#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:35:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181259 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/37/2233756.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233756_Fobs loop_ _publ_author_name 'Abdel-Aziz, Alaa A.-M.' 'El-Azab, Adel S.' 'Alanazi, Amer M.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 2,6-Bis[(S)-1-phenylethyl]-1H,5H-pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetrone ; _journal_coeditor_code BT5823 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o907 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.762 _cell_angle_gamma 90.000 _cell_length_a 5.6401 _cell_length_b 16.1040 _cell_length_c 11.3759 _exptl_crystal_F_000 444.00 _reflns_d_resolution_high 0.7920 _cod_data_source_file bt5823Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21 1898 Friedel pairs' _shelx_refln_list_code 4 _shelx_f_calc_maximum 82.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -19 0 90.35 88.87 1.54 o 2 -19 0 24.77 23.91 0.88 o 0 -18 0 96.42 126.51 2.41 o 1 -18 0 155.08 143.76 1.66 o 2 -18 0 2.45 1.84 0.19 o 3 -18 0 52.74 53.40 1.13 o 1 -17 0 183.48 180.11 9.25 o 2 -17 0 187.16 192.21 15.39 o 3 -17 0 25.33 23.79 0.85 o 0 -16 0 388.42 629.05 6.04 o 1 -16 0 301.16 288.33 8.53 o 2 -16 0 101.12 103.83 3.41 o 3 -16 0 43.20 45.91 1.04 o 4 -16 0 49.77 43.76 0.99 o 1 -15 0 72.64 73.90 1.61 o 2 -15 0 29.92 27.42 0.66 o 3 -15 0 56.83 56.06 1.16 o 4 -15 0 10.98 11.89 0.37 o 0 -14 0 582.12 776.55 7.06 o 1 -14 0 306.55 309.31 5.97 o 2 -14 0 66.46 64.56 1.06 o 3 -14 0 156.78 157.06 4.65 o 4 -14 0 7.09 8.68 0.36 o 5 -14 0 62.16 37.04 0.80 o 1 -13 0 762.83 726.75 14.84 o 2 -13 0 54.01 51.49 0.92 o 3 -13 0 27.51 24.74 0.91 o 4 -13 0 220.52 235.05 2.54 o 5 -13 0 133.43 126.63 1.97 o 1 -12 0 156.29 157.96 3.83 o 2 -12 0 285.18 280.44 3.22 o 3 -12 0 134.17 116.82 1.97 o 4 -12 0 142.67 143.53 2.03 o 5 -12 0 191.94 200.48 2.33 o 1 -11 0 415.89 397.70 4.10 o 2 -11 0 42.91 43.02 0.66 o 3 -11 0 176.17 162.14 3.54 o 4 -11 0 264.05 259.39 2.23 o 5 -11 0 33.43 30.87 0.81 o 0 -10 0 116.13 137.69 2.63 o 1 -10 0 316.35 297.34 3.90 o 2 -10 0 10.69 12.66 0.50 o 3 -10 0 116.21 98.27 1.83 o 4 -10 0 26.73 32.10 1.01 o 5 -10 0 21.12 24.65 0.78 o 1 -9 0 198.84 205.67 2.64 o 2 -9 0 57.84 57.38 1.02 o 3 -9 0 722.71 686.05 6.48 o 4 -9 0 92.40 91.39 1.69 o 5 -9 0 43.61 45.45 1.80 o 6 -9 0 62.94 56.82 1.19 o 0 -8 0 458.80 784.56 4.76 o 1 -8 0 215.93 206.03 1.69 o 2 -8 0 471.51 507.66 3.83 o 3 -8 0 105.66 119.76 2.46 o 4 -8 0 96.27 98.80 1.73 o 5 -8 0 9.31 9.56 0.52 o 6 -8 0 52.11 52.65 0.87 o 1 -7 0 404.06 385.31 2.11 o 2 -7 0 324.61 310.48 3.29 o 3 -7 0 21.60 21.11 0.62 o 4 -7 0 172.00 163.24 2.23 o 5 -7 0 173.22 165.30 2.22 o 6 -7 0 157.75 177.20 1.74 o 1 -6 0 995.22 970.69 4.24 o 2 -6 0 109.55 103.36 1.14 o 3 -6 0 193.20 205.83 1.90 o 4 -6 0 73.07 75.79 2.63 o 5 -6 0 110.32 107.64 1.79 o 6 -6 0 39.77 48.49 0.94 o 1 -5 0 361.49 349.36 1.89 o 2 -5 0 571.59 560.10 3.22 o 3 -5 0 207.81 197.24 1.81 o 4 -5 0 375.66 380.82 6.70 o 5 -5 0 25.06 25.62 0.81 o 6 -5 0 22.97 25.57 0.54 o 0 -4 0 2917.95 2687.82 5.65 o 1 -4 0 2333.29 2087.18 5.67 o 2 -4 0 134.05 124.81 1.44 o 3 -4 0 98.32 121.06 1.72 o 4 -4 0 106.89 105.99 2.52 o 5 -4 0 181.42 175.08 4.39 o 6 -4 0 149.34 152.99 6.86 o 1 -3 0 979.52 923.63 3.54 o 2 -3 0 222.33 235.85 2.57 o 3 -3 0 348.56 345.88 2.30 o 4 -3 0 100.44 101.99 1.79 o 5 -3 0 323.33 314.51 3.95 o 6 -3 0 122.91 132.13 5.78 o 0 -2 0 563.20 690.52 1.94 o 1 -2 0 128.37 111.71 0.72 o 2 -2 0 427.46 413.56 3.22 o 3 -2 0 584.99 647.00 5.14 o 4 -2 0 3.81 2.62 0.27 o 5 -2 0 660.35 643.27 12.55 o 6 -2 0 186.08 178.29 2.86 o 1 -1 0 1140.08 1021.68 3.44 o 2 -1 0 464.03 418.47 3.25 o 3 -1 0 145.84 151.30 2.50 o 4 -1 0 298.19 280.98 4.04 o 5 -1 0 557.71 550.29 5.89 o 6 -1 0 85.52 90.93 2.10 o 1 0 0 4940.53 4084.80 6.83 o 2 0 0 10.33 6.80 0.29 o 3 0 0 17.76 26.58 1.05 o 4 0 0 184.90 183.94 3.29 o 5 0 0 883.84 896.21 7.63 o 6 0 0 204.53 233.58 3.47 o 1 1 0 1136.79 1011.91 3.34 o 2 1 0 463.70 419.63 3.34 o 3 1 0 145.61 151.11 1.80 o 4 1 0 296.92 278.70 4.08 o 5 1 0 559.90 558.47 7.55 o 6 1 0 84.75 91.73 2.20 o 7 1 0 42.35 37.33 0.75 o 0 2 0 565.32 555.02 1.12 o 1 2 0 128.32 113.90 1.12 o 2 2 0 426.49 418.36 2.39 o 3 2 0 584.99 642.28 3.84 o 4 2 0 3.92 2.59 0.40 o 5 2 0 659.39 646.10 11.21 o 6 2 0 185.94 182.91 3.10 o 1 3 0 985.94 942.30 3.50 o 2 3 0 224.42 236.82 1.84 o 3 3 0 351.47 341.83 2.81 o 4 3 0 98.73 101.31 3.16 o 5 3 0 325.84 311.89 5.01 o 6 3 0 122.82 132.53 3.69 o 0 4 0 2918.30 2540.11 3.07 o 2 4 0 137.39 127.14 2.02 o 3 4 0 96.84 116.34 1.69 o 4 4 0 107.52 103.89 1.87 o 5 4 0 182.20 178.02 2.43 o 6 4 0 149.33 154.52 4.31 o 2 5 0 572.82 560.83 4.14 o 3 5 0 206.67 187.64 2.23 o 4 5 0 375.55 379.98 2.88 o 5 5 0 24.58 25.57 0.92 o 6 5 0 22.56 24.38 0.71 o 0 6 0 43.49 47.08 0.44 o 1 6 0 996.07 968.06 4.15 o 2 6 0 107.76 100.72 1.33 o 3 6 0 192.82 200.29 2.38 o 4 6 0 72.83 72.27 1.27 o 5 6 0 109.40 109.39 2.50 o 6 6 0 39.59 48.08 0.96 o 1 7 0 400.63 388.27 2.86 o 2 7 0 320.71 315.07 2.48 o 3 7 0 20.89 19.39 0.76 o 4 7 0 172.76 161.97 1.90 o 5 7 0 175.03 173.75 2.31 o 6 7 0 158.46 174.84 1.67 o 0 8 0 460.79 776.95 4.45 o 1 8 0 216.86 209.19 2.26 o 2 8 0 475.54 503.08 3.30 o 3 8 0 105.76 121.70 1.98 o 4 8 0 95.47 101.35 2.80 o 5 8 0 9.29 9.72 0.51 o 6 8 0 51.57 53.19 1.33 o 1 9 0 200.23 207.43 8.01 o 2 9 0 58.43 56.19 1.54 o 3 9 0 722.33 693.86 4.85 o 4 9 0 92.18 91.85 2.14 o 5 9 0 43.62 46.63 1.71 o 6 9 0 62.72 58.52 1.27 o 0 10 0 119.12 155.05 2.30 o 1 10 0 313.58 313.59 4.67 o 2 10 0 10.75 11.63 0.58 o 3 10 0 116.61 102.26 1.52 o 4 10 0 27.43 32.68 1.10 o 5 10 0 21.21 25.19 0.82 o 6 10 0 36.83 35.46 0.84 o 1 11 0 415.71 433.03 4.83 o 2 11 0 42.27 42.73 0.89 o 3 11 0 176.13 168.57 2.45 o 4 11 0 263.45 258.40 2.98 o 5 11 0 34.29 32.34 0.86 o 0 12 0 328.06 387.68 4.00 o 1 12 0 155.71 153.52 3.00 o 2 12 0 286.02 280.62 2.37 o 3 12 0 134.42 122.28 2.04 o 4 12 0 143.79 142.63 2.84 o 5 12 0 190.18 206.77 1.94 o 1 13 0 763.61 787.05 7.27 o 2 13 0 53.60 52.78 1.97 o 3 13 0 27.65 26.64 0.93 o 4 13 0 218.60 226.16 3.19 o 5 13 0 132.43 124.29 1.87 o 0 14 0 573.74 877.82 7.55 o 1 14 0 308.71 304.04 4.57 o 2 14 0 66.05 62.89 2.14 o 3 14 0 157.98 163.51 2.84 o 4 14 0 7.43 9.19 0.42 o 5 14 0 61.94 62.10 1.04 o 1 15 0 72.05 71.47 2.20 o 2 15 0 30.16 27.25 1.37 o 3 15 0 56.98 57.30 1.54 o 4 15 0 11.15 12.18 0.70 o 0 16 0 388.10 599.58 6.03 o 1 16 0 299.34 283.16 4.18 o 2 16 0 102.03 101.05 1.73 o 3 16 0 43.36 42.23 1.40 o 4 16 0 50.66 48.36 1.12 o 2 17 0 189.48 193.14 5.13 o 3 17 0 25.75 23.78 0.86 o 0 18 0 94.86 95.39 2.10 o 2 18 0 2.37 2.37 0.30 o 3 18 0 53.23 51.43 1.15 o 1 19 0 89.76 89.74 1.32 o 2 19 0 24.97 24.82 0.85 o 0 20 0 9.16 8.00 0.49 o 0 -20 1 26.03 25.42 0.71 o -2 -19 1 42.21 40.47 1.07 o -1 -19 1 233.25 224.94 2.59 o 0 -19 1 6.62 8.38 0.46 o 1 -19 1 4.34 4.72 0.37 o 2 -19 1 24.94 25.90 0.70 o -3 -18 1 46.37 53.36 1.24 o -2 -18 1 9.37 9.56 0.59 o -1 -18 1 93.34 91.70 2.67 o 0 -18 1 39.69 38.68 1.13 o 1 -18 1 10.40 11.36 0.39 o 2 -18 1 135.65 138.11 4.62 o 3 -18 1 90.36 78.65 1.14 o -3 -17 1 56.34 55.66 4.47 o -2 -17 1 62.44 57.48 1.50 o -1 -17 1 3.50 4.09 0.24 o 0 -17 1 71.85 85.83 5.28 o 1 -17 1 308.90 298.03 9.70 o 2 -17 1 72.41 72.75 2.71 o 3 -17 1 18.26 18.87 1.09 o -4 -16 1 35.06 36.90 0.97 o -3 -16 1 52.13 49.27 1.21 o -2 -16 1 19.29 20.57 0.57 o -1 -16 1 316.78 301.57 2.30 o 0 -16 1 991.92 1315.85 104.63 o 1 -16 1 91.52 83.58 2.45 o 2 -16 1 70.10 75.90 1.54 o 3 -16 1 16.25 19.65 0.84 o 4 -16 1 193.49 190.51 2.02 o -4 -15 1 47.76 46.47 0.75 o -3 -15 1 25.27 24.37 0.67 o -2 -15 1 320.92 305.19 4.52 o -1 -15 1 104.85 104.88 1.17 o 0 -15 1 63.62 88.12 7.49 o 1 -15 1 144.01 150.90 2.34 o 2 -15 1 47.02 50.80 0.99 o 3 -15 1 4.20 5.89 0.33 o 4 -15 1 45.74 40.55 1.18 o -5 -14 1 153.49 147.18 1.86 o -4 -14 1 61.04 59.33 0.95 o -3 -14 1 41.46 39.09 1.13 o -2 -14 1 16.09 15.83 0.50 o -1 -14 1 206.49 202.42 5.38 o 0 -14 1 862.59 1195.09 102.72 o 1 -14 1 366.26 360.19 3.13 o 2 -14 1 45.83 45.42 1.00 o 3 -14 1 127.51 118.64 2.11 o 4 -14 1 51.23 62.45 1.36 o -5 -13 1 298.43 305.35 3.18 o -4 -13 1 145.79 138.53 1.95 o -3 -13 1 41.03 35.84 1.03 o -2 -13 1 171.17 175.60 4.21 o -1 -13 1 52.29 57.41 2.88 o 0 -13 1 14.81 20.33 2.15 o 1 -13 1 2.53 2.71 0.21 o 2 -13 1 213.00 210.56 2.13 o 3 -13 1 23.97 21.15 0.65 o 4 -13 1 13.47 16.51 0.90 o 5 -13 1 56.84 55.48 1.20 o -5 -12 1 140.62 134.39 2.39 o -4 -12 1 136.85 122.88 4.45 o -3 -12 1 55.74 44.36 0.98 o -2 -12 1 55.16 55.48 0.85 o -1 -12 1 186.84 180.90 1.77 o 1 -12 1 67.99 64.57 3.24 o 2 -12 1 5.17 4.92 0.27 o 3 -12 1 65.85 69.24 1.20 o 4 -12 1 14.54 12.47 0.59 o 5 -12 1 8.18 8.22 0.35 o -5 -11 1 29.76 29.98 0.79 o -4 -11 1 211.23 197.55 6.08 o -3 -11 1 30.44 29.81 0.79 o -2 -11 1 445.25 439.58 2.44 o -1 -11 1 58.17 61.87 1.71 o 0 -11 1 55.64 108.40 2.11 o 2 -11 1 22.83 25.15 0.52 o 3 -11 1 132.50 144.29 2.17 o 4 -11 1 335.18 308.15 3.06 o 5 -11 1 10.04 10.22 0.45 o -6 -10 1 57.03 47.99 1.00 o -5 -10 1 1.82 2.35 0.33 o -4 -10 1 34.99 35.65 0.85 o -3 -10 1 315.69 314.93 2.34 o -2 -10 1 157.44 167.75 2.66 o -1 -10 1 197.60 191.56 2.78 o 0 -10 1 90.94 184.46 2.61 o 1 -10 1 1735.28 1693.74 8.51 o 2 -10 1 10.37 12.02 0.78 o 3 -10 1 144.87 136.94 2.40 o 4 -10 1 260.57 268.09 2.92 o 5 -10 1 271.77 294.06 2.81 o -6 -9 1 155.96 161.99 2.09 o -5 -9 1 92.31 91.62 1.59 o -4 -9 1 17.12 17.22 0.59 o -3 -9 1 16.89 14.86 0.43 o -2 -9 1 338.09 356.40 2.52 o -1 -9 1 653.40 638.64 3.85 o 0 -9 1 559.72 995.70 21.06 o 1 -9 1 206.34 208.53 1.85 o 2 -9 1 87.53 85.76 2.02 o 3 -9 1 22.69 20.92 0.59 o 4 -9 1 90.84 83.43 1.63 o 5 -9 1 140.66 138.35 1.90 o 6 -9 1 72.53 81.37 1.37 o -6 -8 1 106.29 115.35 2.14 o -5 -8 1 1.62 2.07 0.23 o -4 -8 1 294.57 313.65 5.39 o -3 -8 1 20.15 17.35 0.79 o -2 -8 1 711.58 748.92 7.09 o -1 -8 1 385.77 397.23 2.27 o 0 -8 1 85.12 142.16 2.10 o 1 -8 1 15.36 21.09 0.55 o 2 -8 1 239.72 245.62 5.96 o 3 -8 1 62.00 66.53 1.95 o 4 -8 1 120.70 111.59 2.58 o 5 -8 1 96.32 93.90 1.61 o 6 -8 1 98.28 104.16 1.78 o -6 -7 1 5.82 6.87 0.36 o -5 -7 1 67.34 64.80 1.40 o -4 -7 1 159.01 155.74 2.11 o -3 -7 1 12.65 14.22 0.73 o -2 -7 1 276.37 289.65 2.04 o -1 -7 1 2303.18 2249.84 27.65 o 0 -7 1 388.50 744.33 42.92 o 1 -7 1 194.87 200.98 1.55 o 2 -7 1 1335.75 1354.02 7.31 o 3 -7 1 5.82 7.03 0.62 o 4 -7 1 191.12 185.10 3.46 o 5 -7 1 28.21 30.73 0.93 o 6 -7 1 35.12 34.16 1.11 o -6 -6 1 29.99 30.32 0.78 o -5 -6 1 400.65 397.53 4.87 o -4 -6 1 24.48 25.54 0.64 o -3 -6 1 83.30 93.00 1.30 o -2 -6 1 154.42 164.57 1.45 o -1 -6 1 640.30 624.80 10.93 o 0 -6 1 568.52 1081.45 112.57 o 1 -6 1 42.68 48.26 0.69 o 2 -6 1 679.45 672.56 3.96 o 3 -6 1 48.19 55.28 1.68 o 4 -6 1 50.65 58.97 2.08 o 5 -6 1 265.26 273.62 2.56 o 6 -6 1 135.29 141.43 2.42 o -6 -5 1 286.61 312.54 2.91 o -5 -5 1 112.72 105.69 1.88 o -4 -5 1 97.72 102.25 1.27 o -3 -5 1 190.87 201.82 1.90 o -2 -5 1 75.04 70.34 0.91 o -1 -5 1 1694.84 1586.60 5.15 o 0 -5 1 369.96 403.93 98.37 o 1 -5 1 144.33 145.16 2.64 o 2 -5 1 627.54 654.28 2.65 o 3 -5 1 1097.75 1096.73 7.35 o 4 -5 1 230.70 248.47 10.05 o 5 -5 1 147.21 148.92 2.18 o 6 -5 1 72.02 76.12 1.84 o -6 -4 1 0.99 1.29 0.18 o -5 -4 1 77.61 71.93 1.40 o -4 -4 1 7.47 6.31 0.47 o -3 -4 1 494.42 514.57 3.82 o -2 -4 1 869.97 862.41 4.04 o -1 -4 1 413.25 386.78 2.29 o 0 -4 1 353.36 317.26 1.85 o 1 -4 1 403.37 383.17 2.74 o 2 -4 1 241.31 259.80 1.77 o 3 -4 1 58.20 62.88 1.04 o 4 -4 1 65.87 70.51 3.50 o 5 -4 1 184.22 169.91 2.99 o 6 -4 1 46.33 48.26 1.48 o -6 -3 1 21.69 21.47 0.96 o -5 -3 1 144.81 149.81 2.84 o -4 -3 1 335.39 331.23 3.45 o -3 -3 1 119.88 131.56 1.46 o -2 -3 1 66.06 70.69 0.86 o 0 -3 1 92.87 84.44 0.48 o 1 -3 1 1464.89 1340.67 3.06 o 2 -3 1 777.74 780.11 6.16 o 3 -3 1 487.08 500.96 4.59 o 4 -3 1 135.11 136.70 2.88 o 5 -3 1 33.62 28.43 1.26 o 6 -3 1 244.63 254.82 8.17 o -7 -2 1 21.43 20.25 0.61 o -6 -2 1 171.20 184.88 2.60 o -5 -2 1 60.68 56.91 1.85 o -4 -2 1 357.54 350.40 2.79 o -2 -2 1 334.16 326.42 2.84 o 0 -2 1 689.18 622.45 1.18 o 3 -2 1 505.36 517.78 4.64 o 4 -2 1 100.85 90.18 2.26 o 5 -2 1 306.90 291.45 4.15 o 6 -2 1 45.19 45.83 1.12 o -7 -1 1 20.81 17.60 0.80 o -6 -1 1 79.00 80.29 2.03 o -5 -1 1 8.05 7.80 0.70 o -4 -1 1 8.14 10.69 0.78 o -3 -1 1 60.10 72.59 1.72 o -2 -1 1 288.20 248.37 2.46 o 0 -1 1 2486.50 1978.31 3.39 o 1 -1 1 1270.07 1121.60 3.62 o 2 -1 1 1168.44 1183.35 5.48 o 3 -1 1 226.06 260.77 3.31 o 4 -1 1 2.92 3.94 0.46 o 5 -1 1 113.58 108.59 2.58 o 6 -1 1 62.76 68.49 1.79 o -7 0 1 22.68 20.76 0.47 o -6 0 1 37.97 38.17 1.43 o -5 0 1 40.25 45.52 1.73 o -4 0 1 86.39 108.31 2.52 o -3 0 1 6.19 6.48 0.50 o -2 0 1 1693.21 1561.57 8.21 o -1 0 1 3798.91 3346.16 6.08 o 0 0 1 263.09 227.26 6.44 o 1 0 1 619.49 573.49 2.61 o 2 0 1 2.24 1.48 0.13 o 3 0 1 65.89 59.48 1.57 o 4 0 1 134.31 134.98 2.81 o 5 0 1 15.84 17.69 1.06 o 6 0 1 160.33 174.84 2.56 o -7 1 1 20.51 18.64 0.58 o -6 1 1 79.28 82.07 2.13 o -5 1 1 7.96 7.51 0.47 o -4 1 1 7.86 10.64 0.80 o -3 1 1 59.46 68.33 1.17 o -2 1 1 289.22 242.72 1.71 o -1 1 1 1648.62 1485.53 7.52 o 0 1 1 2491.95 2081.75 3.16 o 1 1 1 1263.88 1119.77 3.61 o 2 1 1 1172.13 1193.66 5.95 o 3 1 1 225.26 262.35 3.43 o 4 1 1 3.11 5.47 0.56 o 5 1 1 115.43 114.19 1.79 o 6 1 1 63.52 69.92 1.85 o -7 2 1 21.24 20.35 0.59 o -6 2 1 173.11 183.83 3.20 o -5 2 1 60.95 60.50 1.39 o -4 2 1 357.65 351.05 4.64 o -3 2 1 989.88 997.80 4.57 o -2 2 1 331.39 321.56 2.87 o -1 2 1 1664.56 1553.86 5.90 o 0 2 1 681.52 628.75 1.85 o 1 2 1 695.52 700.35 2.34 o 2 2 1 321.92 309.31 2.12 o 3 2 1 503.85 516.66 4.61 o 4 2 1 99.66 87.88 2.31 o 5 2 1 304.42 295.09 3.53 o 6 2 1 45.18 46.69 1.50 o -6 3 1 21.99 22.50 0.87 o -5 3 1 143.96 149.11 2.86 o -4 3 1 335.15 339.83 4.68 o -3 3 1 120.65 131.29 1.69 o -2 3 1 65.95 69.27 0.96 o -1 3 1 2296.19 2181.59 3.59 o 1 3 1 1468.67 1337.56 4.24 o 2 3 1 777.53 776.43 5.12 o 3 3 1 487.94 502.53 5.69 o 4 3 1 136.48 135.37 1.61 o 5 3 1 33.95 30.58 0.97 o 6 3 1 244.08 253.47 8.31 o -6 4 1 0.97 1.14 0.17 o -5 4 1 78.45 74.94 1.61 o -4 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