.44 37.85 o 7 -16 0 133.17 177.38 38.00 o 8 -16 0 186.13 120.69 39.01 o 9 -16 0 38.34 64.00 37.55 o 10 -16 0 39.48 39.76 51.38 o 1 -15 0 536.71 612.84 30.51 o 2 -15 0 1328.86 1435.51 44.83 o 3 -15 0 369.16 461.73 35.97 o 4 -15 0 1021.57 1090.23 60.02 o 5 -15 0 69.97 19.90 41.82 o 6 -15 0 595.42 724.68 96.32 o 7 -15 0 277.63 309.67 71.42 o 8 -15 0 42.29 23.87 31.37 o 9 -15 0 88.22 38.55 55.00 o 10 -15 0 1.35 58.02 52.19 o 0 -14 0 2331.29 2942.38 83.64 o 1 -14 0 518.23 554.34 24.85 o 2 -14 0 109.18 117.51 16.87 o 3 -14 0 386.71 532.11 29.58 o 4 -14 0 195.01 182.73 25.05 o 5 -14 0 487.28 680.36 42.68 o 6 -14 0 46.38 -21.37 26.39 o 7 -14 0 480.89 483.60 49.31 o 8 -14 0 27.37 51.26 32.59 o 9 -14 0 134.45 120.96 40.74 o 10 -14 0 5.50 63.83 39.23 o 11 -14 0 5.27 82.11 83.07 o 1 -13 0 234.28 242.81 16.56 o 2 -13 0 1247.29 1174.75 38.42 o 3 -13 0 606.08 649.01 29.92 o 4 -13 0 618.83 647.40 38.56 o 5 -13 0 128.75 147.49 25.32 o 6 -13 0 418.27 414.90 36.49 o 7 -13 0 54.72 62.21 25.66 o 8 -13 0 327.20 435.94 48.25 o 9 -13 0 80.80 58.92 36.30 o 10 -13 0 12.92 4.80 35.74 o 11 -13 0 36.44 21.96 75.43 o 0 -12 0 37.90 69.11 17.03 o 1 -12 0 854.29 827.95 26.71 o 2 -12 0 2527.26 2685.85 60.05 o 3 -12 0 402.13 475.96 26.36 o 4 -12 0 1447.68 1550.03 53.19 o 5 -12 0 671.72 871.39 44.00 o 6 -12 0 1007.26 1192.54 52.49 o 7 -12 0 81.71 94.82 28.44 o 8 -12 0 77.33 97.27 28.11 o 9 -12 0 154.29 166.48 40.93 o 10 -12 0 5.57 49.11 36.22 o 11 -12 0 39.01 7.64 71.61 o 1 -11 0 2063.93 2459.39 46.26 o 2 -11 0 3024.40 3654.37 73.42 o 3 -11 0 1359.63 1588.95 42.18 o 4 -11 0 262.13 243.23 23.46 o 5 -11 0 1239.68 1283.63 50.65 o 6 -11 0 9.54 38.55 21.38 o 7 -11 0 1303.73 1273.37 55.91 o 8 -11 0 178.52 225.75 32.01 o 9 -11 0 192.84 243.53 44.10 o 10 -11 0 61.61 16.30 55.12 o 11 -11 0 60.58 28.43 47.71 o 0 -10 0 8364.50 10320.51 192.93 o 1 -10 0 5554.55 7325.54 107.92 o 2 -10 0 244.60 350.98 22.69 o 3 -10 0 1697.87 1667.04 42.85 o 4 -10 0 809.94 868.77 39.21 o 5 -10 0 156.47 287.94 26.30 o 6 -10 0 29.02 29.92 20.03 o 7 -10 0 63.66 49.70 23.74 o 8 -10 0 163.21 172.76 30.18 o 9 -10 0 95.79 108.38 28.31 o 10 -10 0 4.89 4.38 27.97 o 11 -10 0 40.40 42.90 46.48 o 1 -9 0 12586.45 15552.48 212.13 o 2 -9 0 6235.88 6979.85 122.17 o 3 -9 0 62.32 61.40 15.55 o 4 -9 0 323.84 377.61 28.24 o 5 -9 0 709.17 870.29 40.83 o 6 -9 0 1398.75 1592.15 78.83 o 7 -9 0 114.04 161.24 27.63 o 8 -9 0 23.78 45.20 24.74 o 9 -9 0 150.89 253.59 34.87 o 10 -9 0 0.38 35.66 33.01 o 11 -9 0 247.67 355.91 64.31 o 0 -8 0 1367.97 1433.31 39.12 o 1 -8 0 8779.22 10051.31 139.88 o 2 -8 0 618.04 721.47 26.89 o 3 -8 0 995.67 1101.66 39.55 o 4 -8 0 597.86 715.65 60.36 o 5 -8 0 96.47 166.82 21.38 o 6 -8 0 251.04 224.43 25.47 o 7 -8 0 173.21 163.66 27.09 o 8 -8 0 126.69 100.36 26.13 o 9 -8 0 44.95 21.00 26.19 o 10 -8 0 11.97 -6.37 30.95 o 11 -8 0 18.21 19.37 48.54 o 12 -8 0 11.06 115.51 50.58 o 1 -7 0 7896.62 8767.82 123.08 o 2 -7 0 9576.28 11305.63 185.60 o 3 -7 0 2309.21 2715.22 66.19 o 4 -7 0 1613.95 1665.30 50.75 o 5 -7 0 187.67 195.83 29.22 o 6 -7 0 39.32 36.03 18.53 o 7 -7 0 1496.25 1627.78 59.41 o 8 -7 0 517.23 604.65 45.81 o 9 -7 0 70.17 74.78 29.03 o 10 -7 0 78.62 48.59 33.43 o 11 -7 0 5.37 -16.68 34.70 o 12 -7 0 44.50 10.80 45.22 o 0 -6 0 76853.48 93183.18 1609.84 o 1 -6 0 4336.95 4826.51 97.71 o 2 -6 0 5132.57 5614.80 98.70 o 3 -6 0 3977.26 4339.65 91.39 o 4 -6 0 2929.97 3164.69 75.08 o 5 -6 0 51.91 36.14 17.46 o 6 -6 0 74.07 71.82 19.51 o 7 -6 0 98.68 103.67 23.53 o 8 -6 0 595.95 690.95 50.58 o 9 -6 0 49.47 72.87 26.41 o 10 -6 0 39.37 86.75 34.34 o 11 -6 0 96.70 95.43 97.86 o 12 -6 0 55.95 33.25 47.13 o 1 -5 0 9936.04 12236.94 179.50 o 2 -5 0 2457.02 2659.94 60.49 o 3 -5 0 2169.66 2321.30 56.08 o 4 -5 0 3074.87 3390.33 76.24 o 5 -5 0 1356.57 1638.48 50.70 o 6 -5 0 1509.58 1613.09 52.97 o 7 -5 0 148.98 163.41 25.04 o 8 -5 0 57.31 62.53 23.29 o 9 -5 0 217.09 257.42 38.59 o 10 -5 0 113.29 150.44 37.00 o 11 -5 0 215.63 283.61 54.99 o 12 -5 0 1.75 -10.06 44.89 o 0 -4 0 7.58 5.51 11.85 o 1 -4 0 6667.19 7674.19 125.67 o 2 -4 0 3268.37 3672.26 88.89 o 3 -4 0 1008.55 1037.00 39.24 o 4 -4 0 305.82 340.30 47.27 o 5 -4 0 1284.53 1349.85 44.91 o 6 -4 0 128.34 121.97 20.37 o 7 -4 0 345.86 398.24 56.09 o 8 -4 0 39.91 -4.81 20.95 o 9 -4 0 215.53 228.08 37.03 o 10 -4 0 27.07 19.72 32.22 o 11 -4 0 55.59 56.67 42.81 o 12 -4 0 14.80 50.52 47.59 o 1 -3 0 3238.69 3552.51 59.89 o 2 -3 0 1405.48 1477.37 54.43 o 3 -3 0 1605.48 1773.57 44.99 o 4 -3 0 3051.96 3747.35 81.77 o 5 -3 0 894.55 977.23 49.75 o 6 -3 0 397.65 451.54 33.49 o 7 -3 0 1665.38 1905.25 59.72 o 8 -3 0 116.43 140.04 25.20 o 9 -3 0 7.08 0.96 26.83 o 10 -3 0 202.68 245.52 50.21 o 11 -3 0 9.85 37.70 42.00 o 12 -3 0 150.95 102.75 52.24 o 0 -2 0 10432.17 13273.70 230.37 o 1 -2 0 8991.78 10662.08 255.23 o 2 -2 0 4271.96 4995.48 139.60 o 3 -2 0 248.26 234.56 16.38 o 4 -2 0 1610.37 1867.65 50.87 o 5 -2 0 1911.48 2243.49 58.67 o 6 -2 0 1105.53 1153.65 42.66 o 7 -2 0 1309.32 1397.80 51.38 o 8 -2 0 323.79 508.78 45.72 o 9 -2 0 3.60 -22.94 26.83 o 10 -2 0 6.06 -4.88 62.54 o 11 -2 0 45.54 67.97 49.65 o 12 -2 0 21.70 20.89 44.50 o 1 -1 0 8228.98 9075.74 187.70 o 2 -1 0 37841.59 41526.96 856.81 o 3 -1 0 49.19 50.78 11.05 o 4 -1 0 1070.38 1155.02 38.72 o 5 -1 0 3170.35 3753.59 85.30 o 6 -1 0 93.25 80.64 17.45 o 7 -1 0 1680.07 1693.68 55.13 o 8 -1 0 230.24 176.80 32.35 o 9 -1 0 351.08 391.85 42.05 o 10 -1 0 41.38 7.31 80.20 o 11 -1 0 7.21 -52.22 56.33 o 12 -1 0 21.84 96.46 49.27 o 1 0 0 3196.39 3413.57 90.07 o 2 0 0 16.02 20.70 9.89 o 3 0 0 17.01 2.60 9.31 o 4 0 0 1294.46 1409.46 39.87 o 5 0 0 1719.23 1834.76 50.22 o 6 0 0 147.03 170.55 19.32 o 7 0 0 12.55 -0.71 16.58 o 8 0 0 48.25 33.35 25.34 o 9 0 0 170.66 197.90 45.35 o 10 0 0 0.36 -9.80 36.38 o 11 0 0 0.57 -12.24 38.03 o 12 0 0 6.99 -39.69 39.69 o 1 1 0 8196.44 9243.46 290.73 o 2 1 0 37614.62 41701.27 718.81 o 3 1 0 72.60 65.55 14.33 o 4 1 0 1091.56 1137.18 60.50 o 5 1 0 3145.44 3594.30 80.10 o 6 1 0 128.07 129.37 17.79 o 7 1 0 1668.24 1659.80 65.58 o 8 1 0 262.23 285.60 35.92 o 9 1 0 372.06 310.24 50.81 o 10 1 0 38.63 39.61 37.16 o 11 1 0 4.35 0.14 38.82 o 12 1 0 19.50 -18.09 51.08 o 1 2 0 9023.37 10902.38 219.08 o 2 2 0 4115.23 5053.52 118.39 o 3 2 0 266.77 273.72 16.32 o 4 2 0 1793.80 2032.23 51.82 o 5 2 0 1891.83 2273.76 61.32 o 6 2 0 1085.09 1098.54 47.54 o 7 2 0 1345.34 1343.59 58.78 o 8 2 0 329.43 354.50 38.15 o 9 2 0 1.90 5.82 37.24 o 10 2 0 9.17 -27.82 73.52 o 11 2 0 48.23 -24.55 37.93 o 12 2 0 21.97 0.33 43.91 o 1 3 0 3183.28 3477.39 76.99 o 2 3 0 1403.31 1542.85 43.02 o 3 3 0 1571.71 1743.78 49.90 o 4 3 0 3086.94 3819.56 108.32 o 5 3 0 933.10 942.56 44.93 o 6 3 0 397.71 465.25 27.17 o 7 3 0 1639.99 1799.72 69.98 o 8 3 0 101.54 122.84 70.65 o 9 3 0 9.58 46.71 63.01 o 10 3 0 171.67 187.67 73.99 o 11 3 0 7.50 -35.61 35.61 o 12 3 0 149.97 179.08 82.11 o 1 4 0 6757.56 7892.90 164.55 o 2 4 0 3125.26 3813.64 72.16 o 3 4 0 1041.74 1037.52 61.96 o 4 4 0 283.48 331.73 29.34 o 5 4 0 1227.32 1242.03 36.66 o 6 4 0 133.83 150.29 22.68 o 7 4 0 351.94 304.14 31.94 o 8 4 0 30.15 -1.11 30.29 o 9 4 0 236.19 265.90 82.11 o 10 4 0 25.51 88.10 40.92 o 11 4 0 52.26 135.82 46.35 o 12 4 0 9.82 34.64 45.17 o 1 5 0 9967.25 12381.46 349.92 o 2 5 0 2539.71 2975.25 74.90 o 3 5 0 2117.99 2341.38 62.19 o 4 5 0 3037.86 3272.09 84.80 o 5 5 0 1382.80 1658.83 55.06 o 6 5 0 1489.39 1475.41 57.24 o 7 5 0 144.69 154.30 35.32 o 8 5 0 58.07 112.31 66.36 o 9 5 0 199.85 226.70 51.56 o 10 5 0 109.51 114.02 88.32 o 11 5 0 220.53 272.81 55.02 o 12 5 0 1.87 -12.55 63.49 o 1 6 0 4301.95 4963.85 183.32 o 2 6 0 5324.25 6040.71 128.08 o 3 6 0 3805.30 4360.58 140.23 o 4 6 0 3000.41 3284.88 118.71 o 5 6 0 50.00 45.29 16.44 o 6 6 0 66.88 59.90 19.72 o 7 6 0 93.34 95.77 32.70 o 8 6 0 570.34 519.35 60.66 o 9 6 0 46.68 68.64 42.49 o 10 6 0 38.33 35.52 37.06 o 11 6 0 95.46 146.57 46.74 o 12 6 0 62.99 60.70 53.94 o 1 7 0 7979.53 9142.88 320.80 o 2 7 0 9457.99 11479.00 239.49 o 3 7 0 2322.36 2840.72 60.07 o 4 7 0 1704.26 1825.37 55.71 o 5 7 0 143.73 128.87 19.91 o 6 7 0 36.07 -8.80 23.28 o 7 7 0 1509.92 1505.30 83.21 o 8 7 0 531.08 538.73 60.66 o 9 7 0 74.97 50.99 35.89 o 10 7 0 64.36 87.06 39.82 o 11 7 0 5.65 -12.86 57.29 o 12 7 0 46.00 41.78 45.39 o 1 8 0 8709.46 9808.36 363.77 o 2 8 0 555.47 712.70 33.31 o 3 8 0 989.53 1158.77 33.56 o 4 8 0 571.24 710.33 59.63 o 5 8 0 105.01 211.58 24.28 o 6 8 0 245.06 262.98 38.60 o 7 8 0 167.95 144.22 36.84 o 8 8 0 131.99 63.94 77.34 o 9 8 0 42.08 76.21 56.81 o 10 8 0 8.97 4.15 37.10 o 11 8 0 23.08 -21.81 37.79 o 12 8 0 11.30 -40.19 42.96 o 1 9 0 12517.56 15277.28 555.68 o 2 9 0 6331.16 7151.17 188.12 o 3 9 0 76.03 87.53 21.31 o 4 9 0 347.20 415.17 31.21 o 5 9 0 739.75 828.35 41.21 o 6 9 0 1359.53 1686.79 83.28 o 7 9 0 104.55 141.06 37.25 o 8 9 0 23.80 1.05 30.29 o 9 9 0 166.10 158.67 44.56 o 10 9 0 1.03 50.43 39.46 o 11 9 0 253.04 313.92 100.73 o 12 9 0 3.79 -21.96 66.83 o 1 10 0 5493.92 7570.37 280.70 o 2 10 0 234.53 328.78 28.48 o 3 10 0 1790.60 1927.66 57.87 o 4 10 0 814.23 851.79 40.97 o 5 10 0 125.84 206.54 35.31 o 6 10 0 31.93 -21.13 25.15 o 7 10 0 68.24 65.22 36.76 o 8 10 0 145.54 199.70 63.01 o 9 10 0 82.58 88.31 44.40 o 10 10 0 4.53 -10.28 36.97 o 11 10 0 39.06 10.64 42.52 o 1 11 0 2092.65 2411.75 115.53 o 2 11 0 2991.22 3715.68 118.75 o 3 11 0 1372.92 1642.10 54.63 o 4 11 0 254.02 219.79 23.68 o 5 11 0 1306.41 1281.48 71.41 o 6 11 0 13.79 16.37 27.97 o 7 11 0 1256.90 1124.27 77.56 o 8 11 0 174.55 213.61 44.89 o 9 11 0 191.98 266.60 84.50 o 10 11 0 57.55 90.52 73.52 o 11 11 0 57.82 90.41 47.84 o 0 12 0 37.39 59.20 29.60 o 1 12 0 833.56 817.28 69.70 o 2 12 0 2581.13 2783.25 77.02 o 3 12 0 405.32 415.99 34.19 o 4 12 0 1452.76 1690.47 58.16 o 5 12 0 664.49 720.45 110.75 o 6 12 0 995.52 1252.48 76.52 o 7 12 0 89.93 57.48 34.93 o 8 12 0 71.99 92.85 39.14 o 9 12 0 143.63 38.00 38.60 o 10 12 0 6.95 1.48 38.88 o 11 12 0 39.84 23.05 77.81 o 1 13 0 236.07 283.57 42.01 o 2 13 0 1277.33 1224.43 48.63 o 3 13 0 558.97 563.96 58.58 o 4 13 0 651.11 683.99 56.01 o 5 13 0 156.60 158.59 75.90 o 6 13 0 414.17 475.70 53.81 o 7 13 0 72.57 109.41 36.84 o 8 13 0 337.38 384.93 54.92 o 9 13 0 90.92 104.81 42.52 o 10 13 0 12.71 49.17 41.18 o 11 13 0 42.55 -39.96 39.96 o 0 14 0 2380.05 2875.77 145.13 o 1 14 0 544.13 645.42 63.97 o 2 14 0 104.74 122.72 21.14 o 3 14 0 418.04 534.46 70.71 o 4 14 0 181.30 235.21 99.30 o 5 14 0 503.10 639.56 63.48 o 6 14 0 46.32 60.34 32.48 o 7 14 0 471.97 472.55 106.93 o 8 14 0 20.80 14.45 35.03 o 9 14 0 126.21 193.17 48.78 o 10 14 0 5.44 34.81 42.19 o 11 14 0 4.33 -39.09 39.09 o 1 15 0 530.55 723.72 73.52 o 2 15 0 1390.92 1496.46 57.50 o 3 15 0 352.75 448.35 38.65 o 4 15 0 970.86 1079.91 70.36 o 5 15 0 73.03 61.35 32.32 o 6 15 0 566.46 653.28 66.44 o 7 15 0 282.04 305.75 49.23 o 8 15 0 53.18 7.38 40.58 o 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