#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/37/2233757.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233757_Fobs loop_ _publ_author_name 'Abdel-Aziz, Alaa A.-M.' 'El-Azab, Adel S.' 'Alanazi, Amer M.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 1-Acetyl-4-(phenylsulfanyl)imidazolidin-2-one ; _journal_coeditor_code BT5824 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o908 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.921 _cell_angle_gamma 90.000 _cell_length_a 7.0473 _cell_length_b 14.3274 _cell_length_c 10.7796 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.7925 _[local]_cod_data_source_file bt5824Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 333.91 301.11 4.36 o 4 0 0 407.95 408.96 7.88 o 6 0 0 39.88 48.16 1.54 o 1 1 0 3055.47 2919.09 44.63 o 2 1 0 1734.18 1645.71 5.50 o 3 1 0 953.39 954.16 9.29 o 4 1 0 921.13 880.24 8.16 o 5 1 0 522.42 494.85 7.07 o 6 1 0 198.87 186.00 2.70 o 7 1 0 274.99 292.92 3.70 o 0 2 0 1195.59 1116.45 31.17 o 1 2 0 2351.33 2310.32 6.94 o 2 2 0 262.14 289.01 2.24 o 3 2 0 1283.95 1353.29 6.12 o 4 2 0 758.36 800.51 7.78 o 5 2 0 106.90 110.81 3.36 o 6 2 0 349.67 352.40 3.35 o 7 2 0 68.87 82.62 1.96 o 8 2 0 0.32 0.61 0.54 o 1 3 0 7959.75 7070.78 17.61 o 2 3 0 419.45 405.55 2.97 o 3 3 0 711.67 712.55 5.31 o 4 3 0 96.02 81.21 2.48 o 5 3 0 375.55 360.02 5.96 o 6 3 0 2.50 2.19 0.55 o 7 3 0 0.84 1.93 0.57 o 8 3 0 0.14 0.50 0.49 o 0 4 0 3638.76 3450.61 25.62 o 1 4 0 1300.42 1248.71 7.64 o 2 4 0 2268.58 2265.05 9.89 o 3 4 0 1646.14 1613.81 8.04 o 4 4 0 148.72 153.46 3.43 o 5 4 0 65.20 59.27 1.41 o 6 4 0 1484.22 1552.57 8.91 o 7 4 0 2.00 2.75 0.60 o 8 4 0 0.58 2.27 0.71 o 1 5 0 37.91 41.01 0.58 o 2 5 0 1428.62 1371.37 5.06 o 3 5 0 1007.28 1043.73 7.19 o 4 5 0 923.66 938.10 7.10 o 5 5 0 357.46 355.86 3.47 o 6 5 0 97.85 96.15 2.54 o 7 5 0 0.41 1.00 0.53 o 8 5 0 136.02 140.75 3.00 o 0 6 0 1804.43 1665.92 14.87 o 1 6 0 886.98 926.57 3.90 o 2 6 0 241.46 260.72 3.75 o 3 6 0 15.09 11.54 0.90 o 4 6 0 417.32 386.97 4.66 o 5 6 0 180.13 178.98 2.50 o 6 6 0 2.11 6.86 1.44 o 7 6 0 755.03 749.10 6.16 o 8 6 0 25.40 23.68 1.18 o 1 7 0 234.56 233.29 2.19 o 2 7 0 216.02 205.25 2.38 o 3 7 0 881.67 926.92 5.94 o 4 7 0 218.31 236.17 3.77 o 5 7 0 1502.19 1548.37 22.01 o 6 7 0 53.84 49.12 1.79 o 7 7 0 800.58 814.58 7.41 o 8 7 0 45.85 55.19 2.29 o 0 8 0 9.98 7.24 4.94 o 1 8 0 1615.87 1593.90 12.78 o 2 8 0 0.76 1.77 0.50 o 3 8 0 1633.09 1590.08 8.06 o 4 8 0 192.25 199.00 2.62 o 5 8 0 145.03 184.05 3.42 o 6 8 0 379.13 393.02 4.66 o 7 8 0 334.60 316.67 4.30 o 1 9 0 2419.87 2380.72 12.61 o 2 9 0 296.49 267.64 4.36 o 3 9 0 215.45 206.77 3.22 o 4 9 0 0.45 1.68 0.46 o 5 9 0 24.64 26.80 1.35 o 6 9 0 9.09 10.47 0.82 o 7 9 0 0.37 0.99 0.45 o 0 10 0 58.67 70.00 2.76 o 1 10 0 3.43 3.19 0.83 o 2 10 0 16.76 15.48 1.03 o 3 10 0 228.18 220.58 3.17 o 4 10 0 198.94 189.54 3.10 o 5 10 0 0.01 0.46 0.48 o 6 10 0 1157.49 1129.21 7.96 o 7 10 0 51.43 45.58 1.59 o 1 11 0 124.28 117.53 1.83 o 2 11 0 946.17 942.55 6.46 o 3 11 0 321.90 318.70 5.53 o 4 11 0 540.22 559.17 9.16 o 5 11 0 45.01 44.78 1.75 o 6 11 0 172.97 173.34 2.47 o 7 11 0 71.89 66.95 2.20 o 0 12 0 428.96 413.75 6.32 o 1 12 0 20.26 14.88 0.84 o 2 12 0 3.01 2.97 0.65 o 3 12 0 49.23 45.97 2.20 o 4 12 0 461.37 455.02 6.26 o 5 12 0 91.07 89.06 2.78 o 6 12 0 112.71 105.58 5.45 o 1 13 0 122.23 113.10 2.72 o 2 13 0 353.33 363.56 5.95 o 3 13 0 352.41 360.08 6.15 o 4 13 0 119.57 119.93 3.87 o 6 13 0 17.74 16.43 1.16 o 0 14 0 339.32 327.86 8.54 o 1 14 0 147.95 140.55 4.58 o 2 14 0 170.02 166.50 4.95 o 3 14 0 92.10 99.85 5.39 o 4 14 0 127.45 134.62 5.52 o 5 14 0 4.83 4.04 0.84 o 1 15 0 234.88 253.10 4.60 o 2 15 0 3.68 2.80 1.37 o 3 15 0 71.54 74.52 4.21 o 0 16 0 1.92 3.82 0.74 o 1 16 0 36.45 34.56 1.53 o 2 16 0 32.58 32.12 1.76 o 3 16 0 11.21 10.35 1.23 o 1 17 0 47.99 48.70 2.15 o 2 17 0 0.86 0.79 0.48 o -7 0 1 367.35 386.32 5.13 o -5 0 1 555.61 497.87 9.99 o -3 0 1 4926.88 4931.03 31.45 o -1 0 1 2585.20 2426.56 8.96 o 1 0 1 1153.07 1041.97 10.69 o 3 0 1 2906.36 3135.07 18.50 o 5 0 1 2072.11 2001.88 20.56 o 7 0 1 28.25 31.08 3.03 o -7 1 1 50.70 58.84 1.40 o -6 1 1 372.44 361.13 3.05 o -5 1 1 1030.89 964.87 9.81 o -4 1 1 1239.56 1322.42 12.44 o -3 1 1 1333.96 1304.04 8.17 o -2 1 1 101.51 84.89 1.66 o -1 1 1 5172.83 4586.22 12.72 o 0 1 1 335.29 334.61 0.91 o 1 1 1 37.22 41.03 0.87 o 2 1 1 770.09 758.39 5.78 o 3 1 1 1673.02 1596.50 7.66 o 4 1 1 912.24 862.97 8.29 o 5 1 1 3.97 9.16 1.70 o 6 1 1 538.69 500.60 4.78 o 7 1 1 164.09 170.57 4.36 o -8 2 1 287.05 296.43 4.56 o -7 2 1 156.94 158.67 2.50 o -6 2 1 18.92 15.27 0.70 o -5 2 1 281.55 287.77 5.37 o -4 2 1 16.88 9.32 0.92 o -3 2 1 1.41 4.09 0.71 o -2 2 1 525.15 531.58 3.05 o -1 2 1 701.58 666.84 3.68 o 1 2 1 298.91 343.14 1.89 o 2 2 1 279.76 277.48 2.49 o 3 2 1 410.23 414.47 3.63 o 4 2 1 1.65 2.82 1.07 o 5 2 1 331.70 356.50 6.10 o 6 2 1 851.06 816.15 9.75 o 7 2 1 121.05 111.50 2.56 o -8 3 1 377.07 374.40 4.27 o -7 3 1 72.91 65.28 1.79 o -6 3 1 2039.77 2053.49 9.48 o -5 3 1 114.82 109.53 3.31 o -4 3 1 72.17 85.21 2.69 o -3 3 1 4298.63 4478.17 11.34 o -2 3 1 497.70 469.46 3.75 o -1 3 1 484.80 436.45 7.10 o 0 3 1 24.80 22.95 0.72 o 1 3 1 1750.43 1720.91 6.61 o 2 3 1 402.35 421.04 5.51 o 3 3 1 682.03 751.95 4.76 o 4 3 1 1211.33 1145.98 8.17 o 5 3 1 16.45 17.40 1.08 o 6 3 1 1307.51 1305.64 7.40 o 7 3 1 2.56 2.79 0.58 o -8 4 1 283.98 296.10 3.70 o -7 4 1 112.42 124.14 2.25 o -6 4 1 54.78 42.78 1.57 o -5 4 1 117.75 137.16 2.08 o -4 4 1 2174.68 2169.21 51.18 o -3 4 1 12.45 23.84 0.90 o -2 4 1 14.37 22.50 0.57 o -1 4 1 4793.44 4630.67 28.61 o 0 4 1 8220.14 7469.34 19.79 o 1 4 1 11361.78 10025.58 302.37 o 2 4 1 44.69 29.20 0.64 o 3 4 1 848.00 953.59 5.40 o 4 4 1 49.58 43.88 1.52 o 5 4 1 1.23 1.35 0.35 o 6 4 1 834.29 831.55 6.59 o 7 4 1 268.96 294.43 4.48 o -8 5 1 75.75 82.00 2.37 o -7 5 1 233.61 269.68 3.57 o -6 5 1 67.07 66.73 1.94 o -5 5 1 797.64 800.20 5.11 o -4 5 1 0.55 0.15 0.49 o -3 5 1 909.69 902.69 4.77 o -2 5 1 365.78 319.89 2.43 o -1 5 1 603.37 592.40 4.50 o 1 5 1 2824.78 2724.70 5.80 o 2 5 1 218.70 229.87 2.10 o 3 5 1 1621.44 1563.03 11.51 o 4 5 1 68.45 75.01 2.05 o 5 5 1 74.49 75.88 2.80 o 6 5 1 361.24 362.67 4.32 o 7 5 1 641.55 628.43 7.67 o -8 6 1 87.57 87.89 2.28 o -7 6 1 622.73 609.12 5.15 o -6 6 1 7.26 6.64 0.81 o -5 6 1 353.04 324.53 3.34 o -4 6 1 566.81 592.68 6.43 o -3 6 1 0.98 1.44 0.52 o -2 6 1 187.81 216.50 2.24 o -1 6 1 16.37 24.21 0.69 o 0 6 1 278.75 312.24 2.27 o 1 6 1 9.13 6.07 0.32 o 2 6 1 242.68 255.02 2.34 o 3 6 1 479.27 453.16 4.11 o 4 6 1 191.87 214.96 3.55 o 5 6 1 1018.28 1025.02 7.87 o 6 6 1 5.28 11.57 1.47 o 7 6 1 0.39 1.60 0.69 o -8 7 1 23.08 28.93 1.19 o -7 7 1 179.53 181.23 2.39 o -6 7 1 28.49 37.53 1.63 o -5 7 1 97.51 97.27 2.20 o -4 7 1 263.81 268.64 4.40 o -3 7 1 1585.94 1615.30 9.42 o -2 7 1 305.68 290.20 2.78 o -1 7 1 291.17 301.46 4.02 o 0 7 1 2914.69 2837.75 11.17 o 1 7 1 1.67 2.42 0.34 o 2 7 1 404.99 403.50 3.09 o 3 7 1 38.67 47.39 1.43 o 4 7 1 482.40 492.31 4.38 o 5 7 1 554.72 526.64 10.33 o 6 7 1 269.48 247.18 3.94 o 7 7 1 165.15 175.59 3.37 o -7 8 1 3.06 5.30 0.45 o -6 8 1 32.96 31.72 1.60 o -5 8 1 57.29 49.83 1.59 o -4 8 1 885.02 852.44 7.61 o -3 8 1 593.82 596.56 6.64 o -2 8 1 807.45 780.52 5.81 o -1 8 1 66.94 78.14 1.67 o 0 8 1 1001.81 1037.88 5.55 o 1 8 1 0.40 7.43 2.12 o 2 8 1 2091.69 2054.17 15.25 o 3 8 1 562.81 567.81 5.02 o 4 8 1 127.82 136.27 2.48 o 5 8 1 54.58 46.83 1.96 o 6 8 1 2.41 4.18 0.77 o 7 8 1 195.86 206.32 3.34 o -7 9 1 5.49 6.66 0.54 o -6 9 1 253.75 259.20 3.63 o -5 9 1 17.80 24.77 1.14 o -4 9 1 149.34 151.22 2.56 o -3 9 1 135.87 131.44 3.58 o -2 9 1 644.40 619.23 5.49 o -1 9 1 302.38 317.08 3.50 o 0 9 1 5.76 5.00 0.62 o 1 9 1 41.81 45.54 1.29 o 2 9 1 384.63 378.37 4.53 o 3 9 1 54.78 52.17 1.51 o 4 9 1 5.06 3.95 0.79 o 5 9 1 205.75 219.65 4.08 o 6 9 1 114.43 117.52 2.94 o 7 9 1 61.37 70.61 2.19 o -7 10 1 142.68 150.62 2.33 o -6 10 1 336.91 310.75 3.73 o -5 10 1 0.91 1.70 0.43 o -4 10 1 133.02 127.56 2.82 o -3 10 1 33.56 32.62 1.24 o -2 10 1 171.85 182.32 2.77 o -1 10 1 2540.60 2502.26 30.38 o 0 10 1 0.43 2.35 0.97 o 1 10 1 4.07 5.20 0.90 o 2 10 1 12.92 19.78 0.94 o 3 10 1 1204.60 1172.70 11.18 o 4 10 1 239.00 254.38 4.02 o 5 10 1 97.57 106.37 2.75 o 6 10 1 52.22 53.26 1.81 o 7 10 1 67.62 61.41 2.35 o -7 11 1 120.76 117.02 3.04 o -6 11 1 29.45 29.14 1.03 o -5 11 1 7.07 7.09 0.72 o -4 11 1 99.89 95.22 2.55 o -3 11 1 208.20 197.13 3.81 o -2 11 1 77.01 72.12 1.81 o -1 11 1 89.77 100.84 6.58 o 0 11 1 36.47 36.83 1.18 o 1 11 1 540.79 510.43 5.98 o 2 11 1 25.26 23.56 0.96 o 3 11 1 18.17 17.43 1.36 o 4 11 1 33.60 35.34 2.04 o 5 11 1 0.45 1.03 0.48 o 6 11 1 27.05 29.52 1.50 o -6 12 1 104.48 102.94 3.27 o -5 12 1 396.48 419.07 9.19 o -4 12 1 194.42 204.05 4.25 o -3 12 1 61.70 61.54 1.91 o -2 12 1 438.42 433.88 4.83 o -1 12 1 108.56 106.99 1.95 o 0 12 1 356.83 330.28 3.87 o 1 12 1 378.90 392.97 4.44 o 2 12 1 322.70 309.33 4.00 o 3 12 1 23.72 23.85 1.61 o 4 12 1 119.47 123.54 4.05 o 6 12 1 65.25 69.88 2.84 o -6 13 1 20.39 22.22 1.44 o -5 13 1 72.19 74.78 2.28 o -4 13 1 56.29 53.60 2.65 o -3 13 1 73.89 78.40 2.68 o -2 13 1 755.25 744.75 7.15 o -1 13 1 9.62 10.30 1.12 o 0 13 1 778.38 754.99 5.73 o 1 13 1 17.96 15.03 0.94 o 2 13 1 159.27 159.37 2.89 o 3 13 1 77.03 81.76 5.07 o 5 13 1 0.67 1.47 0.74 o -4 14 1 133.90 139.50 5.58 o -3 14 1 89.44 96.99 5.36 o -2 14 1 65.31 71.71 3.41 o -1 14 1 8.62 11.33 1.18 o 0 14 1 54.15 60.01 2.06 o 1 14 1 55.64 55.27 1.66 o 2 14 1 570.41 577.40 7.91 o 3 14 1 0.57 1.91 1.36 o -3 15 1 78.01 76.04 4.27 o -2 15 1 46.04 51.98 2.06 o -1 15 1 171.29 166.91 3.77 o 0 15 1 0.25 1.84 0.53 o 1 15 1 577.56 583.26 8.26 o 2 15 1 185.49 191.76 6.80 o 3 15 1 390.96 412.03 9.37 o -3 16 1 8.06 9.11 1.39 o -2 16 1 274.51 259.42 13.99 o -1 16 1 772.58 745.26 11.57 o 0 16 1 1.40 1.10 0.72 o 1 16 1 18.10 18.98 1.41 o 2 16 1 5.62 6.42 0.91 o 3 16 1 448.74 412.22 7.26 o -2 17 1 148.05 149.46 4.22 o -1 17 1 0.02 0.78 0.67 o 0 17 1 24.21 20.41 1.83 o 1 17 1 325.45 286.38 6.09 o 2 17 1 62.57 57.44 2.40 o -8 0 2 148.43 158.63 4.53 o -6 0 2 676.61 712.65 5.37 o -4 0 2 9.55 13.04 1.52 o -2 0 2 7797.13 7591.10 21.44 o 0 0 2 89.30 86.35 0.74 o 2 0 2 1079.84 1030.34 6.07 o 4 0 2 592.45 641.29 10.54 o 6 0 2 7.95 9.28 0.99 o -8 1 2 10.71 10.31 0.64 o -7 1 2 2.89 3.19 0.93 o -6 1 2 177.18 171.08 2.19 o -5 1 2 134.15 135.13 3.72 o -4 1 2 1212.78 1298.56 9.99 o -3 1 2 396.81 393.30 3.63 o -2 1 2 541.18 529.40 4.54 o -1 1 2 1973.62 1738.82 5.85 o 1 1 2 2758.72 2493.20 7.94 o 2 1 2 691.49 656.84 2.99 o 3 1 2 326.97 286.92 3.52 o 4 1 2 838.39 879.86 12.77 o 5 1 2 37.70 34.66 1.33 o 6 1 2 339.45 346.62 4.26 o 7 1 2 15.02 14.10 1.69 o -8 2 2 119.00 114.53 2.37 o -7 2 2 41.70 45.77 1.30 o -6 2 2 171.46 160.84 2.42 o -5 2 2 501.80 474.06 6.91 o -4 2 2 441.14 468.25 5.37 o -3 2 2 54.96 54.93 1.43 o -2 2 2 56.67 41.21 1.24 o -1 2 2 4976.85 4601.45 29.12 o 0 2 2 2958.66 2808.88 8.00 o 1 2 2 2056.11 1988.14 13.19 o 2 2 2 190.22 197.01 1.72 o 3 2 2 41.94 45.88 1.22 o 4 2 2 210.44 174.21 4.46 o 5 2 2 1887.31 1874.24 16.69 o 6 2 2 4.30 3.65 0.70 o 7 2 2 404.79 436.82 10.90 o -8 3 2 0.01 1.21 0.44 o -7 3 2 526.23 545.08 4.64 o -6 3 2 347.51 378.32 3.74 o -5 3 2 165.20 150.73 3.92 o -4 3 2 949.89 1000.68 7.05 o -3 3 2 68.23 57.93 1.81 o -2 3 2 412.87 422.10 3.83 o -1 3 2 120.53 126.37 0.94 o 0 3 2 6673.10 6194.22 42.32 o 1 3 2 8548.85 8114.32 27.50 o 2 3 2 141.87 147.21 1.42 o 3 3 2 3541.73 3514.06 15.19 o 4 3 2 497.60 547.64 5.65 o 5 3 2 689.78 653.95 6.77 o 6 3 2 402.33 374.12 4.87 o 7 3 2 26.64 31.84 1.64 o -8 4 2 100.51 101.49 2.21 o -7 4 2 1.15 2.36 0.50 o -6 4 2 102.15 102.46 1.98 o -5 4 2 489.99 512.64 6.31 o -4 4 2 136.24 125.20 4.41 o -3 4 2 822.33 814.38 7.66 o -2 4 2 1641.66 1583.99 11.03 o -1 4 2 953.96 968.04 4.69 o 0 4 2 2619.48 2654.13 6.17 o 1 4 2 2268.48 2163.63 7.46 o 2 4 2 143.16 143.60 1.43 o 3 4 2 42.89 39.88 0.97 o 4 4 2 11.58 17.12 1.00 o 5 4 2 6.29 7.34 0.61 o 6 4 2 0.40 0.53 0.74 o 7 4 2 46.64 46.53 1.94 o -8 5 2 54.83 60.65 1.64 o -7 5 2 318.76 313.11 3.51 o -6 5 2 1126.59 1150.81 7.12 o -5 5 2 21.55 23.56 0.86 o -4 5 2 3.03 11.52 1.17 o -3 5 2 170.40 163.90 2.08 o -2 5 2 513.10 515.66 2.82 o -1 5 2 191.65 189.17 1.43 o 0 5 2 1670.07 1607.69 4.51 o 1 5 2 132.72 147.52 1.77 o 2 5 2 32.29 31.43 0.80 o 3 5 2 422.81 425.85 3.51 o 4 5 2 77.21 76.98 2.10 o 5 5 2 43.35 50.13 1.59 o 6 5 2 1328.82 1357.73 11.19 o 7 5 2 11.69 7.73 0.91 o -8 6 2 239.78 248.07 4.96 o -7 6 2 27.39 28.85 1.21 o -6 6 2 954.61 919.01 7.13 o -5 6 2 92.86 109.34 1.95 o -4 6 2 241.12 232.50 3.92 o -3 6 2 164.20 162.77 2.57 o -2 6 2 499.76 469.62 3.66 o -1 6 2 69.40 83.69 0.94 o 0 6 2 365.21 384.56 2.59 o 1 6 2 150.86 140.20 1.65 o 2 6 2 2502.45 2493.42 9.65 o 3 6 2 25.06 26.74 0.96 o 4 6 2 1302.77 1291.12 8.79 o 5 6 2 0.78 2.34 0.87 o 6 6 2 0.40 1.50 0.70 o 7 6 2 139.74 142.05 3.06 o -8 7 2 10.92 12.39 0.82 o -7 7 2 267.69 287.47 3.53 o -6 7 2 3.37 3.05 0.68 o -5 7 2 10.53 16.39 1.12 o -4 7 2 97.45 77.65 2.36 o -3 7 2 80.56 69.64 1.76 o -2 7 2 439.17 477.77 4.00 o -1 7 2 302.47 281.33 2.69 o 0 7 2 1152.24 1216.40 4.98 o 1 7 2 1267.46 1405.96 9.19 o 2 7 2 89.38 94.39 1.84 o 3 7 2 838.07 791.01 5.89 o 4 7 2 59.33 50.46 1.48 o 5 7 2 434.08 455.99 13.95 o 6 7 2 13.50 18.74 1.55 o 7 7 2 316.56 320.71 5.37 o -7 8 2 17.26 17.35 0.83 o -6 8 2 143.04 145.19 3.03 o -5 8 2 133.49 127.52 3.34 o -4 8 2 459.53 464.19 5.91 o -3 8 2 531.96 479.77 5.96 o -2 8 2 3.76 4.26 0.60 o -1 8 2 917.16 916.08 4.69 o 0 8 2 704.37 765.25 6.98 o 1 8 2 329.15 307.58 3.07 o 2 8 2 97.43 96.42 1.71 o 3 8 2 60.87 56.13 1.93 o 4 8 2 21.65 26.40 0.93 o 5 8 2 122.17 123.25 3.91 o 6 8 2 170.35 186.11 3.77 o 7 8 2 583.09 600.02 6.57 o -7 9 2 361.70 337.96 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