#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181260 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233802.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233802_Fobs loop_ _publ_author_name 'Yin, Weiyan' 'Wang, Zhi' 'Yang, Zi-Wen' _publ_section_title ; 5-({[(E)-Benzylideneamino]oxy}methyl)-1,3,4-thiadiazol-2-amine ; _journal_coeditor_code FY2038 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o769 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.753 _cell_angle_gamma 90.000 _cell_length_a 14.5036 _cell_length_b 9.2724 _cell_length_c 8.3612 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.8413 _cod_data_source_file fy2038Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' T in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 435.56 220.86 9.84 o 2 0 0 315.74 318.01 9.08 o 3 0 0 336.18 298.72 8.69 o 4 0 0 4635.33 4653.18 130.16 o 5 0 0 2996.53 3008.33 132.72 o 6 0 0 20.56 10.35 0.58 o 7 0 0 252.56 241.45 6.90 o 8 0 0 269.63 230.01 6.65 o 9 0 0 187.18 176.99 5.80 o 10 0 0 760.40 743.41 20.80 o 11 0 0 910.74 918.96 25.74 o 12 0 0 40.33 40.59 1.58 o 13 0 0 100.96 84.43 3.83 o 14 0 0 372.28 358.17 13.54 o 15 0 0 709.85 688.76 25.42 o 16 0 0 71.58 63.10 3.19 o 1 1 0 0.41 1.28 0.64 o 2 1 0 1551.77 1495.09 31.06 o 3 1 0 6338.68 6006.52 119.69 o 4 1 0 3117.36 2978.30 58.64 o 5 1 0 787.61 842.14 26.33 o 6 1 0 252.21 284.59 5.72 o 7 1 0 783.58 768.58 15.16 o 8 1 0 164.59 138.03 2.82 o 9 1 0 13.85 13.14 0.93 o 10 1 0 113.54 108.71 2.39 o 11 1 0 31.11 28.49 0.90 o 12 1 0 1247.98 1162.53 24.70 o 13 1 0 282.34 287.09 7.77 o 14 1 0 3.18 1.34 0.54 o 15 1 0 20.09 20.77 1.28 o 16 1 0 4.57 2.50 0.63 o 0 2 0 896.88 777.91 55.25 o 1 2 0 57.87 52.89 3.40 o 2 2 0 212.36 206.42 4.65 o 3 2 0 1888.76 1945.37 38.51 o 4 2 0 2908.72 2925.77 91.41 o 5 2 0 2239.45 2278.23 54.22 o 6 2 0 922.57 916.35 18.05 o 7 2 0 270.74 247.91 5.02 o 8 2 0 1300.02 1313.68 25.83 o 9 2 0 256.96 266.32 5.41 o 10 2 0 27.58 36.16 0.99 o 11 2 0 2.54 3.74 1.36 o 12 2 0 706.95 686.71 15.24 o 13 2 0 226.31 214.75 4.97 o 14 2 0 138.51 153.36 4.47 o 15 2 0 7.22 3.84 0.72 o 16 2 0 6.64 7.65 0.85 o 1 3 0 2096.34 1750.53 217.15 o 2 3 0 1902.42 1730.58 76.77 o 3 3 0 23.92 5.24 1.41 o 4 3 0 7.49 9.46 0.42 o 6 3 0 1405.23 1390.91 28.08 o 7 3 0 52.93 68.75 1.57 o 8 3 0 73.57 65.81 1.53 o 9 3 0 300.89 283.28 6.70 o 10 3 0 0.30 2.18 0.82 o 11 3 0 144.97 147.41 3.60 o 12 3 0 577.12 566.93 16.55 o 13 3 0 428.43 415.20 9.50 o 14 3 0 125.38 129.15 3.88 o 15 3 0 2.67 2.31 1.28 o 0 4 0 2856.65 2803.31 124.42 o 1 4 0 5.18 3.44 0.26 o 2 4 0 34.75 43.00 6.45 o 3 4 0 237.72 254.38 7.30 o 4 4 0 69.66 60.02 2.07 o 5 4 0 143.62 166.60 3.48 o 6 4 0 23.35 28.75 0.84 o 7 4 0 29.19 25.48 0.81 o 8 4 0 29.02 33.86 0.97 o 9 4 0 138.83 135.21 4.31 o 10 4 0 60.31 50.55 2.40 o 11 4 0 981.66 958.74 22.64 o 12 4 0 262.35 238.87 6.71 o 13 4 0 24.17 18.96 0.97 o 14 4 0 315.47 286.33 6.76 o 15 4 0 254.84 260.01 7.23 o 1 5 0 175.77 154.41 3.83 o 2 5 0 818.68 895.20 21.09 o 3 5 0 339.86 411.18 23.80 o 4 5 0 310.68 330.99 18.60 o 5 5 0 24.04 18.05 0.76 o 6 5 0 122.77 123.53 3.02 o 7 5 0 67.85 50.71 1.36 o 8 5 0 9.01 11.10 0.61 o 9 5 0 275.40 265.79 5.32 o 10 5 0 1.45 0.88 0.50 o 11 5 0 1.91 3.66 6.96 o 12 5 0 81.93 69.93 2.02 o 13 5 0 60.22 57.14 2.12 o 14 5 0 64.31 64.78 3.07 o 0 6 0 466.57 522.19 23.38 o 1 6 0 770.25 721.18 18.21 o 2 6 0 52.64 58.35 1.96 o 3 6 0 1652.35 1736.19 45.47 o 4 6 0 247.68 227.73 11.38 o 5 6 0 498.56 510.25 16.74 o 6 6 0 704.09 721.61 27.62 o 7 6 0 775.76 740.18 14.27 o 8 6 0 422.49 419.76 8.36 o 9 6 0 1.59 2.86 0.59 o 10 6 0 40.15 44.53 1.48 o 11 6 0 516.38 490.95 18.81 o 12 6 0 358.13 360.86 12.08 o 13 6 0 145.66 135.18 3.52 o 1 7 0 420.38 401.20 11.63 o 2 7 0 1276.19 1277.78 43.75 o 3 7 0 33.60 39.36 1.65 o 4 7 0 59.52 53.49 1.96 o 5 7 0 269.10 280.75 5.72 o 6 7 0 424.67 424.90 8.67 o 7 7 0 271.48 276.17 7.83 o 8 7 0 23.59 19.35 0.87 o 9 7 0 283.30 286.02 6.72 o 10 7 0 2.28 1.72 0.57 o 11 7 0 4.37 4.39 1.31 o 12 7 0 10.53 11.82 1.27 o 0 8 0 280.37 262.75 12.26 o 1 8 0 714.01 693.01 20.94 o 2 8 0 247.28 246.19 7.51 o 3 8 0 133.63 114.94 3.02 o 4 8 0 9.17 8.87 0.67 o 5 8 0 2.83 2.73 0.65 o 6 8 0 36.27 43.00 1.95 o 7 8 0 565.79 556.11 11.32 o 8 8 0 5.78 4.11 0.76 o 9 8 0 78.13 71.04 2.11 o 10 8 0 9.55 8.44 0.77 o 11 8 0 90.69 94.19 2.67 o 1 9 0 380.14 363.22 22.31 o 2 9 0 389.38 389.02 12.69 o 3 9 0 869.92 862.23 20.62 o 4 9 0 67.14 68.21 3.12 o 5 9 0 280.73 310.83 7.78 o 6 9 0 144.63 152.70 3.45 o 7 9 0 203.58 199.22 4.93 o 8 9 0 173.83 180.07 4.54 o 9 9 0 97.77 102.97 2.89 o 0 10 0 193.21 177.81 8.81 o 1 10 0 146.05 137.11 5.01 o 2 10 0 49.34 45.01 3.56 o 3 10 0 139.45 78.17 3.61 o 4 10 0 1.21 1.44 0.60 o 5 10 0 8.16 5.75 0.69 o 6 10 0 4.30 3.16 0.57 o 1 11 0 74.86 86.30 3.96 o -16 1 1 150.05 167.83 4.92 o -15 1 1 803.87 803.59 20.86 o -14 1 1 77.41 81.95 2.62 o -13 1 1 66.79 53.86 1.90 o -12 1 1 185.67 179.42 4.29 o -9 1 1 3.32 5.36 0.64 o -8 1 1 539.24 539.18 16.85 o -7 1 1 131.95 124.85 4.02 o -6 1 1 164.31 171.17 4.17 o -5 1 1 1070.50 978.04 86.67 o -4 1 1 970.23 864.59 22.84 o -3 1 1 566.04 513.59 11.27 o -2 1 1 5289.16 4982.46 100.86 o -1 1 1 1734.90 1723.42 40.78 o 0 1 1 3987.82 3667.29 83.11 o 1 1 1 10.75 7.54 0.78 o 2 1 1 9578.10 8980.84 180.20 o 3 1 1 8393.16 8004.07 161.29 o 4 1 1 2924.37 2980.86 58.68 o 5 1 1 156.34 162.55 15.82 o 6 1 1 19.50 31.16 0.94 o 7 1 1 3907.49 3878.59 76.71 o 8 1 1 690.48 650.26 20.03 o 9 1 1 20.51 15.07 0.66 o 10 1 1 359.21 349.40 7.09 o 11 1 1 111.10 114.36 2.53 o 12 1 1 5.31 3.45 0.41 o 13 1 1 1.27 0.00 0.44 o 14 1 1 481.40 433.40 11.52 o 15 1 1 392.25 411.76 11.02 o -16 2 1 19.43 19.39 1.31 o -15 2 1 0.21 0.29 0.58 o -14 2 1 126.37 116.80 3.57 o -13 2 1 1146.73 1104.31 28.36 o -12 2 1 429.97 424.21 9.65 o -11 2 1 6.04 0.27 0.30 o -9 2 1 424.02 438.74 22.45 o -8 2 1 19.13 12.61 0.58 o -7 2 1 52.35 47.60 1.49 o -6 2 1 60.67 32.04 1.01 o -5 2 1 2199.08 2162.22 77.75 o -4 2 1 155.71 166.85 3.26 o -3 2 1 1987.97 1904.21 37.49 o -2 2 1 619.68 610.12 14.83 o -1 2 1 6090.73 5823.53 191.48 o 0 2 1 8775.85 7910.58 290.63 o 1 2 1 2394.72 2492.01 58.77 o 2 2 1 4943.04 4745.87 137.89 o 3 2 1 605.25 664.55 13.12 o 4 2 1 365.73 306.12 9.71 o 5 2 1 1539.37 1338.00 26.43 o 6 2 1 4687.14 4740.58 93.30 o 7 2 1 513.78 522.21 10.15 o 8 2 1 85.55 87.39 2.68 o 9 2 1 3.36 3.65 0.40 o 10 2 1 56.32 47.19 1.23 o 11 2 1 157.26 153.54 3.30 o 12 2 1 622.45 549.39 12.11 o 13 2 1 0.17 1.22 0.46 o 14 2 1 29.35 28.24 1.45 o 15 2 1 146.69 147.73 4.38 o -16 3 1 115.72 107.30 3.43 o -15 3 1 176.95 175.13 5.06 o -14 3 1 1.72 2.14 0.64 o -13 3 1 327.83 306.75 7.17 o -12 3 1 581.84 597.01 15.78 o -11 3 1 4.06 3.17 0.53 o -9 3 1 1.52 1.32 0.36 o -8 3 1 64.14 110.74 7.54 o -7 3 1 13.66 12.12 0.52 o -5 3 1 213.56 216.84 6.40 o -4 3 1 363.50 353.34 7.89 o -3 3 1 2.21 3.25 0.51 o -2 3 1 1981.35 1914.26 65.34 o -1 3 1 1883.08 1973.83 43.69 o 0 3 1 7528.31 7253.34 147.66 o 1 3 1 4569.04 4704.52 131.21 o 3 3 1 40.19 21.32 1.29 o 4 3 1 29.56 53.82 1.26 o 5 3 1 35.77 42.40 1.05 o 6 3 1 1732.59 1816.29 36.10 o 7 3 1 70.12 82.65 1.86 o 8 3 1 445.67 428.98 8.45 o 9 3 1 9.74 8.68 0.77 o 10 3 1 796.78 787.58 15.50 o 11 3 1 544.08 498.93 10.79 o 12 3 1 101.24 100.14 2.65 o 13 3 1 17.73 15.26 0.88 o 14 3 1 13.83 12.53 1.16 o 15 3 1 15.20 13.46 2.09 o -15 4 1 238.74 223.66 6.32 o -14 4 1 151.05 150.53 4.43 o -13 4 1 67.31 58.25 1.78 o -12 4 1 18.32 18.98 0.98 o -11 4 1 103.38 110.76 4.30 o -10 4 1 329.46 314.93 13.26 o -8 4 1 739.05 769.55 21.77 o -6 4 1 20.01 18.07 1.14 o -5 4 1 1572.53 1668.56 39.48 o -4 4 1 122.27 132.79 4.85 o -3 4 1 337.54 380.97 10.37 o -2 4 1 1936.40 1893.49 59.27 o -1 4 1 1481.76 1426.92 28.21 o 0 4 1 34.04 19.93 0.63 o 1 4 1 925.43 857.59 20.26 o 2 4 1 730.59 724.72 17.16 o 3 4 1 382.91 436.84 13.94 o 4 4 1 1.37 3.56 0.28 o 5 4 1 326.69 377.01 7.63 o 6 4 1 52.68 41.46 1.07 o 7 4 1 160.35 152.58 3.26 o 8 4 1 21.26 20.38 0.75 o 9 4 1 1030.38 1023.88 20.20 o 10 4 1 106.09 116.60 2.62 o 11 4 1 28.39 30.77 1.19 o 12 4 1 66.65 51.42 2.80 o 13 4 1 415.97 391.36 12.29 o 14 4 1 670.68 667.18 15.07 o -15 5 1 11.53 11.67 1.04 o -14 5 1 138.64 144.07 3.73 o -13 5 1 93.07 96.66 3.07 o -12 5 1 887.09 897.96 20.17 o -11 5 1 1436.11 1416.49 41.50 o -10 5 1 200.85 207.01 4.95 o -9 5 1 335.58 307.47 13.40 o -6 5 1 1873.27 2000.87 63.85 o -5 5 1 83.04 62.93 1.78 o -4 5 1 928.05 835.45 34.39 o -3 5 1 31.20 40.74 1.24 o -1 5 1 164.98 156.69 4.34 o 0 5 1 779.92 827.15 21.00 o 1 5 1 142.54 141.37 3.59 o 2 5 1 1366.58 1438.90 34.10 o 3 5 1 1572.41 1607.79 37.17 o 4 5 1 1629.46 1581.58 42.51 o 5 5 1 150.78 150.27 3.13 o 6 5 1 233.97 223.61 4.67 o 7 5 1 22.27 17.73 0.72 o 8 5 1 392.05 377.22 7.60 o 9 5 1 20.70 21.61 0.85 o 10 5 1 473.05 487.32 11.06 o 11 5 1 86.71 84.39 2.33 o 12 5 1 207.00 220.41 7.04 o 13 5 1 104.05 106.99 2.90 o 14 5 1 100.50 117.66 3.17 o -14 6 1 32.42 28.70 1.26 o -13 6 1 28.16 27.89 1.23 o -12 6 1 110.07 109.94 4.28 o -11 6 1 3.95 3.70 0.55 o -10 6 1 2.37 2.84 0.48 o -9 6 1 222.65 209.36 4.86 o -8 6 1 131.00 116.36 2.57 o -7 6 1 5.18 2.87 0.46 o -6 6 1 35.19 20.69 1.41 o -5 6 1 42.66 20.85 2.88 o -4 6 1 0.37 0.03 0.29 o -3 6 1 1.25 9.54 1.91 o -2 6 1 196.17 185.80 4.26 o -1 6 1 332.40 361.42 7.32 o 0 6 1 404.87 421.49 12.84 o 1 6 1 1205.51 1266.15 35.78 o 2 6 1 162.16 179.31 4.38 o 3 6 1 733.53 696.37 15.84 o 4 6 1 29.48 34.32 2.00 o 5 6 1 1.65 3.62 0.43 o 6 6 1 281.17 299.75 6.17 o 7 6 1 316.90 309.89 6.39 o 8 6 1 0.03 0.00 0.35 o 9 6 1 61.59 64.63 1.68 o 10 6 1 48.09 45.21 1.51 o 11 6 1 113.28 103.57 2.80 o 12 6 1 207.28 195.03 6.21 o 13 6 1 3.49 2.15 1.05 o -13 7 1 24.02 22.49 1.14 o -12 7 1 513.63 519.60 11.93 o -11 7 1 23.72 21.00 1.01 o -10 7 1 240.83 234.87 5.66 o -9 7 1 43.70 44.45 1.49 o -8 7 1 371.38 364.22 10.25 o -7 7 1 308.76 304.52 6.31 o -6 7 1 99.50 104.37 2.43 o -5 7 1 160.78 133.04 3.51 o -4 7 1 1014.51 1031.51 40.52 o -3 7 1 755.60 779.23 41.66 o -2 7 1 3.42 0.31 0.88 o -1 7 1 541.76 497.07 32.21 o 0 7 1 252.36 211.10 13.35 o 1 7 1 352.17 390.48 20.28 o 2 7 1 59.38 46.17 1.50 o 3 7 1 666.15 669.56 16.01 o 4 7 1 66.41 53.66 1.67 o 5 7 1 2.76 1.85 0.62 o 6 7 1 162.55 158.48 3.89 o 7 7 1 6.64 8.61 0.65 o 8 7 1 374.36 393.90 8.10 o 9 7 1 9.13 8.30 0.70 o 10 7 1 135.91 142.73 4.20 o 11 7 1 13.39 16.22 2.17 o 12 7 1 51.96 55.64 2.12 o -11 8 1 4.59 4.40 0.66 o -10 8 1 258.07 273.78 6.56 o -9 8 1 234.16 232.44 5.63 o -8 8 1 142.26 148.27 3.76 o -7 8 1 119.27 117.01 2.66 o -6 8 1 169.52 179.73 4.73 o -5 8 1 66.01 61.95 1.95 o -4 8 1 42.32 40.63 1.41 o -3 8 1 76.29 65.31 3.82 o -2 8 1 132.22 134.66 3.74 o -1 8 1 268.72 281.34 14.81 o 0 8 1 607.06 591.84 18.95 o 1 8 1 425.08 388.75 15.14 o 2 8 1 321.71 310.11 7.71 o 3 8 1 240.81 246.67 6.22 o 4 8 1 549.42 500.56 11.47 o 5 8 1 369.69 352.75 7.30 o 6 8 1 450.84 429.87 8.85 o 7 8 1 0.34 0.00 0.41 o 8 8 1 35.22 38.67 1.64 o 9 8 1 1042.14 1051.86 23.60 o 10 8 1 9.43 14.24 0.91 o -9 9 1 173.05 171.08 4.34 o -8 9 1 0.80 3.67 1.05 o -7 9 1 2.32 4.05 0.94 o -6 9 1 185.29 198.34 4.33 o -5 9 1 0.03 0.41 0.48 o -4 9 1 311.75 283.08 7.08 o -3 9 1 6.21 7.81 0.69 o -2 9 1 1.61 2.78 0.74 o 0 9 1 88.58 71.68 2.65 o 1 9 1 1.66 1.31 0.67 o 2 9 1 33.44 39.45 3.46 o 3 9 1 13.91 10.59 1.29 o 4 9 1 15.94 15.90 1.12 o 5 9 1 100.58 82.04 2.06 o 6 9 1 26.72 28.66 1.45 o 7 9 1 14.70 13.86 1.46 o 8 9 1 36.51 40.77 1.48 o -7 10 1 3.66 2.87 0.72 o -6 10 1 142.70 148.66 3.85 o -5 10 1 55.06 58.24 1.99 o -4 10 1 4.55 5.16 0.98 o -3 10 1 683.30 726.27 23.21 o -2 10 1 1.70 1.25 1.28 o -1 10 1 133.43 123.08 4.04 o 0 10 1 25.76 27.59 1.78 o 1 10 1 14.16 13.03 2.68 o 2 10 1 158.06 98.87 12.13 o 3 10 1 112.92 107.94 4.15 o 4 10 1 170.59 182.82 4.87 o 5 10 1 454.09 487.37 10.05 o 6 10 1 27.70 32.97 1.30 o -17 0 2 28.16 40.88 2.55 o -16 0 2 267.08 228.01 9.07 o -15 0 2 418.91 397.90 15.07 o -14 0 2 134.41 118.67 5.11 o -13 0 2 1173.46 1216.05 44.07 o -12 0 2 20.35 19.03 1.66 o -11 0 2 1377.37 1483.15 53.52 o -10 0 2 1870.65 1990.14 55.56 o -9 0 2 260.87 237.47 6.84 o -8 0 2 3729.46 3799.53 106.60 o -7 0 2 5659.96 5934.02 166.25 o -6 0 2 73.88 63.66 1.98 o -5 0 2 1091.26 1114.19 31.29 o -4 0 2 54.42 46.76 1.56 o -3 0 2 0.54 3.78 0.27 o -2 0 2 133.18 177.34 4.97 o -1 0 2 13752.57 12354.57 569.90 o 1 0 2 6198.29 5693.99 207.44 o 2 0 2 1945.06 1937.69 55.09 o 3 0 2 1153.90 1031.47 29.99 o 4 0 2 1201.23 1175.17 33.66 o 6 0 2 564.56 596.00 16.72 o 7 0 2 1070.99 1097.62 30.59 o 8 0 2 850.30 925.15 30.25 o 9 0 2 744.85 697.85 35.05 o 10 0 2 164.52 174.03 5.21 o 11 0 2 111.50 119.14 7.66 o 12 0 2 186.51 166.95 5.09 o 13 0 2 94.90 82.74 2.87 o 14 0 2 126.27 131.82 5.62 o 15 0 2 54.90 72.94 3.58 o -17 1 2 1.79 3.16 0.72 o -16 1 2 2.29 2.17 0.72 o -15 1 2 152.83 144.84 4.29 o -14 1 2 17.89 15.05 3.51 o -13 1 2 1394.46 1367.17 34.96 o -12 1 2 510.28 512.86 13.37 o -11 1 2 79.94 90.43 4.37 o -10 1 2 899.17 913.03 20.18 o -9 1 2 553.52 520.53 11.61 o -8 1 2 107.26 113.84 2.60 o -7 1 2 112.79 132.76 3.10 o -6 1 2 33.05 58.62 1.46 o -5 1 2 317.58 301.62 6.72 o -4 1 2 1237.80 1264.83 25.02 o -3 1 2 31.99 25.92 0.73 o -2 1 2 18.35 22.74 0.57 o -1 1 2 6113.03 5782.20 139.68 o 0 1 2 2288.92 2237.86 53.25 o 1 1 2 3022.10 2934.13 64.32 o 2 1 2 4557.57 4452.98 99.49 o 3 1 2 1395.82 1336.29 26.35 o 4 1 2 99.46 104.41 2.18 o 5 1 2 2826.72 2637.08 164.10 o 6 1 2 90.53 88.43 1.86 o 7 1 2 3.17 3.22 0.62 o 8 1 2 1.05 1.09 0.44 o 9 1 2 131.65 136.40 2.84 o 10 1 2 128.80 133.56 3.24 o 11 1 2 52.79 52.92 1.37 o 12 1 2 269.12 244.73 5.01 o 13 1 2 0.48 1.35 0.47 o 14 1 2 2.41 2.19 0.64 o 15 1 2 0.62 0.00 0.63 o -16 2 2 55.41 55.19 2.08 o -15 2 2 232.33 243.35 6.77 o -14 2 2 687.11 678.62 17.70 o -13 2 2 47.63 46.59 2.75 o -12 2 2 276.48 279.45 6.24 o -11 2 2 133.61 124.93 2.98 o -10 2 2 0.11 0.64 0.51 o -9 2 2 214.69 234.14 5.37 o -8 2 2 107.31 120.01 3.34 o -7 2 2 1.88 11.63 1.79 o -6 2 2 4.28 2.18 0.41 o -5 2 2 161.45 158.69 3.22 o -4 2 2 1724.96 1775.52 35.10 o -3 2 2 65.01 69.58 1.46 o -2 2 2 4424.62 4587.21 107.88 o -1 2 2 142.86 151.24 3.68 o 0 2 2 738.79 808.91 22.58 o 1 2 2 44.15 35.00 1.92 o 2 2 2 404.88 400.49 8.85 o 4 2 2 38.44 36.49 2.79 o 5 2 2 1076.84 1114.69 21.93 o 6 2 2 1759.52 1756.81 33.91 o 7 2 2 10.07 5.98 0.40 o 8 2 2 1.76 2.89 0.35 o 9 2 2 61.76 59.40 1.70 o 10 2 2 54.22 56.32 1.42 o 11 2 2 213.76 190.32 5.58 o 12 2 2 19.49 10.86 1.11 o 13 2 2 183.78 182.72 4.47 o 14 2 2 9.46 15.37 0.91 o -16 3 2 118.54 124.91 3.84 o -15 3 2 3.19 3.56 0.67 o -14 3 2 16.48 14.41 1.04 o -13 3 2 386.43 363.70 9.71 o -12 3 2 100.67 95.71 2.51 o -11 3 2 72.10 77.31 2.08 o -10 3 2 340.44 324.93 7.44 o -9 3 2 979.53 978.06 21.65 o -8 3 2 335.76 373.85 8.04 o -7 3 2 2294.16 2370.02 52.58 o -6 3 2 956.75 924.32 18.16 o -5 3 2 3077.17 3105.31 61.15 o -4 3 2 521.15 544.17 15.48 o -3 3 2 182.86 164.06 4.00 o -2 3 2 6365.45 6160.98 180.48 o -1 3 2 412.73 431.10 11.75 o 0 3 2 11.09 16.71 1.17 o 1 3 2 1113.80 1091.78 25.82 o 2 3 2 336.15 304.84 9.75 o 3 3 2 23.08 29.09 1.02 o 4 3 2 103.91 104.76 2.26 o 5 3 2 2322.69 2374.73 47.10 o 6 3 2 1497.56 1549.03 29.92 o 7 3 2 32.29 44.07 1.85 o 8 3 2 124.01 123.01 2.64 o 9 3 2 1229.33 1246.35 24.16 o 10 3 2 945.76 976.42 19.37 o 11 3 2 56.24 50.32 1.36 o 12 3 2 239.52 227.18 5.24 o 13 3 2 159.18 175.57 4.33 o 14 3 2 106.28 102.79 4.10 o -16 4 2 22.79 25.89 1.45 o -15 4 2 139.49 141.68 4.25 o -14 4 2 61.95 68.71 2.39 o -13 4 2 10.35 14.04 0.88 o -12 4 2 14.33 12.73 0.85 o -11 4 2 262.63 261.24 6.09 o -10 4 2 95.00 98.93 2.56 o -9 4 2 54.21 48.19 2.11 o -8 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