#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181260 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233805.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233805_Fobs loop_ _publ_author_name 'Schutte, M.' 'Visser, H. G.' 'Roodt, A.' _publ_section_title ; 2-(Ammoniomethyl)pyridinium sulfate monohydrate ; _journal_coeditor_code FY2043 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o914 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.392 _cell_angle_beta 82.874 _cell_angle_gamma 85.193 _cell_length_a 5.2804 _cell_length_b 6.9458 _cell_length_c 12.4262 _exptl_crystal_F_000 236.00 _reflns_d_resolution_high 0.7831 _cod_data_source_file fy2043Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 10Amsc5_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 428.55 444.35 12.14 o 4 0 0 141.10 133.72 4.80 o -6 1 0 78.03 81.44 1.69 o -5 1 0 492.43 474.53 6.27 o -4 1 0 1378.49 1357.85 12.57 o -3 1 0 3.25 2.92 0.23 o -2 1 0 415.52 402.16 3.49 o -1 1 0 690.75 711.73 4.57 o 1 1 0 2245.98 2081.51 12.45 o 2 1 0 142.46 154.77 1.68 o 3 1 0 128.76 123.56 1.39 o 4 1 0 79.08 86.16 1.02 o -6 2 0 171.87 175.53 3.43 o -5 2 0 351.08 340.44 4.78 o -4 2 0 39.56 40.48 0.64 o -3 2 0 1224.86 1249.76 10.03 o -2 2 0 426.38 460.55 3.23 o -1 2 0 410.92 352.16 2.30 o 0 2 0 6532.66 5451.04 100.81 o 1 2 0 11376.98 8859.85 178.15 o 2 2 0 294.16 249.26 1.81 o 3 2 0 240.59 242.64 2.10 o 4 2 0 704.62 691.09 6.04 o 5 2 0 30.33 33.16 0.68 o 6 2 0 381.12 362.23 8.71 o -6 3 0 34.26 34.33 1.21 o -5 3 0 6.17 7.23 0.41 o -4 3 0 2089.86 2022.08 20.72 o -3 3 0 315.17 306.59 2.30 o -2 3 0 342.11 373.84 2.75 o -1 3 0 224.53 248.26 1.82 o 0 3 0 44.99 36.26 0.44 o 1 3 0 45.24 51.94 0.54 o 2 3 0 1035.97 1085.55 7.47 o 3 3 0 344.17 340.66 2.77 o 4 3 0 97.25 98.55 1.41 o 5 3 0 328.76 327.22 4.06 o 6 3 0 1.34 0.80 0.24 o -5 4 0 1.95 1.77 0.48 o -4 4 0 197.53 195.24 2.57 o -3 4 0 124.22 130.29 1.50 o -2 4 0 166.46 160.82 1.75 o -1 4 0 685.00 709.57 6.33 o 0 4 0 21.47 17.43 0.44 o 1 4 0 2694.29 2690.10 21.39 o 2 4 0 479.40 546.95 4.69 o 3 4 0 708.36 704.23 5.58 o 4 4 0 127.49 126.59 1.83 o 5 4 0 69.89 68.18 1.28 o 6 4 0 264.66 264.47 5.12 o -5 5 0 58.52 60.97 1.92 o -4 5 0 228.18 227.82 3.73 o -3 5 0 774.77 766.20 7.48 o -2 5 0 2.35 1.99 0.32 o -1 5 0 341.36 343.14 3.66 o 0 5 0 606.12 578.42 6.31 o 1 5 0 0.22 0.39 0.15 o 2 5 0 394.95 409.08 3.70 o 3 5 0 8.62 10.23 0.36 o 4 5 0 58.70 61.17 1.11 o 5 5 0 0.03 0.16 0.22 o -4 6 0 16.22 13.31 1.04 o -3 6 0 41.09 38.81 1.22 o -2 6 0 281.53 277.89 3.93 o -1 6 0 11.40 10.69 0.60 o 0 6 0 650.62 653.09 8.03 o 1 6 0 385.63 380.16 5.62 o 2 6 0 106.46 113.05 1.61 o 3 6 0 38.86 39.54 0.95 o 4 6 0 59.71 63.39 1.49 o 5 6 0 78.71 81.30 2.00 o -3 7 0 353.34 350.27 6.99 o -2 7 0 41.37 38.05 1.12 o -1 7 0 169.66 163.38 2.76 o 0 7 0 10.46 10.25 0.64 o 1 7 0 102.60 99.97 2.01 o 2 7 0 133.81 130.28 2.05 o 3 7 0 119.90 116.27 2.60 o 4 7 0 1.52 0.46 0.34 o -2 8 0 96.21 98.83 3.50 o -1 8 0 3.36 2.72 0.42 o 0 8 0 31.22 31.94 1.26 o 1 8 0 77.56 75.09 1.52 o 2 8 0 83.98 89.79 1.71 o 3 8 0 8.53 9.65 0.87 o -2 -8 1 32.04 33.93 1.18 o -1 -8 1 68.59 68.60 1.67 o 0 -8 1 15.56 16.33 0.89 o 1 -8 1 57.51 60.26 1.55 o 2 -8 1 129.21 126.92 2.84 o -4 -7 1 0.89 1.56 0.41 o -3 -7 1 120.80 122.80 3.08 o -2 -7 1 22.85 23.31 0.75 o -1 -7 1 146.73 138.87 2.43 o 0 -7 1 278.30 281.09 4.47 o 1 -7 1 401.62 404.41 5.49 o 2 -7 1 0.48 0.85 0.27 o 3 -7 1 1.07 0.70 0.38 o -5 -6 1 0.46 0.42 0.30 o -4 -6 1 300.93 300.68 4.38 o -3 -6 1 718.28 677.55 7.55 o -2 -6 1 32.71 29.58 0.71 o -1 -6 1 42.26 40.36 1.19 o 0 -6 1 550.97 539.13 6.78 o 1 -6 1 82.78 81.29 1.61 o 2 -6 1 223.80 227.37 3.34 o 3 -6 1 1.32 2.20 0.36 o 4 -6 1 13.81 18.60 1.04 o -5 -5 1 54.30 54.68 1.25 o -4 -5 1 53.89 53.02 1.11 o -3 -5 1 102.13 107.15 1.30 o -2 -5 1 194.76 189.24 2.42 o -1 -5 1 359.40 351.74 3.46 o 0 -5 1 0.33 0.22 0.14 o 1 -5 1 1003.52 981.71 9.40 o 2 -5 1 38.33 33.07 0.71 o 3 -5 1 0.21 0.30 0.15 o 4 -5 1 15.81 13.68 0.79 o 5 -5 1 37.38 40.48 1.24 o -6 -4 1 4.39 4.49 0.52 o -5 -4 1 100.32 101.00 2.89 o -4 -4 1 46.79 47.58 0.90 o -3 -4 1 986.98 1015.89 8.42 o -2 -4 1 195.29 199.30 1.96 o -1 -4 1 35.18 43.56 0.63 o 0 -4 1 99.71 99.49 1.62 o 1 -4 1 151.36 152.36 1.69 o 2 -4 1 186.14 177.00 2.05 o 3 -4 1 157.24 159.29 1.87 o 4 -4 1 0.07 0.07 0.16 o 5 -4 1 6.42 6.62 0.45 o -6 -3 1 18.76 18.69 0.79 o -5 -3 1 49.02 48.28 1.01 o -4 -3 1 624.86 606.73 6.58 o -3 -3 1 30.35 34.44 0.42 o -2 -3 1 686.03 695.87 5.09 o -1 -3 1 348.58 358.08 2.61 o 0 -3 1 5.09 16.75 0.32 o 1 -3 1 60.93 55.81 0.79 o 2 -3 1 212.12 212.24 1.76 o 3 -3 1 476.11 479.81 3.63 o 4 -3 1 12.77 11.89 0.45 o 5 -3 1 109.20 104.28 1.90 o 6 -3 1 52.23 49.53 1.52 o -6 -2 1 20.34 21.59 0.76 o -5 -2 1 60.25 59.16 1.09 o -4 -2 1 29.84 31.55 0.48 o -3 -2 1 479.48 480.13 4.25 o -2 -2 1 63.75 62.82 0.58 o -1 -2 1 336.33 386.14 2.59 o 0 -2 1 44.98 62.30 0.68 o 1 -2 1 15.48 11.27 0.18 o 2 -2 1 82.94 98.16 0.82 o 3 -2 1 828.18 790.76 6.90 o 4 -2 1 6.05 7.07 0.26 o 5 -2 1 81.03 82.69 1.47 o 6 -2 1 60.76 55.63 1.45 o -6 -1 1 10.58 11.92 0.45 o -5 -1 1 6.70 5.94 0.29 o -4 -1 1 147.79 138.92 1.33 o -3 -1 1 235.66 240.32 2.28 o -2 -1 1 151.04 154.22 1.42 o -1 -1 1 1132.11 1120.75 6.90 o 0 -1 1 276.86 301.72 11.42 o 1 -1 1 738.23 749.49 4.52 o 2 -1 1 145.45 140.75 1.33 o 3 -1 1 978.12 1031.78 8.81 o 4 -1 1 368.11 360.00 3.22 o 5 -1 1 32.53 32.86 0.66 o 6 -1 1 4.27 4.91 0.35 o -6 0 1 133.59 131.27 2.39 o -5 0 1 146.26 134.48 2.12 o -4 0 1 0.06 0.19 0.05 o -3 0 1 0.05 1.82 0.33 o -2 0 1 7.03 4.22 0.11 o -1 0 1 288.27 290.75 2.18 o 1 0 1 1038.39 1036.64 18.99 o 2 0 1 507.67 605.87 15.57 o 3 0 1 24.81 24.18 1.47 o 4 0 1 141.21 134.90 4.89 o -6 1 1 56.30 58.55 1.35 o -5 1 1 94.85 90.30 1.45 o -4 1 1 1.13 2.13 0.13 o -3 1 1 301.38 284.76 2.97 o -2 1 1 20.78 21.65 0.27 o -1 1 1 1649.79 1623.15 10.92 o 1 1 1 361.86 339.18 2.15 o 2 1 1 1480.32 1522.16 17.20 o 3 1 1 741.90 806.19 10.96 o 4 1 1 588.02 622.12 16.94 o -6 2 1 21.39 21.37 0.86 o -5 2 1 56.91 60.72 1.20 o -4 2 1 325.18 323.97 3.31 o -3 2 1 33.41 32.51 0.87 o -2 2 1 104.02 81.71 0.77 o -1 2 1 3815.49 3590.62 46.65 o 0 2 1 359.11 326.16 2.43 o 1 2 1 1.78 0.93 0.11 o 2 2 1 1.24 -0.06 0.06 o 3 2 1 181.57 188.74 1.79 o 4 2 1 46.55 43.45 0.60 o 5 2 1 11.93 12.08 0.36 o 6 2 1 197.36 194.91 3.46 o -6 3 1 9.20 8.58 0.68 o -5 3 1 54.70 55.57 1.10 o -4 3 1 549.27 539.30 5.93 o -3 3 1 382.47 385.13 3.14 o -2 3 1 7.49 4.41 0.20 o -1 3 1 366.62 371.50 3.10 o 0 3 1 0.26 -0.13 0.13 o 1 3 1 227.66 284.39 2.02 o 2 3 1 281.44 304.56 2.17 o 3 3 1 596.73 619.12 4.33 o 4 3 1 852.68 863.08 8.23 o 5 3 1 191.82 189.15 2.71 o 6 3 1 99.86 100.63 2.84 o -5 4 1 97.41 96.96 1.72 o -4 4 1 81.59 80.74 1.36 o -3 4 1 41.06 38.81 0.66 o -2 4 1 363.32 360.08 3.46 o -1 4 1 402.64 457.44 3.96 o 0 4 1 1476.40 1504.12 15.27 o 1 4 1 10.55 15.07 0.33 o 2 4 1 79.87 76.85 0.92 o 3 4 1 41.89 41.89 0.54 o 4 4 1 164.55 171.83 2.28 o 5 4 1 78.74 82.03 1.44 o 6 4 1 34.31 30.99 1.27 o -5 5 1 148.78 163.32 3.01 o -4 5 1 263.38 273.31 3.84 o -3 5 1 40.10 35.39 0.74 o -2 5 1 169.52 171.70 2.06 o -1 5 1 6.41 7.71 0.43 o 0 5 1 454.62 452.25 5.08 o 1 5 1 248.46 237.11 2.68 o 2 5 1 162.51 164.57 1.85 o 3 5 1 587.58 599.37 5.22 o 4 5 1 15.33 13.76 0.62 o 5 5 1 280.93 272.88 3.79 o -4 6 1 5.20 6.54 1.76 o -3 6 1 41.51 42.95 1.68 o -2 6 1 9.62 11.87 0.92 o -1 6 1 256.48 245.45 3.55 o 0 6 1 612.16 612.48 8.72 o 1 6 1 556.62 554.55 5.68 o 2 6 1 448.31 424.33 4.50 o 3 6 1 12.82 12.68 0.66 o 4 6 1 48.49 50.38 1.30 o 5 6 1 2.67 2.03 0.41 o -3 7 1 159.62 157.24 3.87 o -2 7 1 80.38 88.97 1.83 o -1 7 1 24.58 25.51 1.40 o 0 7 1 149.15 148.31 2.54 o 1 7 1 26.44 27.27 0.80 o 2 7 1 79.97 80.94 1.49 o 3 7 1 232.39 219.09 3.98 o 4 7 1 86.38 84.32 3.34 o -2 8 1 12.61 12.39 0.92 o -1 8 1 257.10 266.67 4.11 o 0 8 1 24.49 25.71 0.99 o 1 8 1 260.41 260.69 3.57 o 2 8 1 0.93 1.21 0.27 o 3 8 1 227.04 229.97 4.37 o -2 -8 2 60.47 65.69 1.65 o -1 -8 2 4.47 4.73 0.51 o 0 -8 2 5.72 7.80 0.93 o 1 -8 2 209.50 204.66 3.40 o -4 -7 2 0.05 0.47 0.33 o -3 -7 2 106.19 95.52 2.35 o -2 -7 2 140.16 138.83 2.19 o -1 -7 2 45.16 48.28 1.28 o 0 -7 2 263.75 259.46 3.89 o 1 -7 2 0.66 0.21 0.22 o 2 -7 2 7.02 7.54 0.65 o 3 -7 2 110.12 103.56 2.94 o -4 -6 2 20.28 19.17 0.83 o -3 -6 2 64.87 68.44 1.34 o -2 -6 2 5.63 4.85 0.77 o -1 -6 2 152.58 153.81 2.86 o 0 -6 2 2.63 1.91 0.30 o 1 -6 2 73.91 71.42 1.50 o 2 -6 2 959.49 955.26 15.29 o 3 -6 2 167.43 169.12 3.13 o 4 -6 2 121.16 118.61 3.08 o -5 -5 2 28.99 28.53 0.90 o -4 -5 2 32.81 35.43 0.89 o -3 -5 2 68.17 70.94 1.00 o -2 -5 2 254.78 273.28 2.67 o -1 -5 2 111.02 109.87 1.48 o 0 -5 2 671.13 654.51 11.15 o 1 -5 2 214.63 222.79 2.58 o 2 -5 2 124.87 118.66 1.61 o 3 -5 2 252.65 251.60 2.86 o 4 -5 2 129.14 126.55 2.46 o 5 -5 2 0.91 1.69 0.33 o -5 -4 2 9.23 8.56 0.50 o -4 -4 2 943.60 918.30 9.79 o -3 -4 2 2.51 1.97 0.25 o -2 -4 2 261.75 265.22 2.66 o -1 -4 2 698.14 724.53 6.74 o 0 -4 2 110.59 104.44 1.38 o 1 -4 2 305.62 298.97 2.93 o 2 -4 2 217.91 209.92 2.36 o 3 -4 2 1156.64 1151.47 10.78 o 4 -4 2 0.31 0.36 0.17 o 5 -4 2 147.26 145.36 2.29 o -6 -3 2 1.46 1.60 0.31 o -5 -3 2 24.92 24.09 0.65 o -4 -3 2 50.85 50.80 0.81 o -3 -3 2 351.82 352.11 2.73 o -2 -3 2 1160.19 1255.95 8.59 o -1 -3 2 904.62 947.82 6.84 o 0 -3 2 573.05 619.92 5.13 o 1 -3 2 125.61 128.02 1.22 o 2 -3 2 68.40 77.89 0.84 o 3 -3 2 141.56 141.23 1.44 o 4 -3 2 545.17 543.93 5.97 o 5 -3 2 101.00 97.04 1.59 o 6 -3 2 160.01 151.77 3.25 o -6 -2 2 44.97 43.94 1.21 o -5 -2 2 126.33 127.71 2.36 o -4 -2 2 748.02 756.41 7.76 o -3 -2 2 1259.12 1270.51 10.08 o -2 -2 2 801.41 823.31 5.38 o -1 -2 2 303.81 380.41 2.59 o 0 -2 2 1536.74 1441.13 11.35 o 1 -2 2 114.37 113.13 0.87 o 2 -2 2 178.07 172.55 1.39 o 3 -2 2 412.96 409.60 3.23 o 4 -2 2 844.63 846.60 8.09 o 5 -2 2 283.08 289.63 3.60 o 6 -2 2 0.18 0.00 0.21 o -6 -1 2 82.36 74.97 1.63 o -5 -1 2 185.99 179.07 2.60 o -4 -1 2 41.21 41.63 0.56 o -3 -1 2 157.74 155.71 1.58 o -2 -1 2 75.90 89.83 0.75 o -1 -1 2 2421.10 2298.62 19.17 o 0 -1 2 447.74 476.28 3.61 o 1 -1 2 1285.92 1153.00 7.14 o 2 -1 2 40.40 48.93 0.44 o 3 -1 2 408.63 402.31 3.57 o 4 -1 2 23.76 27.27 0.45 o 5 -1 2 377.45 368.59 4.97 o 6 -1 2 20.83 22.64 0.78 o -6 0 2 9.58 10.25 0.45 o -5 0 2 410.50 403.32 5.41 o -4 0 2 156.69 157.49 1.59 o -3 0 2 884.39 935.90 8.50 o -2 0 2 532.39 597.24 5.05 o -1 0 2 3086.92 2631.75 41.52 o 0 0 2 1384.74 1103.66 16.31 o 1 0 2 2203.17 2014.90 25.95 o 2 0 2 3679.97 3526.37 39.19 o 3 0 2 38.07 40.23 0.54 o 4 0 2 295.45 299.55 3.55 o -6 1 2 11.20 10.33 1.71 o -5 1 2 0.94 0.99 0.17 o -4 1 2 349.01 348.62 3.35 o -3 1 2 45.55 52.36 0.73 o -2 1 2 270.35 286.36 2.35 o -1 1 2 184.31 195.40 1.48 o 0 1 2 2332.04 2150.19 21.71 o 1 1 2 475.80 453.13 2.85 o 2 1 2 0.10 2.46 0.09 o 3 1 2 1183.65 1203.11 12.09 o 4 1 2 31.35 29.77 0.55 o -6 2 2 44.97 47.74 1.38 o -5 2 2 4.29 4.69 0.30 o -4 2 2 409.56 407.71 4.89 o -3 2 2 797.27 829.32 7.06 o -2 2 2 377.55 393.12 3.06 o -1 2 2 2135.29 2038.92 13.97 o 0 2 2 253.72 218.37 2.02 o 1 2 2 991.71 930.47 6.09 o 2 2 2 16.49 17.33 0.23 o 3 2 2 1303.33 1308.30 12.11 o 4 2 2 17.62 16.09 0.31 o 5 2 2 69.59 65.87 1.07 o 6 2 2 105.38 106.45 2.01 o -6 3 2 34.62 40.75 1.38 o -5 3 2 136.64 133.33 2.03 o -4 3 2 13.82 15.26 0.49 o -3 3 2 492.79 497.77 4.45 o -2 3 2 1489.72 1568.60 12.45 o -1 3 2 6.47 6.26 0.23 o 0 3 2 155.74 155.23 1.40 o 1 3 2 26.23 29.26 0.37 o 2 3 2 0.60 0.45 0.15 o 3 3 2 27.07 27.00 0.34 o 4 3 2 889.49 873.17 7.70 o 5 3 2 22.74 25.48 0.79 o 6 3 2 91.57 90.41 2.15 o -5 4 2 14.97 16.21 0.62 o -4 4 2 127.01 130.19 1.91 o -3 4 2 1.24 3.10 1.37 o -2 4 2 379.16 399.09 4.05 o -1 4 2 349.14 358.39 3.40 o 0 4 2 779.69 748.11 6.89 o 1 4 2 0.31 0.12 0.06 o 2 4 2 285.16 302.03 2.72 o 3 4 2 386.43 386.87 2.90 o 4 4 2 353.84 361.92 4.19 o 5 4 2 88.43 86.53 1.48 o 6 4 2 53.95 53.85 1.81 o -5 5 2 233.97 224.71 3.86 o -4 5 2 6.35 5.11 0.49 o -3 5 2 64.24 69.37 1.04 o -2 5 2 0.72 1.49 0.17 o -1 5 2 663.11 657.16 6.49 o 0 5 2 7.62 11.44 0.56 o 1 5 2 68.03 62.86 0.93 o 2 5 2 342.61 335.35 3.30 o 3 5 2 7.66 6.35 0.49 o 4 5 2 293.35 293.49 5.88 o 5 5 2 65.24 63.57 1.33 o -4 6 2 15.36 16.52 1.18 o -3 6 2 1.09 0.79 0.26 o -2 6 2 16.45 16.26 0.68 o -1 6 2 100.30 102.22 1.88 o 0 6 2 828.59 790.45 9.52 o 1 6 2 64.59 66.53 1.14 o 2 6 2 201.13 196.67 2.39 o 3 6 2 46.96 44.97 0.88 o 4 6 2 68.64 71.10 1.79 o 5 6 2 31.29 28.51 1.07 o -3 7 2 14.30 18.23 1.32 o -2 7 2 47.61 46.83 1.26 o -1 7 2 221.06 221.68 5.90 o 0 7 2 186.10 182.10 3.89 o 1 7 2 43.41 40.69 0.97 o 2 7 2 80.36 80.01 1.47 o 3 7 2 66.11 73.12 1.59 o 4 7 2 92.03 87.95 2.66 o -2 8 2 118.04 120.42 2.75 o -1 8 2 27.78 27.56 1.17 o 0 8 2 103.04 102.44 2.12 o 1 8 2 101.84 107.00 1.89 o 2 8 2 2.87 2.17 0.32 o 3 8 2 56.64 56.19 1.85 o -2 -8 3 100.09 103.94 2.20 o -1 -8 3 0.16 -0.02 0.25 o 0 -8 3 35.18 36.56 1.20 o 1 -8 3 15.55 16.54 0.93 o -3 -7 3 21.31 28.04 1.17 o 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176.11 5.78 o -2 6 10 293.15 293.25 4.40 o -1 6 10 23.46 24.08 1.07 o 0 6 10 91.11 93.86 3.51 o 1 6 10 54.78 56.17 1.64 o 2 6 10 164.44 161.23 3.13 o 3 6 10 135.82 136.66 4.99 o 4 6 10 62.41 63.14 3.13 o -1 7 10 0.94 1.78 0.35 o 0 7 10 72.93 70.56 1.92 o 1 7 10 4.61 5.61 1.16 o 2 7 10 39.50 36.91 1.98 o 3 7 10 315.64 301.13 9.20 o -1 -5 11 37.70 38.23 1.22 o 0 -5 11 301.63 302.61 4.54 o 1 -5 11 32.05 31.96 1.10 o -2 -4 11 80.51 82.87 2.09 o -1 -4 11 37.15 38.71 1.71 o 0 -4 11 6.45 6.61 0.55 o 1 -4 11 57.81 52.04 1.61 o 2 -4 11 1.14 1.05 0.28 o 3 -4 11 255.34 263.74 5.78 o -3 -3 11 11.95 14.44 1.51 o -2 -3 11 32.54 34.23 1.04 o -1 -3 11 392.00 388.54 5.27 o 0 -3 11 149.29 149.22 2.56 o 1 -3 11 401.65 386.34 5.36 o 2 -3 11 188.81 191.51 3.03 o 3 -3 11 157.92 153.79 3.81 o 4 -3 11 10.06 11.10 1.00 o -3 -2 11 15.74 15.84 0.94 o -2 -2 11 161.77 161.09 2.34 o -1 -2 11 105.93 106.54 1.98 o 0 -2 11 154.54 155.29 2.57 o 1 -2 11 267.28 255.98 3.69 o 2 -2 11 71.15 65.86 1.44 o 3 -2 11 199.94 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