#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:35:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181259 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/37/2233764.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233764_Fobs loop_ _publ_author_name 'Rivera, Augusto' 'Maldonado, Mauricio' 'R\'ios-Motta, Jaime' 'Fejfarov\'a, Karla' 'Du\H-Benzimidazol-1-yl)methanol ; _journal_coeditor_code BX2398 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o615 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 95.143(6) _cell_angle_gamma 90 _cell_length_a 13.3181(10) _cell_length_b 4.2677(3) _cell_length_c 12.4795(10) _exptl_crystal_F_000 312 _reflns_d_resolution_high 0.8371 _cod_data_source_file bx2398Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 637.75 607.91 4.03 o 2 0 0 3783.32 3576.16 14.10 o 3 0 0 242.41 193.40 4.17 o 4 0 0 3676.27 3303.35 19.95 o 5 0 0 33.07 23.04 2.00 o 6 0 0 45.11 44.28 3.00 o 7 0 0 51.71 60.53 4.00 o 8 0 0 46.15 43.36 1.61 o 9 0 0 303.38 298.46 5.26 o 10 0 0 59.21 55.19 2.04 o 11 0 0 55.94 55.81 1.74 o 12 0 0 427.15 461.25 4.92 o 13 0 0 2.61 2.25 0.54 o 14 0 0 274.53 286.86 9.35 o 15 0 0 318.52 359.58 6.01 o 1 1 0 3180.42 3087.79 13.02 o 2 1 0 1461.33 1420.97 9.49 o 3 1 0 2402.55 2438.66 15.97 o 4 1 0 176.60 174.85 4.40 o 5 1 0 185.53 198.66 5.17 o 6 1 0 0.01 0.82 0.75 < 7 1 0 167.69 157.33 2.58 o 8 1 0 1.17 3.60 0.42 o 9 1 0 0.01 0.76 0.38 < 10 1 0 209.46 205.45 2.49 o 11 1 0 259.73 260.87 2.90 o 12 1 0 13.44 12.82 0.80 o 13 1 0 61.10 62.06 1.75 o 14 1 0 7.75 8.86 0.59 o 15 1 0 111.34 124.98 2.38 o 0 2 0 30.18 21.64 2.40 o 1 2 0 30.51 24.79 1.49 o 2 2 0 375.53 388.19 6.85 o 3 2 0 4.08 2.95 1.05 < 4 2 0 977.50 1047.10 84.46 o 5 2 0 11.75 8.24 0.59 o 6 2 0 58.91 57.76 2.30 o 7 2 0 2.01 1.31 0.44 < 8 2 0 8.37 7.29 0.67 o 9 2 0 0.17 -0.15 0.35 < 10 2 0 1.31 0.75 0.34 < 11 2 0 61.88 63.83 1.28 o 12 2 0 29.08 27.82 0.93 o 13 2 0 6.83 7.44 0.62 o 14 2 0 39.77 47.48 1.75 o 1 3 0 86.27 97.36 3.80 o 2 3 0 317.87 313.20 10.06 o 3 3 0 29.43 26.47 1.17 o 4 3 0 55.88 52.95 2.21 o 5 3 0 16.79 15.19 0.85 o 6 3 0 9.26 8.68 0.84 o 7 3 0 56.83 55.16 1.89 o 8 3 0 0.84 -0.34 0.34 < 9 3 0 3.86 4.15 0.52 o 10 3 0 48.15 47.85 1.52 o 11 3 0 22.18 22.03 0.96 o 12 3 0 12.30 16.78 0.92 o 0 4 0 29.91 28.93 1.37 o 1 4 0 0.17 0.42 0.50 < 2 4 0 27.91 29.05 0.94 o 3 4 0 41.38 43.27 1.16 o 4 4 0 18.46 17.47 0.66 o 5 4 0 65.77 65.67 2.28 o 6 4 0 29.06 33.08 1.42 o 7 4 0 1.42 -0.35 0.46 < 8 4 0 1.30 2.47 0.49 o 9 4 0 5.09 6.69 0.76 o 1 5 0 2.97 2.14 0.48 o 2 5 0 126.85 143.98 15.36 o 3 5 0 1.51 1.40 0.60 < -15 1 1 54.46 48.92 12.39 o -14 1 1 0.01 0.61 0.31 < -13 1 1 133.63 144.06 3.22 o -12 1 1 123.32 130.53 2.18 o -11 1 1 69.68 69.35 1.50 o -10 1 1 70.09 65.88 1.39 o -9 1 1 30.32 27.22 0.96 o -8 1 1 20.38 15.96 0.71 o -7 1 1 12.78 8.81 0.95 o -6 1 1 674.83 718.37 11.09 o -5 1 1 232.67 257.78 6.66 o -4 1 1 0.94 0.74 1.07 < -3 1 1 2685.60 2886.85 48.34 o -2 1 1 7447.29 7669.61 104.73 o -1 1 1 86.63 88.08 2.41 o 0 1 1 965.97 966.51 26.99 o 1 1 1 853.18 723.69 9.62 o 2 1 1 7208.24 6624.74 94.05 o 3 1 1 549.72 544.79 10.30 o 4 1 1 5.53 4.97 0.64 o 5 1 1 36.47 38.77 2.42 o 6 1 1 20.60 21.59 2.35 o 7 1 1 532.61 559.80 4.09 o 8 1 1 3.61 2.37 0.46 o 9 1 1 42.71 38.63 1.46 o 10 1 1 15.73 15.59 1.14 o 11 1 1 34.27 34.59 1.11 o 12 1 1 31.76 34.05 1.20 o 13 1 1 63.13 68.01 1.79 o 14 1 1 3.36 3.70 0.49 o 15 1 1 41.92 46.31 1.49 o -14 2 1 0.00 1.08 0.54 < -13 2 1 72.88 75.89 1.73 o -12 2 1 22.24 22.94 0.82 o -11 2 1 70.08 65.38 1.29 o -10 2 1 138.86 138.87 1.86 o -9 2 1 310.06 291.06 2.61 o -8 2 1 19.47 13.92 0.92 o -7 2 1 2.43 1.67 0.42 o -6 2 1 119.11 100.96 3.02 o -5 2 1 90.18 93.00 2.03 o -4 2 1 789.34 833.00 17.83 o -3 2 1 4.91 6.05 1.82 o -2 2 1 69.14 74.96 3.09 o -1 2 1 200.76 178.81 4.70 o 0 2 1 194.14 178.59 3.85 o 1 2 1 40.36 48.53 3.45 o 2 2 1 808.15 800.62 9.74 o 3 2 1 265.73 258.98 5.95 o 4 2 1 24.95 14.05 1.65 o 5 2 1 2011.65 1965.91 15.16 o 6 2 1 95.49 82.36 1.38 o 7 2 1 146.01 130.41 2.14 o 8 2 1 137.28 132.36 2.10 o 9 2 1 197.21 197.38 2.63 o 10 2 1 76.25 75.41 1.59 o 11 2 1 11.95 11.91 0.70 o 12 2 1 48.04 46.46 1.18 o 13 2 1 4.32 3.62 0.46 o 14 2 1 37.02 49.51 1.77 o -12 3 1 5.38 7.24 0.63 o -11 3 1 1.70 1.15 0.36 o -10 3 1 16.45 17.20 1.07 o -9 3 1 6.36 7.69 0.63 o -8 3 1 13.27 11.73 0.74 o -7 3 1 0.01 0.64 0.45 < -6 3 1 33.94 30.15 1.22 o -5 3 1 0.50 1.25 0.51 < -4 3 1 2.81 1.59 0.42 o -3 3 1 25.58 24.38 1.21 o -2 3 1 10.71 7.89 0.54 o -1 3 1 48.31 50.63 1.15 o 0 3 1 107.44 100.45 2.04 o 1 3 1 127.07 140.46 6.53 o 2 3 1 18.75 18.34 0.88 o 3 3 1 73.69 72.62 3.45 o 4 3 1 0.08 0.16 0.40 < 5 3 1 13.21 12.71 0.69 o 6 3 1 258.86 254.46 6.22 o 7 3 1 128.50 120.01 1.81 o 8 3 1 111.10 115.08 2.31 o 9 3 1 28.58 24.37 1.01 o 10 3 1 2.17 1.74 0.34 o 11 3 1 30.20 32.65 1.38 o 12 3 1 0.34 -0.14 0.72 < -9 4 1 3.57 4.71 0.61 o -8 4 1 28.96 32.56 1.21 o -7 4 1 0.14 0.43 0.33 < -6 4 1 2.60 3.48 0.41 o -5 4 1 26.11 26.63 1.07 o -4 4 1 1.45 1.25 0.57 < -3 4 1 0.00 0.24 0.47 < -2 4 1 25.89 23.44 0.87 o -1 4 1 31.89 35.09 1.88 o 0 4 1 193.24 213.90 5.53 o 1 4 1 31.02 30.45 0.89 o 2 4 1 10.43 9.45 0.57 o 3 4 1 4.46 3.99 0.48 o 4 4 1 39.57 38.24 1.14 o 5 4 1 39.51 37.24 1.37 o 6 4 1 84.99 85.50 2.03 o 7 4 1 5.18 4.08 0.46 o 8 4 1 4.20 5.08 0.67 o 9 4 1 133.42 152.20 2.66 o -3 5 1 9.22 11.57 1.00 o -2 5 1 9.52 10.62 1.08 o -1 5 1 26.45 29.04 1.30 o 0 5 1 24.45 25.87 1.57 o 1 5 1 2.04 0.84 1.05 < 2 5 1 19.97 19.09 2.86 o -15 0 2 36.77 37.34 1.85 o -14 0 2 132.67 143.42 3.05 o -13 0 2 850.55 894.36 8.15 o -12 0 2 12.62 12.52 0.90 o -11 0 2 196.19 210.57 4.07 o -10 0 2 58.13 53.81 2.64 o -9 0 2 109.42 119.35 5.85 o -8 0 2 781.93 821.18 11.27 o -7 0 2 17.22 27.05 2.55 o -6 0 2 311.14 373.76 29.83 o -5 0 2 448.55 560.42 13.06 o -4 0 2 4102.04 5219.81 34.90 o -3 0 2 497.47 625.51 10.36 o -2 0 2 559.49 731.15 9.23 o -1 0 2 4477.86 6340.82 20.31 o 0 0 2 1186.87 1340.51 5.61 o 1 0 2 3844.62 3676.11 16.87 o 2 0 2 1228.39 1216.68 9.86 o 3 0 2 610.85 555.83 11.29 o 4 0 2 1058.36 1042.40 9.61 o 5 0 2 18.66 21.07 1.88 o 6 0 2 53.08 52.91 3.05 o 7 0 2 676.33 723.04 34.85 o 8 0 2 334.29 328.38 2.61 o 9 0 2 328.97 344.39 3.16 o 10 0 2 1.60 2.53 0.58 o 11 0 2 70.62 70.46 2.34 o 12 0 2 18.42 18.50 2.01 o 13 0 2 25.91 27.66 2.33 o 14 0 2 0.50 0.55 0.65 < 15 0 2 8.64 8.74 1.06 o -15 1 2 18.05 17.31 0.95 o -14 1 2 105.28 107.79 2.04 o -13 1 2 109.62 114.17 1.79 o -12 1 2 80.33 76.29 1.66 o -11 1 2 218.39 209.90 3.21 o -10 1 2 338.17 348.18 11.75 o -9 1 2 1.83 1.08 0.37 < -8 1 2 585.46 582.63 6.58 o -7 1 2 47.00 62.83 3.69 o -6 1 2 110.04 118.89 4.75 o -5 1 2 24.75 31.97 2.41 o -4 1 2 96.67 106.34 3.72 o -3 1 2 208.01 232.88 15.56 o -2 1 2 47.85 56.17 2.13 o -1 1 2 200.68 196.85 4.83 o 0 1 2 50.03 51.89 2.47 o 1 1 2 172.62 153.05 3.60 o 2 1 2 5821.96 5648.37 32.62 o 3 1 2 1089.67 1015.76 17.38 o 4 1 2 2195.71 2169.38 12.68 o 5 1 2 16.06 11.52 1.25 o 6 1 2 25.79 13.68 3.01 o 7 1 2 264.85 266.21 2.39 o 8 1 2 92.02 88.20 1.58 o 9 1 2 6.67 6.44 0.51 o 10 1 2 15.39 16.00 0.74 o 11 1 2 0.84 1.07 0.37 < 12 1 2 49.59 51.28 1.44 o 13 1 2 6.09 5.25 0.60 o 14 1 2 3.69 4.79 0.69 o 15 1 2 2.52 2.49 0.42 o -14 2 2 9.93 9.01 0.71 o -13 2 2 2.59 2.31 0.50 o -12 2 2 4.67 4.06 0.42 o -11 2 2 113.74 111.49 1.81 o -10 2 2 157.38 153.09 1.95 o -9 2 2 260.54 264.29 5.39 o -8 2 2 18.01 12.88 0.83 o -7 2 2 109.17 111.70 1.99 o -6 2 2 0.11 -0.16 0.49 < -5 2 2 0.56 0.57 0.37 < -4 2 2 188.27 219.87 7.71 o -3 2 2 209.54 228.25 6.43 o -2 2 2 44.63 43.59 2.46 o -1 2 2 49.77 45.67 2.41 o 0 2 2 106.35 97.41 3.86 o 1 2 2 11.40 10.40 1.43 o 2 2 2 0.67 1.15 0.78 < 3 2 2 1069.09 1129.30 11.28 o 4 2 2 65.62 55.20 1.41 o 5 2 2 1867.56 1791.87 21.07 o 6 2 2 92.35 87.65 1.44 o 7 2 2 9.76 10.15 0.67 o 8 2 2 49.15 50.84 1.25 o 9 2 2 214.21 199.16 3.31 o 10 2 2 15.11 11.33 0.91 o 11 2 2 6.34 4.80 0.69 o 12 2 2 0.15 0.63 0.42 < 13 2 2 9.77 11.48 1.21 o 14 2 2 21.09 23.22 1.05 o -12 3 2 126.24 135.61 2.55 o -11 3 2 41.95 39.09 1.20 o -10 3 2 42.32 41.34 1.23 o -9 3 2 201.83 203.21 2.33 o -8 3 2 120.74 125.13 3.30 o -7 3 2 88.33 85.32 2.30 o -6 3 2 12.14 11.98 1.27 o -5 3 2 66.07 64.86 1.97 o -4 3 2 15.14 13.04 1.16 o -3 3 2 113.02 114.29 3.15 o -2 3 2 59.13 52.54 1.14 o -1 3 2 1.95 0.84 0.36 < 0 3 2 55.22 53.49 1.55 o 1 3 2 32.00 33.73 0.97 o 2 3 2 0.58 0.48 0.38 < 3 3 2 217.63 226.71 4.44 o 4 3 2 41.11 42.95 1.15 o 5 3 2 181.00 174.71 2.23 o 6 3 2 388.20 403.75 4.07 o 7 3 2 1150.79 1157.35 7.54 o 8 3 2 12.40 12.43 0.77 o 9 3 2 25.46 23.68 0.99 o 10 3 2 37.40 41.14 1.39 o 11 3 2 49.10 58.19 1.30 o 12 3 2 11.32 12.93 1.11 o -9 4 2 10.53 7.51 0.88 o -8 4 2 11.06 10.94 0.56 o -7 4 2 3.59 3.49 0.41 o -6 4 2 106.15 108.04 3.08 o -5 4 2 8.79 9.08 0.66 o -4 4 2 105.18 111.56 2.09 o -3 4 2 27.45 27.65 1.04 o -2 4 2 60.29 67.39 2.07 o -1 4 2 0.04 0.38 0.52 < 0 4 2 6.41 8.03 0.64 o 1 4 2 66.73 75.61 1.45 o 2 4 2 108.63 115.69 1.85 o 3 4 2 0.80 0.05 0.38 < 4 4 2 13.97 12.23 1.02 o 5 4 2 18.71 16.99 0.94 o 6 4 2 82.67 83.10 1.81 o 7 4 2 2.53 1.63 0.68 < 8 4 2 109.37 99.60 3.73 o 9 4 2 37.47 34.00 1.82 o -2 5 2 9.62 9.26 0.60 o -1 5 2 0.56 0.84 0.65 < 0 5 2 26.70 30.17 2.85 o 1 5 2 12.44 12.16 2.36 o 2 5 2 4.89 5.86 0.74 o -15 1 3 78.32 84.35 2.23 o -14 1 3 1.38 1.23 0.42 < -13 1 3 85.02 84.33 1.95 o -12 1 3 21.26 20.36 1.37 o -11 1 3 121.82 110.18 2.40 o -10 1 3 45.79 49.90 1.73 o -9 1 3 0.29 0.66 0.44 < -8 1 3 14.64 19.31 1.31 o -7 1 3 29.99 35.95 1.70 o -6 1 3 1007.12 1146.85 14.40 o -5 1 3 14.07 9.55 1.59 o -4 1 3 229.08 230.22 10.11 o -3 1 3 361.26 368.21 20.92 o -2 1 3 462.42 474.59 18.08 o -1 1 3 125.44 116.31 2.84 o 0 1 3 45.51 36.21 1.22 o 1 1 3 47.11 36.34 1.54 o 2 1 3 905.44 864.84 8.63 o 3 1 3 708.06 661.19 8.93 o 4 1 3 38.72 43.46 5.12 o 5 1 3 2.42 4.13 0.88 o 6 1 3 755.79 798.17 6.79 o 7 1 3 40.91 40.31 0.87 o 8 1 3 0.22 0.19 0.52 < 9 1 3 133.00 133.88 1.82 o 10 1 3 78.55 77.94 1.48 o 11 1 3 0.90 1.35 0.46 < 12 1 3 225.48 224.04 4.96 o 13 1 3 10.60 10.50 1.02 o 14 1 3 21.64 22.17 1.22 o -14 2 3 4.15 4.24 0.46 o -13 2 3 11.89 7.86 0.88 o -12 2 3 4.16 2.78 0.51 o -11 2 3 467.74 485.77 7.52 o -10 2 3 0.54 1.48 0.48 o -9 2 3 27.87 25.54 1.07 o -8 2 3 366.04 370.98 15.72 o -7 2 3 69.32 64.35 2.18 o -6 2 3 258.96 272.75 9.17 o -5 2 3 0.11 0.85 0.46 < -4 2 3 12.91 13.77 0.84 o -3 2 3 50.42 49.75 2.80 o -2 2 3 54.03 51.15 2.64 o -1 2 3 0.67 -1.15 0.91 < 0 2 3 469.42 452.90 8.46 o 1 2 3 143.81 146.74 7.85 o 2 2 3 33.02 33.66 2.72 o 3 2 3 17.92 22.39 1.23 o 4 2 3 1790.46 1785.01 14.62 o 5 2 3 506.06 474.66 2.85 o 6 2 3 3.99 3.63 0.50 o 7 2 3 73.87 68.06 1.70 o 8 2 3 37.64 38.69 1.44 o 9 2 3 198.80 186.04 4.38 o 10 2 3 122.71 124.07 5.68 o 11 2 3 29.77 24.90 1.63 o 12 2 3 10.43 11.28 0.81 o 13 2 3 12.95 10.94 0.94 o -12 3 3 5.48 5.58 0.82 o -11 3 3 24.26 26.93 1.68 o -10 3 3 2.08 2.57 0.43 o -9 3 3 20.96 18.13 1.04 o -8 3 3 35.14 32.48 2.21 o -7 3 3 373.31 377.91 4.34 o -6 3 3 20.05 20.37 1.19 o -5 3 3 74.05 71.92 2.91 o -4 3 3 217.54 208.91 7.86 o -3 3 3 4.12 3.31 0.57 o -2 3 3 7.24 5.77 0.57 o -1 3 3 76.33 73.97 1.84 o 0 3 3 149.32 149.36 3.56 o 1 3 3 9.45 8.90 0.57 o 2 3 3 0.77 1.00 0.35 < 3 3 3 131.96 132.05 2.07 o 4 3 3 7.06 5.83 0.53 o 5 3 3 26.39 23.39 0.85 o 6 3 3 8.73 7.60 0.77 o 7 3 3 363.48 363.26 6.81 o 8 3 3 178.15 167.16 3.03 o 9 3 3 69.61 76.55 2.42 o 10 3 3 0.03 0.51 0.32 < 11 3 3 3.50 2.26 0.43 o 12 3 3 16.59 14.56 1.86 o -9 4 3 35.50 31.38 4.29 o -8 4 3 0.02 0.48 0.28 < -7 4 3 0.39 0.36 0.37 < -6 4 3 0.07 0.88 0.43 < -5 4 3 11.27 12.22 0.73 o -4 4 3 126.47 141.60 3.17 o -3 4 3 1.96 2.46 0.68 o -2 4 3 57.58 62.60 1.58 o -1 4 3 5.71 6.23 0.68 o 0 4 3 0.03 0.61 0.44 < 1 4 3 102.67 113.24 2.25 o 2 4 3 51.51 53.80 1.34 o 3 4 3 2.15 2.52 0.51 o 4 4 3 81.97 81.63 2.33 o 5 4 3 174.57 189.53 4.18 o 6 4 3 5.20 6.61 0.60 o 7 4 3 1.07 1.23 0.39 o 8 4 3 143.69 159.49 8.00 o 9 4 3 41.41 43.48 1.92 o -15 0 4 26.70 25.12 1.58 o -14 0 4 0.71 0.16 0.41 < -13 0 4 35.64 35.25 1.72 o -12 0 4 1.94 3.36 0.95 o -11 0 4 2.97 2.28 0.59 o -10 0 4 10.44 9.81 0.71 o -9 0 4 93.56 99.48 2.57 o -8 0 4 8.81 6.65 1.10 o -7 0 4 0.29 1.20 0.76 < -6 0 4 3354.13 4106.25 40.04 o -5 0 4 215.72 253.10 9.19 o -4 0 4 1089.58 1430.24 19.40 o -3 0 4 235.16 313.15 7.85 o -2 0 4 2236.25 2798.79 19.31 o -1 0 4 2496.81 2661.97 13.92 o 0 0 4 51.88 57.06 3.03 o 1 0 4 6.57 5.79 2.11 < 2 0 4 350.41 421.84 10.80 o 3 0 4 409.93 423.96 11.11 o 4 0 4 232.47 224.53 5.38 o 5 0 4 11.19 8.79 1.54 o 6 0 4 598.74 634.50 8.50 o 7 0 4 24.29 25.87 1.98 o 8 0 4 328.06 357.68 7.22 o 9 0 4 102.42 98.50 2.76 o 10 0 4 242.83 262.58 5.34 o 11 0 4 14.67 12.69 1.73 o 12 0 4 7.93 10.64 1.58 o 13 0 4 107.52 114.53 4.21 o 14 0 4 551.53 628.99 8.44 o -15 1 4 1.90 1.19 0.31 o -14 1 4 10.17 10.69 0.88 o -13 1 4 90.10 98.16 2.63 o -12 1 4 0.60 0.41 0.56 < -11 1 4 68.18 65.13 1.85 o -10 1 4 31.29 33.19 1.58 o -9 1 4 308.28 310.45 9.04 o -8 1 4 1.34 1.78 0.62 < -7 1 4 152.34 159.27 2.78 o -6 1 4 63.57 69.30 1.55 o -5 1 4 169.49 208.46 5.81 o -4 1 4 359.92 412.53 7.36 o -3 1 4 45.52 33.67 2.05 o -2 1 4 272.55 245.55 4.18 o -1 1 4 84.02 112.93 2.69 o 0 1 4 41.11 40.77 2.17 o 1 1 4 36.07 35.78 1.79 o 2 1 4 234.81 253.11 5.07 o 3 1 4 265.80 266.17 10.11 o 4 1 4 532.17 565.90 16.27 o 5 1 4 189.73 198.22 4.86 o 6 1 4 5.62 7.20 0.54 o 7 1 4 293.20 292.11 3.41 o 8 1 4 227.63 222.60 3.73 o 9 1 4 30.45 30.90 1.06 o 10 1 4 8.56 9.65 0.72 o 11 1 4 0.91 2.08 0.68 o 12 1 4 5.58 5.98 0.88 o 13 1 4 65.80 63.56 2.14 o 14 1 4 0.18 0.04 0.65 < -14 2 4 10.49 10.71 0.88 o -13 2 4 37.36 35.14 1.15 o -12 2 4 4.73 3.59 0.54 o -11 2 4 3.33 2.66 0.60 o -10 2 4 116.30 113.91 2.37 o -9 2 4 141.41 133.17 4.97 o -8 2 4 384.02 404.40 13.87 o -7 2 4 149.23 160.19 6.09 o -6 2 4 3.93 5.34 0.61 o -5 2 4 6.82 7.01 0.74 o -4 2 4 397.17 426.51 14.02 o -3 2 4 227.54 264.04 9.02 o -2 2 4 26.06 29.53 1.26 o -1 2 4 241.99 245.76 4.83 o 0 2 4 29.88 29.07 3.87 o 1 2 4 367.26 381.47 8.91 o 2 2 4 0.47 1.05 0.73 < 3 2 4 41.37 37.62 1.29 o 4 2 4 298.47 324.02 9.70 o 5 2 4 146.51 139.42 4.01 o 6 2 4 202.18 198.04 3.81 o 7 2 4 82.39 80.19 2.18 o 8 2 4 5.33 3.56 0.54 o 9 2 4 142.94 132.18 3.65 o 10 2 4 131.80 121.11 2.33 o 11 2 4 33.35 31.05 2.08 o 12 2 4 3.74 4.84 0.72 o 13 2 4 14.70 17.11 0.80 o -12 3 4 0.66 1.39 0.34 o -11 3 4 2.01 0.86 0.51 < -10 3 4 0.11 0.32 0.46 < -9 3 4 4.87 5.96 0.77 o -8 3 4 111.24 107.54 3.67 o -7 3 4 2.39 2.32 0.72 o -6 3 4 432.20 436.29 6.26 o -5 3 4 0.23 0.44 0.69 < -4 3 4 92.02 90.94 2.82 o -3 3 4 4.96 4.02 0.83 o -2 3 4 95.26 92.38 3.64 o -1 3 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8.47 6.96 0.55 o -8 4 6 4.08 4.13 0.48 o -7 4 6 29.13 27.49 1.56 o -6 4 6 0.43 0.48 0.49 < -5 4 6 23.10 25.35 1.49 o -4 4 6 143.36 157.31 3.84 o -3 4 6 0.13 0.77 0.40 < -2 4 6 69.89 77.10 2.53 o -1 4 6 116.73 130.62 2.32 o 0 4 6 90.47 97.84 2.24 o 1 4 6 23.34 22.14 1.12 o 2 4 6 134.42 136.61 3.57 o 3 4 6 3.20 2.21 0.41 o 4 4 6 0.69 1.26 0.46 < 5 4 6 13.26 12.37 0.72 o 6 4 6 2.10 3.78 1.27 < -14 1 7 136.24 145.28 1.68 o -13 1 7 190.36 212.63 4.30 o -12 1 7 8.18 8.33 1.23 o -11 1 7 5.58 4.20 0.53 o -10 1 7 153.12 155.02 2.81 o -9 1 7 146.68 132.02 2.62 o -8 1 7 44.48 49.10 1.95 o -7 1 7 20.56 17.87 0.85 o -6 1 7 83.89 86.19 1.66 o -5 1 7 23.39 22.42 0.92 o -4 1 7 172.85 189.34 5.88 o -3 1 7 48.03 66.03 2.65 o -2 1 7 32.72 36.49 1.72 o -1 1 7 484.20 555.35 5.87 o 0 1 7 9.38 6.60 0.78 o 1 1 7 93.45 101.42 2.34 o 2 1 7 84.72 97.45 1.91 o 3 1 7 2.76 2.65 0.49 o 4 1 7 161.27 172.53 2.29 o 5 1 7 31.36 29.29 1.06 o 6 1 7 0.24 0.56 0.56 < 7 1 7 81.89 78.58 2.05 o 8 1 7 587.76 604.82 5.35 o 9 1 7 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3 7 28.98 31.52 1.35 o 0 3 7 8.31 7.35 0.72 o 1 3 7 235.05 246.74 9.17 o 2 3 7 169.39 174.10 4.09 o 3 3 7 17.10 17.08 1.01 o 4 3 7 44.21 40.52 1.17 o 5 3 7 28.65 30.97 1.01 o 6 3 7 0.02 -0.20 0.35 < 7 3 7 25.80 24.76 1.23 o 8 3 7 16.17 21.82 0.86 o 9 3 7 6.88 6.06 0.52 o -7 4 7 0.56 0.98 0.33 < -6 4 7 0.45 -0.13 0.32 < -5 4 7 35.29 36.03 1.17 o -4 4 7 4.17 4.43 0.46 o -3 4 7 8.13 7.82 0.51 o -2 4 7 18.71 18.70 1.13 o -1 4 7 161.08 168.76 2.79 o 0 4 7 0.05 2.96 0.55 o 1 4 7 31.37 30.30 1.85 o 2 4 7 18.05 18.41 0.86 o 3 4 7 47.17 45.07 1.32 o 4 4 7 14.48 14.98 1.14 o 5 4 7 3.64 5.94 0.91 o -14 0 8 19.77 21.88 1.32 o -13 0 8 17.07 11.76 2.48 o -12 0 8 285.93 278.98 5.95 o -11 0 8 72.99 69.35 2.34 o -10 0 8 40.91 31.78 2.19 o -9 0 8 2.96 2.63 0.73 o -8 0 8 33.74 30.34 1.55 o -7 0 8 765.11 770.15 8.39 o -6 0 8 7.72 4.87 0.82 o -5 0 8 154.88 141.08 4.69 o -4 0 8 98.28 92.45 2.23 o -3 0 8 946.27 996.78 9.77 o -2 0 8 343.47 412.39 13.62 o -1 0 8 0.01 1.45 1.00 < 0 0 8 20.59 31.33 1.97 o 1 0 8 19.18 29.34 1.31 o 2 0 8 492.39 585.72 13.17 o 3 0 8 9.82 10.80 1.16 o 4 0 8 84.19 99.25 4.39 o 5 0 8 245.71 272.70 8.94 o 6 0 8 37.56 36.87 4.72 o 7 0 8 56.26 59.86 2.55 o 8 0 8 782.41 776.15 14.48 o 9 0 8 2.53 2.43 1.27 < 10 0 8 343.57 336.77 6.37 o 11 0 8 51.26 42.96 2.12 o -13 1 8 29.35 30.16 0.96 o -12 1 8 0.33 -0.29 0.34 < -11 1 8 47.70 44.34 2.08 o -10 1 8 130.41 119.14 2.68 o -9 1 8 238.56 209.76 3.56 o -8 1 8 229.25 228.96 2.88 o -7 1 8 250.57 231.26 2.60 o -6 1 8 36.75 32.15 1.13 o -5 1 8 24.65 21.81 0.83 o -4 1 8 99.09 103.75 2.46 o -3 1 8 45.62 44.40 1.68 o -2 1 8 1.75 1.27 0.32 o -1 1 8 162.74 188.16 3.63 o 0 1 8 0.01 0.66 0.48 < 1 1 8 32.78 32.35 1.08 o 2 1 8 72.91 62.85 1.37 o 3 1 8 188.30 192.14 3.39 o 4 1 8 69.45 71.16 1.49 o 5 1 8 628.72 690.66 9.63 o 6 1 8 23.41 26.98 1.22 o 7 1 8 170.04 177.08 2.52 o 8 1 8 1.40 0.73 0.51 < 9 1 8 14.15 16.19 1.02 o 10 1 8 19.36 21.67 0.95 o 11 1 8 6.76 6.25 0.74 o -12 2 8 9.02 9.23 0.51 o -11 2 8 3.56 2.14 0.40 o -10 2 8 114.79 119.80 6.57 o -9 2 8 2.06 1.50 0.55 < -8 2 8 285.58 282.71 4.09 o -7 2 8 7.58 9.44 0.82 o -6 2 8 132.16 117.73 2.17 o -5 2 8 57.76 50.55 1.73 o -4 2 8 2.14 2.22 0.91 < -3 2 8 86.47 81.59 1.98 o -2 2 8 122.21 123.32 3.09 o -1 2 8 88.87 87.34 2.61 o 0 2 8 11.32 11.17 1.14 o 1 2 8 80.18 74.73 1.76 o 2 2 8 99.93 114.23 1.90 o 3 2 8 0.18 0.76 0.45 < 4 2 8 346.94 349.65 4.10 o 5 2 8 2.28 1.73 0.39 o 6 2 8 245.51 229.28 2.96 o 7 2 8 1.71 0.34 0.47 < 8 2 8 2.08 3.48 0.47 o 9 2 8 12.01 11.92 0.86 o 10 2 8 0.02 0.44 0.39 < -10 3 8 118.89 127.23 2.94 o -9 3 8 0.96 0.74 0.37 < -8 3 8 29.86 29.89 1.04 o -7 3 8 43.64 43.83 1.66 o -6 3 8 49.62 45.55 1.56 o -5 3 8 166.22 163.85 3.01 o -4 3 8 268.94 273.02 4.50 o -3 3 8 97.25 102.16 2.24 o -2 3 8 22.70 24.00 1.33 o -1 3 8 68.76 69.99 2.37 o 0 3 8 281.56 271.89 3.95 o 1 3 8 181.26 188.24 3.51 o 2 3 8 40.26 38.17 1.37 o 3 3 8 26.69 26.91 1.07 o 4 3 8 38.10 40.36 1.13 o 5 3 8 0.26 0.23 0.41 < 6 3 8 19.64 19.34 0.89 o 7 3 8 27.50 36.44 2.31 o 8 3 8 40.49 45.20 2.62 o -5 4 8 23.31 22.69 1.06 o -4 4 8 0.05 0.14 0.30 < -3 4 8 1.08 1.89 0.51 o -2 4 8 0.24 -0.19 0.37 < -1 4 8 1.08 2.61 0.37 o 0 4 8 26.64 25.48 1.60 o 1 4 8 22.14 20.33 0.83 o 2 4 8 0.10 -0.38 0.43 < 3 4 8 41.67 44.07 1.77 o 4 4 8 0.40 0.74 0.59 < -13 1 9 0.09 0.39 0.29 < -12 1 9 4.12 3.68 0.48 o -11 1 9 18.71 17.33 1.58 o -10 1 9 6.00 8.52 0.95 o -9 1 9 131.11 127.16 2.39 o -8 1 9 7.08 11.50 0.92 o -7 1 9 42.94 42.43 1.58 o -6 1 9 5.52 5.81 0.78 o -5 1 9 1107.80 1140.78 18.13 o -4 1 9 0.67 0.76 0.49 < -3 1 9 2.26 3.57 0.57 o -2 1 9 9.25 9.16 0.49 o -1 1 9 230.02 244.53 3.23 o 0 1 9 1.97 1.34 0.67 < 1 1 9 35.01 37.48 1.30 o 2 1 9 82.25 86.04 2.07 o 3 1 9 0.87 0.81 0.50 < 4 1 9 125.09 126.49 2.18 o 5 1 9 156.32 155.08 2.91 o 6 1 9 282.99 296.30 4.21 o 7 1 9 106.48 101.26 1.67 o 8 1 9 8.38 4.90 0.71 o 9 1 9 2.40 3.71 0.58 o 10 1 9 256.06 238.16 5.13 o 11 1 9 2.46 2.99 0.75 o -11 2 9 78.81 73.08 5.88 o -10 2 9 3.83 2.81 0.41 o -9 2 9 7.25 8.52 0.67 o -8 2 9 75.33 72.15 2.14 o -7 2 9 265.54 251.91 5.08 o -6 2 9 236.95 240.26 5.07 o -5 2 9 28.68 27.16 1.12 o -4 2 9 1.46 1.18 0.74 < -3 2 9 88.02 84.90 2.73 o -2 2 9 9.81 12.18 1.21 o -1 2 9 269.48 267.27 5.84 o 0 2 9 58.62 55.16 2.09 o 1 2 9 8.74 8.16 0.87 o 2 2 9 5.64 7.41 0.57 o 3 2 9 26.65 27.81 0.81 o 4 2 9 49.58 45.54 1.29 o 5 2 9 16.93 17.11 0.67 o 6 2 9 67.86 68.76 2.38 o 7 2 9 8.14 7.57 0.57 o 8 2 9 22.37 19.45 1.98 o 9 2 9 1.27 1.08 0.38 < 10 2 9 48.08 52.52 2.08 o -9 3 9 33.94 28.31 2.74 o -8 3 9 21.60 18.83 1.08 o -7 3 9 0.31 0.89 0.49 < -6 3 9 4.90 3.11 0.62 o -5 3 9 1.46 1.39 0.47 < -4 3 9 65.90 65.33 2.58 o -3 3 9 12.89 12.24 1.25 o -2 3 9 76.15 74.15 1.94 o -1 3 9 43.69 43.79 1.43 o 0 3 9 0.05 1.05 0.55 < 1 3 9 32.83 29.25 1.23 o 2 3 9 12.20 10.26 0.81 o 3 3 9 0.12 0.69 0.43 < 4 3 9 0.66 2.00 0.53 o 5 3 9 0.97 2.47 0.34 o 6 3 9 2.45 3.63 0.57 o 7 3 9 10.69 12.45 0.93 o -2 4 9 42.64 37.24 1.76 o -1 4 9 9.87 10.55 1.56 o 0 4 9 3.66 2.46 0.82 o 1 4 9 3.55 3.93 0.76 o -11 0 10 136.71 132.21 2.71 o -10 0 10 1.30 1.76 0.62 < -9 0 10 34.65 43.03 1.63 o -8 0 10 240.21 247.16 4.30 o -7 0 10 104.39 100.25 2.54 o -6 0 10 219.33 243.19 4.92 o -5 0 10 736.23 765.23 12.39 o -4 0 10 18.75 19.70 1.26 o -3 0 10 1010.21 1010.21 12.98 o -2 0 10 73.33 81.55 3.03 o -1 0 10 111.82 122.57 3.66 o 0 0 10 114.24 115.31 3.39 o 1 0 10 4.67 4.61 0.89 o 2 0 10 291.30 309.78 8.96 o 3 0 10 252.14 290.29 5.47 o 4 0 10 458.74 484.52 25.04 o 5 0 10 6.65 7.79 1.35 o 6 0 10 55.01 51.95 2.50 o 7 0 10 544.39 523.60 7.00 o 8 0 10 296.17 273.55 4.51 o 9 0 10 256.96 243.94 5.10 o 10 0 10 3.85 5.04 0.83 o -12 1 10 0.10 1.27 0.35 o -11 1 10 1.12 2.20 0.45 o -10 1 10 10.58 9.54 0.82 o -9 1 10 95.09 94.50 2.35 o -8 1 10 50.05 51.79 1.60 o -7 1 10 0.44 0.93 0.61 < -6 1 10 179.04 187.90 3.51 o -5 1 10 7.53 6.76 0.89 o -4 1 10 182.14 181.35 5.64 o -3 1 10 434.04 412.66 7.71 o -2 1 10 69.22 68.63 1.70 o -1 1 10 14.06 11.61 0.79 o 0 1 10 88.85 91.45 1.86 o 1 1 10 35.90 36.95 0.98 o 2 1 10 0.98 1.31 0.47 < 3 1 10 0.19 0.13 0.43 < 4 1 10 0.18 0.63 0.42 < 5 1 10 16.45 14.84 0.99 o 6 1 10 135.68 131.96 2.63 o 7 1 10 1.01 0.30 0.58 < 8 1 10 36.21 28.48 1.58 o 9 1 10 20.70 15.22 1.54 o 10 1 10 54.20 48.25 2.07 o -10 2 10 2.88 3.82 0.39 o -9 2 10 54.79 53.84 1.45 o -8 2 10 7.00 8.73 0.68 o -7 2 10 294.47 286.32 5.81 o -6 2 10 40.86 37.04 1.63 o -5 2 10 41.39 38.12 1.47 o -4 2 10 200.13 202.71 3.31 o -3 2 10 22.04 22.70 1.32 o -2 2 10 159.73 155.53 4.74 o -1 2 10 9.45 10.77 0.81 o 0 2 10 12.17 8.62 0.77 o 1 2 10 31.29 35.10 1.24 o 2 2 10 157.59 150.26 2.07 o 3 2 10 117.08 112.95 2.62 o 4 2 10 0.93 1.10 0.39 < 5 2 10 28.33 25.13 0.99 o 6 2 10 19.22 15.22 1.05 o 7 2 10 5.68 6.95 0.55 o 8 2 10 1.23 0.30 0.61 < -8 3 10 65.25 70.05 5.40 o -7 3 10 80.06 80.78 2.07 o -6 3 10 35.59 34.16 1.87 o -5 3 10 165.15 160.57 5.67 o -4 3 10 2.86 1.53 0.48 o -3 3 10 9.05 8.57 0.87 o -2 3 10 0.13 0.84 0.62 < -1 3 10 0.20 -0.05 0.49 < 0 3 10 92.02 99.02 2.64 o 1 3 10 0.04 0.16 0.47 < 2 3 10 0.22 0.13 0.46 < 3 3 10 7.60 6.59 0.61 o 4 3 10 75.21 73.12 1.85 o 5 3 10 16.02 16.13 1.63 o 6 3 10 3.64 3.44 0.63 o -11 1 11 3.67 4.54 0.50 o -10 1 11 14.33 11.02 1.20 o -9 1 11 71.05 76.22 2.31 o -8 1 11 6.12 6.24 0.63 o -7 1 11 32.41 34.00 1.28 o -6 1 11 130.51 122.92 2.40 o -5 1 11 20.90 18.41 1.07 o -4 1 11 146.10 145.98 3.57 o -3 1 11 12.05 12.78 0.81 o -2 1 11 93.46 87.27 3.72 o -1 1 11 1.37 2.70 0.56 o 0 1 11 346.55 389.48 6.07 o 1 1 11 209.23 243.90 2.93 o 2 1 11 192.16 197.00 4.67 o 3 1 11 52.70 53.46 1.76 o 4 1 11 185.13 184.65 4.29 o 5 1 11 41.18 36.56 1.33 o 6 1 11 30.68 29.75 1.93 o 7 1 11 0.64 0.16 0.47 < 8 1 11 0.06 0.23 0.45 < 9 1 11 6.49 5.12 0.90 o -9 2 11 54.90 51.72 6.48 o -8 2 11 3.50 4.76 0.63 o -7 2 11 17.84 16.57 1.00 o -6 2 11 12.70 13.18 1.02 o -5 2 11 57.21 57.52 1.93 o -4 2 11 0.61 0.57 0.49 < -3 2 11 120.46 112.08 3.02 o -2 2 11 9.93 8.32 0.66 o -1 2 11 78.97 77.15 3.23 o 0 2 11 146.95 146.61 3.29 o 1 2 11 35.39 41.70 1.12 o 2 2 11 317.55 344.25 3.69 o 3 2 11 5.85 5.57 0.49 o 4 2 11 3.92 5.19 0.53 o 5 2 11 8.19 6.81 0.64 o 6 2 11 0.58 1.45 0.43 o 7 2 11 1.00 0.76 0.52 < -6 3 11 0.68 -0.24 0.62 < -5 3 11 0.18 0.79 0.74 < -4 3 11 2.60 2.41 0.36 o -3 3 11 19.09 16.76 0.78 o -2 3 11 37.22 32.56 1.38 o -1 3 11 7.89 7.67 0.60 o 0 3 11 70.33 70.41 1.99 o 1 3 11 59.00 67.26 1.91 o 2 3 11 4.77 4.78 0.55 o 3 3 11 41.57 39.23 1.27 o 4 3 11 43.83 45.36 3.91 o -10 0 12 0.38 -0.34 0.52 < -9 0 12 50.44 62.88 2.79 o -8 0 12 0.07 -0.26 0.68 < -7 0 12 13.92 16.45 0.99 o -6 0 12 7.70 11.33 0.72 o -5 0 12 7.38 10.46 0.88 o -4 0 12 278.93 295.14 4.91 o -3 0 12 7.36 6.10 0.95 o -2 0 12 443.46 454.96 5.09 o -1 0 12 419.27 448.79 6.84 o 0 0 12 48.20 52.36 2.06 o 1 0 12 296.53 312.97 4.46 o 2 0 12 38.92 45.49 1.83 o 3 0 12 44.75 51.84 2.55 o 4 0 12 103.13 97.75 3.36 o 5 0 12 67.63 64.26 2.57 o 6 0 12 2.40 2.71 0.76 o 7 0 12 68.79 69.58 2.14 o -9 1 12 0.00 0.38 0.39 < -8 1 12 20.54 20.02 0.83 o -7 1 12 63.49 73.76 1.87 o -6 1 12 3.44 3.68 0.55 o -5 1 12 2.08 1.35 0.45 o -4 1 12 24.33 23.23 1.62 o -3 1 12 48.54 43.77 1.53 o -2 1 12 133.38 129.55 3.41 o -1 1 12 301.92 301.52 11.06 o 0 1 12 141.81 153.19 4.01 o 1 1 12 5.96 3.59 0.54 o 2 1 12 1.21 2.05 0.48 o 3 1 12 11.11 12.90 0.73 o 4 1 12 8.08 6.97 0.67 o 5 1 12 0.90 1.27 0.71 < 6 1 12 56.49 64.59 1.79 o 7 1 12 4.31 1.95 1.05 < -8 2 12 2.43 1.84 0.76 < -7 2 12 2.69 2.49 0.69 o -6 2 12 17.33 16.23 1.06 o -5 2 12 23.31 23.08 1.11 o -4 2 12 2.84 3.69 0.86 o -3 2 12 75.16 70.92 5.30 o -2 2 12 5.02 6.10 0.97 o -1 2 12 37.70 40.36 1.84 o 0 2 12 78.62 63.96 2.37 o 1 2 12 1.38 1.95 0.42 o 2 2 12 69.27 72.18 2.30 o 3 2 12 0.02 0.72 0.50 < 4 2 12 13.42 13.22 1.00 o 5 2 12 11.26 11.80 1.18 o -1 3 12 95.44 83.69 5.73 o -8 1 13 16.36 15.64 1.04 o -7 1 13 4.16 6.49 0.58 o -6 1 13 5.12 7.01 0.52 o -5 1 13 0.00 -0.19 0.43 < -4 1 13 20.27 15.76 1.21 o -3 1 13 70.35 71.62 3.31 o -2 1 13 21.05 19.31 1.03 o -1 1 13 20.51 17.97 1.04 o 0 1 13 8.26 10.12 0.66 o 1 1 13 42.42 36.64 2.70 o 2 1 13 0.97 0.34 0.44 < 3 1 13 31.10 28.25 3.53 o 4 1 13 73.38 75.33 6.46 o 5 1 13 29.47 34.48 1.20 o -5 2 13 0.19 -0.34 0.65 < -4 2 13 4.69 4.10 0.70 o -3 2 13 95.47 84.38 5.07 o -2 2 13 8.11 10.49 0.99 o -1 2 13 39.22 39.90 1.66 o 0 2 13 0.86 0.53 0.45 < 1 2 13 114.20 103.10 6.83 o 2 2 13 0.02 -0.04 0.48 < 3 2 13 41.47 38.14 1.60 o -6 0 14 111.21 113.78 3.07 o -5 0 14 6.96 4.48 0.71 o -4 0 14 4.01 3.57 0.48 o -3 0 14 28.17 36.87 1.76 o -2 0 14 3.06 2.45 0.69 o -1 0 14 33.43 32.74 1.58 o 0 0 14 10.79 10.63 1.07 o 1 0 14 51.90 55.70 2.11 o 2 0 14 192.81 199.96 3.79 o 3 0 14 1.31 3.91 0.74 o 4 0 14 0.12 0.20 0.57 < -5 1 14 65.58 64.96 10.41 o -4 1 14 3.30 2.67 0.48 o -3 1 14 0.71 0.80 0.81 < -2 1 14 6.07 5.25 0.65 o -1 1 14 6.04 5.71 0.65 o 0 1 14 2.43 2.06 0.50 o 1 1 14 22.20 21.01 3.81 o 2 1 14 7.08 9.76 1.86 o 3 1 14 34.83 35.38 4.81 o