#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233801.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233801_Fobs loop_ _publ_author_name 'Zhao, Shunsheng' 'Liu, Xiangrong' 'L\"u, Xingqiang' 'Feng, Weixu' _publ_section_title ; 4-Bromo-2-methoxy-6-(1-phenyl-1H-benzimidazol-2-yl)phenol ; _journal_coeditor_code FY2036 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o852 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 87.812 _cell_angle_beta 89.045 _cell_angle_gamma 64.652 _cell_length_a 12.3768 _cell_length_b 13.2010 _cell_length_c 17.4736 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.8480 _[local]_cod_data_source_file fy2036Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sun in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 483.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 18.79 8.72 4.03 o 2 0 0 2817.87 2482.26 129.43 o 3 0 0 5930.68 5859.00 137.67 o 4 0 0 995.75 922.99 78.73 o 5 0 0 12491.48 11609.83 263.70 o 6 0 0 2093.28 2235.41 81.58 o 7 0 0 919.04 848.79 54.56 o 8 0 0 3148.11 3189.17 129.22 o 9 0 0 2.20 13.84 29.07 o 10 0 0 179.00 213.72 51.06 o 11 0 0 27.05 18.19 41.32 o 12 0 0 4.59 -16.49 42.98 o 13 0 0 158.39 104.17 72.68 o -12 1 0 184.90 217.17 64.96 o -11 1 0 0.71 32.35 46.95 o -10 1 0 18.22 -10.95 54.51 o -9 1 0 396.88 524.06 156.25 o -8 1 0 587.09 591.36 54.84 o -7 1 0 44.49 19.08 25.07 o -6 1 0 21.57 43.06 23.66 o -5 1 0 519.57 581.90 39.53 o -4 1 0 5723.39 4700.48 301.29 o -3 1 0 1221.33 1200.97 51.53 o -2 1 0 23564.11 24451.78 1300.88 o -1 1 0 3052.38 2611.57 180.48 o 1 1 0 2379.97 2991.79 104.17 o 2 1 0 10.51 -4.85 9.69 o 3 1 0 2015.09 1713.60 53.26 o 4 1 0 6454.03 7032.37 224.43 o 5 1 0 62.38 35.46 17.91 o 6 1 0 723.14 659.82 46.61 o 7 1 0 187.63 170.50 32.25 o 8 1 0 178.21 185.83 37.16 o 9 1 0 6.51 5.19 29.07 o 10 1 0 678.62 590.39 65.17 o 11 1 0 159.31 198.65 65.41 o 12 1 0 727.37 763.09 104.17 o 13 1 0 5.85 19.38 58.14 o -12 2 0 75.49 107.97 63.08 o -11 2 0 121.43 121.13 56.44 o -10 2 0 24.54 29.85 42.41 o -9 2 0 351.55 394.08 61.84 o -8 2 0 161.97 162.44 42.92 o -7 2 0 981.10 1112.85 74.37 o -6 2 0 321.17 340.58 41.43 o -5 2 0 223.29 177.11 51.33 o -4 2 0 661.54 616.61 53.37 o -3 2 0 8485.65 8137.28 259.21 o -2 2 0 1376.50 1262.57 41.72 o -1 2 0 37.16 38.76 12.46 o 0 2 0 556.69 523.49 25.53 o 1 2 0 727.16 749.85 30.27 o 2 2 0 39159.50 41567.69 1291.19 o 3 2 0 3123.54 3108.07 125.97 o 4 2 0 460.11 453.01 41.18 o 5 2 0 489.42 486.92 48.45 o 6 2 0 1146.39 1087.70 75.10 o 7 2 0 6377.14 5668.65 234.98 o 8 2 0 144.79 84.79 36.34 o 9 2 0 638.80 789.74 84.79 o 10 2 0 1191.62 1182.18 109.01 o 11 2 0 8.86 14.54 46.03 o 12 2 0 382.33 499.04 89.63 o 13 2 0 44.50 43.61 60.56 o -11 3 0 58.56 124.16 88.42 o -10 3 0 455.76 559.17 79.94 o -9 3 0 41.05 2.91 38.51 o -8 3 0 525.45 401.08 57.81 o -7 3 0 613.01 877.70 76.31 o -6 3 0 156.01 166.78 82.71 o -5 3 0 6212.70 6541.57 171.68 o -4 3 0 1553.48 1669.69 64.48 o -3 3 0 228.79 270.83 25.39 o -2 3 0 15536.44 14290.40 304.67 o -1 3 0 580.35 606.90 34.47 o 0 3 0 21372.86 22510.95 601.99 o 1 3 0 8016.95 7638.85 196.04 o 2 3 0 497.42 472.70 27.25 o 3 3 0 350.03 377.91 38.76 o 4 3 0 951.87 872.10 60.56 o 5 3 0 9516.16 8725.85 314.93 o 6 3 0 953.79 998.07 75.10 o 7 3 0 886.81 915.71 77.52 o 8 3 0 4649.85 3883.27 186.53 o 9 3 0 55.89 128.39 46.03 o 10 3 0 396.82 515.99 75.10 o 11 3 0 87.88 82.37 53.30 o 12 3 0 7.27 38.76 48.45 o 13 3 0 343.25 411.83 94.48 o 14 3 0 163.92 123.55 75.10 o -11 4 0 27.41 26.65 87.21 o -10 4 0 15.01 68.97 69.04 o -9 4 0 207.90 310.96 102.96 o -8 4 0 24.50 51.62 48.45 o -7 4 0 0.34 0.35 35.49 o -6 4 0 382.94 364.72 81.15 o -5 4 0 2331.48 2627.93 134.45 o -4 4 0 3750.79 3591.12 107.91 o -3 4 0 690.38 676.22 65.01 o -2 4 0 496.07 620.92 43.28 o -1 4 0 2897.20 2447.59 110.22 o 0 4 0 7285.18 6744.41 183.93 o 1 4 0 658.87 576.93 53.30 o 2 4 0 107.52 110.98 19.71 o 3 4 0 990.23 1020.17 87.21 o 4 4 0 15929.08 15632.40 520.84 o 5 4 0 94.23 48.45 29.07 o 6 4 0 59.43 58.14 29.07 o 7 4 0 98.81 234.98 46.03 o 8 4 0 14.17 14.54 29.07 o 9 4 0 57.86 14.54 41.18 o 10 4 0 403.25 363.38 72.68 o 11 4 0 267.95 307.66 72.68 o 12 4 0 203.74 118.70 58.14 o 13 4 0 4.89 -16.96 55.72 o 14 4 0 13.38 14.54 67.83 o -10 5 0 25.64 58.14 99.32 o -9 5 0 247.61 333.15 69.70 o -8 5 0 128.74 169.10 55.29 o -7 5 0 24.96 -6.44 33.61 o -6 5 0 222.77 308.68 50.99 o -5 5 0 159.05 202.18 72.68 o -4 5 0 1390.02 1600.11 85.06 o -3 5 0 1066.10 1186.95 53.83 o 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2153.23 2146.34 135.66 o 9 6 0 603.80 671.03 87.21 o 10 6 0 59.46 -26.65 36.34 o 11 6 0 421.29 532.95 87.21 o 12 6 0 30.52 9.69 58.14 o 13 6 0 125.88 60.56 62.99 o 14 6 0 78.88 -19.38 67.83 o -8 7 0 0.07 -24.23 82.37 o -7 7 0 157.54 142.93 101.75 o -6 7 0 84.47 -26.65 67.83 o -5 7 0 918.53 1130.84 85.46 o -4 7 0 189.17 204.16 32.47 o -3 7 0 408.51 335.40 46.96 o -2 7 0 1236.70 1201.90 71.53 o -1 7 0 164.48 103.26 28.97 o 0 7 0 770.44 812.53 117.49 o 1 7 0 381.56 404.18 44.82 o 2 7 0 2882.70 2958.82 111.49 o 3 7 0 4884.27 5080.94 161.81 o 4 7 0 1764.48 1997.29 86.72 o 5 7 0 405.45 446.87 44.79 o 6 7 0 264.38 252.74 42.39 o 7 7 0 2508.69 2614.76 106.80 o 8 7 0 307.14 339.15 62.99 o 9 7 0 3.57 9.69 41.18 o 10 7 0 28.23 29.07 46.03 o 11 7 0 17.36 -19.38 38.76 o 12 7 0 141.18 174.42 65.41 o 13 7 0 25.23 24.23 60.56 o 14 7 0 31.99 33.92 65.41 o -8 8 0 39.09 138.08 109.01 o -7 8 0 0.30 4.85 87.21 o -6 8 0 288.32 411.83 121.13 o -5 8 0 32.18 16.96 79.94 o -4 8 0 180.86 273.74 101.75 o -3 8 0 18.93 37.55 36.11 o -2 8 0 121.51 148.40 94.48 o -1 8 0 250.19 192.44 41.18 o 0 8 0 502.55 587.11 53.55 o 1 8 0 969.06 840.98 58.27 o 2 8 0 1435.40 1635.66 83.35 o 3 8 0 1687.64 1761.25 88.42 o 4 8 0 235.24 251.14 37.64 o 5 8 0 6341.69 7196.48 219.22 o 6 8 0 2.68 -13.70 30.28 o 7 8 0 289.79 251.18 40.01 o 8 8 0 1027.19 1254.60 141.72 o 9 8 0 305.92 311.40 48.26 o 10 8 0 2002.48 1935.58 140.51 o 11 8 0 107.77 210.76 67.83 o 12 8 0 30.69 65.41 60.56 o 13 8 0 665.10 644.39 109.01 o 14 8 0 76.82 65.41 67.83 o -7 9 0 12.29 -26.65 96.90 o -6 9 0 8.12 89.63 111.44 o -5 9 0 20.57 -41.18 87.21 o -4 9 0 63.94 104.17 101.75 o -3 9 0 0.09 -70.25 70.25 o -2 9 0 743.87 222.87 84.79 o -1 9 0 1238.39 1173.31 98.11 o 0 9 0 31.94 63.65 55.72 o 1 9 0 757.71 847.62 65.29 o 2 9 0 20.81 62.48 30.44 o 3 9 0 9.87 16.88 26.18 o 4 9 0 2478.74 2396.21 106.94 o 5 9 0 2169.33 2283.10 162.31 o 6 9 0 1407.15 1628.53 88.46 o 7 9 0 10.57 13.12 30.28 o 8 9 0 38.92 -9.05 28.52 o 9 9 0 47.00 -10.94 26.40 o 10 9 0 1196.65 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