#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/37/2233769.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233769_Fobs loop_ _publ_author_name 'Zhang, Yan' 'Liu, Min' 'Ma, Jing-Jun' _publ_section_title ; N'-(2-Hydroxy-4-methoxybenzylidene)-4-methylbenzohydrazide ; _journal_coeditor_code CV5243 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o679 _journal_page_last o680 _journal_volume 68 _journal_year 2012 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.646 _cell_angle_gamma 90.000 _cell_length_a 24.8710 _cell_length_b 10.2350 _cell_length_c 23.8550 _exptl_crystal_F_000 2400.00 _reflns_d_resolution_high 0.7981 _[local]_cod_data_source_file cv5243Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 712.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 510.80 482.29 29.62 o 4 0 0 29969.93 29986.53 1202.15 o 5 0 0 124.54 116.23 14.18 o 6 0 0 1260.84 1338.37 61.81 o 7 0 0 987.12 864.48 51.27 o 8 0 0 12215.69 11508.64 472.41 o 9 0 0 72.61 74.85 18.43 o 10 0 0 334.81 245.28 36.97 o 11 0 0 37.93 13.23 17.77 o 12 0 0 31556.01 30425.23 1233.65 o 13 0 0 967.99 1271.13 72.56 o 14 0 0 524.06 509.57 43.66 o 15 0 0 133.76 103.68 29.32 o 16 0 0 778.46 706.73 55.22 o 17 0 0 1453.62 1759.79 96.67 o 18 0 0 468.71 533.60 61.04 o 19 0 0 132.96 139.18 63.74 o 20 0 0 32.26 28.96 34.25 o 21 0 0 52.98 88.43 52.66 o 22 0 0 125.64 155.06 57.53 o 23 0 0 54.59 90.69 54.23 o 24 0 0 101.80 71.37 69.82 o 25 0 0 0.24 75.98 67.49 o 26 0 0 2.20 -9.31 55.95 o 27 0 0 0.68 4.30 63.61 o 28 0 0 266.90 314.22 80.58 o 29 0 0 0.09 146.15 73.56 o 30 0 0 14.11 56.39 70.70 o 1 1 0 361.04 511.99 46.54 o 2 1 0 29059.92 28384.01 1145.63 o 3 1 0 502.97 426.33 18.46 o 4 1 0 3071.00 2972.92 106.98 o 5 1 0 13.22 14.07 7.32 o 6 1 0 12738.70 11575.71 334.60 o 7 1 0 2.06 -2.16 7.80 o 8 1 0 1428.11 1181.19 42.36 o 9 1 0 174.23 140.15 14.72 o 10 1 0 1095.79 1258.64 57.88 o 11 1 0 2.30 -16.85 11.24 o 12 1 0 3494.33 3449.29 110.47 o 13 1 0 0.14 11.76 15.15 o 14 1 0 966.82 1042.91 47.53 o 15 1 0 270.09 230.57 24.17 o 16 1 0 518.68 571.13 35.39 o 17 1 0 168.95 186.01 25.03 o 18 1 0 2898.72 2492.13 91.15 o 19 1 0 52.74 121.85 29.27 o 20 1 0 567.28 642.04 48.57 o 21 1 0 16.63 39.91 39.76 o 22 1 0 44.35 72.42 31.69 o 23 1 0 0.35 20.12 36.02 o 24 1 0 240.84 287.45 51.12 o 25 1 0 133.15 160.46 46.40 o 26 1 0 24.37 17.46 40.71 o 27 1 0 19.60 38.99 42.16 o 28 1 0 98.03 98.91 48.87 o 29 1 0 13.51 106.16 57.10 o 30 1 0 0.26 137.31 75.70 o 0 2 0 4390.28 5027.48 211.12 o 1 2 0 108.77 94.14 15.60 o 2 2 0 42639.85 43085.08 1228.44 o 3 2 0 328.90 343.02 17.77 o 4 2 0 7056.84 6506.00 191.61 o 5 2 0 188.26 329.56 50.93 o 6 2 0 24738.59 23768.13 742.35 o 7 2 0 397.91 386.33 32.96 o 8 2 0 1050.76 960.81 37.79 o 9 2 0 11.70 0.56 10.25 o 10 2 0 341.55 262.15 20.13 o 11 2 0 711.62 635.08 37.81 o 12 2 0 3955.46 3878.34 123.34 o 13 2 0 0.13 2.71 15.15 o 14 2 0 582.55 482.37 38.86 o 15 2 0 92.51 87.56 20.26 o 17 2 0 578.12 511.91 40.63 o 18 2 0 449.95 590.09 44.57 o 19 2 0 5.43 59.32 29.22 o 20 2 0 0.96 -4.66 34.91 o 21 2 0 370.02 409.77 44.11 o 22 2 0 18.77 40.88 32.61 o 23 2 0 17.04 22.87 33.31 o 24 2 0 21.40 -15.66 33.43 o 25 2 0 56.92 186.00 48.46 o 26 2 0 82.08 131.41 49.27 o 27 2 0 121.79 165.06 61.05 o 28 2 0 154.50 148.07 78.78 o 29 2 0 5.61 64.13 74.00 o 0 3 0 10.43 -18.62 14.18 o 1 3 0 476.64 422.05 23.22 o 2 3 0 324.94 388.57 22.67 o 3 3 0 873.55 818.42 34.00 o 4 3 0 498.75 431.25 24.26 o 5 3 0 2232.60 2093.91 70.32 o 6 3 0 732.17 855.10 40.24 o 7 3 0 3753.14 3554.86 120.96 o 8 3 0 3813.56 3797.61 128.91 o 9 3 0 3109.47 2959.74 96.62 o 10 3 0 315.65 378.31 25.27 o 11 3 0 1002.48 978.04 42.80 o 12 3 0 1223.77 1294.99 52.41 o 13 3 0 277.40 363.26 40.24 o 14 3 0 2343.36 2061.52 75.62 o 15 3 0 146.38 170.89 27.28 o 16 3 0 200.35 206.75 30.51 o 17 3 0 10.53 24.65 23.95 o 19 3 0 752.76 792.33 54.08 o 20 3 0 3074.68 2956.43 119.70 o 21 3 0 937.53 1058.44 67.37 o 22 3 0 30.46 31.78 32.26 o 23 3 0 188.66 217.93 41.90 o 24 3 0 59.45 44.47 40.95 o 25 3 0 47.81 31.19 49.58 o 26 3 0 0.48 43.42 65.46 o 27 3 0 68.17 129.63 77.29 o 28 3 0 1.17 17.95 68.18 o 29 3 0 34.75 2.33 72.41 o 0 4 0 7055.12 8270.72 349.75 o 1 4 0 13.48 17.69 14.57 o 2 4 0 475.38 710.73 35.46 o 3 4 0 127.86 123.32 22.46 o 4 4 0 1.65 -16.12 13.20 o 5 4 0 969.30 1098.44 44.97 o 6 4 0 1027.44 872.92 39.46 o 7 4 0 1330.91 1290.67 58.63 o 8 4 0 77.88 111.18 23.68 o 9 4 0 199.75 152.64 26.63 o 10 4 0 761.00 870.84 42.67 o 11 4 0 1031.99 960.95 43.99 o 12 4 0 221.93 250.74 27.06 o 13 4 0 130.53 110.92 25.68 o 14 4 0 40.46 51.01 23.48 o 15 4 0 268.55 293.82 33.69 o 16 4 0 660.30 627.70 48.47 o 17 4 0 258.66 264.81 35.58 o 18 4 0 86.15 170.80 35.56 o 19 4 0 4214.48 4236.71 159.86 o 20 4 0 0.00 115.24 35.46 o 21 4 0 309.85 326.74 51.61 o 22 4 0 5.39 63.91 41.66 o 23 4 0 148.83 134.50 53.21 o 24 4 0 107.27 71.96 52.52 o 25 4 0 0.08 98.64 57.15 o 26 4 0 175.53 193.09 63.10 o 27 4 0 2.74 -17.55 55.49 o 28 4 0 18.41 223.62 216.43 o 0 5 0 5.34 -19.89 20.48 o 1 5 0 119.35 139.41 21.62 o 2 5 0 330.81 414.81 32.35 o 3 5 0 30.39 -3.10 21.12 o 4 5 0 149.61 250.25 24.33 o 5 5 0 580.56 589.33 35.20 o 6 5 0 5034.33 5178.60 163.14 o 7 5 0 5770.88 5441.00 171.46 o 8 5 0 5570.89 5660.71 177.74 o 9 5 0 0.33 18.69 19.45 o 10 5 0 1214.03 1400.61 102.36 o 11 5 0 1071.15 1084.35 56.51 o 12 5 0 1495.08 1463.28 68.24 o 13 5 0 34.35 34.77 24.45 o 14 5 0 286.03 253.44 33.07 o 15 5 0 149.18 128.41 37.04 o 16 5 0 275.65 331.77 38.96 o 17 5 0 280.19 342.06 40.43 o 18 5 0 27.03 105.50 39.46 o 19 5 0 1680.29 1555.15 93.78 o 20 5 0 13.78 69.43 49.22 o 21 5 0 32.96 2.40 48.94 o 22 5 0 16.61 8.11 50.92 o 23 5 0 42.09 72.32 56.75 o 24 5 0 85.23 67.34 53.21 o 25 5 0 1.29 -26.19 51.91 o 26 5 0 109.05 178.51 67.93 o 27 5 0 2.10 65.52 67.93 o 0 6 0 160.99 67.59 45.55 o 1 6 0 11.46 -17.73 18.21 o 2 6 0 116.13 185.13 25.52 o 3 6 0 19.48 55.30 27.44 o 4 6 0 340.90 282.03 28.61 o 5 6 0 320.47 248.61 27.27 o 6 6 0 923.55 845.49 58.04 o 7 6 0 818.25 813.65 49.61 o 8 6 0 27.92 34.19 20.36 o 9 6 0 0.69 -13.20 22.81 o 10 6 0 107.55 106.80 28.00 o 11 6 0 1.47 -8.46 23.33 o 12 6 0 0.01 -38.97 32.75 o 13 6 0 38.49 11.36 26.55 o 14 6 0 13.45 -41.66 27.77 o 15 6 0 69.40 59.77 39.64 o 16 6 0 305.96 293.16 47.63 o 17 6 0 32.20 66.34 49.03 o 18 6 0 17.34 -62.62 43.39 o 19 6 0 195.66 167.94 57.51 o 20 6 0 271.43 300.95 66.55 o 21 6 0 75.83 117.07 75.86 o 22 6 0 61.95 81.05 70.67 o 23 6 0 33.61 12.44 52.80 o 24 6 0 0.00 96.10 58.20 o 25 6 0 6.02 66.70 59.47 o 26 6 0 26.69 111.24 66.75 o 0 7 0 485.86 679.81 64.38 o 1 7 0 82.11 178.80 28.82 o 2 7 0 1465.76 1677.21 73.24 o 4 7 0 5705.61 5457.19 176.47 o 5 7 0 93.60 154.97 26.45 o 6 7 0 1280.57 1299.73 60.94 o 7 7 0 252.03 248.08 39.20 o 8 7 0 118.65 70.94 26.58 o 9 7 0 220.93 258.69 37.12 o 10 7 0 60.55 80.91 29.56 o 11 7 0 28.77 2.07 31.26 o 12 7 0 610.17 427.75 50.85 o 13 7 0 3.67 -69.95 46.63 o 14 7 0 409.40 355.78 87.15 o 15 7 0 169.80 188.70 58.08 o 16 7 0 1498.08 1220.02 169.08 o 17 7 0 182.17 145.19 58.20 o 18 7 0 48.13 60.08 56.07 o 19 7 0 73.93 -4.12 48.37 o 20 7 0 2.98 37.99 54.69 o 21 7 0 11.96 7.19 55.92 o 22 7 0 4.65 -30.25 51.83 o 23 7 0 0.46 122.66 65.24 o 24 7 0 14.38 31.07 58.42 o 25 7 0 3.80 8.13 60.62 o 0 8 0 861.19 885.00 84.63 o 1 8 0 494.11 535.59 44.99 o 2 8 0 776.58 1068.95 74.78 o 5 8 0 261.69 440.30 39.46 o 6 8 0 84.57 183.08 36.19 o 7 8 0 252.97 280.00 38.48 o 8 8 0 6.83 23.74 34.88 o 9 8 0 69.29 161.65 42.90 o 10 8 0 133.94 59.50 52.42 o 11 8 0 39.93 94.73 111.71 o 12 8 0 589.97 531.01 93.35 o 13 8 0 24.56 51.15 49.58 o 14 8 0 5.58 111.28 53.42 o 15 8 0 31.07 85.60 56.81 o 16 8 0 438.64 269.31 68.84 o 17 8 0 70.82 109.42 58.70 o 18 8 0 17.79 9.10 53.88 o 19 8 0 13.81 22.42 58.08 o 20 8 0 91.63 26.35 56.17 o 21 8 0 25.72 -81.15 54.10 o 22 8 0 0.67 56.48 61.62 o 23 8 0 0.93 -23.34 55.14 o 0 9 0 2002.17 2631.05 151.85 o 2 9 0 396.66 679.81 66.76 o 3 9 0 88.42 97.83 37.96 o 4 9 0 549.06 686.75 65.65 o 5 9 0 89.16 112.51 41.41 o 6 9 0 1.20 32.98 43.00 o 7 9 0 64.91 65.04 40.12 o 8 9 0 3.05 35.54 53.63 o 9 9 0 121.32 28.47 102.40 o 10 9 0 144.96 62.84 59.24 o 11 9 0 2.52 41.41 49.03 o 12 9 0 14.47 -29.07 55.12 o 13 9 0 95.37 21.07 66.40 o 14 9 0 16.50 35.08 52.29 o 15 9 0 131.23 102.80 58.57 o 16 9 0 4.48 6.63 55.28 o 17 9 0 37.80 83.05 60.71 o 18 9 0 1.00 -26.24 54.34 o 19 9 0 2.17 155.18 71.90 o 20 9 0 28.37 18.62 61.48 o 21 9 0 1.53 -2.03 68.50 o 0 10 0 392.96 382.15 85.57 o 1 10 0 231.46 302.49 61.15 o 2 10 0 904.68 1059.20 98.11 o 3 10 0 150.25 297.05 54.06 o 4 10 0 20.86 33.63 42.61 o 5 10 0 1.76 8.44 50.15 o 6 10 0 15.46 36.52 63.61 o 7 10 0 55.28 144.29 65.82 o 8 10 0 1.22 -36.14 55.66 o 9 10 0 37.38 134.54 68.88 o 10 10 0 426.52 330.79 70.73 o 11 10 0 2.40 65.02 54.00 o 12 10 0 0.03 63.82 55.22 o 13 10 0 0.00 57.00 59.85 o 14 10 0 20.12 95.74 59.27 o 15 10 0 16.93 -6.39 58.07 o 16 10 0 316.05 261.83 77.32 o 17 10 0 3.39 48.98 62.18 o 18 10 0 299.42 262.22 80.72 o 0 11 0 2.24 -111.71 74.47 o 1 11 0 3.00 -59.84 56.96 o 2 11 0 187.32 62.84 69.12 o 3 11 0 6.82 18.62 65.82 o 4 11 0 879.44 782.13 110.22 o 5 11 0 47.88 50.29 66.93 o 6 11 0 108.39 174.69 139.63 o 7 11 0 6.64 3.49 64.84 o 8 11 0 82.16 47.30 69.34 o 9 11 0 8.31 90.16 58.91 o 10 11 0 4.92 2.41 49.98 o 11 11 0 2.57 2.82 55.46 o 12 11 0 11.23 26.98 56.17 o 13 11 0 10.48 97.59 106.38 o 14 11 0 14.01 101.73 63.56 o 15 11 0 0.22 18.11 62.13 o 3 12 0 33.10 23.27 97.74 o 4 12 0 89.37 172.22 116.36 o 5 12 0 13.69 0.00 93.09 o 6 12 0 7.27 -93.09 83.78 o 7 12 0 191.12 160.97 134.98 o 8 12 0 0.20 -13.96 69.12 o 9 12 0 28.59 18.00 59.98 o 10 12 0 0.95 -22.56 59.00 o -30 1 1 19.89 88.43 51.35 o -29 1 1 92.71 101.20 50.37 o -28 1 1 0.41 65.98 44.99 o -27 1 1 87.68 72.58 45.16 o -26 1 1 84.81 180.98 46.51 o -25 1 1 1.05 17.55 46.72 o -24 1 1 34.23 29.72 38.55 o -23 1 1 424.74 395.84 52.49 o -22 1 1 0.11 62.27 30.99 o -21 1 1 1498.64 1446.36 74.76 o -20 1 1 3.42 39.69 32.80 o -18 1 1 48.58 90.83 22.55 o -17 1 1 1488.18 1322.21 56.39 o -16 1 1 251.91 244.92 25.33 o -15 1 1 739.82 841.14 41.93 o -14 1 1 92.05 80.80 18.58 o -13 1 1 78.94 117.22 18.81 o -12 1 1 375.01 373.57 24.97 o -11 1 1 0.20 -9.98 11.08 o -10 1 1 1210.55 1065.91 40.73 o -9 1 1 374.65 387.00 27.51 o -8 1 1 385.57 391.30 20.60 o -7 1 1 4774.35 4192.76 136.94 o -6 1 1 178.97 183.03 14.28 o -5 1 1 1237.19 1046.63 39.82 o -4 1 1 5.04 8.79 7.96 o -3 1 1 4053.92 3975.74 127.21 o -2 1 1 3556.96 3407.10 108.88 o -1 1 1 33.46 83.78 18.62 o 0 1 1 1319.31 1291.65 69.12 o 1 1 1 37.53 50.64 8.72 o 2 1 1 3.82 7.76 8.06 o 3 1 1 221.60 252.47 16.12 o 4 1 1 194.95 211.78 11.76 o 5 1 1 4044.70 3715.49 111.65 o 6 1 1 250.89 249.64 15.27 o 7 1 1 194.83 213.16 14.54 o 8 1 1 859.34 707.01 29.55 o 9 1 1 325.98 300.36 19.70 o 10 1 1 834.77 736.19 33.21 o 11 1 1 5931.01 5878.96 179.09 o 12 1 1 443.85 458.77 28.27 o 13 1 1 98.01 82.48 18.40 o 14 1 1 598.36 542.46 32.52 o 15 1 1 780.11 693.29 37.85 o 16 1 1 56.52 80.36 20.73 o 17 1 1 130.91 184.39 26.35 o 18 1 1 512.17 538.35 37.35 o 19 1 1 1395.47 1165.59 57.29 o 20 1 1 69.41 144.50 31.46 o 21 1 1 1181.24 1136.35 66.35 o 22 1 1 1.38 42.61 31.17 o 23 1 1 764.66 705.55 64.43 o 24 1 1 33.46 32.32 38.84 o 25 1 1 37.00 -39.14 38.35 o 26 1 1 89.89 129.86 48.00 o 27 1 1 297.50 310.25 57.38 o 28 1 1 3.20 44.26 52.68 o 29 1 1 7.67 51.20 69.12 o -30 2 1 0.23 85.64 73.56 o -29 2 1 24.72 131.34 74.84 o -28 2 1 7.40 39.40 44.72 o -27 2 1 23.91 -14.31 42.05 o -26 2 1 71.10 101.34 46.12 o -25 2 1 263.82 170.97 47.67 o -24 2 1 123.80 152.31 38.87 o -23 2 1 17.66 17.33 32.38 o -22 2 1 13.44 141.90 35.70 o -21 2 1 771.36 781.12 79.97 o -20 2 1 27.91 -3.13 31.03 o -19 2 1 1254.53 1231.25 66.72 o -18 2 1 111.17 130.45 29.75 o -17 2 1 110.44 156.81 55.24 o -16 2 1 58.84 53.39 19.84 o -15 2 1 239.93 252.84 25.72 o -14 2 1 0.14 -21.98 14.65 o -13 2 1 1187.49 1052.33 45.31 o -12 2 1 434.82 433.86 27.53 o -11 2 1 1198.22 1125.22 45.05 o -10 2 1 0.43 2.72 11.06 o -9 2 1 1390.19 1253.91 50.20 o -8 2 1 524.23 477.70 26.30 o -7 2 1 25175.35 24453.28 704.82 o -6 2 1 52.18 56.64 28.47 o -5 2 1 7945.85 6835.96 219.42 o -4 2 1 2865.12 2491.75 85.93 o -3 2 1 2611.56 2285.53 98.23 o -2 2 1 319.92 399.23 28.22 o -1 2 1 169864.19 171846.72 4871.09 o 0 2 1 197.30 231.82 15.35 o 1 2 1 6370.72 6999.49 205.50 o 2 2 1 829.54 912.83 37.81 o 3 2 1 5747.42 6501.21 207.48 o 4 2 1 216.81 205.00 14.84 o 5 2 1 6588.85 7018.46 230.29 o 6 2 1 131.57 123.12 19.71 o 7 2 1 1160.71 1193.47 43.17 o 8 2 1 70.54 59.26 12.48 o 9 2 1 3441.97 3061.26 97.92 o 10 2 1 13.41 -3.13 12.13 o 11 2 1 30.20 44.30 14.59 o 12 2 1 67.24 94.47 18.04 o 13 2 1 546.27 499.17 33.13 o 14 2 1 79.14 41.11 18.18 o 15 2 1 690.01 588.73 36.27 o 16 2 1 336.39 334.02 29.62 o 18 2 1 1021.25 1094.01 64.68 o 19 2 1 143.52 73.84 48.00 o 20 2 1 48.28 66.19 32.26 o 21 2 1 892.93 948.17 67.82 o 22 2 1 6.31 27.73 33.69 o 23 2 1 9.22 80.20 35.92 o 24 2 1 274.91 316.57 54.94 o 25 2 1 80.74 74.96 43.40 o 26 2 1 29.21 181.52 75.70 o 27 2 1 132.63 125.67 72.41 o 28 2 1 8.96 190.83 82.28 o 29 2 1 17.80 123.34 78.99 o -29 3 1 4.22 -46.77 68.88 o -28 3 1 13.85 64.76 75.48 o -27 3 1 73.20 107.05 73.56 o -26 3 1 28.20 76.24 45.59 o -25 3 1 97.38 149.33 42.39 o -24 3 1 4.98 27.25 35.47 o -23 3 1 102.34 124.32 37.90 o -22 3 1 100.87 177.87 37.24 o -21 3 1 499.40 526.00 49.91 o -20 3 1 320.26 379.19 43.53 o -19 3 1 1345.92 1335.36 70.96 o -18 3 1 90.32 110.12 31.49 o -17 3 1 18.34 72.17 25.10 o -16 3 1 1.77 -12.47 26.68 o 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